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General Description of Production, Properties, and Uses of

Sintered Metal Powder Bearings and Structural Parts1


This information serves as a guide to the specifications for sintered metal powder bearings and structural parts (ASTM Designations:
B 255, B 282, B 438/B 438M, B 439, B 458, B 595, B 612, B 715, B 782, B 783, B 817, B 823, B 848, B 853, and B 883).2

Powder metallurgy (P/M) components are made by cold advantages of P/M bearings.
pressing and sintering metal powders. These parts may be used Both copper-base and iron-base P/M bearings are manufac-
as bearings or in structural applications. The P/M process is tured and used. The copper-base bearings have either bronze
used for economic advantage and unique properties. 1,2 (Cu-10Sn) or leaded bronze compositions when considered for
general purpose use. These alloys are also made with graphite
PROCESSING additions in which the added solid lubrication is deemed
The major processing steps are compacting or cold pressing necessary. Iron-base sintered metal bearings are supplied in a
a metal powder and sintering the resultant compact. variety of compositions such as plain iron, iron-carbon, iron-
copper, and iron-copper-carbon. They are used where ample
Cold Pressing lubrication is provided, where higher loads and slower speeds
The initial step is the application of pressure to the desired are prevalent, and where cost factors are significant.
quantity of metal powder in a die. To a large degree, cold
pressing dictates the density, shape, dimensions, and mechani- STRUCTURAL PARTS
cal properties of the finished P/M part. P/M structural parts are used wherever they offer an eco-
nomic advantage. This advantage can be realized in the
Sintering manufacture of unusual shapes, the elimination of secondary
Under properly controlled conditions of temperature, heating machining or grinding operations, and the elimination of scrap
rate, time, and furnace atmosphere, the cold-pressed metal losses. Structural parts can be made to various levels of
powder particles are metallurgically bonded and the compact is mechanical properties, which makes them desirable in upgrad-
converted to a useful part. The sintering temperature has the ing or improving product at little or no extra cost. The
greatest influence on final properties; however, sintering time properties of P/M parts depend upon a number of factors.
and furnace atmosphere can be selected to provide optimum
properties along with cost-effective processing. Composition
As in most metallic materials, chemical composition has a
Secondary Processing major effect on properties. For ferrous parts, those made from
Additional processing steps include coining, sizing, repress- unalloyed iron powder have the lowest strength and hardness.
ing, resintering, impregnation, and infiltration (see Terminol- For stronger parts, iron-copper, iron-carbon, and iron-copper-
ogy B 243). Of course P/M parts can also be heat treated, carbon alloys are used. (Examples of these variations may be
plated, or machined as required. However, since P/M parts are found in Specification B 783.) Iron-copper alloys are usually
less dense than cast or wrought materials, these processing more easily machined than iron-carbon alloys. On the other
steps may have to be modified from typical practice used for hand, sintered iron parts containing combined carbon can be
fully dense parts. heat treated by methods appropriate for cast and wrought steel
parts. It is frequently preferable to quench porous P/M iron-
BEARINGS carbon parts in oil to avoid corrosion problems with water.
P/M bearings (Specifications B 438/B 438M, B 439, B 612, Careful control of sintering and heat-treating atmospheres is
and B 782) are self-lubricating because their porosity is im- necessary to maintain the desired combined carbon level at the
pregnated with lubricants during manufacture. In use, heat part surface. Of course, carburizing and other gaseous surface
causes the lubricant to expand out of the pores, forming a film treatments are applicable to ferrous P/M parts. Depending on
between parts. When operation is suspended, the lubricant the level of porosity, the depth of surface reaction will be
cools and is drawn back into the pores for subsequent reuse. greater for a fixed time compared to fully dense parts.
Low coefficients of friction, minimal maintenance and trouble-
free service life, low cost, and simple installation are the chief Density and Mechanical Properties
An important factor affecting the properties of structural
1
parts is their porosity. (The relative density is equal to one
First published in the compilation of “ASTM Standards on Metal Powders and
Metal Powder Products,” September 1959. Revised February 2002. minus the volume fraction of porosity). In general, increasing
2
These specifications appear in the Annual Book of ASTM Standards, Vol 02.05. the density of a P/M part will increase its tensile strength,

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Sintered Metal Powder Bearings and Structural Parts

compressive strength, and ductility. The indentation hardness will remove the effect of the cold work and result in higher
of a sintered material is also strongly affected by its porosity, ductility.
because the voids in the structure of a material do not Ferrous parts with densities over 7 g/cm3 can be produced by
contribute to the support of the indenter. The indentation of a suitable choice of powders and compacting, sintering, repress-
porous material provides an apparent hardness, which is lower ing, and resintering conditions (Specification B 783). When
than the indentation hardness of a void-free material with density exceeds 7.3 g/cm3, there is no longer any appreciable
identical composition and structure. For a material of given amount of interconnected porosity. Parts can therefore be
composition and structure, there is a direct relationship be- carburized and surface hardened in a manner very similar to
tween density and hardness; the lower the density, the lower wrought steel, and they can also be plated similarly to wrought
will be its apparent hardness. Microhardness techniques are parts without any special precautions. The strength, hardness,
recommended to minimize void effects. Low indenter loads and toughness of high-density steel (iron-carbon alloy) parts
and the small volume of the hardness impression provide this can be improved by quenching and tempering treatments
capability. similar to those used for wrought steels. To increase the
hardenability of these parts, alloying elements may be added to
Low-Density Parts the base iron-carbon composition.
Structural components that have relatively low density and Another method of increasing the density of ferrous parts,
high porosity have the added advantage of self-lubrication as in which is widely used for highly stressed parts, is by infiltration
sintered metal bearings. This self-lubrication provides a lower with copper or a copper alloy (Specification B 783). Infiltration
coefficient of friction and lower wear in applications in which improves the strength, ductility, and impact strength of ferrous
sliding movement is involved as in gears and cams. In plating parts. Infiltrated parts can also be plated without special
low-density parts, special precautions must be observed so that precautions and can be joined by welding or brazing. The
the plating salts are not entrapped in the pores of the parts. This strength of carbon-free copper infiltrated parts may be in-
could cause eventual discoloration of the finish, internal creased by a solution and precipitation treatment. Carbon
corrosion, and “flowering” of the plated surface. Techniques of containing infiltrated parts may be heat treated by quenching
burnishing, carefully controlled shot peening, and resin im- and tempering.
pregnation have been developed to either close the surface
pores or fill all pores and thereby avoid these defects. Ferrous Qualification Tests
parts are being successfully plated with copper, nickel, chro- Generally, standard test specimens cannot be machined from
mium, cadmium, zinc, and other metals; nonferrous parts may structural P/M parts for mechanical property testing. For this
also be plated. reason, the specifications for mechanical properties of struc-
Iron-base P/M parts may be economically finished by steam tural parts provide for qualification tests. These tests should be
treating, in which the parts are heated in an atmosphere of agreed upon by the manufacturer and the purchaser upon
steam, or by oxidation in air. These treatments produce on the consideration of the function which the part is to perform.
parts a black finish which not only improves their corrosion Compressive strength and ductility can be determined by
resistance, but also makes them harder and more wear resistant. deforming the part under compression, or by bending, and
Corrosion resistance can be further enhanced by immersing the observing whether fracture occurs before the part has exhibited
parts in light oil which will remain in the pores providing a sufficient strength or ductility for the intended purpose. Impact
barrier to corrosive media. properties can be determined by dropping a weight upon the
Low-carbon sintered ferrous parts may be carburized and part to be tested. The weight, height of drop, point of impact,
hardened by gas carburizing and quenching. However, for and the method of supporting the test specimen should be
low-density parts, no sharply defined case is formed, since the prescribed.
carbonaceous gas readily penetrates into the core of the parts Hardness may, for certain applications, be used as a quali-
through their interconnected pores. Liquid carburizing of fication test. All normal precautions in hardness testing, such as
low-density parts should be avoided because of possible avoiding an anvil effect in thin parts, must be observed.
corrosion as a result of entrapment of salt within the pores. However, the best manufacturing controls and test procedures
cannot prevent occasional stray hardness readings considerably
Higher Density Parts below, or above, the mean hardness value for a sample lot of
Increased density in structural parts is frequently attainable production sintered metal powder parts. Therefore, the inspec-
by additional manufacturing operations. For this reason, higher tion of production parts for hardness must be done in a
density parts are generally more costly. Coining and repressing prescribed manner to avoid a question of acceptability of lots
of parts are used to increase their density and to cold work of parts.
them. Depending upon the degree of densification and cold Where microhardness test equipment is available, the uni-
working, repressing will increase the hardness and strength of versality of application of the hardness scale provides for a
parts, while decreasing ductility. In brass parts, for instance, the convenient hardness number series. Even though a seemingly
apparent hardness of the sintered part may be of the order of large range of hardness numbers may be obtained by micro-
wrought annealed brass, while coining and repressing may hardness tests, conversion back to a familiar Rockwell scale
increase the apparent hardness to that of one-quarter hard will provide for hardness numbers over a very limited range.
wrought brass. A second sintering operation after repressing If Rockwell hardness tests are used, a wide variety of scales

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Sintered Metal Powder Bearings and Structural Parts

is available to match the test requirements of a given material. (2) The number of indentations per part, or the number of
The choice of scales need not be limited to those presently parts to be checked, or both, should be specified.
designated in the list published by the instrument maker. For (3) The section of a part to be checked should be specified.
example, a combination of 1⁄8-in. carbide ball, 100-kg load, and (4) If parts are thin, a scale must be chosen to ensure that
the black scale will provide hardness data for a wide variety of indentation effects do not penetrate through the part.
medium density, hardenable, ferrous, sintered materials with an
(5) Hardness scale (see discussion above).
acceptable spread of readings, between 0 and 115. The familiar
Rockwell scales such as B, C, and 15T have been used to
advantage. Recommendation
One useful concept for developing a hardness specification The mechanical properties listed in the appendixes to the
for acceptance inspection is “minimum average hardness.” The specifications for structural parts should be considered as
average of a specified number of indentations must not be less typical for parts made by normal production methods. Superior
than a given minimum value. There may be an occasion when mechanical properties can be achieved by special processing
the specified hardness may be no less than a stated minimum methods. It is suggested that the purchaser work closely with
average and no more than a stated maximum average. Thus, a the parts fabricator in the design and development of new parts
hardness specification may include details as follows: or in the conversion to powder metallurgy fabrication of
(1) A minimum (and possibly a maximum) average hard- existing parts.
ness should be specified for acceptance inspection of parts.

BIBLIOGRAPHY

For additional, more detailed information, the following publications (5) “Powder Metallurgy Materials,” in Metallography and Microstructure,
are recommended: ASM Metals Handbook, 9th ed., Vol 9, American Society for Metals,
(1) German, R. M., Powder Metallurgy Science, Metal Powder Metals Park, OH, 1985, pp. 503–530.
Industries Federation, Princeton, NJ, 1984. (6) Powder Metallurgy Design Manual, 3rd ed., Metal Powder Industries
(2) Lenel, F. V., Powder Metallurgy Principles and Applications, Metal Federation, Princeton, NJ, 1998.
Powder Industries Federation, Princeton, NJ, 1980. (7) Powder Metallurgy Design Solutions, 2nd ed., Metal Powder
(3) Materials Standards for P/M Structural Parts (MPIF Standard 35), Industries Federation, Princeton, NJ, 1999.
Metal Powder Industries Federation, Princeton, NJ, 2000. (8) Powder Metal Technologies and Applications, ASM Handbook, Vol 7,
(4) Materials Standards for P/M Self-Lubricating Bearings (MPIF Stan- American Society for Metals, Metals Park, OH, 1998.
dard 35), Metal Powder Industries Federation, Princeton, NJ, 1998.

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