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A = Acetic Acid
B = Water
C = Chloroform
Preparation of
Solution
Prepared A-B
Solutions
Titrate using Chloroform until
first sign of turbidity appears
Preparation of
Solution
Prepared A-B
Concentration V of A (mL) V of C (mL)
Solutions
15% 3.75 21.25
Titrate using water until first 30% 7.5 17.5
sign of turbidity appears 45% 11.25 13.7
60% 15 10
Note: Start with 60% solution to be
70% 17.5 7.5
familiar with the endpoint
Construction of
bimodal curve
After sketching
binodal curve
E. flask with
conjugate phase
250-mL E. flask
Prepared A-B
Solutions