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AN EVALUATION OF THE
ELEVATED TEMPERATURE TENSILE AND CREEP-RUPTURE
PROPERTIES OF WROUGHT CARBON STEEL
Note
The Society is not responsible, as a body, for the statements
and opinions advanced in this publication.
January 1970
Data Series DS 1 lSl
The American Society for Testing and Materials
Related
ASTM Publications
REFERENCE: Smith, G. V., "An Evaluation A summary of the results of the eval-
of the Elevated Temperature Tensile and uations is provided in Fig. 1. In this
Creep-Rupture Properties of Wrought figure, all of the creep and rupture data
Carbon Steel", ASTM Data Series, OS 11 have been treated as if from a single
S-1, American Society for Testing and population, even though there is evidence
Materials, 1970. presented in the body of the report that
material produced to specifications that
ABSTRACT: This report seeks to offer a require ~ minimum tensile strength of
best current assessment of the several 60,000 psi or higher has a greater rup-
elevated temperature properties that com- ture strength than material produced to
monly form the basis for establishing specifications that require minimum ten-
allowable stresses or design stress in- sile strengths less than 60,000 psi.
tensity values. The results are pre- Evidence is also offered for a slight
sented in a form readily usable for that superiority in rupture strength at the
purpose. The data that are evaluated lower end of the creep range of tempera-
are those that have become available ture, of material made to "coarse-grain"
since the publication in 1955 of ASTM practice. The yield and tensile strengths
Data Series Publication OS 11 (formerly of Fig. 1 represent material that had
STP No. 180), "Elevated Temperature Pro- been tempered after hot working or after
perties of Carbon Steels," as well as normalizing, in practical recognition of
selected data from that earlier publica- the liklihood that material will receive
tion. The body of the report provides, such treatment during fabrication, if not
in text, tables and figures, details con- before. The tensile strength curves of
cerning the materials, the evaluation Fig. 1 recognize a distinct difference
procedures that were employed, and the between material made to "coarse-grain"
results. and "fine-grain" practice; however, the
In evaluating rupture strength, ex- differences in yield strength were small,
trapolations to 100,000 hours were per- and scatter large, and the curves of
formed both by direct extension of iso- Fig. 1 are based on a common trend curve
thermal plots of stress and rupture-time for tempered, coarse- and fine-grain
for the individual lots, and by a time- material. Individual trend curves for
temperature parameter, scatter-band pro- yield and tensile strength, expressed as
cedure. Owing to a concern that differ- strength ratios, are compared in Figs. 2
ent populations may be intermixed in a and 3.
scatter band approach, the rupture
strengths shown in the summary Fig. 1 KEY WORDS: elevated temperature, tensile
represent the results of the direct strength, yield strength, creep strength,
individual-lot extrapolations. rupture strength, carbon steel, mechani-
cal properties, data evaluation, elonga-
tion, reduction of area.
2
The yield and tensile strength data of inclusive term for any reheating to the
the present evaluation extended above the temperature range below the critical. The
range in which their levels could be ex- effect of deoxidation practice and heat
pected to govern, but were evaluated to treatment upon the tensile strength was
the limits of the available data. evident for the range of temperature be-
The original tensile test and creep tween about 200 and 600°F, within which
rupture data are tabulated in Tables III dynamic strain aging manifests itself in
and IV, respectively. susceptible steels as an increase in
tensile strength.
Yield Strength and Tensile Strength Largely to reflect common terminology,
but also because a finer classification
In the previous report in this series did not seem warranted, in view of the
(DS 5 S2 on wrought austenitic stainless incomplete character of the reported in-
steels) , an evaluation procedure was em- formation, two categories of deoxidation
ployed that involves expressing the ele- practice, "coarse-grained" and "fine-
vated temperature strength of a partic- grained" have been established. In a num-
ular lot as a ratio to the room tempera- ber of instances, this characterization
ture strength of that particular lot. was made by the original investigator, and
This procedure, based on the premise that when reported was adopted for this report.
the short-time, elevated-temperature The basis for assessment was not always
strength of a specific lot of material evident, but in some instances was based
reflects its relative strength at room upon the results of the McQuaid-Elm grain
temperature, seemed to have certain size test. When an assessment was not
merits. An important advantage in analyz- furnished with the data, and providing
ing the generally unsystematic type of the aluminum analysis had been reported,
data that are gathered in the Metal Pro- a separation was made by classing steels
perties Council solicitations, is that it containing less than 0.015 aluminum as
becomes possible, in principle, to utilize coarse grained. The very few data for
all of the data for which there are cor- semi-killed steel were put in the coarse-
responding test results at room tempera- grained category, inasmuch as the behavior
ture; when evaluated in terms of real seemed to be similar.
values, results of strong or weak lots of With respect to the separation into
material, available only at scattered coarse- or fine-grained steels according
temperatures, may distort the true trend to deoxidation practice, it should be
of variation of strength with temperature. pointed out that the actual grain size
Another advantage of the strength ratio (observable under the microscope) of an as-
procedure that will be brought out in the rolled steel depends primarily on the fin-
present evaluation is that it can better ishing temperature of rolling, a variable
preserve in the scatter band the individ- that is generally not reported. Thus, a
ual characteristics that might otherwise fine-grained steel (as defined by the
be masked in a scatter band. deoxidation practice), finished at rela-
With the particular objective of de- tively high temperature, may exhibit a
termining whether it is possible to es- coarser ferrite grain size than a steel
tablish classes of carbon steels corre- made to coarse grained practice, but fin-
sponding with different manufacturing ished at a relatively low temperature.
practices, individual strength ratio For example, hot-finished steel T 22, made
plots were prepared for heats made to the to coarse-grained practice, had an actual
same specification. In these plots, too grain size of ASTM 7-8.
numerous to include here, distinctions Examination of the individual strength
were preserved as to deoxidation practice, ratio plots further revealed that temper-
whether the material had been tested in ing may effect a significantly lessened
the as-rolled or as-normalized condition, tendency for strain aging of as-rolled or
and whether the material had been stress- as-normalized steels that had been pro-
relieved or tempered. Study and compari- duced to fine-grained practice. No other
son of the individual ratio plots with correlations were evident from inspection
one another revealed considerable and of the data and accordingly four categories
seemingly continuous spread in behavior. of carbon steel were established:
The scatter is presumed to reflect both
the effects of variations in the impor- (1) coarse-grained, not tempered
tant variables and also problems of test (2) coarse-grained, tempered
reproducibility. (3) fine-grained, not tempered
Detailed comparison of the ratio (4) fine-grained, tempered.
plots did reveal the importance to the
tensile strength variations of two factors, Figures 4 through 7 provide plots of the
first, deoxidation practice, and second, data according to this classification. No
whether or not the material had, as a distinction is made in the classification
final treatment, been reheated to the as to whether the material was in the hot
temperature range below the lower criti- finished or normalized conditions, since
cal temperature. Such treatment is com- this seemed unimportant, except possibly
monly termed stress-relief annealing for category 3. Only one lot (P 27a) of
when applied to as-rolled material, and those falling in this category had been
tempering when applied to normalized ma- normalized, and it behaved similarly to
terial; for convenience, the term temper- as-rolled lots; however, this lot had a
ing will be used in this report as an relatively high nitrogen content of 0.02
3
percent. It is possible that a better relatively long creep and rupture tests.
and more representative sample might re- The cold plastic deformation that is
veal the need to distinguish in category required to set the stage for strain-aging
3 between hot-finished and normalized lots, is introduced during the tensile test,
for reasons that will be brought out later. and for that reason, strain aging should,
The scheme of classification adopted in principle, not be evident in the yield
has some support on technical grounds. strength. Yet, some of the steels did
The most prominent feature of the temper- show an increase of yield strength at
ature dependence of yield and tensile intermediate temperatures, and it may be
strength of carbon steel is the occurrence inferred that they had had some measure
of dynamic strain aging, which manifests of prior plastic deformation (perhaps
itself in susceptible steels as a rever- from cold-straightening).
sal, or levelling off, in the trend of Except for a few data which could
tensile strength with increasing tempera- not be encompassed into the four categor-
ture. Strain aging is associated with ies cited above and which will be dis-
the interstitially-dissolving elements cussed later, all of the yield strength
carbon and nitrogen, but with C exceeding and tensile strength data were plotted
the solubility limit in these steels, the in scatter bands in Figs. 4 a, b, c, and
differences in behavior are to be associ- d through Figs. 7 a, b, c, and d, both
ated with differences in the amount of in terms of strengths and also as strength
"available" nitrogen. Nitrogen tends to ratios. The elongation and reduction of
react with elements such as aluminum and area data were also plotted, Figs. 4 e -
silicon, especially the former, that are 7 e. In all of the plots, data represent-
added for deoxidation. The extent of the ing plate have been differentiated from
reaction in a given steel depends upon data representing piping or tubing.
temperature and time, and to the degree (The only data available for bar product
that the reaction occurs, nitrogen be- could not be encompassed within the class-
comes unavailable to cause strain aging. ification scheme and are discussed later) •
In steels that have been air-cooled after The strength plots exhibit scatter,
hot working, nitrogen tends to be avail- a portion of which has its origin in the
able, whether produced to fine- or coarse- grouping together of materials from dif-
grained practice, and hence susceptible ferent specifications, which individually
to strain aging; this will be evident in require different minimum tensile strengths;
the plots. On the other hand, it is com- 1·hese ranged between SS, 000 and 7S, 000 psi,
monly accepted that normalizing is con- with corresponding variation in specified
ducive to the formation of aluminum minimum yield strength. The ratioing pro-
nitride, during heating or holding at cedure proved to be reasonably effective
temperatures, in fine-grained steels. It in "normalizing" the tensile strength
is, in fact, the presence of aluminum data, except within the temperature range
nitride that causes aluminum-deoxidized of dynamic strain aging, where the scat-
steels to be fine-grained in the normal- ter may be presumed to reflect the grad-
ized condition. However, the behavior ation in the degree to which nitrogen is
of lot P 27a, previously mentioned, available to cause strain-aging. The
indicates that in this steel, there must ratio procedure was less effective for
be sufficient nitrogen "available" after the yield strengths, probably reflecting
normalizing to permit strain aging. in part a greater degree of testing error
Reheating for stress-relief or tem- inherent in the yield strength determina-
pering provides a very favorable oppor- tions. It is of interest that for tensile
tunity for inunobilization of nitrogen strength the ratio plots give a truer pic-
provided aluminum is available, the re- ture than the strength plots of the vari-
action proceeding at a rate which in- ation in strain-aging susceptibility of
creases with increase of this temperature. individual steels. Comparisons such as
The data suggest that after conventional Fig. 4 b with Fig. 4 d show that individ-
tempering or stress relief treatment, no ual characteristics can be masked in the
distinction need be made between fine- scatter band of strength. The scatter
grained steels as to prior treatment. In plots were studied to determine whether
a purely practical vein, it is appropri- the trend of variation of strength with
ate to recognize the probability that temperature might exhibit a dependence
material not initially tempered will be upon strength level, but no evidence of
tempered during fabrication. such a dependency could be detected,
Silicon, commonly used as a deoxi- within the limits of the data nor, in the
dant for coarse-grained steels, can also case of plate was there any evident
effect immobilization of nitrogen, but dependence upon section thickness.
the reaction does not proceed as rapidly The variations of strength with tem-
nor to as complete an extent, so that perature were developed from the strength
as the tensile strength ratio plots re- ratio data by polynomial regression; the
veal, tempered material exhibits only data were treated without distinction as
slightly lesser strain-aging susceptibil- to product form in view of the scatter
ity, and so far as can be seen, indepen- and overlapping of data. These trend
dent of the prior condition. curves have been drawn on the ratio plots
It might be mentioned here that the and are also tabulated in Table v. A
nitrogen-immobilizing reactions may tend comparison amongst the different categor-
to occur in either the silicon- or ies is afforded in Fig. 2 and 3. The
aluminum-deoxidized steels during most important distinction that is evident
4
is the difference between the tensile cept that the silicon content was delib-
strength trend curve for fine-grained, erately reduced to below that required
tempered, steel and the other three by specification; the aluminum contents
trend curves, arising from the lessened were 0.020 and 0.015 respectively. Al-
tendency for dynamic strain aging in the though A 516 material is intended for
former. Based upon the small, and pos- "moderate and lower temperature service"
sibly unrepresentative available data, a and, by specification, should be produced
steel produced to fine-grained practice to fine-grained practice, it is evident
may, if not tempered, be as susceptible in Fig. 8 that this material, in the
to strain aging as a steel made to coarse- tempered condition, behaves instead as if
grained practice, for which tempering coarse-grained, perhaps reflecting its
exerts relatively little influence in this borderline aluminum content and low sili-
same respect. The four tensile strength con content. On the other hand, the A 515
trend curves all exhibit the same general material, intended for intermediate and
form. At temperatures both below and higher temperature service, and thus re-
above the strain-aging range, the strength quired to be of coarse-grained practice,
ratios for the different categories differ exhibits pronounced strain-aging sus-
only slightly. The significance of the ceptibility in the as-rolled condition,
differences seems questionable. but, interestingly, not in the normalized
The individual yield strength trend condition. This steel, incidentally had
curves exhibit slight perturbations, but, been vacuum degassed; its reported nitro-
in view of the scatter, it is difficult gen content is slightly greater than for
to argue for their significance; yet, other plate steels.
there are similarities from one to another, A number of miscellaneous data, all
and some resemblance to trend curves de- from ASTM OS 11 are plotted in Fig. 9.
veloped for carbon steel by the British The limits of behavior do not exceed
from extensive, and systematically those exhibited in Figs. 4-8.
generated, data. (1) It is also difficult
to argue that the differences among the Creep and Rupture Properties
yield strength trend curves for the four
categories are real, and further more The criteria for establishing allowable
systematic tests would be required to stresses or design stress intensity values
elucidate this question. The differences in the "creep" range of temperatures com-
are on the order of +10 percent from an monly include the stress for rupture in
average for the 4 categories. 100,000 hours, further reduced by appro-
As noted earlier, the liklihood that priate fractional factors aimed ~t pro-
carbon steel will be reheated to below viding a reasonably long safe period of
the critical temperature either before or usefulness. Since it is seldom possible
during fabrication should be recognized, to conduct tests lasting 100,000 hours
and the trend curve categories reduced (11.5 years), it becomes necessary to
to only two, namely coarse-grained and extrapolate the results of shorter time
tempered and fine-grained and tempered. tests. In the ASME Code, the allowable
Further, if the differences in the yield stress is also limited by the average
strength trend curves are of questionable stress to cause a secondary creep rate of
significance, it would not be inappropri- 0.01% per 1000 hours and extrapolation may
ate to establish a common trend curve for or may not be required. In European codes
the two tempered conditions; such a trend generally, as well as in the draft ISO
curve is also tabulated in Table v. Codes, creep strength is expressed in terms
The plots of percent elongation and of the stress required for a creep strain
percent reduction of area exhibit gener- of 1 percent in 100,000 hours, and except
ally similar trends. With increasing as 100,000 hour tests might be conducted,
temperature, ductility first decreases an extrapolation is necessary. (This
then passes through a minimum and finally extrapolation appears to be particularly
generally increases. The minimum is re- difficult to perform, with few reported
lated to the maximum in the tensile results; the data available to the Metal
strength, previously noted, and is least Properties Council are inadequate to
pronounced in fine-grained and tempered permit an assessment of creep strength
material, as expected. Some scatter at defined in this way.)
higher temperature, particularly evident There are two broad types of proce-
in coarse-grained, not-tempered material, dures for extrapolating time-for-rupture
may have its origin in an increased ten- data, commonly plotted on log-log coordi-
dency to an intergranular mode of fracture nates of stress and time-for-rupture. The
of some lots. second procedure, in which great interest
All of the remaining tensile test has developed in recent years, involves
data, representing heats that could not the concept of a time-temperature para-
be put in one of the foregoing categories meter expressed as a function of the
are plotted (as strength ratios and duc- stress. Both procedures have been con-
tility) in Fig. 8 or 9. These data re- sidered in the present evaluation.
present heats that were unconventional or
inadequately documented with respect to
deoxidation practice and/or processing.
Codes P 29 and P 30, plotted in Fig. 8,
represent material produced to specif ica-
tions A 516 and A 515 respectively, ex-
5
Direct Extrapolation Although bar, pipe-tube, and plate
data, as well as data from ASTM DS 11
In extending the time-for-rupture data at (probably mostly bar), are differentiated
a specific temperature, the extrapolation in Fig. 13 a and b, casual examination
may be performed either by treating dif- does not reveal a clearly evident dis-
ferent lots individually, or alternatively tinction amongst the separate categories.
by treating all of the data together in The data were therefore analyzed by the
a scatter band. The latter procedure as- method of least squares, with temperature
sumes that all of the data are from a as the independent variable. The vari-
single population, independent of such ances of the data were only negligibly,
factors as chemical composition, manu- or not at all, improved by assuming a
facturing practice and product form. As quadratic rather than a linear dependence
will be shown in this evaluation, there is of the variables, and the average trend
evidence that all of the data are not from curves superimposed on the plots there-
the same population. For this reason, and fore represent a linear dependence. On
because of an inherent concern that a the assumption that log strength is
scatter band approach can mask individual normally distributed, a minimum trend
characteristics, even within a given curve has been derived from the variance
population, as illustrated earlier in this of the data and is also drawn on each
report for tensile strength, principal grouping. This minimum has been arbi-
emphasis in the present evaluation is trarily taken at the 90% confidence level,
placed on individual lot evaluations. or the level above which 95 percent of
However, the scatter bands have also been the data should lie. In drawing the
evaluated to permit comparisons. minimum trend curves parallel to the
Individual lot extrapolations were average trend curves, it is assumed that
performed on individual plots, too numer- the average slope has been defined with-
ous to include in this report. However, out error, and that the variances of the
to show both the volume of data and their data are independent of temperature. The
scatter, all of the available data are average and minimum trend curves deline-
shown in isothermal scatter band plots of ated in Figs. 13 a and b are tabulated in
log stress versus log time-for-rupture or Table X (10,000 hours rupture strength),
log secondary creep rate, Figs. 10 a, b, Table XI (100,000 hour rupture strength)
and c, and Figs. 11 a, b, and c. The and Table XII (0.1 and 0.01 percent per
elongation and reduction of area results 1000 hours creep strength) .
are also shown in isothermal scatter band The wide scatter in the creep and
plots, Figs. 12 a, b, c, d, e, and f rupture strengths of carbon steel no doubt
without distinction as to product form. reflects the uncontrolled variation of one
With few exceptions, the individual rup- or more influential factors, and it would
ture-time plots were not extrapolated appear possible in principle (if perhaps
unless data were available for three not in practice) to reduce the degree of
levels of stress, with at least one rup- scatter by more restrictive specifications.
ture time exceeding 1000 hours. The British studies(l) have shown, for example,
creep rate data, also with few exceptions, that the manganese content and the quantity
were not extrapolated by more than 1 log of molybdenum present as a residual impur-
cycle. ity are especially important variables in
Based on an examination of the indi- commercial carbon steel.
vidual plots, and upon the scatter band For many years, based on published
plots as well (see later), the individual literature, it has been held that steel
lot extrapolations of the time-for-rupture made to coarse-grained practice has greater
data were performed, assuming a linear creep and rupture strength than steel
dependence of log time upon log stress. made to fine-grained practice. It is
However, for the variation of log secon- therefore of interest to inquire whether
dary creep rate with log stress, a degree such a distinction is evident in the data
of curvilinearity was exhibited by some here being evaluated. With reference to
lots, and this was recognized in the creep creep strength, there were unfortunately
strength evaluations. The best fit lines too few data to warrant such an attempt;
or curves were developed visually, giving thus, all of the useful data for plate fall
weight to the longer-time or slower-rate in the coarse grained category, and there
data. are no useful 0.01% per 1000 hours creep
The results of the individual iso- strength data for pipe-tube, which is
thermal extrapolations or interpolations commonly made to fine-grained practice.
are tabulated in Tables VI - IX and also However, if possible differences arising
plotted as dependent upon temperature in from other factors such as product form,
Figs. 13 a and b. The rupture and creep processing history and microstructure,
strengths are evaluated at two levels including actual grain size, are ignored,
each -- as the stress for rupture in it is possible to look for a difference
10,000 or in 100,000 hours and as the in rupture strength. Figure 14 a
stress for a secondary creep rate of 0.1 (10,000 hours rupture) and Fig. 14 b
or of 0.01 percent per 1000 hours. (100,000 hours rupture) plot separately
Semilogarithmic coordinates were chosen data corresponding to fine-grained and
for the plots of Fig. 13 because they coarse-grained practices. (not all of
tend to linearize the dependence of log the data of Tables VI and VIII could be
strength upon temperature. categorized in this respect.) The data
6
of the plots were analyzed by the method (and its companion value at 1100°F) has
of least squares with average and been excluded; although produced to speci-
minimum (90% confidence) trend curves fication A 201 A, its tensile strength was
drawn on the plots and tabulated in 64,000 psi in comparison with a minimum
Tables X and XI. Each of the regression requirement of only 55,000 psi. The
lines seemed suitably defined by a linear average and minimum values of Fig. 15
dependence except for the fine-grained, have been incorporated into Table XI. It
100,000 hour rupture data which required is of interest that the differences de-
a second order dependence. pending upon the specified minimum room
At the lowest test temperature, 800°F, temperature tensile strength level are
the results reveal a slight inferiority greater than those associated with dif-
(approximately 10 percent) in 100,000 ferences in deoxidation practice, and
hour rupture strength for material of the difference does not diminish with
fine-grained practice. This difference increasing test temperature.
tends to wash out with increasing tempera- The isothermal scatter bands were
ture. The difference at 800°F also seems evaluated by the method of least squares,
slightly more pronounced at 10,000 hour and average and minimum curves extended
(approximately 25 percent) than at to 100,000 hours. The longer-time test
100,000 hours. Although these differences results were weighted in the evaluations
would seem to be of borderline signifi- by excluding rupture-times less than 100
cance for 100,000 hour rupture strength, hours. The variances were either not
in view of the small sample, and the un- improved significantly, or in some in-
controlled simultaneous variation of stances were actually worsened, in pro-
other factors, it is of interest that ceeding from the assumption of a linear
the observed trend with increasing temper- relation between log stress and log rup-
ature corroborates observations recently ture time to the assumption of a second
reported by Glen and associates(l) for order relation. As pointed out in the
British test results. The tendency for earlier report in this series, covering
the difference in strength to wane with austenitic stainless steels, significant
increasing test time and temperature can differences in the extrapolated 100,000
be attributed to the occurrence of nitro- hour values are found depending upon the
gen-immobilizing precipitation reactions assignment of dependent and independent
during creep and rupture tests, as men- variable in the analysis, and the proper
tioned earlier in this report. choice has been the subject of controversy.
Inspection of the plot of 100,000 The earlier observation that a choice of
hour rupture strength data in Fig. 13b time as independent variable conforms bet-
reveals that a large fraction of the ter with a visual assessment of the data
points lying near the bottom of the scat- has been confirmed in the present evalu-
ter band represent material manufactured ation, and for this reason and others
to specifications requiring relatively which will be discussed in a separate
low levels of specified minimum tensile report, (5) time has been chosen as the
strength; conversely data lying near the independent variable for the least
top of the scatter band tends to repre- squares evaluations which are summarized
sent material produced to somewhat in Fig. 16.
higher specified minimum tensile strengths. The positions of the individual iso-
Since a separation based on differences thermal regression lines in Fig. 16
in specified minimum tensile strength is relative to one another are inconsistent
of possible interest to Code groups in with what would be expected of a real
establishing design stress intensity material, and it can only be concluded
values, the 100,000 hour rupture strengths that different populations are being in-
have been evaluated separately for mater- termixed. In this connection, study of
ial conforming to specified minimum ten- Figs. 10 a, b, and c will suggest the
sile strength of 60,000 psi or higher possibility of different populations re-
and for material produced to specif ica- lated to different product forms. Com-
tions requiring less than 60,000 psi parison of the 100,000 hour rupture
minimum specified tensile strength. strengths defined in Fig. 16 with those
Separation at the level of 60,000 psi defined by the trend curve evaluation,
is arbitrary but convenient. Table XI, reveals the latter to be the
Fig. 15 plots separately data falling more conservative. To the extent that
into the two foregoing categories* and the different populations may be encompassed
regression lines do reveal significantly within the scatter bands, it seems neces-
different levels of rupture strength. In sary to question the appropriateness of
establishing the regression line for the the scatter band procedure of evaluation.
data in the lower portion of the plot, The elongation and reduction of area
the outlying value of 11,000 psi at 900°F at rupture, Figs. 12 a-f, exhibited very
wide scatter. At none of the test tem-
peratures was there evident in the scatter
bands a well defined trend with increas-
*Data for materials not identified as to ing time for rupture. The scatter bands
specification (principally bar) are not were studied in t~e interests of deter-
included in Fig. 15 mining whether ductility could be corre-
lated with deoxidation practice. At both
800 and 900°F, the elongation valu-es
7
for fine grain material lay at the top tests at three or more temperatures are
of the overall scatter band and conversely necessary. Such a quantity of test
elongation for coarse grain material lay data is only infrequently available in
at the bottom of the scatter band; at the data gathered in the Metal Properties
1000°F the values for fine-grained mater- Council solicitations. In the present
ial fell near the bottom of the scatter instance, for example, for only four lots
band, but with no distinct separation to of carbon steel were test results avail-
the high side of values for coarse-grain able for a minimum of three test temper-
material. It was not possible to draw atures. Consequently, an individual para-
any clear distinctions for temperatures metric evaluation could only be performed
of 850, 950 and 1050°F, owing to the on a minimal fraction of the available
character of the samples. data, and has not seemed worthwhile.
Only six of the elongations at rup- A parametric extrapolation procedure
ture were less than 10%. Five of these involving the isothermal scatter bands
represented A 106 C hollow-forged pipe has been developed and employed by the
(Code T7) and one represented A 212 B British Steelmakers' Creep Committee,(3)
plate (Code P la). Inspection of the and in spite of inherent reservations
processing practices and chemical compo- concerning scatter band procedures, it
sition did not suggest any explanation has been deemed desirable to perform a
for the low values. The scatter bands, similar analysis of the present carbon
Figs. 12 a-f, do not provide any basis steel data to provide an opportunity for
for expecting generally reduced ductility comparisons. Following the general form
for rupture in 100,000 hours. of the British evaluation procedure, the
isothermal regression lines of Fig. 16
Parameter Extrapolation have been employed in a graphical cross-
plot of log time versus reciprocal tem-
In recent years, a great deal of interest perature for several constant stresses.
has developed in the possible use of In satisfying the Larson-Miller parameter,
time-temperature parameters for correla- these isostress lines should converge at
ting creep and rupture strengths. In -C for reciprocal temperature equal to
brief, the parameter techniques make zero. In fact, the isostress lines inter-
possible an estimate of the stress for sected the ordinate axis over a range of
rupture (or stress for a particular values, the average of which approximated
creep rate or creep strain) in a relative- 20 (a value suggested by Larson and
ly long time at some temperature of prac- Miller(2) as the best single value approx-
tical interest from tests of relatively imately suitable for a variety of materi-
short duration at higher temperature. A als). The isostress data were also evalu-
number of different parameters have ated mathematically using a least squares,
been proposed, and their relative merits computer procedure suggested by Manson
have been argued frequently in published and Mendelson; (4) by this procedure, the
literature. Typical of these and suffi- Larson-Miller constant had a value of
cient for present purposes is the para- 19.6.
meter suggested by Larson and Miller(2): A value of 20 for the constant was
therefore adopted and individual values
P T (C + log t) = F(a) of the parameter computed for every test
for which the rupture time exceeded 5
where T is the temperature in degrees hours. It then became possible to exa-
Rankine, t is the time for rupture in mine by polynomial regression analysis
hours and C is a material constant. the variation of parameter with stress.
The possible usefulness of parameters This was done for all the data grouped
for evaluating data of the type being together, as if from a single population,
considered in the present report is being and also in various subgroupings to ex-
explored by the Metal Properties Council plore for possible differences arising
in a separate program to be reported from differences in product form or
separately. However, it has seemed deoxidation practice. For illustration,
appropriate to give some consideration in Figs. 17 a, b, and c show plots of
the present evaluation to the use of stress versus parameter for bar, pipe-
parameters. Accordingly a view point has tube, and plate respectively. Shown on
been adopted for the present evaluation, the plots are the best-fit, least squares
based upon considerations which can only results along with the 90% confidence-
be briefly summarized in this report. level minimum. Plots for the combined
Firstly, the constant C has been reported data and for different deoxidation
to vary with such factors as chemical practices were not made, owing to the
composition, microstructure, fracture large volume of data that would have had
mode, environment and even temperature to be plotted. However, the results of
or stress range; therefore, it must be the least squares analysis for these
evaluated from the test results. This groupings are tabulated, for comparison
suggests that each lot of material 4.ust with one another and with the direct log-
be evaluated individually for extrapola- log extrapolations, in Table X (rupture
tion by any specific parameter procedure. in 10,000 hours) and Table XI (rupture
Furthermore, in order to evaluate the in 100,000 hours). Fig. 18 provides a
constant, and to assess properly the graphical comparison of the regression
ranges of variables within which it lines for coarse-grained and fine-grained
holds true, it is generally agreed that material in relation to the combined
8
data, and also compares the regression 5. G. v. Smith: Evaluation of Elevated
lines for the different product forms. Temperature Strength Data; 1969
Study of Tables X and XI reveal that the Gillette Memorial Lecture, Amer.
trends evident in the parameter extrapol- Soc. for Testing and Materials;
ations closely resemble those evident in to be published in Journal of
the direct extrapolations both insofar as Materials.
the temperature dependence of strength,
and also with respect to the difference
between coarse-grained and fine-grained
materials. The differences amongst the
different product forms, revealed by the
parameter evaluations are of interest.
It is possible that these differences re-
late to basic differences in composition
and practice. For example, the superior-
ity of plate relative to pipe-tube at the
lower temperatures (lower values of para-
meter) may reflect, principally, the wide-
spread use of coarse-grained deoxidation
pracitce for plate and of fine-grained
practice for pipe-tube.
Whether the results of the direct
extrapolations or of the parameter extra-
polations offer the better assessment of
the strength of carbon steel is probably
not capable of convincing resolution,
except as 100,000 hour test results be-
come available. However, the differences
for all data are not large, amounting
to only 1-2 percent at 800°F and increas-
ing progressively to about 11% at 1000°F,
with the direct extrapolation always the
more conservative. It is of interest
that the disparity between the two types
of extrapolation is of about the same
percentage magnitude at 10,000 hours as
at 100,000 hours. Yet, the error in
the extrapolated value is expected to
increase with increasing time for rupture.
Acknowledgments
References
9
TABLE I-P
1 2
Code No. Specification Deoxid. Heat Treatment ASTM :"ro<~cict Data
Number Pract. Grain Size Source
Size
10
Table I-P, continued
1 2 Data
Code No. Specification Deoxid. Heat Treatment ASTM Pr'oduct
Number Pract. Grain Size Source
Size
11
Table 1-P, continued
1 2
Code No. Specification Deoxid. Heat Treatment ASTM Product Data
Number Pract. Grain Size Source
Size
P-30 b II
" N 1650°F (bottom " II
(Bot.) of plate)
Note: Plate steel data on pages 33-39 of ASTM DS 11 are identical with
Code Nos. p 20-P 25 of this report.
12
TABLE I-T
T-1 A-210 F. G.; Si- T 1300°f 6-8 ME 3 /4" Bar Babcock and
Al Wilcox Co.
T-2 a A-210 Not given N 1600°F 5" OD x "
. 500"
T-2 b " Not given N 1600°F 2-1/2" x "
. 280 11
T-3 A-210 Not given N 1650°F; 2" OD x "
T 1300°f . 500"
T-4 A-192-A Si-Al N 1700°F 3/4" Bar "
T-5 A 106-B F. G.; As Rolled 6-8 ME 10-5/8" x 11
S.i.-Al . 843"
T-6 A 106-B C. G.; s i- As Rolled 7-8 8-5/8 11 OD "
Al-Ti x . 9 06"
T-7 A 106-C Not given N 1600°F; Hollow "
SR 1150°f Forged
Pipe
13
Table I-T, continued
11
T-22 b " " SR 1150°F " "
T-23 A 192 F. G.; Al CD; A 1275°F 2.50"0D x U.S. Steel
.150" Corp.
T-24 11
" " " 11
T-25 " fl
" " "
T-26 11 11 11
" "
T-27 " " " " "
-_': Some lots although made to pipe or tube specification were tested as
forged bar.
OS Identi-
fication
ST-1 A 192-A Si-Al N 1700°F 3/4" Bar Pg. 18, No.l
ST-2 1020 "Prob. 2 . 4 11 OD x Pg. 3 2 ' No.5
Annealed" 1/4"
ST-3 A-210 F.G.; Si-Al T 1300°F 6-8 3/4 11 Bar Pg. 32, No.6
ME
Note: Pipe steel data on pages 41-46 of AS.TM DS 11
are identical with Code Nos. T 20- T 22
14
TABLE I-B
B-1 Not given Al(.8 lb)- N 1650°F 1-3 l" U.S. Steel
Ti(.3 lb) 5-7 Corp.
B-2 " F. G.; Si-Al N 1650°F 6-8 l" "
(1. 4 lb)
B-3 " F. G.; Al N 1650°F 6-8 1" "
( 1. 8 lb)
B-4 " C. G.; Si N 1650°F 1-3 l" "
rr
B-5 C. G.; Si-Al N 1650°F 1-3 l" "
(. 4 lb)
B-6 " F. G.; Al N 1650°F 6-8 l" "
( 1. 4 lb)
B-7 " F. G.; Si-Al N 1650°F 6-8 l" "
( 1. 4 lb)
B-8 " F. G. ; Al N 1650°F 6-8 l" "
(1. 2 lb)-
Ti ( . 3 lb)
15
Table I-B, continued
SB-7 b Not given Si-Al Hot Rolled 5-6 ME 111 Pg. 20,
No. 10
SB-7 c II II
N 1725°F; II II
Pg. 20,
T 1200°f No. 11
(1 hr)
SB-7 d II II
N 1725°F; II II
Pg. 21,
T 1200°f No. 12
(1 wk)
SB-8 a II
Si-Al Hot Rolled 4-5 ME It
Pg. 21,
No. 13
SB-8 b II II
N 1725°F; II II
Pg. 21,
T 1200°f No. 14
(1 hr)
SB-8 c Not Given Si-Al A 1550°F 4-5 ME 111 Pg. 21,
No. 15
II
SB-8 d II
N 1725°F; II II
Pg. 2 2'
T 1200°f No. 16
(1 wk)
SB-9 a II
''Killed 11 N 1650°F; 1 ii Pg. 22,
T 12Q00f No. 17
(100 hrs)
SB-9 b II II
N 1650°f II
Pg. 22,
No. 18
II II II
SB-9 c T 1300°F Pg. 22,
(100 hrs) No. 19
II
SB-10 Si-Al N 1650°f 6-8 Pg. 22,
No. 20
II
SB-11 Si-Al N 1650°f 7-8 Pg. 23,
( 2. 5 lbs) No. 21
II
SB-12 Si-Al N 1650°f 7-8 Pg. 23,
( 2 lbs) No. 23
SB-13 II
Si-Al-Ti N 1650°f 7-8 Pg. 23,
No. 24
SB-14 II
Si A 1625 1-4 ME 7 I 8 II Pg. 31,
No. 2
II
SB-15 Si-Ti N 1650°f 6-8 Pg. 31,
No. 3
SB-16 II
Si A 1550°F 3 I 4 II Pg. 31,
No. 4
SB-17 II
Si-Al N 1650°f 8. 9 Pg. 32,
( 1. l3 lbs) No. 7
II
SB-18 Si N 1650°F 4-8 Pg. 50,
No. 1
SB-19 a II
Si-Al A 1550°f 8 Pg. 51,
( 1. 2 lb) No. 7
16
Table I-B, continued
17
TABLE II
Chemical Composition of Carbon Steels - Weight Per Cent
Code No. c Mn p s Si Cr Ni Mo Cu Al N v Co Sn
Plate
P-1 a,b . 28 .74 .012 .023 . 27 . 02 . 02 .04 .007
P-2 . 28 .71 .012 .022 .19 . 07 .007
P-3 a,b . 27 . 65 .017 .021 . 22 .15 .006
P-4 . 28 . 70 . 25 . 02 Nil . 03 . 07
P-5 . 23 . 73 .018 .011 .18 . 05 . 01 . 01 . 05
P-6 .15 .51 .008 .022 .19 . 01 .005
P-7 .24 . 96 . 011 . 027 .043 .058 .002 .006
.......
00
P-8 a,b .15 .51 .008 .022 .19 . 01 .01 .005 .13 .005 .004 .005
P-9 a,b .15 . 50 .011 .031 .19 .028 .01 .005 . 07 .005 .007--.005
P-10 a,b . 29 . 80 .009 .016 . 25 . 011 . 01 .005 .12 .005 .006
P-11 a,b . 29 . 78 .018 .027 . 23 .027 . 02 .005 . 07 .005 .007 .005
P-12 . 20 .40 .007 .016 . 03 .010 .009 .002 .10 .005 .003 . 00 5 .021
P~l3 . 21 .40 .007 .018 . 06 .014 .015 .002 . 06 .005 .005 .005 .022
P-14 .12 . 76 .011 .017 . 23 . 05 . 08 .01 .11 . 05 .0076 . 01
P-15 .12 . 76 .012 .024 .17 .10 . 07 .01 .12 .047 .0065 . 01
P-16 . 23 1. 01 .010 .019 .17 . 06 . 08 .01 . 07 .032 .0062 . 01
P-17 a,b . 28 .74 .012 .023 . 27 . 02 . 02 .04 .007
P-18 a,b .27 . 65 .017 .021 . 22 .15 .006
P-19 . 28 . 71 .012 .022 .19 . 07 .007
P-20 .16 . 55 .013 .032 .24 .005 .004
P-21 .19 . 57 .023 .034 .19 .006 .005
P-22 . 20 .66 .028 .034 . 27 .015 .005
Table II, continued
Code No. c Mn p s Si Cr Ni Mo Cu Al N v Co Sn
Code No. c Mn p s Si Cr Ni Mo Cu Al N v Co Sn
Code No. c Mn p s Si Cr Ni Mo Cu Al N Ti Sn
B-6 .27 .54 .008 .028 .054 .038 .009 .004 .032 .005
B-7 .26 .48 .007 .025 .27 .026 .011 .06 .029 . 00 6
B-8 .18 .40 .007 .021 .032 .022 .007 .003 .016 .004 .006
-
t.:>
Table I I I - p
22
Table III-P, continued
Code No. Test Yd. St. Tensile St. Elong. Red. Area
Temp. °F
23
Table III-P, continued
Code No. Test Yd. St. Tensile St. Elong. Red. Area
Temp. Of
P-13 75 3 2. 3 58. 6 3 8. 0 6 3. 5
200 3 0. 5 5 9. 3 25.0 59.0
400 29. 5 77.8 20.0 45.2
500 2 5. 6 74.1 27.0 48.7
600 25. 3 65.5 37.0 62. 0
800 23.4 44.2 44.0 76.4
1000 15.8 26.9 5 3. 5 77.5
24
Table III-P, continued
Code No. Test Yd. St. Tensile St. Elong. Red. Area
Temp. Of
25
Table III-P, continued
Code No. Test Yd. St. Tensile St. Elong. Red. Area
Temp. Of
26
Table III-P, continued
Code No. Test Yd. St. Tensile St. Elong. Red. Area
Temp. Of
27
Table III-P, continued
Code No. Test Yd. St. Tensile St. Elong. Red. Area
Temp. °F
28
Table III-P, continued
Code No. Test Yd. St. Tensile St. Elong. Red. Area
Temp. Of
29
Table III-P, continued
Code No. Test Yd. St. Tensile St. Elong. Red. Area
Temp. °F
30
Table 111-P, continued
Code No. Test Yd. St. Tensile St. Elong. Red. Area
Tern Of
31
Table III - T
32
Table III-T, continued
33
Table III-T, continued
T-22 a 75 3 7. 5 72.0 3 8. 5 6 0. 0
200 34.0 67. 6 31. 5 60.0
400 34.5 75.05 21. 0 48.0
600 31. 0 73.8 36.0 59. 0
800 30. 3 57. 0 40.0 76.0
1000 23. 3 33. 2 59. 5 81. 0
~·,
This value lS unreasonable and lS assumed to be erroneous.
34
Table III - B
35
Table IV - P
( 2)
Code No. Temp. 1000 psi Test(l) Larsen- Min. Creep At Rupture - %
°F Stress Duration Miller Rate %/hour Elong. R.A.
Hours Parameter
oo-3)
(1) All tests to rupture except those designated C, which were discontinued
before rupture.
( 2) P=T(C+log t), where T is degrees Rankine, t is time for rupture in hours,
and C is a constant here assumed to have a value of 20.
36
Table IV-P, continued
( 2)
Code. No. Temp. 1000 psi Test(l) Larsen- Min. Creep At Rupture - %
°F Stress Duration Miller Rate %/hour Elong. R.A.
Hours Parameter
oo-3)
37
Table IV-P, continued
( 2)
Code. No. Temp. 1000 psi Test(l) Larsen- Min. Creep At Rupture - %
°F Stress Duration Miller Rate %./hour Elong. R.A.
Hours Parameter
(10-3)
38
Table IV-P, continued
( 2)
Code No. Temp. 1000 psi Test(l) Larsen- Min. Creep At Rupture - %
°F Stress Duration Miller Rate %/hour Elong. R.A.
Hours Parameter
c10-3)
Test(l) ( 2)
Code No. Temp. 1000 psi Larsen- Min. Creep At Rupture - %
Of Stress Duration Miller Rate %/hour Elong. R.A.
Hours Parameter
(l0-3)
40
Table IV-P, continued
Test (1) ( 2)
Code No. Temp. 1000 psi Larsen- Min. Creep At Rupture - %
or Stress Duration Miller Rate %/hour Elong. R.A.
Hours Parameter
oo-3)
41
Table IV - T
Test(l) ( 2)
Code No. Temp. 1000 psi Larsen- Min. Creep At Rupture - %
Of Stress Duration Miller Rate %/hour Elong. R.A.
Hours Parameter
oo-3)
(1) All tests to rupture except those designated c' which were discontinued
before rupture.
( 2) P=T(C+log t); c assumed to have value of 20
42
Table IV-T, continued
( 2)
Code. No. Temp. 1000 psi Test(l) Larsen- Min. Creep At Rupture - %
°F Stress Duration Miller Rate %/hour Elong. R.A.
Hours Parameter
oo-3)
43
Table IV-T, continued
( 2)
Code. No. Temp. 1000 psi Test(l) Larsen- Min. Creep At Rupture - %
°F Stress Duration Miller Rate %/hour Elong. R.A.
Hours Parameter
oo-3)
44
Table IV-T, continued
( 2)
Code No. Temp. 1000 psi Test(l) Larsen- Min. Creep At Rupture - %
°F Stress Duration Miller Rate %/hour Elong. R.A.
Hours Parameter
oo- 3)
45
Table IV-T, continued
Test(l) ( 2)
Code No. Temp. 1000 psi Larsen- Min. Creep At Rupture - %
Of Stress Duration Miller Rate %/hour Elong. R.A.
Hours Parameter
c10-3)
46
Table IV-B
Code No. Temp. 1000 psi Test(l) Larsen-( 2 ) Min. Creep Percent
°F Stress Duration Miller Rate-%/hr Elong Red. Area
Hours Parameter
(10-3)
47
Table IV-B, continued
(2)
Code No. Temp. 1000 psi Test(l) Larsen- Min. Creep Percent
°F Stress Duration Miller Rate-%/hr Elong. R. A.
Hours Parameter
c10-3)
48
Table IV-B, continued
Test(l) ( 2)
Code No. Temp. 1000 psi Larsen- Min. Creep Percent
Of Stress Duration Miller Rate-%/hr. Elong. R. A.
Hours Parameter
<10-3)
49
Table V
Carbon Steel
Temp.°F CG-NT CG-T FG-NT FG-T (CG+FG)-T CG-NT CG-T FG-NT FG-T
75 1. 00 1. 0 1. 0 1. 0 1. 0 1. 0 1. 00 1. 0 1. 0
100 .978 .975 . 99 .987 .985 .988 .980 .975 .975
200 .927 .911 .959 .936 .928 .961 .941 .932 .919
300 .945 .908 .943 .875 .880 1. 07 3 1. 015 1. 013 .930
400 0 938 .879 .918 .801 .830 1.162 1. 094 1. 090 .953
500 .891 .813 .881 .748 . 7 80 1. 172 1. 117 1.106 .962
600 .825 .738 .836 .708 .732 1.101 1. 07 5 1. 048 .935
700 .773 .688 . 79 0 .674 .688 .976 .978 .931 .864
800 .750 .673 .748 .637 .649 .833 .848 .785 .753
900 .728 .640 .703 .583 .606 .689 .702 .639 .614
1000 .608 .554 .635 .503 .542 .519 .541 .511 .467
1100 .500 .385 .391
1200 .265 .227
50
Table VI
Plate
P-1 a 2 3. 0 6.4
P-1 b 24.0 6. 6
P-2 25.0 14.1 6. 8
P-3 a 15.4
P-3 b 15.0
P-4 6.4
P-5 30.0 16.2
P-8 a 21. 8 10.1 5. 7
P-8 b 21. 5 10. 3 5.6
P-10 a 24.5 13.0 7.4
P-10 b 6.0
P-20 7.1
P-21 5.4
P-22 6. 3
P-23 a 7. 3
P-24 a 6.9
P-25 7.0
P-26 a 15.2 3. 4
Pi:ee-tube
T-1 15.6 8. 6
T-2 a 19.0 8.4
T-2 b 15.4 8.5
T-3 19.9 11.1
T-4 12.1 6.5
T-5 (same as T-20 a)
T-6 (same as T-22 a)
T-7 25.1 13.8
T-8 10.6 5. 8
T-9 16.4 9.5
T-10 20.5
T-11 19.5
T-12 2 0. 8 8. 8
T-13 18.8 8.4
T-14 21. 5 8. 7
T-20 a 6. 6
T-21 a 6.7
T-22 a 7.6
T-23 15.1 8.7
T-24 15.2 9. 0
T-25 16.6 10.0
T-26 15.2 10.0
T-27 14.7 8.4
51
Table VI, continued
Bar
SB-2 13.2
SB-3 13.0
SB-4 26.8 15.0 6. 8
SB-10 20.7
SB-11 13.l
Sb-12 13.1
SB-13 17.1
SB-15 19.2
SB-17 17.0
SB-18 20.0
SB-22
SB-24 14.2
SB-25 17.2
52
Table VII
Plate
P-1 a 21.1 3. 3
P-1 b 22.8 2. 7
P-2 23.2 9. 5 4.8
P-3 a 12.8
P-3 b 25.2 9. 2 4.1
P-5 36.0 15.0
P-8 a 23.0 6.5 3. 7
P-8 b 22.0 8.1 4.5
P-10 a 20.2 9. 0 3.4
P-10 b 26.0 10.0
P-20 3. 9
P-21 4.8
P-22 5.1
P-23 a ?
P-24 a ?
P-25 ?
P-26 a 14.0
Pipe-tube
T-2 b 18.5
T-7 21. 5 10.5
T-20 a 5. 4
T-21 a 5. 3
T-22 a 6.1
Bar
53
Table VII, continued
SB-13 13.0
SB-14 19.2 11. 2 7.1
SB-15 17.2
SB-16 12.2 3.4
SB-17 a 7.1
SB-23 13.8 8.1 3.0
SB-26 2. 2
SB-27 13. 3 4. 3
54
Table VIII
Plate
Pipe-tube
T-1 11. 8 6. 0
T-2 a 13.5 4.8
T-2 b 10.4 5. 6
T-3 16.4 8.0
T-4 8. 9 4.4
T-5 3. 9
T-6 4.7
T-7 19.0 9.1
T-8 7.7 3. 9
T-9 11. 9 7.2
T-10 17. 0 ,•: ~':
T-12 16.1 5. 7
T-13 14.3 5. 3
T-14 16.5 5. 6
T-20 a (same as TS)
T-21 a 4.1
55
Table VIII, continued
Code No. Temperature Of
800 850 900 950 1000 1050
Bar
SB-2 10.0
SB-3 9. 6
SB-4 21. 0 10. 8 2. 8
SB-10 16. 8i:
SB-11 9. 0 ,•:
SB-12 '"' :'"' :
SB-13 13.5
SB-15 15.0
SB-17 13. 5'':
SB-18 15. 5'':
SB-22 ~': ~·:
56
TABLE IX
Plate
Pipe-tube
T-2 b
T-7
T-20 a 3. 2 ;':
T-21 a 3 . 1 ~·:
Bar
57
Table IX, continued
SB-13 10.0
SB-14 13.2 8.4 2.1
SB-15 13.5
SB-16 7. 6 2.1
SB-19 a 4.7
SB-23 8. 5 5. 5 1. 4
SB-26 1. 4
SB-27 b 9. 6 3.1
58
Table X
Average
Temp. Of All data C.G. f.G. All data C.G. f.G. Bar Pipe- Plate
Tube
800 21. 35 24.83 18.2 21. 6 24.8 18.3 21. 0 19.0 25.1
850 15.58 17.2 13.4 16.5 18.4 14.3 15.8 15.2 18.5
900 11.37 12.4 10.0 12.3 13. 4 11. 0 11. 5 12. 0 13.3
950 8.30 8.7 7.4 9.1 9. 6 8. 5 8.0 9. 4 9.4
1000 6.05 6.31 5. 5 3 6. 7 6. 8 6. 5 5. 5 7.4 6. 8
1050 4.41 4.4 4.05 4.9 4.7 ·l: ·;': ~·:
5 .1
Temp. Of All data C.G. f.G. All data C.G. f.G. Bar Pipe- Plate
Tube
800 15.7 19.2 13.8 15.3 19.6 14.0 15.8 13.6 19.5
850 11. 3 13.7 10. 0 11. 8 14.7 10.9 11. 8 10.9 14.3
900 8. 2 9. 7 7. 5 8. 8 10.7 8.4 8. 6 8.6 10.3
950 6. 0 6. 9 5. 5 6. 5 7.6 6. 5 6. 0 6. 8 7.4
1000 4.4 4.9 4.1 4.8 5.4 4.9 4.1 5. 3 5. 3
3. 5 3.7 ~·: ~·: ~·:
1050 3. 2 3. 5 3.05 4.0
59
Table XI
Average
800 15.85 15.94 14. 2 12.8 17.7 16.2 18.0 14.1 15.5 15.0 18.3
850 11. 35 11. 40 9. 6 9. 0 12.3 11. 9 13.0 10.8 11.1 11. 9 12.8
900 8.11 8.18 6.94 6.4 8.8 8.7 9. 2 8.1 7. 7 9. 2 9.1
950 5. 8 0 5. 9 0 5. 36 4.5 6.3 6.4 6.4 6.2 5. 2 7.1 6. 5
1000 4.15 4.17 4.42 3.35 4. 5 4.6 4.3 '': '"' : ,•: 4.8
1050
800 11. 0 12.0 11. 2 10.8 13.2 11. 7 14.5 10.8 11. 7 10.8 14.1
850 7. 8 8. 5 7. 7 7. 7 9.4 8. 6 10.3 8. 2 8.3 8.4 10.0
900 5. 6 6.1 5. 5 5.4 6. 7 6.3 7. 3 6. 2 5. 8 6. 6 7.1
950 4.0 4.15 4.25 3. 9 4.7 4. 6 5.1 4. 7 3. 9 5.1 5.1
1000 2.9 3.1 3. 55 2.75 3. 3 3. 7 3.4 "t': ,•: "i': 3.8
1050
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x:
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:
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_; r:;+;~ .ITT:~ ~t ;:"li-;;i
.:;;.-=- :rr..+-rr; ~i.~-~ ~ :f +r , E ~Bf~~ :F~ ~:g
~9- S~J -.: ~i ,. -" ~ r.n. :§; m H~ ·ff· r~- ¥ ·:.::;
-~= =.::i~ ::-;·:~--~ nS: ~ ;:.;:l:.'.f~:,...:1-:IJ§ff: ~
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Fig. 4b Variation of tensile strength with temperature; coarse-grain, not tempered
63
Fig. 4c Variation of yield strength ratio with temperature; coarse grain, not tempered
Fig. 4d Variation of tensile strength ratio with temperature; coarse-grain, not tempered
64
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tempered.
66
Fig. Sc Variation of yield strength ratio with temperature;
coarse-grain, tempered.
67
TEMPERATURE °F
Fig. 5e Fracture ductility of coarse-grain~ tempered steels.
68
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69
Fig, 6c Variation of yield strength ratio with temperature;
fine-grain, not tempered.
70
Fig. 6e Fracture ductility of fine-grain, not-tempered steels.
71
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Fig. 7a Variation of yield strength with temperatuee;
fine-grain, tempered
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73
TEMPERATURE °F
Fig. 7e Fracture ductility of fine-grain, tempered steels.
74
Fig. Ba Variation of yield and tensile strength ratios with
temperature for miscellaneous carbon steels.
75
Fig. 8b Variation of fracture ductility with temperature
for miscellaneous carbon steels.
76
1-:!-·-
77
Fig. 9b Variation of fracture ductility with temperature for
miscellaneous carbon steels from DS 11.
78
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Fig. lOa Stress vs time for rupture; all data: 800 and 850 F .
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Fig. lOb Stress vs time for rupture; all data: 900 and 950 F
79
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Fig. lOc Stress vs time for rupture; all data: 1000 and 1050 F.
100
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Fig. lla Stress vs secondary creep rate; all data: 800 and 850 F.
80
Creep Rate - Per Cent per 100,000 hrs.
Fig. llb Stress vs secondary creep rate; all data: 900 and 950 F.
Fig. llc. Stress vs secondary creep rate; all data: 1000 and 1050 F.
81
10 100 1000 10,000 100,000
TIME TO RUPTURE - hours
Fig. 12a Variation of rupture ductility with time fQ.r rupture; all. data: 800 F .
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Fig. 12b Variation of rupture ductility with time for rupture; all data: 850 F
82
TIME TO RUPTURE - hours
Fig 12c Variation of rupture ductility with time for rupture; all data: 900 F.
Fig. 12d Variation of rupture ductility with time for rupture; all data: 950 F.
83
TIME FOR RUPTURE - hours
Fig. 12e Variation of rupture ductility with time for rupture; all data: 1000 F.
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Fig. 12f Variation of rupture ductility with time for rupture; all data: 1050 F
84
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Fig. 13a Variation of creep strength (0.1% per 1000 hrs) and rupture
strength (10000 hrs) w<ith temperature; all data.
85
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Fig. 13b Variation of creep strength (0.01% per 1000 hrs) and
rupture strength (100,000 hrs) with temperature; all data.
86
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strength (10,000 hrs)
87
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89
Fig. 16 Linear regression lines for log-log scatter bands of
stress vs rupture time, extended to 100,000 hrs. Time taken
as independent variable.
90
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Fig. 17a Variation of Larson-Miller parameter with stress for
rupture of carbon steel bar.
91
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rupture of carbon steel pipe and tube.
92
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Fig. 18 Effect of deoxidation practice and product form on
average Larson-Miller parameter regression curves.
94