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The document provides instructions for preparing different types of test samples for analysis. For solids like sugars, the materials should be ground and mixed thoroughly. For semisolids, 50g should be weighed, crystals dissolved in water, and diluted to 100g. For liquids like molasses, the materials must be mixed thoroughly and any crystals dissolved by gentle heating to avoid water evaporation. All results should be calculated based on the weight of the original substance.
The document provides instructions for preparing different types of test samples for analysis. For solids like sugars, the materials should be ground and mixed thoroughly. For semisolids, 50g should be weighed, crystals dissolved in water, and diluted to 100g. For liquids like molasses, the materials must be mixed thoroughly and any crystals dissolved by gentle heating to avoid water evaporation. All results should be calculated based on the weight of the original substance.
The document provides instructions for preparing different types of test samples for analysis. For solids like sugars, the materials should be ground and mixed thoroughly. For semisolids, 50g should be weighed, crystals dissolved in water, and diluted to 100g. For liquids like molasses, the materials must be mixed thoroughly and any crystals dissolved by gentle heating to avoid water evaporation. All results should be calculated based on the weight of the original substance.
01 250 mL volumetric flask, dilute to volume, and mix thoroughly; or
AOAC Official Method 920.175 weigh 50 g test portion and dilute with H2O to 100 g. If insoluble Preparation of Test Sample material remains, mix uniformly by shaking before taking aliquots First Action 1920 by volume or by weight for determinations. Final Action (a) Solids (sugars, etc.).—Grind, if necessary, and mix to (c) Liquids (molasses, syrups, etc.).—Mix materials thoroughly. uniformity. Thoroughly mix raw sugars with spatula in minimum If crystals of sugar are present, dissolve them by heating gently time. Break up any lumps either on glass plate with glass or iron (avoiding loss of H2O by evaporation), or by weighing whole mass, rolling pin, or in large, clean, dry mortar, with pestle. then adding H2O, heating until completely dissolved, and after (b) Semisolids (massecuites, etc.).—Weigh 50 g test portion, cooling, reweighing. Calculate all results to weight of original dissolve crystals of sugar in minimum volume of H2O, wash into substance.