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PT.

Wilmar Nabati Indonesia

STANDARD OPERATION PROCEDURE SOP-QA-09-032

STANDARDIZATION OF ACID Revision No. 00


SOLUTION
Effective Date 01.01.10

Prepared by: Reviewed by: Approved by:

DRS. SUDIRMAN ROSALINA INDRA TANOTO


QA Supervisor QA Manager Deputy General Manager

1. Purpose 1. Tujuan
To determine normality of acid. Menetukan normalitas/konsentrasi asam.

2. Scope 2. Ruang Lingkup


Could be applied to HCL. Dapat diterapkan HCL.

3. Responsible 3. Tanggung jawab


QA Analyst, foreman and Asst Supevisor. QA Analyst, foreman dan Asst Supervisor.

4. Apparatus 4. Peralatan
4.1 Analytical balance, accurate up to 0.0001 gram 4.1 Timbangan analitik dengan akurasi 0.0001 gram.
4.2 Metrom dosimat titrator with magnetic stirrer or 4.2 Methrom dosimat titrator dengan magnetic stirrer
equivalent apparatus atau dengan alat lain yang sejenis.
4.3 Elenmayer flask, 250 of 300 milliliter 4.3 Erlenmeyer flask, 250 atau 300 ml.

5. Reagents 5. Reagents
5.1 Sodium hydroxide standard solution than already 5.1 Larutan standar sodium hidroksida yang telah
standardization process. distandarisasi
5.2 Fenolftalein (PP) indicator solution. Make soluble 5.2 Larutan indicator fenolftalein (PP). Larutkan 1.0
1.0 gram PP into 1 liter with ethyl alcohol. gram PP dalam 1 liter ethanol.

6. Procedure 6. Prosedur
6.1 Moved in a quantitative manner with Metrohm 6.1 Pindahkan secara kwantitatif dengan Metrohm
Dosimat tritrator in two part chloride acid solution, Dosimat titrator 2 bagian larutan asam klorida, 20
20 milliliter every part into two erlenmayer flask ml setiap bagian ke dalam dua labu Erlenmeyer
250 milliliter. 250 ml.
6.2 Added 100 milliliter cold and neutral aquadest. 6.2 Tambahkan 100 ml aquadest dingin dan netral.
Stirring in a slowly manner until perfect soluble. Aduk secara perlahan sampai terlarut sempurna.

6.3 Add 3 molasses PP indicator solution and titration 6.3 Tambahkan 3 tetes larutan indicator PP dan
with sodium hydroxide solution until color unripe titrasi dengan larutan sodium hidroksida sampai
red the first time change during 30 second. warna merah muda yang pertama tidak berubah
selama 30 detik.

7. Calculation 7. Perhitungan
Acid solution of normalization can be calculate Normalitas larutan asam dapat dihitung dengan
with formula such as : rumus:
VxN
20 VXN
20
Where : Dimana :
V : Milliliter of sodium hydroxide solution used V : ml larutan sodium hidroksida yang terpakai untuk
for titration. titrasi
N : Normality of sodium hydroxide solution N : Normalitas larutan sodium hidroksida.
normalization of sodium hydroxide solution.

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PT. Wilmar Nabati Indonesia

STANDARD OPERATION PROCEDURE SOP-QA-09-032

STANDARDIZATION OF ACID Revision No. 00


SOLUTION
Effective Date 01.01.10

Quarrel between two of result normalization act of Selisih antara kedua hasil penentuan normalitas yang
determining then permitting is 0.0002. Calculation di izinkan yaitu 0.0002 Hitung rata-rata normalitas ke
average normalization to 0.0001 so near. 0.0001 unit terdekat.

8. Note 8. Catatan
Standardization is done after solution finish to Standarisasi dilakukan setelah larutan dibuat
make or every 2 week. atau setiap 2 minggu.

9. Reason for Issue / Revision 9. Alasan Penerbitan / Perubahan


9.1 January 1st, 2010, Update to ISO 9001: 2008. 9.1 01 Januari, 2010, Menyesuaikan dengan ISO
9001: 2008.

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