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The correlations of air content measurements obtained with a new air Current ASTM and CSA specifications'·2 outline a
meter, called the mini air meter, and two other ASTM standard air number of procedures for determining the air content
meters were examined to establish the reliability of the new appara-
tus. The mini air meter uses the volumetric principle to determine the
of freshly mixed concrete. One of the most frequently
air content of fresh concrete. It weighs 8 lb (3.63 kg) and requires a used methods is the pressure method, ASTM C 231,
concrete sample approximately 1I 11 and 1128 the size of that needed Air Content of Freshly Mixed Concrete by the Pressure
by the conventional roller and pressure meters, respectively. The lab- Method. This procedure consists of applying a prede-
oratory work involved testing the air content of 21 concrete mixtures termined air pressure over a constant column of water
using the mini, roller, and pressure air meters. Both ¥a and 1 in. (9.5
and 25.4 mm) nominal size aggregates were used to make normal-
that is poured in a tight chamber containing a 345.6 in. 3
weight and lightweight concretes. The water-cementitious materials (5663 ml) concrete sample. The pressure compresses air
ratios of the mixes ranged between 0.22 and 0.51. The cement con- bubbles in the concrete and causes a drop in the water
tent varied from 450 to 910 lb/yd' (267 to 540 kglm'), with silica level at the neck of the device, which is calibrated to
fume added to some mixes. All mixes incorporated superplasticizers, read the total air volume. Since the applied pressure can
and air-entraining agents were also added to yield air content be-
tween 1.25 and 12.5 percent.
force water and air into aggregate voids, this method is
Results indicate that the mini air meter exhibits excellent linear limited to concrete that contains relatively dense aggre-
correlations with the other standard tests and provides a quick means gate. The results obtained with this method are sensi-
to monitor air content. For the materials employed in this investiga- tive to the degree of aggregate saturation, magnitude of
tion, the accuracy of air volume measurements recorded using the the applied pressure, and changes in barometric pres-
mini air meter does not seem to be influenced by the density of the
aggregate, nominal size of the aggregate, cement content, water-to-
sure. Therefore, the instrument needs to be calibrated
cementitious materials ratio, or the presence of additives. often to reflect the correct air content, especially when
low pressures are applied to detect large air volumes.
Another frequently used device is the volumetric air
Keywords: air entraining agents; air entrainment; air meters; fresh concretes;
measuring instruments; plasticizers. meter, ASTM C 173, Air Content of Freshly Mixed
Concrete by the Volumetric Method, or the roller me-
ter. This test consists of pouring water over a concrete
Air is entrapped naturally in fresh concrete and fre- sample, then sealing the chamber and agitating the wa-
quently is entrained to enhance the workability and co- ter to free the air from the fresh concrete. The inter-
hesiveness of fresh concrete. The presence of a well- mingling of the water and concrete washes the air out
dispersed air system can enhance the resistance of of the mortar. The rising air causes a drop in the water
hardened concrete to destructive cycles of freezing and level at the tapered neck of the apparatus, which is cal-
thawing, and to damage resulting from exposure to ibrated to reflect air volume. This test does not cause
seawater and deicing salts. Most specifications call for water to migrate into aggregate voids; therefore, it is
a total air content of 4 to 7 percent. However, an ex- suitable for concrete made with either dense or porous
cessive air volume can sharply reduce the strength of aggregates. This volumetric air meter requires a 130 in. 3
the concrete, especially in rich mixes. The actual air (2130 ml) sample, and when full, weighs approximately
content during placement may be considerably lower 38 lb (17 .2 kg). Considerable effort is therefore needed
than that initially intended, depending on the duration
of agitation and handling of the fresh concrete, its
temperature, and its fluidity. Therefore, the air content
should be monitored at the job site before accepting ACI Materials Journal, V. 87, No.4, July-August 1990.
and placing the fresh concrete to maintain effective Received Oct. 31, 1988, and reviewed under Institute publication policies.
Copyright © 1990, American Concrete Institute. All rights reserved, including
control over its quality and insure the desired proper- the making of copies unless permission is obtained from the copyright propri-
etors. Pertinent discussion will be published in the May-June 1991 ACI Mate-
ties of air entrainment in hardened concrete. rials Journal ifreceived by Feb. I, 1991.
Fig. 1-Pressure, roller, and mint air meters Fig. 2-Four components of the mini air meter
i 356 ACI Materials Journal I July-August 1990
measurements using this device was checked by mea- Table 1 - Procedure for using the mini air meter
r
I
suring the air volume of a concrete mix made with a
water-cement ratio of 0.60 and an aggregate-cement ra-
tio of 7 .0. 4 The performance of the new device was
1.
2.
Fill the inner bowl with freshly mixed concrete in two layers
of equal depth. Rod each layer 10 times with tapping rod at-
tached to the lid, and tap sides lightly.
Strike off the surface flush with the top of the bowl. Fill half
compared to that of a standard pressure meter. The of the outer tare with water and place the inner bowl inside
standard deviation and coefficient of variation of 16 it.
different measurements taken from 16 reproduced 3. Align the notches located on the flange of the top tapered
mixes were 0.5 and 10.5, respectively, using the mini air section with the pins protruding from the bottom tare edges.
Rotate the top section clockwise to insure a tight closure.
meter, and 0.32 and 7.0 using the pressure meter.
4. Fill the chamber with water. About 10 percent can be re-
placed with isopropyl alcohol.
EXPERIMENTAL PROGRAM
An experimental research program was undertaken at 5. Tighten the screw lid to seal the chamber, then invert and
j the University of California to evaluate the effects of
shake the apparatus 10 times to agitate the concrete and wa-
ter and cause the air to be removed from the concrete by
washing action. The device should be rotated at the end of
i aggregate size and porosity, content of cementitious
materials, and presence of admixtures on measuring the
each tip to facilitate mixing.
6. Set the apparatus in the upright position and allow one min-
air volume of fresh concrete using the mini air meter. ute for the air to bleed to the top.
The performance of the new device was also compared 7. Remove top cap and insert a slender nail down the tapered
to other conventional devices. A wide range of mate- section to clear any clogging.
rials and mix proportions were adopted; they included 8. Using a well-graduated syringe, fill the apparatus with iso-
the following parameters. propyl alcohol to dispel the foamy mass from the water sur-
face. Cover the top with a plastic cap to avoid evaporation
and allow one minute for air bubbles to continue rising to
Aggregates the top. Add more alcohol if needed to completely fill the
Two rounded gravels with maximum-size aggregate chamber.
(MSA) of % and 1 in. (9.5 and 25.4 mm) were used for 9. Record the volume of the added alcohol milliliter to the
nearest 0.5 mi., V
making normal-density concretes. An expanded-shale Air content, percent = [(V- 6)/200) · 100 = (V- 6)/2
aggregate of %-in. (9.5 mm) MSA was used for casting where 200 ml = sample volume and 6 ml = volume dis-
placed by the rod.
lightweight concretes. All mixes contained natural river
sand for the fine aggregate. The aggregate gradations 10. Whenever a large volume of air is expected in cohesive con-
crete, it is advisable to add more alcohol and agitate the
are plotted in Fig. 3. concrete until no significant changes can be detected. The fi-
nal air content should then be calculated as
Air content, percent = [V- (6 · T)] I 2
Water-cementitious materials ratios (w/cm) where T= number of test repetitions.
The w/em of normal weight concretes were chosen to
11. If the concrete mix contains aggregates larger than 1 in. (25.4
be 0.22, 0.33, and 0.50 to test the performance of very mm), wet-sieve the concrete as outlined in Section 4 of
high, moderate, and conventional strength concretes, ASTM C 172 to remove these large particles.
Q
LLI 80
z
Ci
1-
LLI
a: 60
fl.
LLI
> 40
i=
cr
..J
::;) PEA GRAVEL
::::&
::;) 20
0
SIEVE OPENING
l
EXPERIMENTAL RESULTS AND DISCUSSION M = 0.91 P + 0.34 (2)
Linear regression analysis was used to correlate air
volume measurements recorded with the different air where P is the percentage of air content estimated us-
meters. Fig. 4 compares the results of the mini air me- ing the pressure method. This line has a correlation
ter to those recorded by the other standard devices for coefficient of 0.986. The best-fit line relating the roller
17 normal-density concretes. Four of the concretes had and mini air measurements for all 21 normal-weight
1 in. (25.4 mm) MSA, and the remaining 13 had Vs in. and lightweight concretes was found to be virtually the
(9.5 mm) MSA. The analysis indicates a linear relation- same as that obtained with concretes containing nor-
ship between the measurements of the mini and roller mal-density aggregate [Eq. (1)]. The mini-roller rela-
air meters. The correlation coefficient was 0.991, with tionship for all tested concretes has a correlation coef-
a linear expression as follows ficient of 0.991 and can be written as follows
M = 1.03 R (1)
M = 1.03 R (3)
where M and R are the percentages of air content re-
corded using the mini and roller meters, respectively. The standard errors for predicting the value of M
Fig. 4 also shows a best-fit line between the air mea- from the linear relationships 1 and 2, using actual R
surements obtained by the pressure and mini air me- and P measurements, were computed to be 0.27 per-
ters. Unlike the mini-roller relationship [Eq. (1)], the cent and 0.36 percent, respectively. The 95 percent
mini-pressure linear estimate is not parallel to the 45 confidence limits of these estimates were found to be
deg line, which designates a 1: 1 correlation between all within ± 0.25 and ± 0.50 percent for Eq. (1) and
measurements from different devices. The deviation within ± 0.10 and ± 0.50 percent for Eq. (2).
from that line was especially large when the air content Fig. 6 shows three graphs that were fitted through
was greater than 7.5 percent. These high values were points relating the average of air content values that
estimated by exerting lower pressures, then multiplying were recorded by all three air meters versus individual
the readings by correction factors. However, these fac- measurements from each device. All air apparatuses
tors seemed to exaggerate the actual air content and yielded measurements that corresponded very well to
render the pressure meter unreliable for accurately the mean air volumes with best-fit lines close and nearly
measuring air volumes in excess of 7.5 percent, unless parallel to the 45 deg line. These equations are as fol-
the device is calibrated frequently. lows
13
•
A
PRESSURE METER
ROLLER METER
M= 1.03 R
CORR. = 0.991
11
a: NORMAL WEIGHT
LIJ
1- CONCRETE
LIJ 9
:::E
z
:E 7
a:
< 5 M = 0.80P+ 0.72
CORR. = 0.988
0~
3 5 7 9 11 13
% AIR • OTHER METERS
1
1 3 5 7 9 11 13
% AIR • OTHER METERS
13
t/)
a: •.. PRESSURE METER
ROLLER METER
AVO.= 0.98 M- 0.13
w 11 CORR. = 0.998
1- a MINI METER
w
::::&
w 9
w
a: AVO. = 1.02 R + 0.01
::c
1- CORR. = 0.997
u.. 7
0 AVO.= 0.94 P + 0.16
ci CORR. = 0.996
>
c
5
a: 3
cc
'#.
3 5 7 9 11 13
% AIR • INDIVIDUAL METER
Fig. 6-Comparison of averager0ir volumes to individual results for all tested con-
cretes
avg = 0.94 P + 0.16 (4) spectively. The average discrepancy between the calcu-
lated mean air content and each of the pressure, roller,
and mini air meter measurements were -0.05, 0.15,
avg = 1.02 R + 0.01 (5) and -0.10 percent, respectively.
It is especially interesting to determine the precision
avg = 0.98 M- 0.13 (6) of each device in measuring the air content of concretes
containing various amounts of mixing water and ce-
mentitious materials. Results obtained with the mini air
where avg is the calculated average air volume, ex- meter were compared to those recorded by the other
pressed in percent. These three linear equations have standard devices for conventional concrete (average
correlation coefficients of 0.996, 0.997, and 0.998, re- wlcm = 0.50), moderate-strength concrete (wlcm =
360 ACI Materials Journal I July-August 1990
a:
w
Iii
::&
z
iii
EQUALITY LINE
3 5 5 7 9 11
% AIR - PRESSURE METER % AIR • ROLLER METER
Fig. 7-Comparison of mini and pressure meters for Fig. 8-Comparison of mini and roller meters for var-
various normal weight concretes ious normal weight concretes
0.33), and very high-strength mixes (w/cm = 0.22), ial equations can be used instead of these linear equa-
Mixes P-1 through P-13. The results relating air con- tions. The polynomial equations relating measured air
tents measured using the mini air meter and the pres- volume by the mini and roller methods to unit weights
sure and roller meters are plotted in Fig. 7 and 8. The have correlation coefficients of 0.935 and 0.944, in-
new air meter and each of the other two meters yielded stead of the 0.932 and 0.941 values associated with the
similar air contents when testing concretes made with linear equations. The difference in predicted air vol-
wlcm of 0.22 and 0.33. Air-volume measurements as- ume between the linear and polynomial equations seems
sociated with concretes made with 0.50 wlcm were too small to justify the use of the latter in the field.
slightly offset from the equality line. However, the Therefore, whenever one of these volumetric air meters
maximum deviation from equality was limited to 0.5 is employed to monitor air content of normal-density
percent, which is within the precision limits established concrete, and the unit weight of the concrete is mea-
for the new air meter. 4 As shown in Fig. 7, slightly sured, Eq. (7) or (8) can be used to double-check the
lower air contents were recorded using the mini air me- tested air content.
ter than with the pressure meter for 0.5 wlcm concretes
containing moderate air volumes. The two mixes show-
CONCLUSIONS
ing this trend had low consistency levels; therefore, it is
The accuracy of the new mini air meter was deter-
possible that some of the air was trapped within the
mined by comparing measurements taken by it to those
mortar, which was not the case when the pressure me-
obtained by standard pressure and volumetric air me-
ter was used. It is thus advisable to increase the agita-
ters. Both normal-weight and lightweight concretes
tion effort of the mini device whenever concrete is co-
containing ¥s and 1 in. (9.5 and 25.4 mm) nominal-size
hesive, and to continue monitoring the air volume until
aggregates were used in this investigation. All mixes in-
no significant increase in air volume can be detected.
corporated superplasticizers, and some included other
Unit-weight measurements of freshly mixed con-
additives such as air-entraining agents, silica fume, anti-
crete, which are necessary for calculating yields, can
washout admixtures, and de-airing additives. For the
also be used to approximate air content. For the mate-
type of materials used in this experimental program, the
rials used in this research program, linear equations re-
following conclusions can be drawn:
lating unit weights of fresh concretes to air volume
1. A very close correlation can be derived between air
measurements made with the mini and roller air meters
content measurements obtained with the mini air meter
can be written as
M and the roller meter R, for both normal-weight and
lightweight concretes. The relationship relating the two
M = -0.48 W + 75.91 (7) values can be expressed as