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Fast RGA 1058 on Agilent 7890

Contents

Contents
Contents............................................................................................................... ii
Pre-installation Requirements ........................................................................ 1-2
Gas Requirements............................................................................................ 1-3
Gas Purity ........................................................................................................ 1-3
Physical Requirements.................................................................................... 1-4
Electrical Requirements .................................................................................. 1-5
Recording Important Numbers ....................................................................... 1-6
Installing the Hardware.................................................................................... 2-2
Introduction ...................................................................................................... 2-2
Cabling (General) ............................................................................................ 2-2
Connecting the gases ...................................................................................... 2-3
Column Installation .......................................................................................... 2-3
Introduction ...................................................................................................... 3-2
PAC RGA 1058 Separation Range.................................................................. 3-2
Configuration.................................................................................................... 3-3
Sequence of Analysis ...................................................................................... 3-6
Front channel (FID).......................................................................................... 3-6
TCD 2B channel .............................................................................................. 3-7
TCD 3C channel .............................................................................................. 3-8
Separation overview ........................................................................................ 3-9
Refinery Gas Analysis ..................................................................................... 3-9
Front (FID) Channel # 1............................................................................... 3-9
TCD Channel # 2 ......................................................................................... 3-9
Back (TCD) Channel # 3.............................................................................. 3-9
LPG analysis.................................................................................................. 3-11
Special Calculations ...................................................................................... 3-13
Operation ........................................................................................................ 3-14
Calibration....................................................................................................... 3-15
Calibration Procedure .................................................................................... 3-15
Method description ........................................................................................ 3-16
Spare parts kit and consumables kit PAC Fast RGA .................................. 3-17

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1

Pre-installation Fast RGA


Pre-installation Fast RGA
Pre-installation Requirements
Pre-installation Requirements
This chapter contains pre-installation procedures for PAC Refinery Gas Analyzer.
Because the PAC Refinery Gas Analyzers are based upon the Agilent 7890
Series gas chromatograph (GC), make sure your laboratory meets the
environmental, weight, power, and gas requirements as described in the Site
Preparation and Installation Manual for the Agilent GC. This section contains gas
requirements, physical requirements, electrical requirements, a pre-installation
checklist for the PAC Refinery Gas Analyzer, and a record form.

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Pre-installation Fast RGA
Gas Requirements
Gas Requirements
Gas Purity
Some gas suppliers furnish “instrument” or “chromatographic” purity grades of
gas that are intended specifically for chromatographic use. We recommend only
these grades for use with Agilent GC detectors.

Only very low ppm levels (≤0.5 ppm) of oxygen and total hydrocarbons should be
present in the gas supplies. Oil-pumped air supplies are not recommended
because they may contain large amounts of hydrocarbons. The addition of high-
quality moisture, hydrocarbon, and oxygen traps immediately after the main tank
pressure is highly recommended. Refer to the section "Gas Plumbing" of the
Agilent GC Site Preparation and Installation Manual for more information on
using traps.
Table 1-1. Gas Purity Recommendations
Carrier Gases
Gas type Helium Hydrogen Nitrogen
Pre- 6 bar 6 bar 5 bar
pressure 90 psi 90 psi 75 psi
Percent 99.995% 99.995% 99.995%
purity

Flame Ionization Detector Support Gases


Gas type Hydrogen Makeup gas Air
(same as carrier
gas)
Percent 99.995% 99.995% (water- and oil-
purity free) from a
compressor

Note It is preferred not to combine the air for valve switching with the air for the FID.

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Pre-installation Fast RGA
Physical Requirements
Physical Requirements
• Width - Approximately 2.1 meters (7 feet) for the complete system.

• Depth - Approximately 0.6 meters (2 feet) for the complete system.

• Height - Approximately 0.8 meters (2 feet 8 inches) for the complete system.

• Weight - 70 KG (155 lb.)

The analyzer may be installed in any reasonably accessible area.

WARNING THE GAS CHROMATOGRAPH WILL VENT HOT OVEN AIR FROM THE REAR
OF THE GAS CHROMATOGRAPH WHEN THE OVEN IS COOLING DOWN TO
AMBIENT TEMPERATURE. ENSURE NOTHING IS PLACED BEHIND THE
GAS CHROMATOGRAPH THAT MAY CONTACT THE HOT EXHAUST AIR.
PAC MANUFACTURES AN ALUMINUM "OVEN EXHAUST DEFLECTOR"
THAT DEFLECTS THE EXHAUST AIR UP, AWAY FROM THE REAR OF THE
GAS CHROMATOGRAPH. THIS DEVICE EASILY AND QUICKLY ATTACHES
TO THE REAR OF THE GAS CHROMATOGRAPH. PLEASE CONTACT YOUR
LOCAL PAC OFFICE SHOULD YOU DESIRE TO INSTALL THIS DEVICE.

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Pre-installation Fast RGA
Electrical Requirements
Electrical Requirements

Note A proper earth ground is required for GC operations.

For North America and geographical areas that use 110 - 120 VAC :
• Gas chromatograph: 110 - 120 VAC, 20 Amp grounded service. Please refer
to the Agilent manual for additional information if required.

• All accessories: 110 - 120 VAC, 4 standard 3 prong grounded outlets.

For Europe and geographical areas that use 220 - 240 VAC :

• Gas chromatograph: 220 - 240 VAC, 16 Amp grounded service. Please refer
to the Agilent manual for additional information if required.

• All accessories: 220 - 240 VAC, 4 grounded outlets

Maximum power consumption of the 7890 gas chromatograph is 2,250 VA for a


regular oven and 2,950 for a fast-heating oven.

Maximum power consumption of the TCD controller is 100 W.

Note Do not turn on the oven until all electrical and gas connections have been
completed and checked for correctness and leaks.

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Pre-installation Fast RGA
Electrical Requirements

Recording Important Numbers


In any verbal or written correspondence with PAC or Agilent concerning your
PAC Software or Data system software, you will need to know the following
information:

Take a few minutes now to fill in the empty boxes above. The revision code is
found on the diskettes or CD-ROM. The license numbers are found on the
documentation shipped with the software.

Gas XLNC License No.

Agilent G2070B Revision Code Example B.03.0X

Agilent G2070BA License No.

Microsoft Windows Type and Revision Code

Microsoft Windows License No.

Agilent Gas Chromatograph Serial No.

Agilent Computer Serial No.

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2

Installation Fast RGA


Installation Fast RGA
Installing the Hardware
Installing the Hardware
Introduction
This chapter contains installation procedures for the AC Hi-Speed Refinery
Gas Analyzers for the Agilent 7890 Series gas chromatograph (GC). Refer to
the Site Preparation and Installation Manual of the GC for installation
information.

Cabling (General)
The Agilent GC communicates electronically with other instruments through
cables. Refer to the section “Connecting Cables” of the Site Preparation and
Installation Manual of the GC.
• The Agilent 7890 Series GC is connected to the computer through LAN

Printer Computer
Hi speed RGA
7890

Mouse

1 - LAN interface PC - GC

Figure 2-1 Cabling configuration for the Agilent 7890 Series GC.

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Installation Fast RGA
Installing the Hardware

Connecting the gases


Connect the gases to the rear of the GC as indicated in Figure 2-2,

1 Connect the carrier gases; Nitrogen and Helium

2 Connect the instrument Air en FID Air (separate supply of the instrument air is
recommended)

3 Open the gas supplies and check the connections for leaks.

FID Air
Hydrogen
Aux 3
Aux 1

Aux 2

He He N2 N2
Nitrogen
Helium

Instrument Air

Figure 2-2 Rear side connections

Column Installation
AC Refinery Gas Analyzers come with pre-installed and checked-out columns.
WARNING TEMPERATURE-SENSITIVE ITEMS (GAS CYLINDERS, CHEMICALS,
REGULATORS, ETC) SHOULD NOT BE LOCATED IN THE PATH OF THE HEATED
EXHAUST. ALSO, EXERCISE CARE WORKING AT THE REAR OF THE
INSTRUMENT DURING COOL-DOWN CYCLES TO PREVENT POSSIBLE BURNS.

Please refer to the appropriate chapter in the Agilent GC manual for correct
installation of the capillary column.

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3

Operating the Fast RGA 1058


Operating the Fast RGA 1058
Introduction
Introduction
This section describes the operation, configuration, and analysis of the PAC Fast
Refinery Gas Analyzer 1058. This instrument is based upon the Agilent 7890 Series gas
chromatograph (GC). For more information, refer to the appropriate Agilent manuals for
detailed information on the Agilent GC.

The PAC RGA 1058 determines hydrocarbons from C1 up to C5+, carbon dioxide,
carbon monoxide, nitrogen, oxygen, helium, hydrogen and hydrogen sulfide. The
dedicated software controls all events within the system, performs calibration, and
reports the calculated physical properties and the individual component concentrations
of the refinery gas streams.

PAC RGA 1058 Separation Range


Hydrocarbons: C1–C5, C5+
Inert gases: oxygen, nitrogen, helium, hydrogen, carbon monoxide and carbon
dioxide
Hydrogen sulfide

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Operating the Fast RGA 1058
Configuration
Configuration
The PAC RGA 1058 application for determining the composition of refinery gases uses
an Agilent 7890 Series GC with electronic pneumatics control (EPC) configured with
six packed GC columns, a flame ionization detector (FID), two thermal conductivity
detectors (TCD), a sample shutoff valve, three injection/back-flush valves and a bypass
valve. The PAC RGA 1058 is a dedicated analyzer, which carries out the automatic
analysis of refinery gases.

The next figures illustrate the flow diagram, column positions, sequence of analysis,
chromatogram, data base and the report for the PAC RGA 1058. The tables show the
description and part numbers for the columns, the valves used in the instrument, the GC
method set points and the runtime table for the PAC RGA 1058.

off/on
Gas
Sample in
N2 (Aux 3) V1
Column 1 Column 5
2 1 2 1
10 10
3 9 3 9

4 8
FID 4 8

PCM A-1 H2
5
6
7 1A 5
6
7

V2 V3
Column 2 TCD
2B
TCD
V4 V5 3C
Column 3 Column 6
Sample out 2 1 1
10
3
NV 2 6
9
Column 6
He (Aux 1) 4 8 Vent bypass 3 5
5 7 Helium
6 He (Aux 2) 4

Column 4

Figure 3-1 The PAC RGA 1058 flow diagram.

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Operating the Fast RGA 1058
Configuration

Column 1

Column 2

Column 3

Column 4

Column 5

Column 6

Figure 3-2 The PAC RGA 1058 column positions in the GC oven.
Table 3-1 Columns for the RGA 1058 Configuration

Column Description Part No. for Maximum


Replacement temp °C
1 2 ft x 1/8 in., 2.1% Carbowax 1540 on Porasil C 84.51.010 150
(80/100)
2 17 ft x 1/8 in., 27.5% BIS 2 (EEA) on Chromosorb P 84.50.510 175
AW (45/60)* + 10 ft x 1/8 in., 2.1 % Carbowax 1540
on Porasil C (80/100)* + 5 in x 1/8 in., 0.4% Carbowax
1500 on Carbopak B (60/80)
3 1.2 m x 1/8 in., HayeSep Q (60/80) 84.58.110 250
4 6 in x 1/8 in., HayeSep T (80/100) 10.70.159 165
5 4 ft x 1/8 in., HayeSep Q (60/80) + 10 ft x 1/8 in., 84.50.210 250
Molecular Sieve 5A (45/60)
6 2.7 m ft x 1/8 in., Molecular Sieve 13X (45/60)* 84.56.010 375

The length of these columns is nominal. The columns are conditioned and tuned at the
factory to give the required separation and timing. All columns should be conditioned in
the system at 110°C except for column 6.

* Column 6 should be conditioned at 350°C. Therefore the column must be


removed and conditioned in a separate GC.

The maximum oven temperature is 175°C.

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Operating the Fast RGA 1058
Configuration

Table 3-2 Valves Used in the Instrument


Valves Function

Valve 1 Sample Shutoff Valve


Valve 2 Injection and fore flush / back flush Valve column 1
Valve 3 Injection and fore flush / back flush Valve column 5
Valve 4 Injection and fore flush / back flush Valve column 3
Valve 5 Bypass Valve column 6

Valve 1 is used to make reproducible and operator-independent injections. Valve 1


blocks the gas sample to the sample loops after flushing, allowing the pressure in the
sample loops to become atmospheric. The sample flush time and injection time are
sampling valve settings. (Gas Sampling Valve)

Note Valve 1 is configured as a gas sampling valve and the on/off settings are also in the
runtable. This allows the user to start the analysis both from the data system (run
method) as well as from the start button on the display of the GC.

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Operating the Fast RGA 1058
Sequence of Analysis
Sequence of Analysis
The actual analysis consists of three analytical channels that are operated
simultaneously.

Front channel (FID)


The sequence of analysis of the front channel of the AC RGA 1058 is as follows:

FID 1A Channel

Standby

FID
PCM A-1 H 2 Column 2 Column 1
1A

Injection (Valve 2 On)


Sample loop

FID
PCM A-1 H 2 Column 1 Column 2 1A

Backflush column 1 (Valve 2 Off)

FID
PCM A-1 H 2 Column 2 Column 1
1A

Figure 3-3: Sequence of analysis of the FID front channel

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Operating the Fast RGA 1058
Sequence of Analysis
TCD 2B channel
The sequence of analysis of the TCD 2B channel of the AC RGA 1058 is as follows:

TCD 2B Channel
Standby

TCD
Aux 3 (N2) Column 5
2B

Injection (Valve 3 On)


Sample loop

TCD
Aux 3 (N2) Column 5
2B

Backflush Column 5 (V3 Off)

TCD
Aux 3 (N2) Column 5 2B

Figure 3-4: Sequence of analysis of the TCD 2B channel.

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Operating the Fast RGA 1058
Sequence of Analysis
TCD 3C channel
The sequence of analysis of the TCD 3C channel of the AC RGA 1058 is as follows:

TCD 3C Channel
Standby

TCD
Aux 1 Column 4 Column 6
3C

Aux 2 Column 3 Vent He

Injection (Valve 4 On)

Sample loop

Aux 1 TCD
Column 3 Column 4 Column 6
3C

Aux 2 Vent He

Stopflow Column 6, backflush Column 3, elution Column 4


(Valve 5 On, Valve 4 Off)

TCD
Aux 1 Column 4 Column 6
3C

Aux 2 Column 3 Vent He

Elution column 6 (Valve 5 Off)

Aux 1 TCD
Column 4 Column 6
3C

Aux 2 Column 3 Vent He

Figure 3-5: Sequence of analysis of the TCD 3C channel.

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Operating the Fast RGA 1058
Separation overview
Separation overview
Refinery Gas Analysis
The RGA model 1058 determines helium, hydrogen, oxygen, nitrogen, carbon
monoxide, carbon dioxide, hydrogen sulfide, C1-C5 hydrocarbons and C5=+ in 20
minutes. The system consists of six columns and is subdivided into three separate
analytical channels. The first channel is the FID channel, here the C2 to C5
Hydrocarbons are determined. The second channel determines helium and hydrogen.
The third channel is used to determine oxygen, nitrogen, carbon monoxide, carbon
dioxide and hydrogen sulfide.

Front (FID) Channel # 1


This channel consists of one ten-port valve, a pre column, and a combi column
configured in series. Hydrogen gas is utilized as a carrier gas. An electronic flow
regulator controls the flow, and a FID detects the components.

The sample is introduced into the system using a sample loop that can be switched into
the flow using valve 2. The hydrocarbons are separated on column 1, back flushing
C5=/C6+ while the hydrocarbons C1 to C5 are separated on the second column. Ethane
and Ethylene co-elute and are therefore quantified on the TCD channel 3. Methane is
also quantified on this TCD.

TCD Channel # 2
The second channel consists of one ten-port valve and one column (column 5). The
carrier gas is Nitrogen, and a constant pressure regulator (Aux 3) controls the flow.

After the sample has been introduced into the system by switching valve 3 on, the
helium and hydrogen are separated on column 5. After the elution of hydrogen, the
heavier components are back flushed by switching valve 3 off again.

Back (TCD) Channel # 3


The third channel consists of one ten-port valve, one six-port valve, two HayeSep
columns and a Molsieve 13X column. The carrier gas is helium, and two electronic
constant pressure regulators (Aux 1 and Aux 2) control the flows.

The sample will be introduced into the system by switching valve 4 on. Oxygen,
nitrogen, methane and carbon monoxide quickly pass column 3 and 4 and are trapped on
the Molsieve column by switching valve 5 on.

The C2 gases, hydrogen sulfide and carbon dioxide elute from column 3 to column 4.
Just before the elution of the Propane, valve 4 is switched off, thereby back flushing all
remaining components from column 3 to vent. In the meantime the C2 components,
hydrogen sulfide and carbon dioxide are separated on column 4 and are detected by
TCD.

After the elution of Hydrogen sulfide from column 4, column 6 is put in flow again
(valve 5 off) and the permanent gases are separated and finally detected on TCD.

The next figures illustrate the chromatograms of the RGA 1058 analysis. All three
channels are operated simultaneously, yielding three chromatograms and one combined
report.

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Operating the Fast RGA 1058
Separation overview

Note Methane and Ethane/Ethylene are not calibrated on the FID. Acetylene is not calibrated
on the TCD.

pA
FID 1A signal

3.643 - Propane
2.606 - Ethane /Ethylene *
2.128 - Methane *

5.433 - iso-Butane
5000
1.522 - C5=/C6+

6.527 - n-Butane
4000
4.172 - Propylene

10.350 - 1,3-Butadiene
8.803 - t-2-Butene
3000
7.565 - 1-Butene
7.922 - iso-Butylene
3.966 - Acetylene

6.015 - Propadiene

9.389 - c-2-Butene

2000

11.870 - i-Pentane

14.605 - n-Pentane
1000

2.5 5 7.5 10 12.5 15 17.5 20 min

25 µV
TCD 2B signal
0.660 - Hydrogen

300

200

100

-100

-200

-300

-400

-500

2.5 5 7.5 10 12.5 15 17.5 20 min

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Operating the Fast RGA 1058
Separation overview
25 µV

14.925 - Nitrogen
TCD 3C signal
1750

1500

1250

1000
3.787 - Carbondioxide

18.525 - Carbonmonoxide
750

11.914 - Hydrogen sulfide


6.403 - Ethane

16.754 - Methane
5.228 - Ethylene

7.989 - Acetylene *

14.044 - Oxygen
500

250

2.5 5 7.5 10 12.5 15 17.5 20 min

Figure 3-6 The AC Refinery Gas Analyzer 1058 analysis.

LPG analysis
Optionally, the PAC RGA 1058 can be configured with a Liquid Sampling Valve
(LSV) for LPG analysis. The LSV allows the user to reproducibly introduce liquefied
samples (LPG) into the refinery gas analyzer, for the analysis of hydrocarbons only.

In that case, the liquid sampling valve is located in a left-hand side compartment of the
chromatograph and is actuated by an air actuator that is controlled by valve 6. See flow
diagram below.

The LPG sample is injected through the liquid sampling valve and enters the packed pre
column. The sample quickly passes on to the analysis column, where the LPG is
separated in an isothermal oven run. No back flush is used for LPG analysis.

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Operating the Fast RGA 1058
Separation overview
off/on
Gas
Sample in
N2 (Aux 3) V1
PCM A-1 H2
Column 1 Column 5
2 1 2 1
10 10
Liquid 3 9 3 9
Sample In
4 8
FID 4 8
S P
5
6
7 1A 5
6
7

w C V2 V3
0.06 µl Column 2 TCD
2B
V6
TCD
Liquid V4 V5 3C
Sample Out
Column 3 Column 6
Sample out 2 1 1
10
3
NV 2 6
9
Column 6
He (Aux 1) 4 8 Vent bypass 3 5
5 7 Helium
6 He (Aux 2) 4

Column 4

Figure 3-7 The PAC RGA 1058 configured with a liquid sampling valve

FID 1A signal
5.415 - IsoButane
6.582 - n-Butane
3.633 - Propane

12.306 - IsoPentane

15.357 - n- Pentane
2.587 - Ethane

0 2.5 5 7.5 10 12.5 15 17.5 20.0


min

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Operating the Fast RGA 1058
Special Calculations
Special Calculations
The AC RGA 1058 system defines many calculations for the analyst.
Table 3-3 Standard Gas Calculations Available
Refinery Gas Standard 1058

Compressibility of mixture
Ideal calorific value on molar basis (inferior and superior)
Ideal calorific value on mass basis (inferior and superior)
Ideal calorific value on volume basis (inferior and superior)
Real calorific value on volume basis (inferior and superior)
Ideal wobbe index (superior)
Real wobbe index (superior)
Density
Relative Density of LPG
Vapor Pressure of LPG

Gasxlnc software can be used to reduce operator involvement. The software contains a
standard data base for components. A user-friendly edit mode allows authorized users to
edit the data base. The software includes several standard report formats, and you can
create customized reports easily.

The AC RGA 1058 uses the Gasxlnc fully integrated with the data system in a Microsoft
Windows environment to control all GC functions. This integrated software package
automates all aspects of the calibration, calculation and customized reporting.

Note The calculations of the RGA method are based on a temperature of 288.15 K and a
pressure of 101,325 Pa. Contact PAC if calculations are required for a different
temperature.

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Operating the Fast RGA 1058
Operation
Operation
For detailed information on how to operate the data system, refer to the manuals of the
supplier. For information about the GasXLNC, refer to the corresponding manual.

For the RGA 1058 application, the following methods are supplied:
FASTRGA—a GC method for the Agilent 7890 Series GC
LPG—a GC method for the Agilent 6890N Series GC equipped with LSV
FASTRGA6890—a GC method for the Agilent 6890N Series GC

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Operating the Fast RGA 1058
Calibration
Calibration
Use GASXLNC for the calibration of your components. Refer to the operating manual of
GASXLNC for more information regarding calibration.

It is recommended that you perform calibrations on a regular basis. The system consists
of three detectors, one FID and two TCDs. The absolute response factors for each
detector are determined with calibration standards.

Note Because the PAC GAS XLNC operates on mole percentages, the concentrations must be
specified in mole %.

Warning The concentration of the calibration components must be within a 10% window of the
concentration of same components in the samples to be analyzed. A good practice is too
bracket your sample with a multilevel calibration using calibration concentrations just
below and above the final concentration of the sample components.

Calibration Procedure
1 Create a calibration set for your calibration gases

2 Use Gas XLNC to inject the calibration gas containing all compounds on both channels.

Note Set the sequence event for the first calibration analysis to “Start new calibration”.
3 Perform more calibration runs if you wish to average the response factors.

4 Use the calibration browser to view the calibration points in a plot and to discard
analyses that are faulty.

5 Recalibrate the calibration set if analyses are removed or updated.

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Operating the Fast RGA 1058
Method description
Method description
Table 3-4 GC Method set points PAC Refinery Gas Analyzer 1058
Oven
Initial temperature: 60°C
Initial time: 20.0 min
Front Inlet (H2) 225 kPa Flow front inlet (H2) 30 ml/min
Aux 1 (He) 280 kPa Flow (V3 off) 30 ml/min
Aux 2 (N2) (at Det.) 110 kPa Flow (V4 off) 30 ml/min
Aux 3 (N2) (at Vent N2) 250 kPa Flow (V3 on) 30 ml/min
Aux 2 (Valve box) 60 °C
FID TCD (Back detector)
Temperature: 190°C Temperature: 150°C
Hydrogen: 5 ml/min Reference Flow Nitrogen 45 ml/min
Air: 350 ml/min
TCD (aux detector leftside)
Temperature: 150°C
Reference Flow Helium 40 ml/min

Valve 1 0.01 Load Time Flush sample loops


Valve 1 0.90 Inject Time Stop flushing sample loops
Specifier Typical Time * Parameter and Description
set point
Valve 1 0.01 ON
Valve 2 0.10 ON Inject sample on FID channel
Valve 3 0.10 ON Inject sample on channel 2
Valve 4 0.10 ON Inject sample on channel 3
Valve 1 0.20 OFF
Valve 3 1.00 OFF Back flush column 5
Valve 2 1.10 OFF Back flush column 1
Valve 5 2.30 ON Close column 6
Valve 4 4.60 OFF Back flush column 3
Valve 5 13.80 OFF Elution column 6

*Times will be fine-tuned and included with checkout documentation for each gas analyzer.

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Operating the Fast RGA 1058
Spare parts kit and consumables kit PAC Fast RGA
Spare parts kit and consumables kit PAC Fast RGA
Spares parts kit RGA Model 1058 CCG2340.100
Valve 6-port nitronic 60 10.25.029
Valve 10-port nitronic 60 10.25.031
Actuator LSV/6, 10-port GSV 28431.002
Solenoid valve 5/2 24V smal 10.11.106
Valve, needle 10.15.009

Consumables kit RGA Model 1058 CCG2340.200


Molsieve 13X column (column 6) 84.56.010
Three column set RGA (Combi column) (column 2) 84.50.510
CW 1540 pre-column (column 1) 84.51.010
Hydrogen channel RGA column (column 5) 84.50.210
HayeSep T column (column 4) 10.70.159
HayeSep Q column (column 3) 84.58.110
GC, Filter, Triple for base 10.30.210
Gas sampling loop Sulfinert 50µL G1530A.974
Gas sampling loop Sulfinert 250 µL G1530A.976
Gas sampling loop Sulfinert 5 µL G1530A.971

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