EXPERIMENT 9 Data sheet

COMPLEXOMETRIC TITRATION
Group number Section Score
Seat number Name Date

1. Preparation and Standardization of EDTA solution

I II

Mass of CaC03

Final volume reading (EDTA solution)

Initial volume reading (EDTA solution)

Volume consumed (EDTA solution)

Computed Molarity of EDTA solution

Mean Molarity

Computed Normality of EDTA solution

Mean Normality

Equatlon/s involved:

Computations:

·-
11. Determination of Total Hardness of Water

Source of water sample:

I II

Volume of water sample

Final volume reading (EDTA solution)

Initial volume reading (EDTA solution)

Volume consumed (EDTA solution)

Molarity of standard EDTA solution used

Total hardness of water (ppm CaC03)

Average Total Hardness

Equation/s Involved:

Computations:
 EXPERIMENT 9 Post-lab
COMPLEXOMETRIC TITRATION
Group number Section Score
Seat number Name Date

1. Determine the molar concentration of an EDTA solution of which 26.44 ml were required to titrate a
sample containing 287.4 mg of primary standard CaCO 3•

2. Discuss the color changes that occurred in EDTA titration. Show the formula if necessary.

3. What does hardness of water mean?

4. What are the disadvantages of using hard water?

s. A 50.00-ml aliquot of standard CaCO3 (0.3834 g CaCO3 per liter) consumed 42.35 ml of EDTA solution .
The same EDTA standard solution was used for the titration of a 3.00-ml water sample. This required
30.56 ml of the titrant. Calculate the molar concentration of EDTA standard solution. What is the total
hardness of water sample?
EXPERIMENT 10 Pre-Lab
REDOX TITRATION

Group number Section Score

Seat number Name Date

1. Why Is it required to use pre-boiled distilled water and Na 2C0 3 in the preparation of standard
Na2S203 solution?

2. Write the balanced reaction involved in the standardization of Na 2S2 0 3 • Describe the endpoint in
this process.

3. Ascorbic acid can also be determined by acid-base titration. What is the advantage of using
redox titration in the determination of ascorbic acid instead of acid-base titration?