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Committee D27

Proficiency Test Program


Dissolved Gas Analysis
Sample ID: DGA1808
August 2018
Report Issue Date: November 9, 2018

Copyright© 2018 ASTM International, West Conshohocken, PA . All rights reserved. This material may not be reproduced or copied, in whole or in part, in any printed,
mechanical, electronic, film or other distribution and storage media, without the written consent of the publisher.
Table of Contents
Program Report Cycle Information..............................................................................................................................3
How to Use This Program Report ...............................................................................................................................4
Revision 3 Issued July 9, 2018 ....................................................................................................................................4
Overview .....................................................................................................................................................................4

Recommended Report Review Sequence.............................................................................................................4

Use of PTP Reports and Data .................................................................................................................................5

Program Result Summary Table Description ........................................................................................................5

Method Summary Tables (Numeric and Non-Numeric).......................................................................................6

Plots & Charts (Numeric and Non-Numeric)..........................................................................................................7

Data Preparation........................................................................................................................................................8

Statistics (for Numeric Results) ...............................................................................................................................8

Statistics (for Non-Numeric Results) ....................................................................................................................11

Summary of Symbols and Abbreviations Used in PTP Reports.......................................................................11

Alphabetical Listing of Laboratories ..........................................................................................................................12


Results Summary for All Methods .............................................................................................................................16
Vacuum Extraction, A, Acetylene, D3612-02(2017) .......................................................................................19
Vacuum Extraction, A, Carbon Dioxide, D3612-02(2017) .............................................................................22
Vacuum Extraction, A, Carbon Monoxide, D3612-02(2017) .........................................................................25
Vacuum Extraction, A, Ethane, D3612-02(2017) ............................................................................................28
Vacuum Extraction, A, Ethylene, D3612-02(2017) .........................................................................................31
Vacuum Extraction, A, Hydrogen, D3612-02(2017) .......................................................................................34
Vacuum Extraction, A, Methane, D3612-02(2017) .........................................................................................37
Vacuum Extraction, A, Nitrogen, D3612-02(2017)..........................................................................................40
Vacuum Extraction, A, Oxygen, D3612-02(2017)...........................................................................................43
Vacuum Extraction, A, Propane, D3612-02(2017)..........................................................................................46
Vacuum Extraction, A, Propylene, D3612-02(2017).......................................................................................48
Stripper Column Extraction, B, Acetylene, D3612-17 ....................................................................................50
Stripper Column Extraction, B, Carbon Dioxide, D3612-17...........................................................................53

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Stripper Column Extraction, B, Carbon Monoxide, D3612-17.......................................................................56
Stripper Column Extraction, B, Ethane, D3612-17 .........................................................................................59
Stripper Column Extraction, B, Ethylene, D3612-17 ......................................................................................62
Stripper Column Extraction, B, Hydrogen, D3612-17.....................................................................................65
Stripper Column Extraction, B, Methane, D3612-17 ......................................................................................68
Stripper Column Extraction, B, Nitrogen, D3612-17 .......................................................................................71
Stripper Column Extraction, B, Oxygen, D3612-17 ........................................................................................74
Stripper Column Extraction, B, Propane, D3612-17.......................................................................................77
Stripper Column Extraction, B, Propylene, D3612-17 ....................................................................................79
Headspace Sampling, C, Acetylene, D3612-02(2017) ..................................................................................81
Headspace Sampling, C, Carbon Dioxide, D3612-02(2017).........................................................................88
Headspace Sampling, C, Carbon Monoxide, D3612-02(2017).....................................................................95
Headspace Sampling, C, Ethane, D3612-02(2017) .....................................................................................102
Headspace Sampling, C, Ethylene, D3612-02(2017) ..................................................................................109
Headspace Sampling, C, Hydrogen, D3612-02(2017).................................................................................116
Headspace Sampling, C, Methane, D3612-02(2017) ..................................................................................123
Headspace Sampling, C, Nitrogen, D3612-02(2017) ...................................................................................130
Headspace Sampling, C, Oxygen, D3612-02(2017) ....................................................................................137
Headspace Sampling, C, Propane, D3612-02(2017) ...................................................................................144
Headspace Sampling, C, Propylene, D3612-02(2017) ................................................................................149
Water Content, D1533-12.................................................................................................................................153
Participant Comments...............................................................................................................................................160

A copy of the data entry worksheet for this cycle is available under Documents at ptp2.astm.org.

November 9, 2018 www.astm.org 2


ASTM International Proficiency Testing Program
Sponsored by ASTM Committee D27

Program Report Cycle Information


Dissolved Gas Analysis (DGA)
DGA1808, August 2018

Contact Information
Authorized By: Amy Meacock
Address: ASTM International
100 Barr Harbor Drive
West Conshohocken, PA
19428-2959
Email: ptp@astm.org
Phone: 1-610-832-9585
Fax 1-610-832-9668

Sample Information
Identification: Dissolved Gas Analysis(DGA) DGA1808
Source: Confidential, donated
Preparation, Distribution: Doble Engineering Company, 85 Walnut Street, Watertown, MA
United States 02472
Phone: 6173932981
Distribution Dates: Week of August 10, 2018
Homogeneity Confirmed prior to distribution and by analysis of returned data.
Stability: Sample packaged and sealed to ensure stability during
shipment. Once received, sample stability is the responsibility of
the recipient.

Report Information
Result Submission Due Date: October 5, 2018
Data Analysis & Reporting: ASTM International PTP Office
Report Issue Date: November 9, 2018

November 9, 2018 www.astm.org 3


How to Use This Program Report
Revision 3 Issued July 9, 2018

Overview

The Program Report shows results for all participating laboratories. It is similar to the
Laboratory Report, but without reference to a specific laboratory. The intent of the Program
Report is to assess the performance of a method, rather than a specific lab. The Program
report is directed to PTP program managers, to the subcommittees responsible either for the
test methods or for the product’s specifications, and to laboratories desiring to investigate
overall test method performance.

Recommended Report Review Sequence

1) Review Program Result Summary Table

Numeric Methods
 Average column—Consider cases where the Average for any test method is
unusual for the product.
 Precision Performance column—Consider any test method where the “These
Data R” is considered “Worse” than the “ASTM R.”
 Normal column—Consider possible impact on identified outliers for any test
method where the Anderson-Darling Statistic indicates non-normality.

Non-Numeric Methods

 Modal% column—Consider implications of test methods where the “Modal %” is


less than 50-70%.

2) Review Individual Numeric Methods

 Summary Table—Consider results for any “Comparison Lab.”


 Data Distribution—Consider significant deviations from linearity and distinct
‘stairs’ pattern.
 Histogram—Consider unusual, bimodal or skewed distributions.
 Results Table—View historic Z-scores.

3) Review Individual Non-Numeric Methods

 Summary Table—Consider unusual or broad distributions.


 Frequency Chart—Consider unusual or broad distributions. 

November 9, 2018 www.astm.org 4


Use of PTP Reports and Data

This agreement is presented to participants on screen prior to their clicking on the “accept”
link to submit payment for services.

“You agree the data generated as a result of the proficiency testing services and provided to
ASTM is confidential information and you further agree not to disclose or provide this data to
anyone else without ASTM's written consent. You also acknowledge and agree that the
report generated as a result of this proficiency testing program will be copyrighted by ASTM
International. You may however share data with an accreditation body for auditing purposes
only. You hereby assign to ASTM any rights you may have in data you provide to ASTM
International by clicking on the link.”

Program Result Summary Table Description

Numeric Methods

 Designation—Includes year date.


 Measured Property with Conditions—Includes conditions like test temperature.
 Units

Method Performance Statistics

 Conforming Results—Number of results conforming to reporting requirements.


 Results Used—Number of results used once outliers removed.
 Average
 StdDev—Standard deviation for “These Data.”
 ASTM R—Calculated in accordance with the published test method. No ASTM R is
calculated when the Average is outside the reproducibility scope listed in the test
method.
 These Data R
 Precision Performance—Classified as Better, Consistent, or Worst, based on F-Test
criteria discussed.
 Anderson Darling—Normality statistic, see D6299
 Normal?—Classified as Normal, Acceptably Normal, Marginally Normal, or No,
based on criteria discussed in Statistics (for Numeric Results) section below.

Non-Numeric Methods

 Designation—Includes year date.


 Measured Property with Conditions—Includes conditions like test temperature.

Method Performance Statistics

 Conforming Results—Number of results conforming to reporting requirements.


 Results Used—No outlier rejection for non-numeric results.

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 Unique Results
 Mode
 Modal%

Method Summary Tables (Numeric and Non-Numeric)

For each method, the summary table appears first, followed by the Results Table and
historic Z-scores, the Data Distribution chart (Q-Q plot), and the Histogram. There is one set
of these tables and plots for each numeric test method. All results reported by participating
laboratories are included in the summary tables. All results except for non-conforming results
and those rejected as GESD outliers are then used for calculations and generating statistics.
Z-Score results from a Comparison Lab will be included when available.

Program Numeric Method Summary Table (one for each Test Method)
The Program Numeric Method Summary Table is a summary of the statistics generated for
that specific test method. No specific laboratory’s result is highlighted. If there are
“comparison labs,” their results, Z-Scores and notes are shown. If there are no comparison
labs, as is most often the case, then that portion of the table is omitted.

Program Numeric Results Table and Z-Scores (one for each Test Method)
Each laboratory is identified by a randomly selected code with the same laboratory code
applying throughout the entire report. This table shows performance statistics for all of the
methods in a specific PT program on a single or consecutive pages. Program Report –
Results Summary Table includes results from all participating laboratories. All results except
for GESD outliers and non-conforming results are then used for calculations and generating
statistics.

This table shows historic Z-Scores for all laboratories for each test method. This table
shows, for each laboratory: a randomized Lab Code, test result, deviation, Z-score, notes,
historic Z-scores from the six most recent cycles, count, average Z-score, and standard
deviation for the Z-scores collected for each laboratory. The pooled standard deviation
across all laboratory Z-scores is also provided.

Program Non-Numeric Method Summary (one for each Test Method)


The Non-Numeric Method Summary Tables provide frequency tables for the distributions of
results from non-numeric methods. For a specific program, method, and cycle there is a
table with a row for every distinct result submitted. The rows are in the same order as the
list of valid results for the method. There are columns for the results, the numbers of labs
obtaining those results, and the percentage of labs that obtained the results. The mode for
each distribution is highlighted. No specific laboratory’s result is highlighted on a Program
Non-Numeric Method Summary Table. Each Non-Numeric Method Summary Table is
followed by the corresponding frequency plot.

November 9, 2018 www.astm.org 6


Plots & Charts (Numeric and Non-Numeric)

Data Distribution – Q-Q Plots (one for each Test Method)


A distribution plot of numerical results is simply a plot of the results against their rank order.
The results are plotted against the percentiles of a normal distribution corresponding to the
rank of each result. Distribution plots are non-descending, that is, they go from the lower left
of the plot to the upper right. The quantile-quantile (Q-Q) version used in this report has the
property that the points will fall close to a line if the distribution of the results is nearly normal.
A best-fit line is provided for reference. The closeness to the line is closely related to the
Anderson-Darling statistic – when the A-D statistic is large, the points are not close to a line.

Histogram (one for each Test Method where results ≥ 20)


A histogram is a bar graph, with vertical bars, each representing the number of results taking
values in a given range. The bars are of equal width (the ranges all have the same length,
and the same number of response resolutions) and bars in contiguous ranges touch one
another. The heights of the bars are proportional to the number (frequency) of results that
are in the range, that is, they represent the data intensity within that range. The median of
the data is shown as a vertical black line. Limits representing the 1 and 99 percentile are
shown on the graph when the number of data are ≥ 100.

Frequency Charts (Non-Numeric Results) (one for each Test Method)


Frequency Charts are graphical versions of Non-Numeric Method Summary Tables. A bar
for every distinct observed result have uniform widths and heights proportional to the
frequency of the result’s occurrence in data set.

Box & Whisker Plots (not always provided)


Two or more such plots are presented on a single graphic in order to compare distinct
distributions of results. A minimum of 12 data are required for each parameter for these
plots.

The graphic is plotted above a horizontal line scaling the range of results. An individual plot
is comprised of a rectangle (“box”) with the left end at the first quartile and the right end at
the third quartile. The height of the rectangle is chosen so as to produce a pleasing picture,
but it is usually substantially less than the width. The rectangle is divided by a vertical line
segment at the median of the distribution. A line segment which is an extension of the
horizontal bisector of the rectangle (a “whisker”) extends from the left end of the rectangle
down to the value of the smallest observed result that is no more than 1.5 interquartile
ranges less than the first quartile. A similar line extends from the right end of the rectangle
to the value of the greatest observed result that is no more than 1.5 interquartile ranges
more than the third quartile. The extreme ends of the two rays are capped with a small,
unobtrusive T. Finally, for any result smaller than the first quartile minus 1.5 interquartile
ranges, a marker is plotted on an invisible extension of the left whisker, and all results larger
than 1.5 interquartile ranges plus the third quartile are plotted beyond the end of the right
whisker.

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Data Preparation

Data Entry Screen Conformance/Validity Checks


The data collection reporting system accessible via the ASTM PTP Portal is designed to
alert submitters to non-conforming results.

Submitted Data Validity Check


Results that do not conform to the requirements of the method are not used for statistical
compilations. For numeric methods non-conforming results include any non-numeric
response (e.g., <, >), any numeric response that is beyond a validity limit, or outside a range
of validity that is explicitly given in the method. If a “< a specified limit” or “>a specified limit”
or both are allowed in the method, then these are allowed and considered conforming. [The
same applies to a “ND (not detected)” result allowed by the test method. These are the only
non-numeric responses allowed, and for statistical calculations such results will be
“adjusted” to a specified limit for statistical computations. If more than 18% of the results
submitted on a method in a single cycle are an allowed non-numeric, then statistics for that
method cycle will not be computed.

Non-Conforming results will be listed in the respective Program Numeric Results Table along
with a NCR in the Notes column.

For non-numeric methods, the method generally provides – or one can infer – a list of all
possible valid results. Any submitted result that is not on such a list is non-conforming.

Maintaining Raw Data


Raw data, exactly as submitted, is maintained with the ASTM database. When reporting
coded individual lab results in tables (e.g., Program Summary Tables, Method Summary
Tables, or Z-score) they are always display exactly as submitted, with the same resolution
(displayed significant digits).

Statistics (for Numeric Results)

GESD Outlier Identification


See Practice D7915-14, Standard Practice for Application of Generalized Extreme
Studentized Deviate (GESD) Technique to Simultaneously Identify Multiple Outliers in a
Data Set. The GESD procedure is used to simultaneously identify up to a pre-determined
number of outliers in a data set, without having to pre-examine the data set and make a
priori decisions as to the location and number of potential outliers.

Average (or arithmetic mean)


X   Xi n Report to the same resolution as the standard deviation, s.

Standard Deviation, s

November 9, 2018 www.astm.org 8


 X X n  1
2
s i
Report to one-tenth the reporting resolution of the method.

srepro, and srepeat are the corresponding reproducibility standard deviation and the
repeatability standard deviation as calculated using the proficiency testing data.

sASTM R and sASTM r when needed are determined from the corresponding ASTM
reproducibility (R) and ASTM repeatability (r) as:

sASTM R = ASTM R / 2.77

sASTM r = ASTM r / 2.77

Pooled Standard Deviation, sp


As presented in the “Results Table and Z-score” tables:

Where:
ni is the number of Z-scores listed for a given laboratory
si is the corresponding standard deviation for those Z-scores
k is the number of laboratories with historic Z-scores

Reproducibility, R
ASTM R – Extracted from or calculated using equations in the referenced ASTM Test
Method. Reported to the resolution given in the method or to the same resolution as the
reproducibility standard deviation.

These Data R – Calculated using the reproducibility standard deviation, srepro, determined for
These Data as per the following equation:

These Data R = 2.77 × srepro

Repeatability, r
ASTM r – Extracted from or calculated using equations in the referenced ASTM Test
Method. Reported to the resolution given in the method or to the same resolution as the
repeatability standard deviation.

These Data r – Calculated using the repeatability standard deviation, srepeat, determined for
These Data as per the following equation

These Data r = 2.77 × srepeat

November 9, 2018 www.astm.org 9


Precision Performance
Precision Performance is based on the outcome of the F-Test. For the F-Test, the ratio of
the standard deviations squared (larger divided by smaller) is compared to the 95th
percentile of Fisher’s F distribution. The two standard deviations are the published
reproducibility standard deviation for the ASTM test method (sASTM R) and the standard
deviation for These Data (srepro). For determining the F-Distribution, the degrees of freedom
for These Data is the number of conforming data used in the calculation of the standard
deviation and the degrees of freedom for the ASTM standard deviation is assumed to be 30.

As with the t-test, the risk of Type I error is held to 5% only if the distributions are nearly
normal. This statistical test evaluates whether or not the PT precision is better than,
consistent with or worse than the ASTM precision in accord with the following table

F Distribution PT Precision Performance


< 0.025 Better
0.025 – 0.975 Consistent
>0.975 Worse

Anderson-Darling Statistic (Resolution-Sensitive)


The Anderson-Darling (AD) Statistic is a quantitative measure of the difference between the
distribution of a set of observed numeric data, and the theoretical normal distribution with the
same average and standard deviation. This version (ADRS) is designed not to signal non-
normality when presented with normally distributed data that have poor resolution or are
coarsely rounded. Practice D6299, Standard Practice for Applying Statistical Quality
Assurance and Control Charting Techniques to Evaluate Analytical Measurement System
Performance describes the AD approach and in a to be published Research Report,
available from ASTM, describes the ADRS approach.

Normal?
The following conclusions are made regarding the normalcy of the “These Data” distribution
based on the Anderson-Darling Statistic:

Normal AD < 0.75


Marginally Normal AD = 0.75 – 1.3
Not Normal AD > 1.3

Z-Score (for a result Xi)

Z i  X i  X  s Report to nearest 0.01

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Statistics (for Non-Numeric Results)

Unique Results
Number of unique non-numeric results reported by all laboratories submitting results

Mode
The mode is the most frequently occurring non-numeric result.

Modal
Frequency of Mode divided by n and expressed as a percent. (Resolution = 0.1 %.)

Summary of Symbols and Abbreviations Used in PTP Reports

$ Applies to past Z-Scores possibly meaning:


 All lab results submitted were the same, therefore Z-Scores non-existent
 Statistics were not performed for test (see NSP)
 Submitted result was non-conforming (see NCR)
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside of range -2 to 2
# Z-Score greater than 90
ASTM r ASTM repeatability
ASTM R ASTM Reproducibility
NCR Non-Conforming Result
ND Not Detected
NDS No data submitted
NSP No Statistics Performed: < 6 results submitted, or mixed data set w/ > 18%
non-numeric results, or statistics not calculated as per program review.
R Outlier; data rejected by GESD

November 9, 2018 www.astm.org 11


Alphabetical Listing of Laboratories
Submitting Results for DGA1808

Lab Name (as given in Registration) City State/Province Country


ABB LTDA - Pereira Colombia Pereira/Dodquebradas Colombia
ABB S.A. - Lima Peru Lima Peru
AS "Augstsprieguma tikls" Riga Latvia
Al-Ahleia Switchgear Co. SUBHAN INDUSTRIAL AREA Kuwait
Alabama Power Company Calera AL United States
Alstom Grid Australia Archerfield QLD Australia
Ameren Missouri ST. LOUIS MO United States
Antung Trading Corporation Taoyuan City, Taiwan
Applus Norcontrol S.L.U. Madrid Spain
Astor Transformator Enerji Tur. Ins. Ve Pet. A.S. ANKARA Turkey
Boryeong Thermal Power Site Division Boryeong-si Korea, Republic of
CENNIX LABORATORY (M) SDN BHD Selangor Malaysia
CIDET Angioquia, Sabaneta Colombia
Cennix Laboratory (M) Sdn Bhd Selangor Malaysia
Central Electricity Generating Company Aqaba Jordan
Chec Sa Esp MANIZALES CA Colombia
Cmc Ltda MIAMI FL United States
Con Edison LONG ISLAND CITY NY United States
Constellation Power Source BALTIMORE MD United States
Consumers Energy JACKSON MI United States
Doble Engineering Company WATERTOWN MA United States
Dugan Enerji Teknoloji Çözümleri San. Tic. Ltda Sakarya Turkey
Duke Energy Corp HUNTERSVILLE NC United States
EMCALI EICE ESP Cali Valle De Cauca Colombia
East KY Power Corp WINCHESTER KY United States
Electrotechnica Arteche Hnos SL. Mungia Bizkaia - C.P. Spain
Emirates Global Aluminium United Arab Emirates

November 9, 2018 www.astm.org 12


Lab Name (as given in Registration) City State/Province Country
Eskom - JHB Johannesburg Gauteng South Africa
Eskom-Bloemfontein Johannesburg Gauteng South Africa
Eskom-Brackenfell Johannesburg South Africa
Eskom-Klerksdorp Klerksdorp South Africa
Eskom-Pietermaritzburg Johannesburg South Africa
Eskom-Rotek Johannesburg Gauteng South Africa
Eskom-Witbank Witbank Mpumalanga South Africa
FPL Central Laboratory WEST PALM BEACH FL United States
First Energy MAYFIELD VILLAGE OH United States
Fortune Electric Co., Ltd. Taoyuan Taiwan
GE Grid Solutions (UK) LTD Lab 2 Lisburn United Kingdom
GMT Laboratorios, S.A. C.V. Ecatepec Mexico
Ge Grid Solutions (Uk) Ltd Lisburn United Kingdom
Geo Chem Middle East DUBAI United Arab Emirates
HV Oil Incorporated - Edmonton EDMONTON AB Canada
HV Oil Incorporated - Saskotoon Saskatoon Canada
Hawaiian Electric Co Pearl City HI United States
Hydro-Quebec Montreal Canada
Inci Makina San. LTD Cayirova Turkey
Industrial Support Services Dammam Saudi Arabia
Inspectorate (Singapore) Pte Ltd - Singapore Singapore Singapore
Inspectorate International Ltd - Dubai Dubai United Arab Emirates
Integrys Business Support, LLC Green Bay WI United States
Intertek - Johannesburg Johannesburg South Africa
Intertek - Singapore SINGAPORE Singapore
Jet-Care International Inc CEDAR KNOLLS NJ United States
Jorpa Ingenieria S.A. SANTIAGO Chile
Kesir Muhendislik Elektrik Mak Ins San ve Tic Ltd Sti Umraniye Turkey
Kicer Technology Co. Ltd. New Taipei City 235 Taiwan
Kinectrics Inc. Toronto Canada
L.M.P. S.R.L. SETTEVILLE DI GUIDONIA Italy
LADAA Irapuato GTO Mexico
LGE-KU Ghent KY United States
Lab Oil Srl TORINO Italy
November 9, 2018 www.astm.org 13
Lab Name (as given in Registration) City State/Province Country
Laboratoire Oksman Ramonville St Agne France
Les Services SET Saint-Jean-Sur-Richelieu Canada
Lubrisider Chile SA Santiago Chile
Manitoba Hydro Selkirk Canada
Marafiq Yanbu Saudi Arabia
Morgan Schaffer LASALLE Canada
Mva Diagnostics, Inc Canton OH United States
Oil Reclaiming Sa De Cv ATLACOMULCO Mexico
Oncor Electric Delivery LANCASTER TX United States
PG&E SAN RAMON CA United States
PGI Industries Pte Ltd Singapore Singapore
Powertech Labs Inc. SURREY Canada
Proindulek Sa de Cv Monterrey Mexico
Pseg Mts South Plainfield NJ United States
Ray International Muscat Oman
Rondar Inc HAMILTON Canada
S D Myers Inc TALLMADGE OH United States
SGS - Herguth Labs Inc - Vallejo, CA VALLEJO CA United States
San Diego Gas & Electric San Diego CA United States
Sea Marconi Technologies Sas COLLEGNO (TO) Italy
Sertin Lab S.A. Quito Ecuador
Siemens S.A. Tenjo Colombia
Socotec Uk Doncaster United Kingdom
T V A Central Labs Services CHATTANOOGA TN United States
TJ-H2b Analytical Services Sacramento CA United States
TJH2B Latina SAC Lima Peru
TNBR QATS Sdn Bhd Kajang Malaysia
Talen Energy HAZLETON PA United States
Tampa Electric Company TAMPA FL United States
Tertec Taoyuan Taiwan
Testmark Laboratories Ltd MISSISSAUGA Canada
Transequipos Ltda. COTA Colombia
Transfo Services Laboratory CHATEAUBOURG France
Transformer Fitness Pty Ltd Welshpool Australia
November 9, 2018 www.astm.org 14
Lab Name (as given in Registration) City State/Province Country
Transformer Oil Lab & Services Sdn Bhd Selangor Malaysia
UTE Laboratory Montevideo Uruguay
United Power Services Inc NASHVILLE TN United States
We Energies MILWAUKEE WI United States
Weidmann Electrical Technology - Bensalem, PA BENSALEM PA United States
Weidmann Electrical Technology - Brookside Village, TX Brookside Village TX United States
Weidmann Electrical Technology - Burlington, Ontario BURLINGTON Canada
Weidmann Electrical Technology - Calgary CALGARY Canada
Weidmann Electrical Technology - Dorval DORVAL Canada
Weidmann Electrical Technology - Indianapolis, IN INDIANAPOLIS IN United States
Weidmann Electrical Technology - Sacramento, CA Rancho Cordova CA United States
Weidmann Electrical Technology - Waukesha, WI WAUKESHA WI United States

November 9, 2018 www.astm.org 15


Results Summary for All Methods
Dissolved Gas Analysis - DGA1808

Numeric Methods Method Performance Statistics

Measured Property With Conforming Results Precision Anderson


Designation Units Average StdDev ASTM R These Data R TPI Normal?
Conditions Results Used Performance Darling
Headspace Sampling, C,
D3612-02(2017) ppm 92 89 6.8 2.0 5.6 2.88 Not Normal
Acetylene
Headspace Sampling, C,
D3612-02(2017) ppm 92 92 1096.0 237.5 657.8 0.55 Normal
Carbon Dioxide
Headspace Sampling, C,
D3612-02(2017) ppm 92 89 37.8 14.5 40.1 2.11 Not Normal
Carbon Monoxide
Headspace Sampling, C,
D3612-02(2017) ppm 92 88 20.3 2.9 8.1 0.84 Marginally Normal
Ethane
Headspace Sampling, C,
D3612-02(2017) ppm 92 89 19.6 2.9 8.1 0.37 Normal
Ethylene
Headspace Sampling, C,
D3612-02(2017) ppm 91 89 25.2 6.6 18.3 0.72 Normal
Hydrogen
Headspace Sampling, C,
D3612-02(2017) ppm 92 92 119.6 23.1 64.1 0.80 Marginally Normal
Methane
Headspace Sampling, C,
D3612-02(2017) ppm 91 91 57128.3 12259.4 33958.4 0.27 Normal
Nitrogen
Headspace Sampling, C,
D3612-02(2017) ppm 91 91 24633.6 6070.2 16814.5 0.71 Normal
Oxygen
Headspace Sampling, C,
D3612-02(2017) ppm 23 21 2.0 3.3 9.2 3.14 Not Normal
Propane
Headspace Sampling, C,
D3612-02(2017) ppm 18 18 22.1 13.8 38.1 1.07 Marginally Normal
Propylene
Stripper Column
D3612-17 ppm 8 7 7.3 0.7 2.1 0.47 Normal
Extraction, B, Acetylene
Stripper Column
Extraction, B, Carbon D3612-17 ppm 8 8 1093.6 285.0 853.0 789.4 Consistent 1.08 0.46 Normal
Dioxide
Stripper Column
Extraction, B, Carbon D3612-17 ppm 8 8 38.8 19.3 53.4 0.34 Normal
Monoxide

November 9, 2018 www.astm.org 16


Numeric Methods Method Performance Statistics

Measured Property With Conforming Results Precision Anderson


Designation Units Average StdDev ASTM R These Data R TPI Normal?
Conditions Results Used Performance Darling
Stripper Column
D3612-17 ppm 8 7 19.7 4.5 12.5 0.67 Normal
Extraction, B, Ethane
Stripper Column
D3612-17 ppm 8 6 18.7 2.9 8.0 0.40 Normal
Extraction, B, Ethylene
Stripper Column
D3612-17 ppm 8 7 43.5 33.9 93.9 0.54 Normal
Extraction, B, Hydrogen
Stripper Column
D3612-17 ppm 8 8 130.5 18.8 79.6 52.2 Consistent 1.53 0.54 Normal
Extraction, B, Methane
Stripper Column
D3612-17 ppm 8 8 58383.0 9017.2 20434.1 24977.7 Consistent 0.82 0.37 Normal
Extraction, B, Nitrogen
Stripper Column
D3612-17 ppm 8 8 25435.8 4962.8 13746.9 0.22 Normal
Extraction, B, Oxygen
Stripper Column
D3612-17 ppm 2 NSP
Extraction, B, Propane
Stripper Column
D3612-17 ppm 2 NSP
Extraction, B, Propylene
Vacuum Extraction, A,
D3612-02(2017) ppm 12 12 6.1 3.4 9.5 0.72 Normal
Acetylene
Vacuum Extraction, A,
D3612-02(2017) ppm 12 12 813.2 361.2 618.0 1000.4 Worse 0.62 0.63 Normal
Carbon Dioxide
Vacuum Extraction, A,
D3612-02(2017) ppm 12 12 33 12 32 0.21 Normal
Carbon Monoxide
Vacuum Extraction, A,
D3612-02(2017) ppm 12 12 15.0 7.4 20.5 0.54 Normal
Ethane
Vacuum Extraction, A,
D3612-02(2017) ppm 12 12 15.3 7.6 21.0 0.38 Normal
Ethylene
Vacuum Extraction, A,
D3612-02(2017) ppm 12 12 22.5 12.4 34.4 0.15 Normal
Hydrogen
Vacuum Extraction, A,
D3612-02(2017) ppm 12 10 117.2 16.0 84.4 44.5 Better 1.90 0.19 Normal
Methane
Vacuum Extraction, A,
D3612-02(2017) ppm 12 12 43744.9 28519.1 11811.1 78997.8 Worse 0.15 1.00 Marginally Normal
Nitrogen
Vacuum Extraction, A,
D3612-02(2017) ppm 12 12 22010.4 11681.4 32357.4 1.76 Not Normal
Oxygen
Vacuum Extraction, A,
D3612-02(2017) ppm 2 NSP
Propane
Vacuum Extraction, A,
D3612-02(2017) ppm 2 NSP
Propylene
Water Content D1533-12 mg/kg 57 55 10.0 3.7 14.0 10.4 Better 1.35 1.36 Not Normal

November 9, 2018 www.astm.org 17


Non-Numeric Methods Method Performance Statistics
Measured Property Conforming Results Unique
Designation Mode Modal%
With Conditions Results Used Results

NSP - No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.

November 9, 2018 www.astm.org 18


Vacuum Extraction, A, Acetylene, D3612-02(2017)
Data Report
Vacuum Extraction, A, Acetylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 12 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 12
$ Z-Score not calculated
Average 6.1
StdDev 3.4
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 9.5
TPI
ADrs Statistic 0.72 Normal

November 9, 2018 www.astm.org 19


Results Table and Z-Scores
Vacuum Extraction, A, Acetylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 3 -3.1 -0.91 NDS NDS NDS 1 -0.91
0021 7 0.9 0.26 0.74 0.68 0.66 4 0.59 0.22
0030 7 0.9 0.26 NDS 0.75 0.82 3 0.61 0.31
0041 7.9 1.8 0.52 0.74 0.39 0.66 4 0.58 0.15
0068 7 0.9 0.26 NDS NDS NDS 1 0.26
0090 5 -1.1 -0.32 NDS 0.61 NDS 2 0.15 0.66
0097 7 0.9 0.26 NDS NDS NDS 1 0.26
0103 4 -2.1 -0.61 0.74 -0.29 -0.77 4 -0.23 0.68
0105 5 -1.1 -0.32 0.26 0.32 -0.30 4 -0.01 0.35
0110 1.346275 -4.753725 -1.39 -2.05 NDS NDS 2 -1.72 0.47
0113 15 8.9 2.60 3 NDS -0.29 NDS 2 1.16 2.04
0123 4 -2.1 -0.61 -0.22 -1.44 -0.14 4 -0.60 0.59

Pooled StdDev of Z: 0.62


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 20


Distribution of Results

November 9, 2018 www.astm.org 21


Vacuum Extraction, A, Carbon Dioxide, D3612-02(2017)
Data Report
Vacuum Extraction, A, Carbon Dioxide by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 12 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 12
$ Z-Score not calculated
Average 813.2
StdDev 361.2
ASTM R 618.0
These Data R 1000.4 Worse than ASTM R
TPI 0.62
ADrs Statistic 0.63 Normal

November 9, 2018 www.astm.org 22


Results Table and Z-Scores
Vacuum Extraction, A, Carbon Dioxide by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 173 -640.2 -1.77 NDS NDS NDS 1 -1.77
0021 1189 375.8 1.04 0.12 0.59 0.50 4 0.56 0.38
0030 1130 316.8 0.88 NDS 0.70 0.54 3 0.71 0.17
0041 1220 406.8 1.13 0.63 0.29 0.98 4 0.76 0.38
0068 978 164.8 0.46 NDS NDS NDS 1 0.46
0090 1007 193.8 0.54 NDS 0.38 NDS 2 0.46 0.11
0097 392 -421.2 -1.17 NDS NDS NDS 1 -1.17
0103 659 -154.2 -0.43 1.88 0.21 -0.07 4 0.40 1.02
0105 795 -18.2 -0.05 -1.11 1.73 0.86 4 0.36 1.22
0110 266.143405 -547.056595 -1.51 -0.68 NDS NDS 2 -1.10 0.59
0113 987 173.8 0.48 NDS -0.44 NDS 2 0.02 0.65
0123 962 148.8 0.41 -0.53 -0.95 -0.41 4 -0.37 0.57

Pooled StdDev of Z: 0.69


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 23


Distribution of Results

November 9, 2018 www.astm.org 24


Vacuum Extraction, A, Carbon Monoxide, D3612-02(2017)
Data Report
Vacuum Extraction, A, Carbon Monoxide by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 12 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 12
$ Z-Score not calculated
Average 33
StdDev 12
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 32
TPI
ADrs Statistic 0.21 Normal

November 9, 2018 www.astm.org 25


Results Table and Z-Scores
Vacuum Extraction, A, Carbon Monoxide by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 18 -15 -1.28 NDS NDS NDS 1 -1.28
0021 38 5 0.44 0.79 1.59 0.10 4 0.73 0.64
0030 29 -4 -0.33 NDS 0.34 -0.46 3 -0.15 0.43
0041 43 10 0.86 0.79 0.54 0.04 4 0.56 0.37
0068 30 -3 -0.25 NDS NDS NDS 1 -0.25
0090 14 -19 -1.62 NDS -1.38 NDS 2 -1.50 0.17
0097 37 4 0.35 NDS NDS NDS 1 0.35
0103 50 17 1.46 0.29 0.25 -0.98 4 0.26 1
0105 27 -6 -0.51 0.66 1.30 0.07 4 0.38 0.78
0110 49.86342 16.86342 1.45 8.48R NDS NDS 1 1.45
0113 37 4 0.35 NDS -0.71 NDS 2 -0.18 0.75
0123 22 -11 -0.93 -1.45 -1.29 -0.98 4 -1.16 0.25

Pooled StdDev of Z: 0.76


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 26


Distribution of Results

November 9, 2018 www.astm.org 27


Vacuum Extraction, A, Ethane, D3612-02(2017)
Data Report
Vacuum Extraction, A, Ethane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 12 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 12
$ Z-Score not calculated
Average 15.0
StdDev 7.4
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 20.5
TPI
ADrs Statistic 0.54 Normal

November 9, 2018 www.astm.org 28


Results Table and Z-Scores
Vacuum Extraction, A, Ethane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 3 -12 -1.62 NDS NDS NDS 1 -1.62
0021 17 2 0.27 -0.68 0.53 0.33 4 0.11 0.54
0030 20 5 0.68 NDS 0.86 0.90 3 0.81 0.12
0041 20.4 5.4 0.73 1.06 1.00 0.65 4 0.86 0.2
0068 21 6 0.81 NDS NDS NDS 1 0.81
0090 11 -4 -0.54 NDS 0.86 NDS 2 0.16 0.99
0097 20 5 0.68 NDS NDS NDS 1 0.68
0103 9 -6 -0.81 1.06 -0.28 -0.75 4 -0.20 0.87
0105 16 1 0.14 0.48 1.00 0.74 4 0.59 0.37
0110 1.33104 -13.66896 -1.84 -8.92R NDS NDS 1 -1.84
0113 25 10 1.35 NDS 0.72 NDS 2 1.04 0.45
0123 16 1 0.14 -1.26 -1.38 -0.19 4 -0.67 0.76

Pooled StdDev of Z: 0.56


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 29


Distribution of Results

November 9, 2018 www.astm.org 30


Vacuum Extraction, A, Ethylene, D3612-02(2017)
Data Report
Vacuum Extraction, A, Ethylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 12 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 12
$ Z-Score not calculated
Average 15.3
StdDev 7.6
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 21.0
TPI
ADrs Statistic 0.38 Normal

November 9, 2018 www.astm.org 31


Results Table and Z-Scores
Vacuum Extraction, A, Ethylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 3 -12.3 -1.62 NDS NDS NDS 1 -1.62
0021 18 2.7 0.36 0.38 0.73 0.73 4 0.55 0.21
0030 22 6.7 0.88 NDS 1.02 0.68 3 0.86 0.17
0041 20.5 5.2 0.68 0.56 0.73 0.72 4 0.67 0.08
0068 22 6.7 0.88 NDS NDS NDS 1 0.88
0090 10 -5.3 -0.70 NDS 0.67 NDS 2 -0.02 0.97
0097 19 3.7 0.49 NDS NDS NDS 1 0.49
0103 10 -5.3 -0.70 0.90 -0.19 -0.72 4 -0.18 0.76
0105 16 0.7 0.09 0.38 0.96 1.01 4 0.61 0.45
0110 2.20919 -13.09081 -1.73 -2.14 NDS NDS 2 -1.94 0.29
0113 26 10.7 1.41 NDS 0.73 NDS 2 1.07 0.48
0123 15 -0.3 -0.04 -0.13 -1.29 -0.02 4 -0.37 0.62

Pooled StdDev of Z: 0.48


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 32


Distribution of Results

November 9, 2018 www.astm.org 33


Vacuum Extraction, A, Hydrogen, D3612-02(2017)
Data Report
Vacuum Extraction, A, Hydrogen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 12 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 12
$ Z-Score not calculated
Average 22.5
StdDev 12.4
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 34.4
TPI
ADrs Statistic 0.15 Normal

November 9, 2018 www.astm.org 34


Results Table and Z-Scores
Vacuum Extraction, A, Hydrogen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 5 -17.5 -1.41 NDS NDS NDS 1 -1.41
0021 31 8.5 0.68 0.76 1.19 1.20 4 0.96 0.28
0030 28 5.5 0.44 NDS 0.63 0.49 3 0.52 0.1
0041 36 13.5 1.09 0.10 -0.14 1.36 4 0.60 0.73
0068 20 -2.5 -0.20 NDS NDS NDS 1 -0.20
0090 14 -8.5 -0.68 NDS -1.05 NDS 2 -0.87 0.26
0097 22 -0.5 -0.04 NDS NDS NDS 1 -0.04
0103 16 -6.5 -0.52 0.76 0.42 -2.33 4 -0.42 1.39
0105 25 2.5 0.20 0.98 0.21 0.26 4 0.41 0.38
0110 0 -22.5 -1.81 -1.39 NDS NDS 2 -1.60 0.3
0113 43 20.5 1.65 NDS 1.33 NDS 2 1.49 0.23
0123 30 7.5 0.60 0.17 -1.97 -0.38 4 -0.40 1.12

Pooled StdDev of Z: 0.74


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 35


Distribution of Results

November 9, 2018 www.astm.org 36


Vacuum Extraction, A, Methane, D3612-02(2017)
Data Report
Vacuum Extraction, A, Methane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 12 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 10
$ Z-Score not calculated
Average 117.2
StdDev 16.0
ASTM R 84.4
These Data R 44.5 Better than ASTM R
TPI 1.90
ADrs Statistic 0.19 Normal

November 9, 2018 www.astm.org 37


Results Table and Z-Scores
Vacuum Extraction, A, Methane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 5 -112.2 -6.99 R NDS NDS NDS 0
0021 141 23.8 1.48 0.82 1.40 1.13 4 1.21 0.3
0030 129 11.8 0.74 NDS 0.75 0.46 3 0.65 0.16
0041 137 19.8 1.23 0.33 0.46 0.78 4 0.70 0.4
0068 119 1.8 0.11 NDS NDS NDS 1 0.11
0090 89 -28.2 -1.76 NDS 0.11 NDS 2 -0.83 1.32
0097 121 3.8 0.24 NDS NDS NDS 1 0.24
0103 99 -18.2 -1.13 0.95 0.31 -0.59 4 -0.12 0.93
0105 112 -5.2 -0.32 0.19 0.90 0.90 4 0.42 0.59
0110 17.419935 -99.780065 -6.22 R -2.06 NDS NDS 1 -2.06
0113 114 -3.2 -0.20 NDS -0.44 NDS 2 -0.32 0.17
0123 111 -6.2 -0.39 -0.12 -0.98 0.47 4 -0.26 0.6

Pooled StdDev of Z: 0.6


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 38


Distribution of Results

November 9, 2018 www.astm.org 39


Vacuum Extraction, A, Nitrogen, D3612-02(2017)
Data Report
Vacuum Extraction, A, Nitrogen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 12 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 12
$ Z-Score not calculated
Average 43744.9
StdDev 28519.1
ASTM R 11811.1
These Data R 78997.8 Worse than ASTM R
TPI 0.15
ADrs Statistic 1.00 Marginally Normal

November 9, 2018 www.astm.org 40


Results Table and Z-Scores
Vacuum Extraction, A, Nitrogen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 21576 -22,168.9 -0.78 2 NDS NDS NDS 1 -0.78
0021 76798 33,053.1 1.16 2 -0.53 0.08 0.63 4 0.34 0.73
0030 61100 17,355.1 0.61 2 NDS 36.15R 0.61 2 0.61 0
0041 70500 26,755.1 0.94 2 1.49 -0.38 1.72 4 0.94 0.94
0068 5666 -38,078.9 -1.34 2 NDS NDS NDS 1 -1.34
0090 61026 17,281.1 0.61 2 NDS 0.23 NDS 2 0.42 0.27
0097 58 -43,686.9 -1.53 2 NDS NDS NDS 1 -1.53
0103 53968 10,223.1 0.36 1.03 0.02 -0.87 4 0.14 0.79
0105 55282 11,537.1 0.40 -0.92 1.76 0.93 4 0.54 1.12
0110 46.18743561 -43,698.7125644 -1.53 2 18.32R NDS NDS 1 -1.53
0113 54588 10,843.1 0.38 NDS -0.30 NDS 2 0.04 0.48
0123 64330 20,585.1 0.72 2 -0.42 -0.40 0.29 4 0.05 0.56

Pooled StdDev of Z: 0.94


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 41


Distribution of Results

November 9, 2018 www.astm.org 42


Vacuum Extraction, A, Oxygen, D3612-02(2017)
Data Report
Vacuum Extraction, A, Oxygen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 12 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 12
$ Z-Score not calculated
Average 22010.4
StdDev 11681.4
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 32357.4
TPI
ADrs Statistic 1.76 Not Normal

November 9, 2018 www.astm.org 43


Results Table and Z-Scores
Vacuum Extraction, A, Oxygen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 6708 -15,302.4 -1.31 NDS NDS NDS 1 -1.31
0021 26961 4,950.6 0.42 -0.73 -0.22 -0.34 4 -0.22 0.48
0030 27500 5,489.6 0.47 NDS 28.23R 0.11 2 0.29 0.25
0041 32000 9,989.6 0.86 1.46 -0.24 1.05 4 0.78 0.73
0068 2376 -19,634.4 -1.68 NDS NDS NDS 1 -1.68
0090 27093 5,082.6 0.44 NDS 0.07 NDS 2 0.26 0.26
0097 26588 4,577.6 0.39 NDS NDS NDS 1 0.39
0103 28935 6,924.6 0.59 0.64 0.83 -0.78 4 0.32 0.74
0105 26167 4,156.6 0.36 -1.23 1.40 0.92 4 0.36 1.14
0110 18.31860898 -21,992.081391 -1.88 16.96R NDS NDS 1 -1.88
0113 31770 9,759.6 0.84 NDS -0.18 NDS 2 0.33 0.72
0123 28008 5,997.6 0.51 0.37 -1.14 0.15 4 -0.03 0.76

Pooled StdDev of Z: 0.87


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 44


Distribution of Results

November 9, 2018 www.astm.org 45


Vacuum Extraction, A, Propane, D3612-02(2017)
Data Report
Vacuum Extraction, A, Propane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 2 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used
$ Z-Score not calculated
Average NSP
StdDev
ASTM R
These Data R
TPI
ADrs Statistic

November 9, 2018 www.astm.org 46


Results Table and Z-Scores
Vacuum Extraction, A, Propane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0068 0 $ NDS NDS NDS 0
0110 1.44970 $ $ NDS NDS 0

Pooled StdDev of Z: 0
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 47


Vacuum Extraction, A, Propylene, D3612-02(2017)
Data Report
Vacuum Extraction, A, Propylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 2 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used
$ Z-Score not calculated
Average NSP
StdDev
ASTM R
These Data R
TPI
ADrs Statistic

November 9, 2018 www.astm.org 48


Results Table and Z-Scores
Vacuum Extraction, A, Propylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0068 0 $ NDS NDS NDS 0
0110 1.44970 $ $ NDS NDS 0

Pooled StdDev of Z: 0
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 49


Stripper Column Extraction, B, Acetylene, D3612-17
Data Report
Stripper Column Extraction, B, Acetylene by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 8 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 7
$ Z-Score not calculated
Average 7.3
StdDev 0.7
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 2.1
TPI
ADrs Statistic 0.47 Normal

November 9, 2018 www.astm.org 50


Results Table and Z-Scores
Stripper Column Extraction, B, Acetylene by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 6 -1.3 -1.80 -0.85 -0.97 NDS 3 -1.21 0.52
0044 7 -0.3 -0.46 0.06 1.81 -5.56R 3 0.47 1.19
0052 8 0.7 0.88 -0.40 0.21 -1.39 4 -0.18 0.96
0067 8 0.7 0.88 -0.85 -1.03 -1.39 4 -0.60 1.01
0069 7.4 0.1 0.08 0.78 0.57 0.28 4 0.43 0.31
0093 27 19.7 26.36 R 1.87 -1.15 -6.39R 2 0.36 2.14
0120 7 -0.3 -0.46 0.06 NDS NDS 2 -0.20 0.37
0121 8 0.7 0.88 1.87 NDS NDS 2 1.38 0.7

Pooled StdDev of Z: 0.84


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 51


Distribution of Results

November 9, 2018 www.astm.org 52


Stripper Column Extraction, B, Carbon Dioxide, D3612-17
Data Report
Stripper Column Extraction, B, Carbon Dioxide by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 8 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 8
$ Z-Score not calculated
Average 1093.6
StdDev 285.0
ASTM R 853.0
These Data R 789.4 Consistent with ASTM R
TPI 1.08
ADrs Statistic 0.46 Normal

November 9, 2018 www.astm.org 53


Results Table and Z-Scores
Stripper Column Extraction, B, Carbon Dioxide by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 885 -208.6 -0.73 -0.99 -1.58 NDS 3 -1.10 0.44
0044 1165 71.4 0.25 0.45 0.98 -1.63 4 0.01 1.14
0052 962 -131.6 -0.46 -0.30 0.23 -0.81 4 -0.34 0.43
0067 1140 46.4 0.16 -0.60 -0.67 -0.45 4 -0.39 0.38
0069 969 -124.6 -0.44 0.56 0.50 0.26 4 0.22 0.46
0093 1201 107.4 0.38 -2.26 0.37 0.64 4 -0.22 1.37
0120 742 -351.6 -1.23 0.50 NDS NDS 2 -0.37 1.22
0121 1685 591.4 2.08 3 6.47R NDS NDS 1 2.08

Pooled StdDev of Z: 0.77


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 54


Distribution of Results

November 9, 2018 www.astm.org 55


Stripper Column Extraction, B, Carbon Monoxide, D3612-17
Data Report
Stripper Column Extraction, B, Carbon Monoxide by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 8 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 8
$ Z-Score not calculated
Average 38.8
StdDev 19.3
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 53.4
TPI
ADrs Statistic 0.34 Normal

November 9, 2018 www.astm.org 56


Results Table and Z-Scores
Stripper Column Extraction, B, Carbon Monoxide by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 50 11.2 0.58 -1.47 1.59 NDS 3 0.23 1.56
0044 24 -14.8 -0.77 -0.05 0.29 -1.27 4 -0.45 0.7
0052 37 -1.8 -0.10 -0.36 0.08 -1.39 4 -0.44 0.66
0067 16 -22.8 -1.18 -0.72 -0.13 -0.04 4 -0.52 0.53
0069 26.7 -12.1 -0.63 0.97 0.76 1.13 4 0.56 0.81
0093 48 9.2 0.48 -1.07 0.18 -0.79 4 -0.30 0.75
0120 32 -6.8 -0.35 1.37 NDS NDS 2 0.51 1.22
0121 77 38.2 1.98 6.48R NDS NDS 1 1.98

Pooled StdDev of Z: 0.85


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 57


Distribution of Results

November 9, 2018 www.astm.org 58


Stripper Column Extraction, B, Ethane, D3612-17
Data Report
Stripper Column Extraction, B, Ethane by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 8 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 7
$ Z-Score not calculated
Average 19.7
StdDev 4.5
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 12.5
TPI
ADrs Statistic 0.67 Normal

November 9, 2018 www.astm.org 59


Results Table and Z-Scores
Stripper Column Extraction, B, Ethane by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 17 -2.7 -0.60 -0.68 -1.25 NDS 3 -0.84 0.35
0044 15 -4.7 -1.05 -0.68 -0.26 -1.18 4 -0.79 0.41
0052 21 1.3 0.29 1.43 1.18 0.18 4 0.77 0.63
0067 19.0 -0.7 -0.16 -0.42 -0.33 -0.11 4 -0.26 0.14
0069 19 -0.7 -0.16 1.35 0.07 0.79 4 0.51 0.69
0093 98 78.3 17.40 R 8.83R -0.92 -1.62 2 -1.27 0.49
0120 18 -1.7 -0.38 0.38 NDS NDS 2 0.00 0.54
0121 29 9.3 2.06 3 8.04R NDS NDS 1 2.06

Pooled StdDev of Z: 0.47


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 60


Distribution of Results

November 9, 2018 www.astm.org 61


Stripper Column Extraction, B, Ethylene, D3612-17
Data Report
Stripper Column Extraction, B, Ethylene by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 8 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 6
$ Z-Score not calculated
Average 18.7
StdDev 2.9
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 8.0
TPI
ADrs Statistic 0.40 Normal

November 9, 2018 www.astm.org 62


Results Table and Z-Scores
Stripper Column Extraction, B, Ethylene by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 39 20.3 7.07 R 1.82 -1.30 NDS 2 0.26 2.21
0044 15 -3.7 -1.28 -0.98 0.01 -1.59 4 -0.96 0.69
0052 22 3.3 1.16 0.22 1.09 0.37 4 0.71 0.48
0067 17 -1.7 -0.58 -1.11 -0.53 -0.08 4 -0.58 0.42
0069 19 0.3 0.12 0.41 0.24 0.53 4 0.33 0.18
0093 43 24.3 8.46 R -0.45 -0.92 -1.76 3 -1.04 0.66
0120 17 -1.7 -0.58 -0.18 NDS NDS 2 -0.38 0.28
0121 22 3.3 1.16 1.95 NDS NDS 2 1.56 0.56

Pooled StdDev of Z: 0.7


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 63


Distribution of Results

November 9, 2018 www.astm.org 64


Stripper Column Extraction, B, Hydrogen, D3612-17
Data Report
Stripper Column Extraction, B, Hydrogen by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 7 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 7
$ Z-Score not calculated
Average 43.5
StdDev 33.9
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 93.9
TPI
ADrs Statistic 0.54 Normal

November 9, 2018 www.astm.org 65


Results Table and Z-Scores
Stripper Column Extraction, B, Hydrogen by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 52 8.5 0.25 $ $ NDS 1 0.25
0044 22 -21.5 -0.64 -0.83 -1.64 0.62 4 -0.62 0.93
0052 9 -34.5 -1.02 -0.61 -0.65 0.59 4 -0.42 0.7
0067 23.0 -20.5 -0.61 -0.30 -0.09 -0.92 4 -0.48 0.36
0069 53.8 10.3 0.30 1.12 0.62 0.68 4 0.68 0.34
0093 34 -9.5 -0.28 0.24 1.82 -2.18 4 -0.10 1.65
0120 <13 $ NCR $ NDS NDS 0
0121 111 67.5 1.99 2.37 NDS NDS 2 2.18 0.27

Pooled StdDev of Z: 0.82


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 66


Distribution of Results

November 9, 2018 www.astm.org 67


Stripper Column Extraction, B, Methane, D3612-17
Data Report
Stripper Column Extraction, B, Methane by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 8 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 8
$ Z-Score not calculated
Average 130.5
StdDev 18.8
ASTM R 79.6
These Data R 52.2 Consistent with ASTM R
TPI 1.53
ADrs Statistic 0.54 Normal

November 9, 2018 www.astm.org 68


Results Table and Z-Scores
Stripper Column Extraction, B, Methane by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 153 22.5 1.19 0.97 -0.57 NDS 3 0.53 0.96
0044 119 -11.5 -0.61 -0.60 0.06 0.17 4 -0.25 0.42
0052 125 -5.5 -0.29 0.22 0.26 -0.04 4 0.04 0.26
0067 119 -11.5 -0.61 -0.79 -0.76 -0.78 4 -0.74 0.08
0069 117 -13.5 -0.72 1.36 1.23 1.10 4 0.74 0.98
0093 144 13.5 0.72 -1.95 -0.23 -2.30 4 -0.94 1.43
0120 108 -22.5 -1.19 -0.20 NDS NDS 2 -0.70 0.7
0121 159 28.5 1.51 5.46R NDS NDS 1 1.51

Pooled StdDev of Z: 0.73


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 69


Distribution of Results

November 9, 2018 www.astm.org 70


Stripper Column Extraction, B, Nitrogen, D3612-17
Data Report
Stripper Column Extraction, B, Nitrogen by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 8 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 8
$ Z-Score not calculated
Average 58383.0
StdDev 9017.2
ASTM R 20434.1
These Data R 24977.7 Consistent with ASTM R
TPI 0.82
ADrs Statistic 0.37 Normal

November 9, 2018 www.astm.org 71


Results Table and Z-Scores
Stripper Column Extraction, B, Nitrogen by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 66703 8,320 0.92 0.47 -1.17 NDS 3 0.07 1.1
0044 45409 -12,974 -1.44 -0.65 -1.56 -0.79 4 -1.11 0.46
0052 61732 3,349 0.37 -0.79 0.57 0.54 4 0.17 0.65
0067 57300 -1,083 -0.12 -0.07 -0.36 -0.32 4 -0.22 0.14
0069 60729 2,346 0.26 -0.53 1.37 2.12 4 0.81 1.17
0093 70852 12,469 1.38 -0.67 1.47 -1.63 4 0.14 1.54
0120 58535 152 0.02 0.58 NDS NDS 2 0.30 0.4
0121 45804 -12,579 -1.40 2.03 NDS NDS 2 0.32 2.43

Pooled StdDev of Z: 0.93


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 72


Distribution of Results

November 9, 2018 www.astm.org 73


Stripper Column Extraction, B, Oxygen, D3612-17
Data Report
Stripper Column Extraction, B, Oxygen by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 8 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 8
$ Z-Score not calculated
Average 25435.8
StdDev 4962.8
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 13746.9
TPI
ADrs Statistic 0.22 Normal

November 9, 2018 www.astm.org 74


Results Table and Z-Scores
Stripper Column Extraction, B, Oxygen by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 32073 6,637.2 1.34 0.50 -1.13 NDS 3 0.24 1.26
0044 16840 -8,595.8 -1.73 -0.77 -1.38 -0.61 4 -1.12 0.52
0052 27245 1,809.2 0.36 -0.37 0.92 -0.28 4 0.16 0.6
0067 25900 464.2 0.09 0.26 0.15 0.12 4 0.16 0.07
0069 29954 4,518.2 0.91 -0.16 1.96 1.58 4 1.07 0.93
0093 20655 -4,780.8 -0.96 -0.47 0.18 -0.67 4 -0.48 0.48
0120 27372 1,936.2 0.39 0.79 NDS NDS 2 0.59 0.28
0121 23447 -1,988.8 -0.40 2.64 NDS NDS 2 1.12 2.15

Pooled StdDev of Z: 0.83


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 75


Distribution of Results

November 9, 2018 www.astm.org 76


Stripper Column Extraction, B, Propane, D3612-17
Data Report
Stripper Column Extraction, B, Propane by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 2 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used
$ Z-Score not calculated
Average NSP
StdDev
ASTM R
These Data R
TPI
ADrs Statistic

November 9, 2018 www.astm.org 77


Results Table and Z-Scores
Stripper Column Extraction, B, Propane by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0044 4.4 $ $ $ NDS 0
0121 0 $ $ NDS NDS 0

Pooled StdDev of Z: 0
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 78


Stripper Column Extraction, B, Propylene, D3612-17
Data Report
Stripper Column Extraction, B, Propylene by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 2 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used
$ Z-Score not calculated
Average NSP
StdDev
ASTM R
These Data R
TPI
ADrs Statistic

November 9, 2018 www.astm.org 79


Results Table and Z-Scores
Stripper Column Extraction, B, Propylene by D3612-17 (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0044 0 $ $ $ NDS 0
0121 45 $ $ NDS NDS 0

Pooled StdDev of Z: 0
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 80


Headspace Sampling, C, Acetylene, D3612-02(2017)
Data Report
Headspace Sampling, C, Acetylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 92 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 89
$ Z-Score not calculated
Average 6.8
StdDev 2.0
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 5.6
TPI
ADrs Statistic 2.88 Not Normal

November 9, 2018 www.astm.org 81


Results Table and Z-Scores
Headspace Sampling, C, Acetylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 7 0.2 0.10 0.25 0.25 0.29 4 0.22 0.08
0002 5.29 -1.51 -0.74 NDS -0.81 NDS 2 -0.78 0.05
0004 4.3 -2.5 -1.22 -0.52 -1.00 0.15 4 -0.65 0.61
0005 16 9.2 4.52 R 0.25 0.49 NDS 2 0.37 0.17
0007 5.8 -1 -0.49 -0.06 3.65 0.74 4 0.96 1.86
0008 6 -0.8 -0.39 -0.14 0.30 0.42 4 0.05 0.38
0009 8 1.2 0.59 -0.52 -0.37 -1.62 4 -0.48 0.91
0011 7 0.2 0.10 0.63 0.11 0.02 4 0.22 0.28
0012 7 0.2 0.10 0.25 1.36 0.29 4 0.50 0.58
0013 7 0.2 0.10 -0.91 0.73 -0.80 4 -0.22 0.78
0014 8 1.2 0.59 1.02 0.54 NDS 3 0.72 0.26
0015 8 1.2 0.59 1.02 NDS 0.15 3 0.59 0.44
0016 8 1.2 0.59 -0.14 1.46 -0.39 4 0.38 0.83
0017 7.3 0.5 0.25 -0.10 0.38 -0.12 4 0.10 0.25
0022 7 0.2 0.10 0.63 0.78 0.07 4 0.40 0.36
0024 6.4 -0.4 -0.19 NDS -0.61 -0.67 3 -0.49 0.26
0025 4 -2.8 -1.37 NDS -0.04 4.11R 2 -0.71 0.94
0026 12.69556 5.89556 2.90 3 2.94 2.07 NDS 3 2.64 0.49
0028 6 -0.8 -0.39 0.25 0.78 0.56 4 0.30 0.51
0029 7 0.2 0.10 -0.14 0.11 0.15 4 0.06 0.13
0031 7 0.2 0.10 NDS -1.00 NDS 2 -0.45 0.78
0032 6 -0.8 -0.39 -0.52 NDS NDS 2 -0.46 0.09
0034 8 1.2 0.59 0.84 NDS NDS 2 0.72 0.18
0035 1.45 -5.35 -2.62 3 -0.85 -1.15 -1.11 4 -1.43 0.8
0036 5 -1.8 -0.88 NDS NDS NDS 1 -0.88
0038 8.8 2 0.99 NDS 0.70 NDS 2 0.85 0.21
0039 7.2 0.4 0.20 1.40 0.59 NDS 3 0.73 0.61
0040 5 -1.8 -0.88 -0.14 0.11 # 3 -0.30 0.51

November 9, 2018 www.astm.org 82


StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0041 9.0 2.2 1.08 -0.14 -1.53 NDS 3 -0.20 1.31
0042 10 3.2 1.57 1.02 -0.95 0.15 4 0.45 1.1
0043 12.2 5.4 2.65 3 0.32 NDS NDS 2 1.49 1.65
0045 7.6 0.8 0.40 NDS -0.32 0.70 3 0.26 0.52
0047 8 1.2 0.59 -0.14 0.45 0.42 4 0.33 0.32
0048 5 -1.8 -0.88 NDS -0.14 -0.53 3 -0.52 0.37
0049 8 1.2 0.59 0.63 0.45 0.15 4 0.46 0.22
0051 6 -0.8 -0.39 0.63 1.50 0.97 4 0.68 0.8
0054 7 0.2 0.10 -0.27 -0.56 -0.26 4 -0.25 0.27
0056 8 1.2 0.59 2.56 NDS NDS 2 1.58 1.39
0057 7.8 1 0.49 NDS NDS NDS 1 0.49
0059 6.3 -0.5 -0.24 -0.91 NDS NDS 2 -0.58 0.47
0060 7 0.2 0.10 0.63 0.54 0.63 4 0.48 0.25
0061 7 0.2 0.10 -0.91 0.45 NDS 3 -0.12 0.71
0063 7 0.2 0.10 -0.14 -1.00 NDS 3 -0.35 0.58
0064 7.4 0.6 0.30 -2.45 1.84 NDS 3 -0.10 2.17
0065 6 -0.8 -0.39 -0.14 -0.13 NDS 3 -0.22 0.15
0066 4 -2.8 -1.37 -0.52 -1.24 NDS 3 -1.04 0.46
0068 7 0.2 0.10 NDS NDS NDS 1 0.10
0070 4 -2.8 -1.37 -0.91 -0.71 -0.26 4 -0.81 0.46
0071 7 0.2 0.10 -0.14 0.20 NDS 3 0.05 0.17
0072 6 -0.8 -0.39 0.25 -0.13 NDS 3 -0.09 0.32
0073 16 9.2 4.52 R -0.52 -0.04 NDS 2 -0.28 0.34
0076 4.7 -2.1 -1.03 -1.37 -0.76 NDS 3 -1.05 0.31
0077 7 0.2 0.10 -0.14 0.93 0.56 4 0.36 0.48
0078 8 1.2 0.59 NDS -0.18 1.24 3 0.55 0.71
0079 5 -1.8 -0.88 -2.06 NDS NDS 2 -1.47 0.83
0080 9 2.2 1.08 NDS -0.85 0.02 3 0.08 0.97
0081 7.152 0.352 0.18 0.25 0.49 0.56 4 0.37 0.18
0082 7 0.2 0.10 0.25 1.55 1.65 4 0.89 0.83
0083 20 13.2 6.48 R NDS NDS 1.11 1 1.11
0084 7 0.2 0.10 -0.52 -0.90 NDS 3 -0.44 0.5
0085 7 0.2 0.10 -1.68 NDS -2.17 3 -1.25 1.19
November 9, 2018 www.astm.org 83
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0086 12 5.2 2.55 3 NDS NDS NDS 1 2.55
0087 6.89 0.09 0.05 6.41R NDS NDS 1 0.05
0088 8 1.2 0.59 1.02 -0.08 -0.67 4 0.22 0.74
0089 6 -0.8 -0.39 -1.64 -1.09 NDS 3 -1.04 0.63
0091 5 -1.8 -0.88 -0.52 -0.32 -0.39 4 -0.53 0.25
0092 8.9 2.1 1.03 1.52 2.24 1.34 4 1.53 0.51
0094 9 2.2 1.08 NDS 0.16 0.97 3 0.74 0.5
0095 6.16 -0.64 -0.31 NDS -0.08 -0.26 3 -0.22 0.12
0096 6 -0.8 -0.39 -0.14 NDS NDS 2 -0.27 0.18
0098 6 -0.8 -0.39 0.25 -0.90 0.70 4 -0.09 0.7
0099 6 -0.8 -0.39 NDS NDS NDS 1 -0.39
0101 7.5 0.7 0.35 1.02 0.59 NDS 3 0.65 0.34
0102 7 0.2 0.10 -0.52 -0.04 0.02 4 -0.11 0.28
0104 6 -0.8 -0.39 -0.14 -1.09 -1.07 4 -0.67 0.48
0105 7 0.2 0.10 NDS NDS NDS 1 0.10
0106 7 0.2 0.10 0.63 0.25 0.15 4 0.28 0.24
0107 8 1.2 0.59 0.63 0.25 0.15 4 0.41 0.24
0108 0.000 -6.8 -3.33 1,3 -1.68 -1.29 -1.79 4 -2.02 0.9
0112 7 0.2 0.10 -0.14 -0.13 -0.39 4 -0.14 0.2
0115 9 2.2 1.08 1.02 1.17 0.15 4 0.86 0.47
0117 6 -0.8 -0.39 -3.61 -0.47 2.61 4 -0.47 2.54
0119 6 -0.8 -0.39 -0.14 0.16 -0.12 4 -0.12 0.22
0121 7 0.2 0.10 1.79 NDS NDS 2 0.95 1.2
0122 7 0.2 0.10 -0.14 -0.66 -0.94 4 -0.41 0.47
0123 9 2.2 1.08 -0.52 -1.24 1.52 4 0.21 1.3
0124 8 1.2 0.59 1.02 0.78 0.70 4 0.77 0.18
0125 5.93 -0.87 -0.42 NDS 0.35 0.15 3 0.03 0.4
0126 7 0.2 0.10 -0.14 -0.32 0.29 4 -0.02 0.27
0127 2 -4.8 -2.35 3 NDS NDS NDS 1 -2.35
0128 0 -6.8 -3.33 1,3 NDS 1.41 NDS 2 -0.96 3.35
0129 8.6 1.8 0.89 NDS NDS NDS 1 0.89

November 9, 2018 www.astm.org 84


Pooled StdDev of Z: 0.81
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 85


Distribution of Results

November 9, 2018 www.astm.org 86


Frequency Histogram

November 9, 2018 www.astm.org 87


Headspace Sampling, C, Carbon Dioxide, D3612-02(2017)
Data Report
Headspace Sampling, C, Carbon Dioxide by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 92 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 92
$ Z-Score not calculated
Average 1096.0
StdDev 237.5
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 657.8
TPI
ADrs Statistic 0.55 Normal

November 9, 2018 www.astm.org 88


Results Table and Z-Scores
Headspace Sampling, C, Carbon Dioxide by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 1051 -45 -0.19 0.20 1.74 0.26 4 0.50 0.85
0002 702.97 -393.03 -1.66 NDS -1.01 NDS 2 -1.34 0.46
0004 471.6 -624.4 -2.63 3 -1.89 -1.31 -2.13 4 -1.99 0.55
0005 998 -98 -0.41 -0.31 -0.84 NDS 3 -0.52 0.28
0007 1294.8 198.8 0.84 0.91 1.10 0.14 4 0.75 0.42
0008 1004 -92 -0.39 -0.39 -0.26 -0.26 4 -0.33 0.08
0009 1183 87 0.37 -0.03 -0.11 -0.94 4 -0.18 0.55
0011 1053 -43 -0.18 0.16 -0.04 -0.02 4 -0.02 0.14
0012 1430 334 1.41 2.31 1.30 0.61 4 1.41 0.7
0013 1150 54 0.23 0.18 0.56 -0.68 4 0.07 0.53
0014 1068 -28 -0.12 1.23 -0.47 NDS 3 0.21 0.9
0015 1315 219 0.92 0.65 NDS 0.11 3 0.56 0.41
0016 1099 3 0.01 -0.15 0.49 -0.70 4 -0.09 0.49
0017 798.5 -297.5 -1.25 0.00 0.64 0.43 4 -0.05 0.85
0022 1101 5 0.02 -0.01 1.43 -0.01 4 0.36 0.72
0024 823 -273 -1.15 NDS -1.00 -0.61 3 -0.92 0.28
0025 1080 -16 -0.07 NDS -0.06 -0.09 3 -0.07 0.02
0026 1294.79768 198.79768 0.84 0.53 0.36 NDS 3 0.58 0.24
0028 1010 -86 -0.36 0.28 -0.29 -0.10 4 -0.12 0.29
0029 1113 17 0.07 -0.29 -0.16 -0.03 4 -0.10 0.16
0031 1202 106 0.45 NDS -0.78 NDS 2 -0.17 0.87
0032 700 -396 -1.67 0.35 NDS NDS 2 -0.66 1.43
0034 1298 202 0.85 1.15 NDS NDS 2 1.00 0.21
0035 877.45 -218.55 -0.92 -1.33 -0.38 -1.16 4 -0.95 0.41
0036 1836 740 3.12 1,3 NDS NDS NDS 1 3.12
0038 1415.2 319.2 1.34 NDS 1.19 NDS 2 1.27 0.11
0039 1011 -85 -0.36 0.61 -0.37 NDS 3 -0.04 0.56
0040 973 -123 -0.52 -1.91 0.15 0.42 4 -0.47 1.04

November 9, 2018 www.astm.org 89


StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0041 1157 61 0.26 1.35 -0.86 NDS 3 0.25 1.11
0042 1190 94 0.40 0.71 0.62 0.06 4 0.45 0.29
0043 1424 328 1.38 0.74 NDS NDS 2 1.06 0.45
0045 1147 51 0.21 NDS 0.33 0.54 3 0.36 0.17
0047 1114 18 0.08 -0.32 -0.46 0.18 4 -0.13 0.31
0048 961 -135 -0.57 NDS 0.33 0.26 3 0.01 0.5
0049 1154 58 0.24 -0.14 -0.26 0.34 4 0.05 0.29
0051 1488 392 1.65 2.69 6.58R 2.11 3 2.15 0.52
0054 1120 24 0.10 0.30 0.41 0.66 4 0.37 0.23
0056 696 -400 -1.68 NDS NDS NDS 1 -1.68
0057 1058.8 -37.2 -0.16 NDS NDS NDS 1 -0.16
0059 1109.0 13 0.05 -0.58 NDS NDS 2 -0.27 0.45
0060 1186 90 0.38 1.15 0.96 0.68 4 0.79 0.34
0061 1251 155 0.65 0.43 2.57 NDS 3 1.22 1.18
0063 871 -225 -0.95 -1.57 -1.61 NDS 3 -1.38 0.37
0064 1187 91 0.38 1.47 -0.09 NDS 3 0.59 0.8
0065 939 -157 -0.66 -0.82 -0.80 NDS 3 -0.76 0.09
0066 1008 -88 -0.37 -0.11 -0.29 NDS 3 -0.26 0.13
0068 978 -118 -0.50 NDS NDS NDS 1 -0.50
0070 968 -128 -0.54 -0.76 -0.14 0.26 4 -0.30 0.45
0071 1023 -73 -0.31 0.10 1.09 NDS 3 0.29 0.72
0072 865 -231 -0.97 -0.16 -0.66 NDS 3 -0.60 0.41
0073 1130 34 0.14 -1.09 -0.91 NDS 3 -0.62 0.66
0076 832.4 -263.6 -1.11 0.31 -0.41 NDS 3 -0.40 0.71
0077 1133 37 0.16 1.03 0.71 0.37 4 0.57 0.38
0078 1269 173 0.73 NDS 0.54 0.22 3 0.50 0.26
0079 898 -198 -0.83 -0.69 NDS NDS 2 -0.76 0.1
0080 1580 484 2.04 3 NDS 1.49 -0.11 3 1.14 1.12
0081 1105.536 9.536 0.04 0.24 0.46 0.23 4 0.24 0.17
0082 1190 94 0.40 0.64 0.89 0.99 4 0.73 0.26
0083 1164 68 0.29 NDS NDS 0.01 2 0.15 0.2
0084 929 -167 -0.70 -1.16 -0.84 NDS 3 -0.90 0.24
0085 1213 117 0.49 0.53 NDS -0.70 3 0.11 0.7
November 9, 2018 www.astm.org 90
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0086 1131 35 0.15 NDS NDS NDS 1 0.15
0087 1145.37 49.37 0.21 0.51 NDS NDS 2 0.36 0.21
0088 1456 360 1.52 -1.24 0.04 -1.81 4 -0.37 1.48
0089 1352 256 1.08 -0.31 0.44 NDS 3 0.40 0.7
0091 954 -142 -0.60 -0.67 -0.06 -0.10 4 -0.36 0.32
0092 1419.4 323.4 1.36 1.57 1.53 1.24 4 1.43 0.15
0094 1378 282 1.19 NDS 1.11 1.05 3 1.12 0.07
0095 1155.64 59.64 0.25 NDS 1.36 0.82 3 0.81 0.56
0096 808 -288 -1.21 -2.06 NDS NDS 2 -1.64 0.6
0098 970 -126 -0.53 -0.35 -0.74 -0.27 4 -0.47 0.21
0099 1262 166 0.70 NDS NDS NDS 1 0.70
0101 722.1 -373.9 -1.57 -3.01 0.34 NDS 3 -1.41 1.68
0102 1220 124 0.52 0.72 0.39 0.20 4 0.46 0.22
0104 1154 58 0.24 0.34 0.42 0.09 4 0.27 0.14
0105 801 -295 -1.24 NDS NDS NDS 1 -1.24
0106 1102 6 0.03 -0.31 0.24 0.17 4 0.03 0.24
0107 894 -202 -0.85 -0.05 1.84 0.73 4 0.42 1.15
0108 987.755 -108.245 -0.46 -0.34 0.02 -1.28 4 -0.52 0.55
0112 1468 372 1.57 -0.37 -2.99 0.86 4 -0.23 2.01
0115 1178 82 0.35 0.48 0.31 0.24 4 0.35 0.1
0117 756 -340 -1.43 -0.24 -0.16 0.14 4 -0.42 0.69
0119 1199 103 0.43 0.37 0.74 0.16 4 0.43 0.24
0121 1677 581 2.45 3 5.12R NDS NDS 1 2.45
0122 1029 -67 -0.28 -0.50 -0.01 -0.29 4 -0.27 0.2
0123 768 -328 -1.38 0.47 -1.01 0.67 4 -0.31 1.03
0124 1118 22 0.09 0.53 0.21 0.39 4 0.31 0.19
0125 955.22 -140.78 -0.59 NDS -0.33 0.21 3 -0.24 0.41
0126 1027 -69 -0.29 -0.54 -0.37 -0.43 4 -0.41 0.11
0127 447 -649 -2.73 3 NDS NDS NDS 1 -2.73
0128 1423 327 1.38 NDS 0.24 NDS 2 0.81 0.81
0129 1180 84 0.35 NDS NDS NDS 1 0.35

November 9, 2018 www.astm.org 91


Pooled StdDev of Z: 0.67
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 92


Distribution of Results

November 9, 2018 www.astm.org 93


Frequency Histogram

November 9, 2018 www.astm.org 94


Headspace Sampling, C, Carbon Monoxide, D3612-02(2017)
Data Report
Headspace Sampling, C, Carbon Monoxide by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 92 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 89
$ Z-Score not calculated
Average 37.8
StdDev 14.5
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 40.1
TPI
ADrs Statistic 2.11 Not Normal

November 9, 2018 www.astm.org 95


Results Table and Z-Scores
Headspace Sampling, C, Carbon Monoxide by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 23 -14.8 -1.02 -0.34 -0.11 0.10 4 -0.34 0.49
0002 23.23 -14.57 -1.01 NDS -0.21 NDS 2 -0.61 0.57
0004 17.2 -20.6 -1.42 -0.46 -0.81 1.74 4 -0.24 1.38
0005 28 -9.8 -0.68 -0.67 -0.61 NDS 3 -0.65 0.04
0007 62.9 25.1 1.73 1.84 0.61 0.50 4 1.17 0.71
0008 39 1.2 0.08 -0.42 -0.01 -0.81 4 -0.29 0.41
0009 26 -11.8 -0.81 -0.46 -0.51 -0.27 4 -0.51 0.22
0011 34 -3.8 -0.26 0.19 0.14 0.13 4 0.05 0.21
0012 72 34.2 2.36 3 4.68R 0.65 0.00 3 1.00 1.22
0013 45 7.2 0.50 1.17 2.30 -0.14 4 0.96 1.04
0014 29 -8.8 -0.61 0.80 0.85 NDS 3 0.35 0.83
0015 175 137.2 9.47 R -0.50 NDS -0.30 2 -0.40 0.14
0016 45 7.2 0.50 0.92 2.05 -0.30 4 0.79 0.98
0017 71.5 33.7 2.33 3 -0.95 0.48 -0.10 4 0.44 1.39
0022 28 -9.8 -0.68 0.19 0.45 0.78 4 0.19 0.63
0024 30.3 -7.5 -0.52 NDS -0.51 -0.61 3 -0.55 0.06
0025 40 2.2 0.15 NDS 0.35 1.94 3 0.81 0.98
0026 44.60403 6.80403 0.47 0.07 -0.20 NDS 3 0.11 0.34
0028 61 23.2 1.60 3.21 1.70 0.40 4 1.73 1.15
0029 29 -8.8 -0.61 -0.63 0.09 -0.67 4 -0.46 0.36
0031 24 -13.8 -0.95 NDS -1.46 NDS 2 -1.21 0.36
0032 29 -8.8 -0.61 -0.63 NDS NDS 2 -0.62 0.01
0034 38 0.2 0.01 -0.29 NDS NDS 2 -0.14 0.21
0035 9.46 -28.34 -1.96 -0.44 -1.79 1.02 4 -0.79 1.39
0036 73 35.2 2.43 3 NDS NDS NDS 1 2.43
0038 35.4 -2.4 -0.17 NDS 1.20 NDS 2 0.52 0.97
0039 27.8 -10 -0.69 0.03 -0.01 NDS 3 -0.22 0.4
0040 40 2.2 0.15 -0.26 1.05 1.84 4 0.70 0.94

November 9, 2018 www.astm.org 96


StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0041 40 2.2 0.15 1.53 -1.51 NDS 3 0.06 1.52
0042 32 -5.8 -0.40 0.51 -0.21 -0.84 4 -0.24 0.56
0043 33.4 -4.4 -0.30 -0.30 NDS NDS 2 -0.30 0
0045 35 -2.8 -0.19 NDS 0.30 0.67 3 0.26 0.43
0047 34 -3.8 -0.26 0.15 0.04 0.00 4 -0.02 0.17
0048 28 -9.8 -0.68 NDS -0.81 -1.14 3 -0.88 0.24
0049 47 9.2 0.64 0.03 0.04 -1.24 4 -0.13 0.79
0051 68 30.2 2.09 3 7.08R 1.45 1.94 3 1.83 0.33
0054 38 0.2 0.01 -0.15 -0.81 -1.74 4 -0.67 0.8
0056 39 1.2 0.08 NDS NDS NDS 1 0.08
0057 25 -12.8 -0.88 NDS NDS NDS 1 -0.88
0059 26.4 -11.4 -0.79 3.11 NDS NDS 2 1.16 2.76
0060 25 -12.8 -0.88 0.27 0.35 1.03 4 0.19 0.79
0061 42 4.2 0.29 4.19R 0.80 NDS 2 0.55 0.36
0063 47 9.2 0.64 0.60 -0.81 NDS 3 0.14 0.83
0064 47.5 9.7 0.67 -1.57 1.45 NDS 3 0.18 1.57
0065 68 30.2 2.09 3 1.21 0.04 NDS 3 1.11 1.03
0066 22 -15.8 -1.09 -0.99 -1.11 NDS 3 -1.06 0.06
0068 25 -12.8 -0.88 NDS NDS NDS 1 -0.88
0070 31 -6.8 -0.47 -0.83 -0.41 -0.81 4 -0.63 0.22
0071 103 65.2 4.50 R 7.45R 0.04 NDS 1 0.04
0072 48 10.2 0.70 0.31 -0.66 NDS 3 0.12 0.7
0073 41 3.2 0.22 0.31 -0.51 NDS 3 0.01 0.45
0076 43.9 6.1 0.42 -0.60 -0.71 NDS 3 -0.30 0.62
0077 34 -3.8 -0.26 -0.14 1.00 0.73 4 0.33 0.63
0078 45 7.2 0.50 NDS 0.50 1.20 3 0.73 0.4
0079 29 -8.8 -0.61 -1.20 NDS NDS 2 -0.91 0.42
0080 34 -3.8 -0.26 NDS -0.16 -0.77 3 -0.40 0.33
0081 37.287 -0.513 -0.03 -0.50 0.80 0.53 4 0.20 0.58
0082 29 -8.8 -0.61 0.07 0.90 1.27 4 0.41 0.84
0083 48 10.2 0.70 NDS NDS 7.33R 1 0.70
0084 35 -2.8 -0.19 -1.24 -1.16 NDS 3 -0.86 0.58
0085 30 -7.8 -0.54 0.03 NDS -0.61 3 -0.37 0.35
November 9, 2018 www.astm.org 97
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0086 36 -1.8 -0.12 NDS NDS NDS 1 -0.12
0087 55.93 18.13 1.25 -0.91 NDS NDS 2 0.17 1.53
0088 51 13.2 0.91 0.23 -0.26 -1.38 4 -0.13 0.96
0089 23 -14.8 -1.02 -1.67 -1.71 NDS 3 -1.47 0.39
0091 21 -16.8 -1.16 -1.44 -0.71 NDS 3 -1.10 0.37
0092 41.5 3.7 0.26 -0.43 1.20 3.00 4 1.01 1.49
0094 58 20.2 1.40 NDS 0.45 1.04 3 0.96 0.48
0095 33.9 -3.9 -0.27 NDS 0.14 -0.47 3 -0.20 0.31
0096 33 -4.8 -0.33 -0.02 NDS NDS 2 -0.18 0.22
0098 23 -14.8 -1.02 0.27 -0.36 0.47 4 -0.16 0.67
0099 27 -10.8 -0.75 NDS NDS NDS 1 -0.75
0101 60.5 22.7 1.57 0.19 0.95 NDS 3 0.90 0.69
0102 32 -5.8 -0.40 -0.38 -0.11 -0.94 4 -0.46 0.35
0104 38 0.2 0.01 0.84 -0.76 -1.18 4 -0.27 0.89
0105 46 8.2 0.57 NDS NDS NDS 1 0.57
0106 24 -13.8 -0.95 0.07 -0.06 0.57 4 -0.09 0.63
0107 70 32.2 2.22 3 -0.42 0.60 0.23 4 0.66 1.12
0108 19.958 -17.842 -1.23 -0.55 -1.01 0.64 4 -0.54 0.83
0112 22 -15.8 -1.09 0.56 -0.21 0.20 4 -0.14 0.71
0115 34 -3.8 -0.26 0.47 0.55 0.63 4 0.35 0.41
0117 34 -3.8 -0.26 -0.55 -0.81 19.79R 3 -0.54 0.28
0119 167 129.2 8.92 R 1.98 0.60 0.47 3 1.02 0.84
0121 81 43.2 2.98 3 4.96R NDS NDS 1 2.98
0122 34 -3.8 -0.26 -0.99 -0.81 -1.54 4 -0.90 0.53
0123 26 -11.8 -0.81 -0.46 -1.61 0.57 4 -0.58 0.9
0124 33 -4.8 -0.33 0.96 0.85 0.93 4 0.60 0.62
0125 42.95 5.15 0.36 NDS 0.60 -0.17 3 0.26 0.39
0126 27 -10.8 -0.75 -0.63 -0.36 -0.10 4 -0.46 0.29
0127 12 -25.8 -1.78 NDS NDS NDS 1 -1.78
0128 49 11.2 0.77 NDS 1.95 NDS 2 1.36 0.83
0129 41.7 3.9 0.27 NDS NDS NDS 1 0.27

November 9, 2018 www.astm.org 98


Pooled StdDev of Z: 0.83
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 99


Distribution of Results

November 9, 2018 www.astm.org 100


Frequency Histogram

November 9, 2018 www.astm.org 101


Headspace Sampling, C, Ethane, D3612-02(2017)
Data Report
Headspace Sampling, C, Ethane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 92 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 88
$ Z-Score not calculated
Average 20.3
StdDev 2.9
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 8.1
TPI
ADrs Statistic 0.84 Marginally Normal

November 9, 2018 www.astm.org 102


Results Table and Z-Scores
Headspace Sampling, C, Ethane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 18 -2.3 -0.77 -0.14 -0.19 -0.27 4 -0.34 0.29
0002 13.55 -6.75 -2.30 3 NDS -1.77 NDS 2 -2.04 0.37
0004 14.5 -5.8 -1.97 -0.14 -1.70 1.46 4 -0.59 1.59
0005 23 2.7 0.94 0.33 -1.17 NDS 3 0.03 1.09
0007 18.7 -1.6 -0.53 0.52 0.44 -0.66 4 -0.06 0.62
0008 19 -1.3 -0.43 -0.37 -0.57 0.45 4 -0.23 0.46
0009 20 -0.3 -0.09 -1.08 -0.26 -1.78 4 -0.80 0.78
0011 21 0.7 0.25 0.57 0.49 0.25 4 0.39 0.16
0012 22 1.7 0.60 0.80 1.77 1.44 4 1.15 0.55
0013 23 2.7 0.94 -0.37 0.19 -0.20 4 0.14 0.58
0014 24 3.7 1.28 1.28 1.32 NDS 3 1.29 0.02
0015 23 2.7 0.94 0.10 NDS 0.47 3 0.50 0.42
0016 18 -2.3 -0.77 -0.85 0.57 -0.48 4 -0.38 0.65
0017 19.7 -0.6 -0.19 0.92 0.81 0.07 4 0.40 0.55
0022 19 -1.3 -0.43 0.10 0.57 -0.04 4 0.05 0.41
0024 18.4 -1.9 -0.64 NDS -1.02 -0.41 3 -0.69 0.31
0025 19 -1.3 -0.43 NDS -1.09 2.44 3 0.31 1.88
0026 21.11083 0.81083 0.29 0.57 0.42 NDS 3 0.43 0.14
0028 18 -2.3 -0.77 1.51 0.41 0.56 4 0.43 0.94
0029 20 -0.3 -0.09 -0.61 -0.34 0.18 4 -0.22 0.34
0031 20 -0.3 -0.09 NDS -1.70 NDS 2 -0.90 1.14
0032 17 -3.3 -1.12 -0.37 NDS NDS 2 -0.75 0.53
0034 23 2.7 0.94 1.09 NDS NDS 2 1.02 0.11
0035 18.38 -1.92 -0.64 -0.96 -1.10 -0.21 4 -0.73 0.4
0036 17 -3.3 -1.12 NDS NDS NDS 1 -1.12
0038 23.1 2.8 0.97 NDS 1.70 NDS 2 1.34 0.52
0039 19.7 -0.6 -0.19 1.04 -0.19 NDS 3 0.22 0.71
0040 19 -1.3 -0.43 -2.02 0.26 -5.76R 3 -0.73 1.17

November 9, 2018 www.astm.org 103


StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0041 22.9 2.6 0.90 -0.37 -1.92 NDS 3 -0.46 1.41
0042 24 3.7 1.28 1.04 -0.19 0.27 4 0.60 0.68
0043 24.3 4 1.38 0.45 NDS NDS 2 0.92 0.66
0045 20 -0.3 -0.09 NDS 0.57 0.30 3 0.26 0.33
0047 22 1.7 0.60 0.10 -0.26 0.22 4 0.17 0.35
0048 17 -3.3 -1.12 NDS -0.11 0.17 3 -0.35 0.68
0049 21 0.7 0.25 0.10 0.94 0.40 4 0.42 0.37
0051 5 -15.3 -5.23 R -0.14 0.72 0.88 3 0.49 0.55
0054 19 -1.3 -0.43 -0.07 0.34 0.66 4 0.13 0.48
0056 21 0.7 0.25 1.04 NDS NDS 2 0.65 0.56
0057 17 -3.3 -1.12 NDS NDS NDS 1 -1.12
0059 20.9 0.6 0.22 -3.13 NDS NDS 2 -1.46 2.37
0060 16 -4.3 -1.46 -0.14 0.19 0.37 4 -0.26 0.83
0061 22 1.7 0.60 -0.37 2.30 NDS 3 0.84 1.35
0063 19 -1.3 -0.43 -0.61 -1.09 NDS 3 -0.71 0.34
0064 22.2 1.9 0.66 -2.02 0.41 NDS 3 -0.32 1.48
0065 19 -1.3 -0.43 -0.14 -0.64 NDS 3 -0.40 0.25
0066 16 -4.3 -1.46 -1.08 -1.47 NDS 3 -1.34 0.22
0068 21 0.7 0.25 NDS NDS NDS 1 0.25
0070 18 -2.3 -0.77 -0.85 -0.57 -0.21 4 -0.60 0.29
0071 18 -2.3 -0.77 -0.37 -0.26 NDS 3 -0.47 0.27
0072 17 -3.3 -1.12 0.10 -0.72 NDS 3 -0.58 0.62
0073 28 7.7 2.65 3 -0.37 0.04 NDS 3 0.77 1.64
0076 20.7 0.4 0.15 -0.04 -0.26 NDS 3 -0.05 0.21
0077 20 -0.3 -0.09 -0.14 0.57 0.56 4 0.23 0.39
0078 21 0.7 0.25 NDS 0.26 0.12 3 0.21 0.08
0079 15 -5.3 -1.80 -0.85 NDS NDS 2 -1.33 0.67
0080 29 8.7 3.00 3 NDS -1.62 -0.55 3 0.28 2.42
0081 19.691 -0.609 -0.19 0.33 0.79 0.16 4 0.27 0.41
0082 18 -2.3 -0.77 -0.61 1.02 0.77 4 0.10 0.92
0083 36 15.7 5.39 R NDS NDS 0.35 1 0.35
0084 20 -0.3 -0.09 -0.61 -0.72 NDS 3 -0.47 0.34
0085 13 -7.3 -2.49 3 -1.79 NDS -1.55 3 -1.94 0.49
November 9, 2018 www.astm.org 104
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0086 20 -0.3 -0.09 NDS NDS NDS 1 -0.09
0087 20.89 0.59 0.22 0.57 NDS NDS 2 0.40 0.25
0088 24 3.7 1.28 1.51 -0.11 -1.81 4 0.22 1.53
0089 18 -2.3 -0.77 -2.21 -0.42 NDS 3 -1.13 0.95
0091 20 -0.3 -0.09 0.10 -0.49 -0.71 4 -0.30 0.37
0092 22.9 2.6 0.90 1.18 2.64 1.35 4 1.52 0.77
0094 24 3.7 1.28 NDS 2.15 1.35 3 1.59 0.48
0095 19.85 -0.45 -0.14 NDS 1.62 1.00 3 0.83 0.89
0096 20 -0.3 -0.09 -0.61 NDS NDS 2 -0.35 0.37
0098 17 -3.3 -1.12 0.10 -0.79 -0.39 4 -0.55 0.53
0099 20 -0.3 -0.09 NDS NDS NDS 1 -0.09
0101 128.9 108.6 37.23 R 0.80 1.70 NDS 2 1.25 0.64
0102 21 0.7 0.25 0.57 0.26 0.33 4 0.35 0.15
0104 19 -1.3 -0.43 0.10 -0.19 0.00 4 -0.13 0.23
0105 20 -0.3 -0.09 NDS NDS NDS 1 -0.09
0106 20 -0.3 -0.09 0.10 0.41 0.05 4 0.12 0.21
0107 24 3.7 1.28 0.80 1.02 0.51 4 0.90 0.33
0108 26.500 6.2 2.14 3 -1.08 0.04 -0.96 4 0.04 1.49
0112 21 0.7 0.25 -0.14 -0.11 -0.54 4 -0.14 0.32
0115 23 2.7 0.94 0.80 0.49 -0.01 4 0.56 0.42
0117 19 -1.3 -0.43 0.57 -0.42 -1.38 4 -0.42 0.8
0119 20 -0.3 -0.09 0.33 0.41 0.24 4 0.22 0.22
0121 26 5.7 1.97 5.99R NDS NDS 1 1.97
0122 18 -2.3 -0.77 -0.85 -1.25 -0.92 4 -0.95 0.21
0123 24 3.7 1.28 1.98 -0.79 1.41 4 0.97 1.21
0124 19 -1.3 -0.43 0.10 0.26 0.35 4 0.07 0.35
0125 18.09 -2.21 -0.74 NDS 0.26 0.47 3 0.00 0.65
0126 20 -0.3 -0.09 -0.37 -0.42 -0.29 4 -0.29 0.15
0127 8 -12.3 -4.20 R NDS NDS NDS 0
0128 25 4.7 1.62 NDS 0.49 NDS 2 1.06 0.8
0129 20.8 0.5 0.19 NDS NDS NDS 1 0.19

November 9, 2018 www.astm.org 105


Pooled StdDev of Z: 0.86
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 106


Distribution of Results

November 9, 2018 www.astm.org 107


Frequency Histogram

November 9, 2018 www.astm.org 108


Headspace Sampling, C, Ethylene, D3612-02(2017)
Data Report
Headspace Sampling, C, Ethylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 92 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 89
$ Z-Score not calculated
Average 19.6
StdDev 2.9
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 8.1
TPI
ADrs Statistic 0.37 Normal

November 9, 2018 www.astm.org 109


Results Table and Z-Scores
Headspace Sampling, C, Ethylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 17 -2.6 -0.90 -0.10 -0.17 -0.20 4 -0.34 0.37
0002 13.00 -6.6 -2.28 3 NDS -1.74 NDS 2 -2.01 0.38
0004 14.0 -5.6 -1.93 -0.31 -1.74 1.34 4 -0.66 1.52
0005 23 3.4 1.16 -0.10 -1.00 NDS 3 0.02 1.08
0007 18.5 -1.1 -0.39 0.06 0.15 -0.57 4 -0.19 0.35
0008 16 -3.6 -1.24 0.34 -1.16 0.17 4 -0.47 0.84
0009 22 2.4 0.82 -0.10 0.07 -1.77 4 -0.25 1.09
0011 20 0.4 0.13 0.55 0.73 0.21 4 0.41 0.28
0012 21 1.4 0.47 0.55 1.22 1.26 4 0.88 0.42
0013 18 -1.6 -0.56 -1.18 1.63 -0.03 4 -0.04 1.21
0014 22 2.4 0.82 1.42 0.81 NDS 3 1.02 0.35
0015 22 2.4 0.82 0.34 NDS 0.57 3 0.58 0.24
0016 17 -2.6 -0.90 -0.53 2.29 -0.59 4 0.07 1.49
0017 19.8 0.2 0.06 0.18 0.45 0.18 4 0.22 0.17
0022 18 -1.6 -0.56 -0.10 0.32 -0.14 4 -0.12 0.36
0024 17.5 -2.1 -0.73 NDS -1.00 -0.42 3 -0.72 0.29
0025 20 0.4 0.13 NDS -0.67 3.06 3 0.84 1.96
0026 23.61748 4.01748 1.37 0.77 0.32 NDS 3 0.82 0.53
0028 16 -3.6 -1.24 0.34 0.32 -0.20 4 -0.20 0.74
0029 19 -0.6 -0.21 -0.96 -0.50 0.02 4 -0.41 0.42
0031 21 1.4 0.47 NDS -1.65 NDS 2 -0.59 1.5
0032 17 -2.6 -0.90 0.12 NDS NDS 2 -0.39 0.72
0034 21 1.4 0.47 0.69 NDS NDS 2 0.58 0.16
0035 17.66 -1.94 -0.67 -1.13 0.23 -0.15 4 -0.43 0.59
0036 15 -4.6 -1.59 NDS NDS NDS 1 -1.59
0038 22.7 3.1 1.06 NDS 1.23 NDS 2 1.15 0.12
0039 20 0.4 0.13 1.20 -0.34 NDS 3 0.33 0.79
0040 17 -2.6 -0.90 -0.31 -0.17 0.83 4 -0.14 0.72

November 9, 2018 www.astm.org 110


StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0041 21.9 2.3 0.78 0.12 -2.06 NDS 3 -0.39 1.49
0042 23 3.4 1.16 0.55 -0.83 -0.01 4 0.22 0.85
0043 23.2 3.6 1.23 0.29 NDS NDS 2 0.76 0.66
0045 20 0.4 0.13 NDS 0.15 0.43 3 0.24 0.17
0047 27 7.4 2.54 3 0.55 0.40 0.24 4 0.93 1.08
0048 16 -3.6 -1.24 NDS 0.07 0.41 3 -0.25 0.87
0049 21 1.4 0.47 0.55 0.73 0.71 4 0.62 0.13
0051 13 -6.6 -2.28 3 0.55 1.14 1.41 4 0.21 1.7
0054 19 -0.6 -0.21 -0.25 -0.17 0.20 4 -0.11 0.21
0056 21 1.4 0.47 1.20 NDS NDS 2 0.84 0.52
0057 24.6 5 1.71 NDS NDS NDS 1 1.71
0059 20.4 0.8 0.27 -2.13 NDS NDS 2 -0.93 1.7
0060 18 -1.6 -0.56 0.55 0.57 0.57 4 0.28 0.56
0061 21 1.4 0.47 -0.53 1.72 NDS 3 0.55 1.13
0063 20 0.4 0.13 -0.31 -1.32 NDS 3 -0.50 0.74
0064 21.6 2 0.68 -3.34 2.95 NDS 3 0.10 3.19
0065 21 1.4 0.47 0.34 -0.01 NDS 3 0.27 0.25
0066 20 0.4 0.13 0.12 -1.00 NDS 3 -0.25 0.65
0068 22 2.4 0.82 NDS NDS NDS 1 0.82
0070 17 -2.6 -0.90 -0.75 -0.67 -0.20 4 -0.63 0.3
0071 18 -1.6 -0.56 -0.31 -0.42 NDS 3 -0.43 0.13
0072 18 -1.6 -0.56 -0.31 -0.83 NDS 3 -0.57 0.26
0073 26 6.4 2.19 3 -0.96 -0.26 NDS 3 0.32 1.65
0076 18.7 -0.9 -0.32 -0.31 -0.42 NDS 3 -0.35 0.06
0077 19 -0.6 -0.21 0.12 0.73 0.45 4 0.27 0.41
0078 22 2.4 0.82 NDS 0.24 0.39 3 0.48 0.3
0079 14 -5.6 -1.93 -1.61 NDS NDS 2 -1.77 0.23
0080 28 8.4 2.88 3 NDS -1.16 -0.46 3 0.42 2.16
0081 19.410 -0.19 -0.07 0.34 0.40 0.01 4 0.17 0.23
0082 20 0.4 0.13 0.77 0.89 0.58 4 0.59 0.33
0083 35 15.4 5.28 R NDS NDS 0.34 1 0.34
0084 19 -0.6 -0.21 -0.96 -1.16 NDS 3 -0.78 0.5
0085 22 2.4 0.82 -2.69 NDS -2.59 3 -1.49 2
November 9, 2018 www.astm.org 111
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0086 22 2.4 0.82 NDS NDS NDS 1 0.82
0087 19.96 0.36 0.12 0.12 NDS NDS 2 0.12 0
0088 44 24.4 8.38 R 1.20 0.65 -1.76 3 0.03 1.57
0089 18 -1.6 -0.56 -2.02 -0.67 NDS 3 -1.08 0.81
0091 19 -0.6 -0.21 -0.10 -0.67 -0.64 4 -0.41 0.29
0092 22.9 3.3 1.13 1.20 2.09 1.33 4 1.44 0.44
0094 24 4.4 1.50 NDS 1.47 1.10 3 1.36 0.22
0095 17.85 -1.75 -0.61 NDS 2.13 1.54 3 1.02 1.44
0096 18 -1.6 -0.56 4.66R NDS NDS 1 -0.56
0098 17 -2.6 -0.90 0.12 -0.83 -0.07 4 -0.42 0.52
0099 19 -0.6 -0.21 NDS NDS NDS 1 -0.21
0101 21.1 1.5 0.51 0.77 1.39 NDS 3 0.89 0.45
0102 20 0.4 0.13 0.12 -0.09 0.05 4 0.05 0.1
0104 19 -0.6 -0.21 0.12 -0.34 -0.23 4 -0.17 0.2
0105 19 -0.6 -0.21 NDS NDS NDS 1 -0.21
0106 19 -0.6 -0.21 0.12 0.07 0.13 4 0.03 0.16
0107 24 4.4 1.50 0.77 0.65 0.32 4 0.81 0.5
0108 16.3111 -3.2889 -1.14 -0.96 -0.91 -1.05 4 -1.02 0.1
0112 19 -0.6 -0.21 -0.53 -0.67 -0.49 4 -0.48 0.19
0115 21 1.4 0.47 0.34 0.48 0.13 4 0.36 0.16
0117 18 -1.6 -0.56 0.12 -0.50 -1.34 4 -0.57 0.6
0119 19 -0.6 -0.21 0.34 0.48 0.00 4 0.15 0.31
0121 21 1.4 0.47 3.15 NDS NDS 2 1.81 1.9
0122 16 -3.6 -1.24 -0.96 -1.65 -1.08 4 -1.23 0.3
0123 23 3.4 1.16 1.63 -1.00 1.39 4 0.80 1.21
0124 19 -0.6 -0.21 0.34 0.15 0.43 4 0.18 0.28
0125 13.89 -5.71 -1.97 NDS -0.01 -5.62R 2 -0.99 1.39
0126 20 0.4 0.13 -0.31 -0.59 -0.35 4 -0.28 0.3
0127 7 -12.6 -4.34 R NDS NDS NDS 0
0128 16 -3.6 -1.24 NDS 1.39 NDS 2 0.08 1.86
0129 20.8 1.2 0.40 NDS NDS NDS 1 0.40

November 9, 2018 www.astm.org 112


Pooled StdDev of Z: 0.92
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 113


Distribution of Results

November 9, 2018 www.astm.org 114


Frequency Histogram

November 9, 2018 www.astm.org 115


Headspace Sampling, C, Hydrogen, D3612-02(2017)
Data Report
Headspace Sampling, C, Hydrogen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 91 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 89
$ Z-Score not calculated
Average 25.2
StdDev 6.6
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 18.3
TPI
ADrs Statistic 0.72 Normal

November 9, 2018 www.astm.org 116


Results Table and Z-Scores
Headspace Sampling, C, Hydrogen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 22 -3.2 -0.48 -0.70 -0.36 -0.13 4 -0.42 0.24
0002 17.43 -7.77 -1.17 NDS -0.82 NDS 2 -1.00 0.25
0004 19.9 -5.3 -0.80 -0.40 -0.97 1.18 4 -0.25 0.98
0005 48 22.8 3.45 1,3 -0.40 1.10 NDS 3 1.38 1.94
0007 30.6 5.4 0.82 -0.01 0.73 0.39 4 0.48 0.38
0008 27 1.8 0.28 1.95 -0.13 -0.71 4 0.35 1.14
0009 22 -3.2 -0.48 -0.55 -0.36 -1.37 4 -0.69 0.46
0011 29 3.8 0.58 0.77 0.10 0.18 4 0.41 0.32
0012 31 5.8 0.88 -0.11 1.33 -0.39 4 0.43 0.81
0013 24 -1.2 -0.18 -0.26 1.87 -1.68 4 -0.06 1.46
0014 28 2.8 0.43 0.77 0.33 NDS 3 0.51 0.23
0015 32 6.8 1.03 1.36 NDS 0.03 3 0.81 0.69
0016 22 -3.2 -0.48 -0.11 1.71 -1.19 4 -0.02 1.24
0017 27.3 2.1 0.32 -3.34 -0.38 -0.60 4 -1.00 1.61
0022 25 -0.2 -0.03 -0.11 0.41 0.12 4 0.10 0.23
0024 26.4 1.2 0.19 NDS -0.44 -0.34 3 -0.20 0.34
0025 38 12.8 1.94 NDS 0.26 0.60 3 0.93 0.89
0026 27.39197 2.19197 0.34 0.48 -0.30 NDS 3 0.17 0.42
0028 23 -2.2 -0.33 -0.11 1.71 -0.98 4 0.07 1.15
0029 25 -0.2 -0.03 -0.40 -0.36 -0.36 4 -0.29 0.17
0031 24 -1.2 -0.18 NDS -1.05 NDS 2 -0.62 0.62
0032 27 1.8 0.28 0.18 NDS NDS 2 0.23 0.07
0034 34 8.8 1.34 -0.18 NDS NDS 2 0.58 1.07
0035 25.19 -0.01 0.00 -0.32 -0.67 -0.08 4 -0.27 0.3
0036 32 6.8 1.03 NDS NDS NDS 1 1.03
0038 31.1 5.9 0.90 NDS 0.85 NDS 2 0.88 0.04
0039 25.8 0.6 0.10 0.48 -0.05 NDS 3 0.18 0.27
0040 27 1.8 0.28 0.04 0.49 1.73 4 0.64 0.75

November 9, 2018 www.astm.org 117


StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0041 28 2.8 0.43 0.48 -1.89 NDS 3 -0.33 1.35
0042 18 -7.2 -1.08 -0.55 -0.97 -0.26 4 -0.72 0.38
0043 35.9 10.7 1.62 -0.02 NDS NDS 2 0.80 1.16
0045 27 1.8 0.28 NDS 0.10 0.29 3 0.22 0.11
0047 26 0.8 0.13 -0.26 0.10 -0.41 4 -0.11 0.27
0048 13 -12.2 -1.84 NDS -0.36 -0.61 3 -0.94 0.79
0049 27 1.8 0.28 -0.11 0.33 0.11 4 0.15 0.2
0051 20 -5.2 -0.78 -2.90 1.41 3.63 4 0.34 2.81
0054 27 1.8 0.28 1.06 -0.28 0.11 4 0.29 0.56
0056 30 4.8 0.73 3.27 NDS NDS 2 2.00 1.8
0057 24.7 -0.5 -0.07 NDS NDS NDS 1 -0.07
0059 24.7 -0.5 -0.07 4.69R NDS NDS 1 -0.07
0060 15 -10.2 -1.54 0.48 0.49 0.63 4 0.02 1.04
0061 24 -1.2 -0.18 -1.14 1.25 NDS 3 -0.02 1.2
0063 30 4.8 0.73 0.48 -1.13 NDS 3 0.03 1.01
0064 18.5 -6.7 -1.01 -1.73 0.79 NDS 3 -0.65 1.3
0065 27 1.8 0.28 1.21 -0.05 NDS 3 0.48 0.65
0066 22 -3.2 -0.48 -0.84 -1.43 NDS 3 -0.92 0.48
0068 20 -5.2 -0.78 NDS NDS NDS 1 -0.78
0070 21 -4.2 -0.63 -0.70 -0.51 -1.00 4 -0.71 0.21
0071 16 -9.2 -1.39 0.18 -0.05 NDS 3 -0.42 0.85
0072 20 -5.2 -0.78 -0.70 -1.28 NDS 3 -0.92 0.31
0073 30 4.8 0.73 -0.26 -0.44 NDS 3 0.01 0.63
0076 18.0 -7.2 -1.08 0.45 -0.90 NDS 3 -0.51 0.84
0077 29 3.8 0.58 1.21 0.33 0.71 4 0.71 0.37
0078 31 5.8 0.88 NDS -0.05 0.86 3 0.56 0.53
0079 13 -12.2 -1.84 0.04 NDS NDS 2 -0.90 1.33
0080 31 5.8 0.88 NDS -0.67 -0.52 3 -0.10 0.85
0081 24.380 -0.82 -0.12 0.18 0.18 0.53 4 0.19 0.27
0082 31 5.8 0.88 -0.26 0.03 0.20 4 0.21 0.48
0083 63 37.8 5.72 R NDS NDS 0.81 1 0.81
0084 24 -1.2 -0.18 -0.84 -1.13 NDS 3 -0.72 0.49
0085 24 -1.2 -0.18 0.92 NDS 0.31 3 0.35 0.55
November 9, 2018 www.astm.org 118
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0086 29 3.8 0.58 NDS NDS NDS 1 0.58
0087 23.27 -1.93 -0.29 -0.99 NDS NDS 2 -0.64 0.49
0088 13 -12.2 -1.84 0.33 -0.36 -0.34 4 -0.55 0.92
0089 28 2.8 0.43 -1.82 -1.97 NDS 3 -1.12 1.34
0092 32 6.8 1.03 0.34 1.18 1.32 4 0.97 0.43
0094 29 3.8 0.58 NDS 0.72 0.99 3 0.76 0.21
0095 12.5 -12.7 -1.92 NDS -0.13 -0.71 3 -0.92 0.91
0096 13 -12.2 -1.84 -1.73 NDS NDS 2 -1.79 0.08
0098 23 -2.2 -0.33 0.33 -0.67 0.35 4 -0.08 0.5
0099 27.3 2.1 0.32 NDS NDS NDS 1 0.32
0101 30.6 5.4 0.82 0.33 0.64 NDS 3 0.60 0.25
0102 25 -0.2 -0.03 -0.40 -0.36 -0.37 4 -0.29 0.17
0104 24 -1.2 -0.18 -0.40 -0.59 -0.26 4 -0.36 0.18
0105 26 0.8 0.13 NDS NDS NDS 1 0.13
0106 24 -1.2 -0.18 -0.11 0.26 0.03 4 0.00 0.19
0107 38 12.8 1.94 0.33 0.49 0.38 4 0.79 0.77
0108 16.341 -8.859 -1.34 -0.26 -0.59 2.98 4 0.20 1.91
0112 23 -2.2 -0.33 -0.55 0.03 -0.56 4 -0.35 0.28
0115 37 11.8 1.79 -0.11 0.49 0.60 4 0.69 0.8
0117 14 -11.2 -1.69 -0.11 -0.74 -1.43 4 -0.99 0.71
0119 29 3.8 0.58 0.77 0.18 0.51 4 0.51 0.25
0121 121 95.8 14.50 R 7.23R NDS NDS 0
0122 24 -1.2 -0.18 -0.55 -1.05 -1.33 4 -0.78 0.51
0123 23 -2.2 -0.33 1.21 -0.97 1.03 4 0.24 1.06
0124 33 7.8 1.18 1.06 0.10 0.18 4 0.63 0.57
0125 21.08 -4.12 -0.62 NDS 0.33 -0.45 3 -0.25 0.51
0126 26 0.8 0.13 -0.55 0.03 0.07 4 -0.08 0.32
0127 5 -20.2 -3.05 1,3 NDS NDS NDS 1 -3.05
0128 20 -5.2 -0.78 NDS 1.71 NDS 2 0.47 1.76
0129 29.7 4.5 0.69 NDS NDS NDS 1 0.69

Pooled StdDev of Z: 0.86


November 9, 2018 www.astm.org 119
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 120


Distribution of Results

November 9, 2018 www.astm.org 121


Frequency Histogram

November 9, 2018 www.astm.org 122


Headspace Sampling, C, Methane, D3612-02(2017)
Data Report
Headspace Sampling, C, Methane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 92 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 92
$ Z-Score not calculated
Average 119.6
StdDev 23.1
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 64.1
TPI
ADrs Statistic 0.80 Marginally Normal

November 9, 2018 www.astm.org 123


Results Table and Z-Scores
Headspace Sampling, C, Methane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 102 -17.6 -0.76 0.25 0.16 0.26 4 -0.02 0.49
0002 84.96 -34.64 -1.50 NDS -0.76 NDS 2 -1.13 0.52
0004 93.2 -26.4 -1.14 0.01 -1.01 1.30 4 -0.21 1.13
0005 116 -3.6 -0.15 -0.97 -0.71 NDS 3 -0.61 0.42
0007 126.3 6.7 0.29 0.21 0.32 -0.25 4 0.14 0.27
0008 127 7.4 0.32 1.25 0.41 0.69 4 0.67 0.42
0009 118 -1.6 -0.07 -0.62 -0.18 -1.65 4 -0.63 0.72
0011 130 10.4 0.45 0.74 0.55 0.40 4 0.54 0.15
0012 146 26.4 1.14 1.02 1.14 1.20 4 1.13 0.08
0013 122 2.4 0.10 -0.50 1.82 -0.28 4 0.29 1.05
0014 119 -0.6 -0.03 1.18 0.41 NDS 3 0.52 0.61
0015 151 31.4 1.36 0.90 NDS 0.79 3 1.02 0.3
0016 117 -2.6 -0.11 -0.29 1.77 -0.31 4 0.27 1.01
0017 132.9 13.3 0.58 -4.78R 0.93 0.75 3 0.75 0.18
0022 115 -4.6 -0.20 0.60 0.70 0.23 4 0.33 0.41
0024 105.3 -14.3 -0.62 NDS -0.62 -0.48 3 -0.57 0.08
0025 107 -12.6 -0.54 NDS -0.67 1.28 3 0.02 1.09
0026 136.95882 17.35882 0.75 0.06 -0.04 NDS 3 0.26 0.43
0028 106 -13.6 -0.59 -0.52 0.41 -0.36 4 -0.27 0.46
0029 125 5.4 0.23 -0.52 -0.03 0.33 4 0.00 0.38
0031 98 -21.6 -0.93 NDS -1.69 NDS 2 -1.31 0.54
0032 100 -19.6 -0.85 0.27 NDS NDS 2 -0.29 0.79
0034 147 27.4 1.18 1.67 NDS NDS 2 1.43 0.35
0035 110.24 -9.36 -0.40 -1.08 -0.36 -0.54 4 -0.60 0.33
0036 99 -20.6 -0.89 NDS NDS NDS 1 -0.89
0038 151.5 31.9 1.38 NDS 0.95 NDS 2 1.17 0.3
0039 129 9.4 0.41 1.67 0.16 NDS 3 0.75 0.81
0040 125 5.4 0.23 0.27 0.99 1.48 4 0.74 0.6

November 9, 2018 www.astm.org 124


StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0041 144.6 25 1.08 1.88 -1.74 NDS 3 0.41 1.9
0042 109 -10.6 -0.46 -0.50 -0.91 -0.18 4 -0.51 0.3
0043 140 20.4 0.88 0.11 NDS NDS 2 0.50 0.54
0045 129 9.4 0.41 NDS 0.50 0.64 3 0.52 0.12
0047 140 20.4 0.88 0.13 0.36 0.52 4 0.47 0.32
0048 88 -31.6 -1.36 NDS -1.88 -0.41 3 -1.22 0.75
0049 128 8.4 0.36 2.19 0.70 -1.09 4 0.54 1.35
0051 112 -7.6 -0.33 0.64 0.21 1.74 4 0.57 0.88
0054 124 4.4 0.19 0.18 -0.67 1.96 4 0.42 1.11
0056 141 21.4 0.93 0.50 NDS NDS 2 0.72 0.3
0057 96.3 -23.3 -1.01 NDS NDS NDS 1 -1.01
0059 106.7 -12.9 -0.56 0.59 NDS NDS 2 0.02 0.81
0060 109 -10.6 -0.46 1.11 0.60 1.07 4 0.58 0.73
0061 126 6.4 0.28 -0.90 10.00R NDS 2 -0.31 0.83
0063 132 12.4 0.54 -0.45 -1.10 NDS 3 -0.34 0.83
0064 117.5 -2.1 -0.09 -2.46 1.19 NDS 3 -0.45 1.85
0065 123 3.4 0.15 0.34 0.02 NDS 3 0.17 0.16
0066 99 -20.6 -0.89 -0.95 -1.20 NDS 3 -1.01 0.16
0068 119 -0.6 -0.03 NDS NDS NDS 1 -0.03
0070 106 -13.6 -0.59 -0.73 -0.28 -0.19 4 -0.45 0.25
0071 104 -15.6 -0.67 -0.38 -0.52 NDS 3 -0.52 0.15
0072 95 -24.6 -1.06 -0.27 -0.76 NDS 3 -0.70 0.4
0073 108 -11.6 -0.50 -0.59 -0.28 NDS 3 -0.46 0.16
0076 98.4 -21.2 -0.92 -1.01 -0.62 NDS 3 -0.85 0.2
0077 123 3.4 0.15 0.29 0.84 0.71 4 0.50 0.33
0078 146 26.4 1.14 NDS 0.70 0.98 3 0.94 0.22
0079 87 -32.6 -1.41 -1.11 NDS NDS 2 -1.26 0.21
0080 191 71.4 3.09 1,3 NDS 0.06 -0.06 3 1.03 1.79
0081 123.348 3.748 0.16 0.53 0.60 0.22 4 0.38 0.22
0082 111 -8.6 -0.37 -0.88 0.65 0.17 4 -0.11 0.66
0083 144 24.4 1.05 NDS NDS 0.66 2 0.86 0.28
0084 99 -20.6 -0.89 -1.48 -1.45 NDS 3 -1.27 0.33
0085 149 29.4 1.27 1.13 NDS 0.34 3 0.91 0.5
November 9, 2018 www.astm.org 125
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0086 127 7.4 0.32 NDS NDS NDS 1 0.32
0087 106.76 -12.84 -0.55 -0.73 NDS NDS 2 -0.64 0.13
0088 166 46.4 2.01 3 0.46 -0.18 -3.29 4 -0.25 2.23
0089 120 0.4 0.02 -2.63 -1.20 NDS 3 -1.27 1.33
0091 104 -15.6 -0.67 -0.81 0.06 NDS 3 -0.47 0.47
0092 152.7 33.1 1.43 1.31 1.87 NDS 3 1.54 0.29
0094 144 24.4 1.05 NDS 0.94 0.91 3 0.97 0.07
0095 102.91 -16.69 -0.72 NDS 0.60 0.27 3 0.05 0.69
0096 98 -21.6 -0.93 -1.16 NDS NDS 2 -1.05 0.16
0098 107 -12.6 -0.54 0.22 -0.57 0.06 4 -0.21 0.41
0099 133 13.4 0.58 NDS NDS NDS 1 0.58
0101 128.9 9.3 0.40 0.15 1.28 NDS 3 0.61 0.59
0102 130 10.4 0.45 0.01 0.11 -0.22 4 0.09 0.28
0104 111 -8.6 -0.37 -0.31 -0.47 -0.09 4 -0.31 0.16
0105 120 0.4 0.02 NDS NDS NDS 1 0.02
0106 121 1.4 0.06 0.64 0.36 0.49 4 0.39 0.25
0107 169 49.4 2.14 3 0.62 0.89 0.37 4 1.01 0.79
0108 77.846 -41.754 -1.80 -1.39 -0.86 -0.73 4 -1.20 0.49
0112 122 2.4 0.10 0.13 -0.08 -0.38 4 -0.06 0.23
0115 145 25.4 1.10 0.27 0.50 0.33 4 0.55 0.38
0117 41 -78.6 -3.40 1,3 -1.02 -0.81 -1.25 4 -1.62 1.2
0119 121 1.4 0.06 0.53 0.80 0.16 4 0.39 0.34
0121 155 35.4 1.53 6.60R NDS NDS 1 1.53
0122 106 -13.6 -0.59 -0.95 -1.01 -0.96 4 -0.88 0.19
0123 122 2.4 0.10 0.88 -1.20 1.20 4 0.25 1.07
0124 128 8.4 0.36 0.67 0.45 0.69 4 0.54 0.16
0125 114.56 -5.04 -0.22 NDS 0.75 0.32 3 0.28 0.49
0126 129 9.4 0.41 -0.34 -0.23 -0.15 4 -0.08 0.33
0127 38 -81.6 -3.53 1,3 NDS NDS NDS 1 -3.53
0128 120 0.4 0.02 NDS 0.84 NDS 2 0.43 0.58
0129 132 12.4 0.54 NDS NDS NDS 1 0.54

November 9, 2018 www.astm.org 126


Pooled StdDev of Z: 0.74
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 127


Distribution of Results

November 9, 2018 www.astm.org 128


Frequency Histogram

November 9, 2018 www.astm.org 129


Headspace Sampling, C, Nitrogen, D3612-02(2017)
Data Report
Headspace Sampling, C, Nitrogen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 91 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 91
$ Z-Score not calculated
Average 57128.3
StdDev 12259.4
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 33958.4
TPI
ADrs Statistic 0.27 Normal

November 9, 2018 www.astm.org 130


Results Table and Z-Scores
Headspace Sampling, C, Nitrogen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 44749 -12,379.3 -1.01 -0.38 -0.30 0.08 4 -0.40 0.45
0002 47356 -9,772.3 -0.80 NDS 0.16 NDS 2 -0.32 0.68
0004 42874.1 -14,254.2 -1.16 -0.07 0.43 1.13 4 0.08 0.96
0005 61989 4,860.7 0.40 1.07 0.05 NDS 3 0.51 0.52
0007 51410 -5,718.3 -0.47 0.51 0.32 1.33 4 0.42 0.74
0008 70714 13,585.7 1.11 -0.90 0.83 0.93 4 0.49 0.94
0009 53319 -3,809.3 -0.31 0.38 -0.91 -1.75 4 -0.65 0.9
0011 65467 8,338.7 0.68 -0.62 0.12 0.23 4 0.10 0.54
0012 68973 11,844.7 0.97 1.85 3.21 1.53 4 1.89 0.95
0013 52524 -4,604.3 -0.38 -0.14 0.24 -1.03 4 -0.33 0.53
0014 61992 4,863.7 0.40 -0.75 0.10 NDS 3 -0.08 0.6
0015 78709 21,580.7 1.76 -0.53 NDS 1.32 3 0.85 1.22
0016 45655 -11,473.3 -0.94 -0.04 0.27 -0.65 4 -0.34 0.55
0017 57853 724.7 0.06 2.52 0.81 -0.36 4 0.76 1.27
0022 54374 -2,754.3 -0.22 -0.94 0.41 0.03 4 -0.18 0.57
0024 39431 -17,697.3 -1.44 NDS -2.12 -1.60 3 -1.72 0.36
0025 58398 1,269.7 0.10 NDS 1.01 -1.16 3 -0.02 1.09
0026 58307.9 1,179.6 0.10 -2.13 -0.19 NDS 3 -0.74 1.21
0028 45412 -11,716.3 -0.96 -0.16 0.05 -0.35 4 -0.36 0.44
0029 58820 1,691.7 0.14 0.13 -0.40 -0.42 4 -0.14 0.31
0031 42308 -14,820.3 -1.21 NDS -1.83 NDS 2 -1.52 0.44
0032 51004 -6,124.3 -0.50 -0.47 NDS NDS 2 -0.49 0.02
0034 71650 14,521.7 1.18 1.72 NDS NDS 2 1.45 0.38
0035 43971.31 -13,156.99 -1.07 0.09 -0.90 -1.03 4 -0.73 0.55
0036 59400 2,271.7 0.19 NDS NDS NDS 1 0.19
0038 72473.2 15,344.9 1.25 NDS 5.01R NDS 1 1.25
0039 62531 5,402.7 0.44 -0.88 0.20 NDS 3 -0.08 0.7
0040 66022 8,893.7 0.73 0.38 1.81 1.30 4 1.06 0.63

November 9, 2018 www.astm.org 131


StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0041 74181 17,052.7 1.39 1.92 -1.89 NDS 3 0.47 2.06
0042 55994 -1,134.3 -0.09 -0.03 -0.12 -0.53 4 -0.19 0.23
0043 71830 14,701.7 1.20 1.31 NDS NDS 2 1.26 0.08
0045 62956 5,827.7 0.48 NDS 0.06 0.42 3 0.32 0.23
0047 77363 20,234.7 1.65 0.78 0.66 0.50 4 0.90 0.51
0048 48424 -8,704.3 -0.71 NDS -1.21 -1.24 3 -1.05 0.3
0049 68260 11,131.7 0.91 0.53 0.65 0.66 4 0.69 0.16
0051 37105 -20,023.3 -1.63 0.06 -1.06 -1.46 4 -1.02 0.76
0054 67100 9,971.7 0.81 -1.16 -0.67 -0.84 4 -0.47 0.87
0056 64300 7,171.7 0.58 NDS NDS NDS 1 0.58
0057 42000 -15,128.3 -1.23 NDS NDS NDS 1 -1.23
0059 51509 -5,619.3 -0.46 2.22 NDS NDS 2 0.88 1.9
0060 87120 29,991.7 2.45 3 0.42 1.03 0.68 4 1.15 0.91
0061 57297 168.7 0.01 0.58 1.77 NDS 3 0.79 0.9
0063 67465 10,336.7 0.84 0.58 2.41 NDS 3 1.28 0.99
0064 50657 -6,471.3 -0.53 -1.82 -0.29 NDS 3 -0.88 0.82
0065 68029 10,900.7 0.89 0.33 0.64 NDS 3 0.62 0.28
0066 47473 -9,655.3 -0.79 0.82 -0.42 NDS 3 -0.13 0.84
0068 45278 -11,850.3 -0.97 NDS NDS NDS 1 -0.97
0070 26290 -30,838.3 -2.52 3 -1.70 -1.79 -0.92 4 -1.73 0.65
0071 66270 9,141.7 0.75 -0.19 0.21 NDS 3 0.26 0.47
0072 55200 -1,928.3 -0.16 0.29 0.58 NDS 3 0.24 0.37
0073 55301 -1,827.3 -0.15 0.00 -0.55 NDS 3 -0.23 0.28
0076 54818.5 -2,309.8 -0.19 0.87 -0.91 NDS 3 -0.08 0.9
0077 65061 7,932.7 0.65 1.10 0.70 0.67 4 0.78 0.21
0078 72001 14,872.7 1.21 NDS 0.72 0.96 3 0.96 0.25
0079 46741 -10,387.3 -0.85 -1.13 NDS NDS 2 -0.99 0.2
0080 80145 23,016.7 1.88 NDS 2.49 -0.64 3 1.24 1.66
0081 58376.896 1,248.596 0.10 -0.92 0.28 0.20 4 -0.09 0.56
0082 62100 4,971.7 0.41 1.40 0.39 0.81 4 0.75 0.47
0083 63413 6,284.7 0.51 NDS NDS 0.23 2 0.37 0.2
0084 51337 -5,791.3 -0.47 -1.05 -0.60 NDS 3 -0.71 0.3
0085 59959 2,830.7 0.23 -0.71 NDS -0.41 3 -0.30 0.48
November 9, 2018 www.astm.org 132
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0086 66903 9,774.7 0.80 NDS NDS NDS 1 0.80
0087 44556.19 -12,572.11 -1.03 -0.46 NDS NDS 2 -0.75 0.4
0088 55247 -1,881.3 -0.15 1.99 0.36 -0.60 4 0.40 1.13
0089 59022 1,893.7 0.15 5.27R -0.19 NDS 2 -0.02 0.24
0091 49336 -7,792.3 -0.64 -1.35 -0.48 NDS 3 -0.82 0.46
0092 71749.1 14,620.8 1.19 2.18 1.33 1.00 4 1.43 0.52
0094 73963 16,834.7 1.37 NDS 0.85 1.05 3 1.09 0.26
0095 52514 -4,614.3 -0.38 NDS 0.22 0.30 3 0.05 0.37
0096 38026 -19,102.3 -1.56 -0.44 NDS NDS 2 -1.00 0.79
0098 53862 -3,266.3 -0.27 -0.59 -0.88 0.47 4 -0.32 0.58
0099 58097 968.7 0.08 NDS NDS NDS 1 0.08
0101 61915 4,786.7 0.39 0.29 0.60 NDS 3 0.43 0.16
0102 63300 6,171.7 0.50 -0.88 0.23 -0.52 4 -0.17 0.64
0104 58200 1,071.7 0.09 -0.68 -0.39 -0.32 4 -0.33 0.32
0105 59272 2,143.7 0.17 NDS NDS NDS 1 0.17
0106 56718 -410.3 -0.03 0.84 0.09 0.00 4 0.23 0.41
0107 69436 12,307.7 1.00 -1.12 0.68 -0.23 4 0.08 0.96
0108 32553.598 -24,574.702 -2.00 -0.92 -0.43 0.60 4 -0.69 1.08
0115 68296 11,167.7 0.91 0.23 -0.07 0.56 4 0.41 0.42
0117 36785 -20,343.3 -1.66 -1.01 -1.56 -1.30 4 -1.38 0.29
0119 54949 -2,179.3 -0.18 -0.64 -0.33 -0.41 4 -0.39 0.19
0121 48477 -8,651.3 -0.71 1.06 NDS NDS 2 0.18 1.25
0122 53657 -3,471.3 -0.28 -1.14 -0.57 -0.80 4 -0.70 0.36
0123 47430 -9,698.3 -0.79 0.96 -2.20 1.19 4 -0.21 1.59
0124 72409 15,280.7 1.25 -0.31 0.25 0.34 4 0.38 0.65
0125 48347.52 -8,780.78 -0.72 NDS 0.70 0.06 3 0.01 0.71
0126 61702 4,573.7 0.37 0.28 -0.24 0.24 4 0.16 0.27
0127 12903 -44,225.3 -3.61 1,3 NDS NDS NDS 1 -3.61
0128 58410 1,281.7 0.10 NDS 0.19 NDS 2 0.15 0.06
0129 61600 4,471.7 0.36 NDS NDS NDS 1 0.36

Pooled StdDev of Z: 0.77


November 9, 2018 www.astm.org 133
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 134


Distribution of Results

November 9, 2018 www.astm.org 135


Frequency Histogram

November 9, 2018 www.astm.org 136


Headspace Sampling, C, Oxygen, D3612-02(2017)
Data Report
Headspace Sampling, C, Oxygen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 91 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 91
$ Z-Score not calculated
Average 24633.6
StdDev 6070.2
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 16814.5
TPI
ADrs Statistic 0.71 Normal

November 9, 2018 www.astm.org 137


Results Table and Z-Scores
Headspace Sampling, C, Oxygen by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 20192 -4,441.6 -0.73 -0.08 0.52 0.26 4 -0.01 0.54
0002 21085 -3,548.6 -0.58 NDS 0.37 NDS 2 -0.11 0.67
0004 17134.3 -7,499.3 -1.24 -0.11 0.52 0.76 4 -0.02 0.89
0005 24798 164.4 0.03 1.16 -0.07 NDS 3 0.37 0.68
0007 22601 -2,032.6 -0.33 0.18 0.29 0.81 4 0.24 0.47
0008 29755 5,121.4 0.84 -0.65 0.94 0.78 4 0.48 0.75
0009 26411 1,777.4 0.29 0.62 -0.28 -1.28 4 -0.16 0.83
0011 28476 3,842.4 0.63 -0.51 0.38 0.23 4 0.18 0.49
0012 27538 2,904.4 0.48 1.31 1.22 1.16 4 1.04 0.38
0013 22069 -2,564.6 -0.42 -0.23 -0.04 -0.09 4 -0.20 0.17
0014 27718 3,084.4 0.51 -0.63 0.68 NDS 3 0.19 0.71
0015 30740 6,106.4 1.01 -0.37 NDS 1.32 3 0.65 0.9
0016 21712 -2,921.6 -0.48 0.17 0.29 0.00 4 -0.01 0.34
0017 15371 -9,262.6 -1.53 2.09 -0.08 -0.09 4 0.10 1.49
0022 24578 -55.6 -0.01 -0.69 -1.51 0.30 4 -0.48 0.8
0024 18434 -6,199.6 -1.02 NDS -1.60 -1.17 3 -1.26 0.3
0025 26136 1,502.4 0.25 NDS 0.89 -0.08 3 0.35 0.49
0026 29460.8 4,827.2 0.80 -2.45 0.37 NDS 3 -0.43 1.77
0028 20058 -4,575.6 -0.75 0.00 0.02 -0.38 4 -0.28 0.36
0029 28526 3,892.4 0.64 0.19 0.48 0.10 4 0.35 0.25
0031 15908 -8,725.6 -1.44 NDS -2.07 NDS 2 -1.76 0.45
0032 24253 -380.6 -0.06 -0.38 NDS NDS 2 -0.22 0.23
0034 31654 7,020.4 1.16 2.05 NDS NDS 2 1.61 0.63
0035 18852.62 -5,780.98 -0.95 0.06 -1.57 -0.33 4 -0.70 0.72
0036 25000 366.4 0.06 NDS NDS NDS 1 0.06
0038 29417.1 4,783.5 0.79 NDS NDS NDS 1 0.79
0039 28727 4,093.4 0.67 -0.48 0.88 NDS 3 0.36 0.73
0040 26708 2,074.4 0.34 0.27 1.63 0.47 4 0.68 0.64

November 9, 2018 www.astm.org 138


StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0041 36091 11,457.4 1.89 1.92 -1.36 NDS 3 0.82 1.89
0042 27210 2,576.4 0.42 0.34 0.63 0.09 4 0.37 0.22
0043 34630 9,996.4 1.65 1.85 NDS NDS 2 1.75 0.14
0045 27677 3,043.4 0.50 NDS 0.45 0.31 3 0.42 0.1
0047 32796 8,162.4 1.34 0.68 0.74 0.11 4 0.72 0.5
0048 17870 -6,763.6 -1.11 NDS -1.39 -1.71 3 -1.40 0.3
0049 26967 2,333.4 0.38 0.67 0.15 1.00 4 0.55 0.37
0051 8906 -15,727.6 -2.59 3 -0.52 -2.31 -1.18 4 -1.65 0.97
0054 31100 6,466.4 1.07 -0.93 -0.03 0.09 4 0.05 0.82
0056 26100 1,466.4 0.24 NDS NDS NDS 1 0.24
0057 17900 -6,733.6 -1.11 NDS NDS NDS 1 -1.11
0059 22379 -2,254.6 -0.37 2.13 NDS NDS 2 0.88 1.77
0060 34592 9,958.4 1.64 0.56 1.18 0.70 4 1.02 0.49
0061 25335 701.4 0.12 -0.18 -0.45 NDS 3 -0.17 0.29
0063 28524 3,890.4 0.64 0.45 0.81 NDS 3 0.63 0.18
0064 24016 -617.6 -0.10 -1.35 0.12 NDS 3 -0.44 0.79
0065 29182 4,548.4 0.75 0.49 0.94 NDS 3 0.73 0.23
0066 21772 -2,861.6 -0.47 0.84 0.08 NDS 3 0.15 0.66
0068 15218 -9,415.6 -1.55 NDS NDS NDS 1 -1.55
0070 18804 -5,829.6 -0.96 -1.21 -0.59 -0.19 4 -0.74 0.45
0071 28783 4,149.4 0.68 -1.86 -3.37 NDS 3 -1.52 2.05
0072 24400 -233.6 -0.04 0.48 1.06 NDS 3 0.50 0.55
0073 24667 33.4 0.01 0.20 -0.08 NDS 3 0.04 0.14
0076 14756.6 -9,877 -1.63 0.31 -0.47 NDS 3 -0.60 0.98
0077 28557 3,923.4 0.65 1.05 1.14 0.55 4 0.85 0.29
0078 31958 7,324.4 1.21 NDS 1.21 0.65 3 1.02 0.32
0079 20879 -3,754.6 -0.62 -0.92 NDS NDS 2 -0.77 0.21
0080 37266 12,632.4 2.08 3 NDS 2.03 -0.08 3 1.34 1.23
0081 26726.761 2,093.161 0.34 -0.67 0.75 0.17 4 0.15 0.6
0082 29100 4,466.4 0.74 1.74 1.13 0.93 4 1.14 0.43
0083 23716 -917.6 -0.15 NDS NDS 0.12 2 -0.02 0.19
0084 23531 -1,102.6 -0.18 -1.00 -0.40 NDS 3 -0.53 0.42
0085 36395 11,761.4 1.94 -0.14 NDS -0.22 3 0.53 1.22
November 9, 2018 www.astm.org 139
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0086 28908 4,274.4 0.70 NDS NDS NDS 1 0.70
0087 18970.53 -5,663.07 -0.93 -0.38 NDS NDS 2 -0.66 0.39
0088 32870 8,236.4 1.36 1.44 0.07 -0.57 4 0.58 0.99
0089 22031 -2,602.6 -0.43 4.23R -0.27 NDS 2 -0.35 0.11
0091 21478 -3,155.6 -0.52 -1.19 -0.17 0.35 4 -0.38 0.65
0092 28968.5 4,334.9 0.71 1.94 1.32 0.43 4 1.10 0.67
0094 31815 7,181.4 1.18 NDS 0.89 -0.21 3 0.62 0.73
0095 24493 -140.6 -0.02 NDS 0.30 0.44 3 0.24 0.24
0096 18012 -6,621.6 -1.09 -0.31 NDS NDS 2 -0.70 0.55
0098 24369 -264.6 -0.04 -0.36 -0.32 0.50 4 -0.06 0.4
0099 23812 -821.6 -0.14 NDS NDS NDS 1 -0.14
0101 25213 579.4 0.10 0.25 0.75 NDS 3 0.37 0.34
0102 27700 3,066.4 0.51 -0.82 0.13 -0.14 4 -0.08 0.56
0104 22600 -2,033.6 -0.34 -0.90 -0.44 -0.34 4 -0.51 0.27
0105 26819 2,185.4 0.36 NDS NDS NDS 1 0.36
0106 25000 366.4 0.06 0.74 0.01 0.13 4 0.24 0.34
0107 23889 -744.6 -0.12 -0.83 0.59 0.16 4 -0.05 0.6
0108 16138.5 -8,495.1 -1.40 -0.79 0.07 0.30 4 -0.46 0.79
0115 5942 -18,691.6 -3.08 1,3 -1.88 -4.50R -3.09 3 -2.68 0.7
0117 24915 281.4 0.05 -1.18 -1.51 -1.02 4 -0.92 0.67
0119 20509 -4,124.6 -0.68 -0.71 -0.01 -0.37 4 -0.44 0.33
0121 24855 221.4 0.04 1.20 NDS NDS 2 0.62 0.82
0122 24508 -125.6 -0.02 -0.83 0.00 -0.08 4 -0.23 0.4
0123 15251 -9,382.6 -1.55 0.40 -1.76 0.78 4 -0.53 1.31
0124 31242 6,608.4 1.09 -0.21 0.66 0.36 4 0.48 0.55
0125 24159.72 -473.88 -0.08 NDS 0.45 0.18 3 0.18 0.27
0126 28500 3,866.4 0.64 0.55 0.22 0.50 4 0.48 0.18
0127 5881 -18,752.6 -3.09 1,3 NDS NDS NDS 1 -3.09
0128 28595 3,961.4 0.65 NDS 0.53 NDS 2 0.59 0.08
0129 23100 -1,533.6 -0.25 NDS NDS NDS 1 -0.25

Pooled StdDev of Z: 0.78


November 9, 2018 www.astm.org 140
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 141


Distribution of Results

November 9, 2018 www.astm.org 142


Frequency Histogram

November 9, 2018 www.astm.org 143


Headspace Sampling, C, Propane, D3612-02(2017)
Data Report
Headspace Sampling, C, Propane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 23 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 21
$ Z-Score not calculated
Average 2.0
StdDev 3.3
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 9.2
TPI
ADrs Statistic 3.14 Not Normal

November 9, 2018 www.astm.org 144


Results Table and Z-Scores
Headspace Sampling, C, Propane by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0007 0 -2 -0.60 -0.57 0.83 -0.71 4 -0.26 0.73
0013 11 9 2.70 3 1.57 -0.78 2.04 4 1.38 1.51
0016 6 4 1.20 1.57 -0.78 1.85 4 0.96 1.19
0017 27.9 25.9 7.76 R 2.46 -0.78 1.17 3 0.95 1.63
0026 0 -2 -0.60 NDS -0.78 NDS 2 -0.69 0.13
0043 0.75 -1.25 -0.38 -0.43 NDS NDS 2 -0.41 0.04
0051 0 -2 -0.60 -0.57 -0.78 0.70 4 -0.31 0.68
0057 0 -2 -0.60 NDS NDS NDS 1 -0.60
0060 3 1 0.30 -0.57 -0.78 -0.71 4 -0.44 0.5
0061 0 -2 -0.60 -0.57 1.01 NDS 3 -0.05 0.92
0064 19.2 17.2 5.15 R NDS -0.78 NDS 1 -0.78
0068 0 -2 -0.60 NDS NDS NDS 1 -0.60
0076 0.2 -1.8 -0.54 NDS 1.01 NDS 2 0.24 1.1
0085 9 7 2.10 3 1.78 NDS 0.83 3 1.57 0.66
0087 0.28 -1.72 -0.52 -0.57 NDS NDS 2 -0.55 0.04
0089 0.00 -2 -0.60 -0.57 NDS NDS 2 -0.59 0.02
0096 0 -2 -0.60 -0.57 NDS NDS 2 -0.59 0.02
0099 5.8 3.8 1.14 NDS NDS NDS 1 1.14
0107 1 -1 -0.30 -0.36 1.90 -0.69 4 0.14 1.19
0108 0.18897 -1.81103 -0.55 -0.57 7.24R -0.71 3 -0.61 0.09
0117 0 -2 -0.60 -0.57 -0.78 -0.71 4 -0.67 0.1
0121 0 -2 -0.60 -0.14 NDS NDS 2 -0.37 0.33
0127 5 3 0.90 NDS NDS NDS 1 0.90

Pooled StdDev of Z: 0.85


Legend
NDS No Data Submitted

November 9, 2018 www.astm.org 145


NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 146


Distribution of Results

November 9, 2018 www.astm.org 147


Frequency Histogram

November 9, 2018 www.astm.org 148


Headspace Sampling, C, Propylene, D3612-02(2017)
Data Report
Headspace Sampling, C, Propylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 18 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 18
$ Z-Score not calculated
Average 22.1
StdDev 13.8
ASTM R not determined - average is
ASTM R outside range specified for Reproducibility
in test method.
These Data R 38.1
TPI
ADrs Statistic 1.07 Marginally Normal

November 9, 2018 www.astm.org 149


Results Table and Z-Scores
Headspace Sampling, C, Propylene by D3612-02(2017) (ppm)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0007 29.7 7.6 0.55 0.52 2.29 0.57 4 0.98 0.87
0043 36.7 14.6 1.06 0.72 NDS NDS 2 0.89 0.24
0051 0 -22.1 -1.60 -1.36 -0.63 -0.80 4 -1.10 0.46
0057 15.1 -7 -0.51 NDS NDS NDS 1 -0.51
0060 25 2.9 0.21 0.52 -0.63 0.98 4 0.27 0.68
0061 28 5.9 0.43 0.40 1.31 NDS 3 0.71 0.52
0063 27 4.9 0.36 0.40 NDS NDS 2 0.38 0.03
0064 19.2 -2.9 -0.21 NDS -0.63 NDS 2 -0.42 0.3
0068 0 -22.1 -1.60 NDS NDS NDS 1 -1.60
0076 28.1 6 0.44 NDS -0.63 NDS 2 -0.10 0.76
0087 30.08 7.98 0.58 0.58 NDS NDS 2 0.58 0
0089 23 0.9 0.07 -0.07 NDS NDS 2 0.00 0.1
0096 30 7.9 0.57 0.34 NDS NDS 2 0.46 0.16
0099 0 -22.1 -1.60 NDS NDS NDS 1 -1.60
0107 33 10.9 0.79 0.76 1.31 1.00 4 0.97 0.25
0108 26.76 4.66 0.34 -0.33 12.99R -0.73 3 -0.24 0.54
0117 0 -22.1 -1.60 -0.33 -0.63 -0.72 4 -0.82 0.55
0121 46 23.9 1.74 -0.51 NDS NDS 2 0.62 1.59

Pooled StdDev of Z: 0.75


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated

November 9, 2018 www.astm.org 150


R Rejected by GESD

November 9, 2018 www.astm.org 151


Distribution of Results

November 9, 2018 www.astm.org 152


Water Content, D1533-12
Data Report
Water Content by D1533-12 (mg/kg)
Dissolved Gas Analysis - DGA1808

Summary of Results Legend


Conforming Results 57 NSP No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
Results Used 55
$ Z-Score not calculated
Average 10.0
StdDev 3.7
ASTM R 14.0
These Data R 10.4 Consistent with ASTM R
TPI 1.35
ADrs Statistic 1.36 Not Normal

November 9, 2018 www.astm.org 153


Results Table and Z-Scores
Water Content by D1533-12 (mg/kg)
Dissolved Gas Analysis - DGA1808

StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 9.6 -0.4 -0.11 0.13 2.08 NDS 3 0.70 1.2
0005 34 24 6.40 R -0.91 -0.68 NDS 2 -0.80 0.16
0008 7 -3 -0.80 NDS -0.27 NDS 2 -0.54 0.37
0011 7 -3 -0.80 -1.20 -0.27 NDS 3 -0.76 0.47
0012 7 -3 -0.80 -0.01 0.33 NDS 3 -0.16 0.58
0013 15 5 1.33 1.47 1.94 NDS 3 1.58 0.32
0015 9 -1 -0.27 0.28 NDS NDS 2 0.01 0.39
0016 15 5 1.33 0.58 1.54 NDS 3 1.15 0.5
0017 7.0 -3 -0.80 -0.31 -1.58 NDS 3 -0.90 0.64
0021 6 -4 -1.07 -1.20 NDS NDS 2 -1.14 0.09
0026 15.30 5.3 1.41 5.93R NDS NDS 1 1.41
0029 3 -7 -1.87 -0.61 -2.89 NDS 3 -1.79 1.14
0032 8 -2 -0.53 NDS NDS NDS 1 -0.53
0035 4.7 -5.3 -1.41 3.25 NDS NDS 2 0.92 3.3
0040 8 -2 -0.53 2.36 -1.48 NDS 3 0.12 2
0041 7 -3 -0.80 -1.20 -0.27 NDS 3 -0.76 0.47
0042 8 -2 -0.53 -0.91 -0.27 NDS 3 -0.57 0.32
0043 8 -2 -0.53 NDS NDS NDS 1 -0.53
0047 14 4 1.07 0.28 0.13 NDS 3 0.49 0.51
0049 10 0 0.00 -0.01 0.13 NDS 3 0.04 0.08
0051 10 0 0.00 NDS NDS NDS 1 0.00
0052 15 5 1.33 -0.01 NDS NDS 2 0.66 0.95
0054 8 -2 -0.53 -0.67 0.94 NDS 3 -0.09 0.89
0056 10 0 0.00 -1.20 -0.68 NDS 3 -0.63 0.6
0059 12.0 2 0.53 NDS NDS NDS 1 0.53
0061 21 11 2.93 3 NDS 0.13 NDS 2 1.53 1.98
0065 9 -1 -0.27 6.52R 3.15 NDS 2 1.44 2.42
0066 3 -7 -1.87 -1.50 -1.28 NDS 3 -1.55 0.3

November 9, 2018 www.astm.org 154


StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0067 10 0 0.00 0.28 NDS NDS 2 0.14 0.2
0068 12 2 0.53 NDS NDS NDS 1 0.53
0070 10 0 0.00 NDS -0.27 NDS 2 -0.14 0.19
0071 10 0 0.00 0.58 0.33 NDS 3 0.30 0.29
0072 10 0 0.00 0.28 NDS NDS 2 0.14 0.2
0073 12 2 0.53 0.88 -0.27 NDS 3 0.38 0.59
0076 10.0 0 0.00 0.43 0.53 NDS 3 0.32 0.28
0079 8 -2 -0.53 NDS NDS NDS 1 -0.53
0081 11 1 0.27 NDS NDS NDS 1 0.27
0084 10 0 0.00 -0.61 -0.07 NDS 3 -0.23 0.33
0085 6 -4 -1.07 -0.61 NDS NDS 2 -0.84 0.33
0087 23.11 13.11 3.50 1,3 -0.61 NDS NDS 2 1.45 2.91
0090 12.48 2.48 0.66 NDS NDS NDS 1 0.66
0093 13 3 0.80 0.88 0.13 NDS 3 0.60 0.41
0094 7 -3 -0.80 NDS -0.68 NDS 2 -0.74 0.08
0095 9.3 -0.7 -0.19 NDS 0.13 NDS 2 -0.03 0.23
0096 11 1 0.27 -0.01 NDS NDS 2 0.13 0.2
0099 13 3 0.80 NDS NDS NDS 1 0.80
0101 8 -2 -0.53 2.36 -0.07 NDS 3 0.59 1.55
0102 7 -3 -0.80 -1.20 -0.68 NDS 3 -0.89 0.27
0104 10 0 0.00 -0.31 0.13 NDS 3 -0.06 0.23
0106 10 0 0.00 -0.31 0.13 NDS 3 -0.06 0.23
0107 12 2 0.53 0.58 NDS NDS 2 0.56 0.04
0115 9 -1 -0.27 -0.61 -0.48 NDS 3 -0.45 0.17
0120 7 -3 -0.80 NDS NDS NDS 1 -0.80
0125 51.83 41.83 11.16 R NDS 1.07 NDS 1 1.07
0126 9 -1 -0.27 -0.31 -0.27 NDS 3 -0.28 0.02
0127 16 6 1.60 NDS NDS NDS 1 1.60
0129 7.5 -2.5 -0.67 NDS NDS NDS 1 -0.67

Pooled StdDev of Z: 0.88

November 9, 2018 www.astm.org 155


Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD

November 9, 2018 www.astm.org 156


Distribution of Results

November 9, 2018 www.astm.org 157


Frequency Histogram

November 9, 2018 www.astm.org 158


November 9, 2018 www.astm.org 159
Participant Comments

Dissolved Gas Analysis


Sample ID: DGA1808
AUGUST 2018

Lab - 0001
General Comments Nothing abnormal to report

Lab - 0002
General Comments We observed air bubble in the sample syringe when received (slightly
less than 1 ml)

PTP Response: As long as the air bubbles weren't larger than 10ml, it's
always ok to agitate the sample back and forth and continue with testing.

Lab - 0013
General Comments Sample Number No 211781

Lab - 0035
General Comments We thank you for your efforts

Lab - 0038
General Comments The document pouch was not fully sealed down, but the paperwork did
not come out in transit.

Lab - 0052
General Comments Gas bubble was present in the syringe. PTP Response: As long as the
air bubbles weren't larger than 10ml, it's always ok to agitate the sample
back and forth and continue with testing.

Lab - 0059
General Comments There are bubbles in the sample。PTP Response: AS long as the air
bubbles weren't larger than 10ml; it's always ok to agitate the sample
back and forth and continue with testing.

Lab - 0061
General Comments The sample contained a large bubble. PTP Response: As long as the air
bubbles weren't larger than 10ml, it's always ok to agitate the sample
back and forth and continue with testing.

Lab - 0066
General Comments Moisture - automated method

Lab - 0067

November 9, 2018 www.astm.org 160


General Comments good.

Lab - 0069
General Comments All OK

Lab - 0070
General Comments no comment

Lab - 0071
General Comments Not sure why two lab results for Hydrogen and Co are different.

Lab - 0073
General Comments A bubble of approximately 1 ml or more was present in the syringe. It
could not be dissolved completely. A small bubble persisted. In an effort
to completely dissolve the bubble, the continuous pressure applied by
hand on the plunger allowed for traces of oil to leak past the plunger.
PTP Response; As long as the air bubbles weren't larger than 10ml, it's
always ok to agitate the sample back and forth and continue with testing.

Lab - 0076
General Comments The sample was received in order by Witbank Lab Syringe no.:31405 ,
DGA1808

Lab - 0077
General Comments Syringe contained 0.5ml bubble.

PTP Response: As long as the air bubbles weren't larger than 10ml, it's
always ok to agitate the sample back and forth and continue with testing.

Lab - 0092
General Comments Box arrived very quickly and in good state.

Lab - 0101
General Comments The syringe number for JHB LAB is 31001

Lab - 0125
General Comments Good morning, we have had problems with the contact address, we hope
that the same will not happen for the next evaluation

PTP Response: ASTM PTP will contact you to verify all shipping
information.

November 9, 2018 www.astm.org 161


This is the end of the report

November 9, 2018 www.astm.org 162

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