Академический Документы
Профессиональный Документы
Культура Документы
1. Purpose 1. Tujuan
To determine the concentration of Thiosulfate Menentukan konsentrasi larutan Thiosulfate.
solution.
3. Apparatus 3. Peralatan
4.1 Analytical balance, accurate up to 0.0001 gram. 4.1 Analytical balance, dengan akurasi 0.0001 gram.
4.2 Methrom dosimat titrator with magnetic stirrer or 4.2 Methrom dosimat titrator dengan magnetic stirrer
equivalent apparatus atau alat sejenis.
4.3 Timer 4.3 Alat Pengukur waktu.
4.4 Repeater pipette with filling flask, 20 milliliter. 4.4 Repeater pipette with filling flask, 20 ml.
4.5 Measuring pipette, 5 milliliter 4.5 Measuring pipette, 5 ml
4.6 Glass stoppered iodine flask, 250 millimeter. 4.6 Glass stoppered iodine flask, 250 ml.
4. Reagents 4. Reagents
4.1 Kalium dikromat, reagent grade, roller to soft and 4.1 Kalium dikromat, reagent grade, digiling halus
make to dry in temperature 110 degree C before dan dikeringkan pada 110 OC sebelum digunakan
using minimal 2 hour. min 2 jam.
4.2 Make Soluble kalium iodine, 10% maker with 4.2 Larutan kalium iodide, 10% dibuat dengan
soluble 10 gram KI (reagent grade) into 100 melarutkan 10 gram KI (reagent grade) dalam
milliliter aquadest. 100 ml aquadest.
4.3 HCL reagent grade concentrated. 4.3 HCl reagent grade
4.4 Make soluble starch 1% already check sensitivity 4.4 Larutan kanji 1 %, telah di uji kepekaannya (jika
(if needed) make pasta from 1 gram starch and a diperlukan) buat pasta dari 1 gram kanji dan
little aquadest. At the same time mixing added sedikit aquadest. Sambil diaduk tambahkan 100
100 milliliter boil water. Moved 5 milliliter the ml air mendidih. Pindahkan 5 ml larutan ini ke
solution into 100 milliliter aquadest and added dalam 100 ml aquadest dan tambahkan 0.05 ml
0.05 milliliter KI 0.1 the color dark blue disappear KI 0.1 warna biru gelap harus hilang setara
be equal with adding 0.05 milliliter Na2Ss)3 0.1N. dengan penambahan 0.05 ml Na2S2O3 0.1 N.
5. Procedure 5. Prosedur
5.1 Weighing until 0.0001 gram a near, 0.1 +- 0.01 5.1 Timbang sampai 0.0001 gram terdekat, 0.1 ±
gram kalium dikromat into flask iodine 250 0.01 gram kalium dikromat ke dalam labu iodine
milliliter and added 25 milliliter aquadest. The 250 ml dan tambahkan 25 ml aquadest. Berat ini
weight appropriate for Na2S2O3 o.1 N and mush memadai untuk Na2S203 0.1 N dan harus
be appropriated with comparing 0.05 milliliter disesuaikan dengan perbandingan berat yang
Na2S2O3 0.1N. sama bila akan menstrandarisasi larutan standar
yang berbeda kosentrasinya.
5.2 Weighing 5 milliliter HCL concentrated and 20
5.2 Tambahkan 5 ml HCl dan 20 ml larutan kalium
milliliter kalium iodine solution. Stir in older than
iodide. Aduk agar bercampur.
mix.
5.3 Biarkan 5 menit dan tambahkan aquadest melalui
5.3 So that 5 minute and added aquadest pass
mulut labu tanpa melepas tutupnya.
through mouth of flask without release the closed.
6. Calculation 6. Perhitungan
N = W . N = W
0.04903 x V 0.04903 x V
Where :
N : Normalization Na2S2O3 solution N : Normalitas larutan Na2S2O3
W : Weight of Sodium dicromat (gram) W : Berat kalium dikromat (gram)
V : Milliliter of Na2S2O3 then needed in V : ml Na2S2O3 yang di butuhkan
filtration process. dalam titrasi
Page 2 of 2