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Analyzer
Service Manual
July 2009
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1. GENERAL INFORMATION
Organization of the manual . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-1
Using This Manual. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-2
2. FUNCTIONAL DESCRIPTION
Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1
New Product Features . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-2
Cabinetry & Sample Chamber . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-2
Interior Modules. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-2
Software . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-2
Instrument Components . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-3
Cabinetry/Sample Chamber . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-3
Top Panel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-3
Front . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-3
Instrument Back . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-4
Side Panels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-5
Interior Modules. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-6
Gas entrance manifold . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-6
Dosing volume manifold . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-6
Sample analysis manifold. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-7
Schematic Board & Software. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-8
Printed Circuit Boards (PCBs) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-9
Analysis Transducer Interface PCB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-9
Card Cage. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-9
DSP-ISA CPU . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-10
Digital Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-10
Backplane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-10
Power Module . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-11
4. PREINSTALLATION
5. INSTALLATION
Jul 09 i
Table of Contents TriStar II 3020 Service Manual
6. OPERATOR TRAINING
7. MAINTENANCE DOCUMENTS
8. CALIBRATION PROCEDURE
Electrical . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-1
11. SOFTWARE
ii Jul 09
TriStar II 3020 Service Organization of the manual
1. GENERAL INFORMATION
This service manual contains information and instructions for providing instrument
service on the Micromeritics TriStar II 3020 Analyzer and is intended for use by
Micromeritics' factory-trained and supported service personnel.
Chapter 4 PREINSTALLATION
Provides Preinstallation requirements and checklist.
Chapter 5 INSTALLATION
Provides Installation Instructions.
Jul 09 1-1
Using This Manual TriStar II 3020 Service
Chapter 11 SOFTWARE
Contains the demo software for the TriStar II 3020 Analyzer.
1-2 Jul 09
TriStar II 3020 Service Overview
2. FUNCTIONAL DESCRIPTION
This chapter describes the systems and components that comprise the TriStar II 3020 Analyzer. It includes
graphics showing the location of major systems, modules, and components, as well as functional
descriptions.
Overview
As the latest addition to the TriStar Analyzer family, the TriStar II 3020 is a fully automated,
three-station physisorption instrument that provides high-quality surface area and porosimetry
measurements on solid materials by using the gas adsorption technique.
The TriStar II 3020 has three ports, allowing analysis of up to three samples simultaneously
and independently. A user can operate up to four TriStar analyzers with one Windows-based
computer.
Jul 09 2-1
New Product Features TriStar II 3020Service
• The TriStar II 3020 is smaller than the TriStar 3000 due to elimination of the vacuum
pump cavity.
• The rotating door allows easier access to the sample ports for mounting and removing
sample tubes.
Interior Modules
• An additional port has been added to the gas inlet manifold to bring the total number of
ports, for readily available gases, to four.
Software
• The use of any of the IUPAC standard measurement units is available on the TriStar II
3020.
• Data from the TriStar 3000 and Gemini can be imported to the 3020 to allow overlay plots
and other comparisons to be generated.
• Information can be scanned directly into input fields using a bar code reader. This elimi-
nates human error on data entry.
• The TriStar II 3020 software allows opening of multiple sample files simultaneously for
editing.
• Diagnostics may be performed remotely by way of the Internet. This allows MIC engi-
neers to access the instrument and run diagnostics programs.
2-2 Jul 09
TriStar II 3020 Service Instrument Components
Instrument Components
The TriStar 3020 Analyzer is comprised of these major components and modules:
• Cabinetry/Sample Chamber
• Interior
• Printed Circuit Boards (PCBs)
• Power Module
Cabinetry/Sample Chamber
Due to the elimination of the vacuum pump cavity, the redesigned TriStar II 3020 analyzer is
significantly smaller than its predecessor.
Top Panel
Communications status
indicator
Sample Tubes
Door
Dewar
Elevator
Top Panel
The top panel of the TriStar provides access to the interior analysis module and its
subassemblies. The top panel is molded from plastic and internally coated with a special
conductive coating to prevent radio frequency interference.
Front
The redesigned front of the TriStar II 3020 consists of a tinted and transparent rounded sample
chamber door. The front panel is intended to shield the operator from any flying debris
resulting from a sample tube explosion or liquid nitrogen splatter. When the door is opened, it
allows for easy, 270-degree access to the three sample ports.
Jul 09 2-3
Cabinetry/Sample Chamber TriStar II 3020Service
Elevator
The TriStar II 3020 elevator raises the dewar to the sample tubes. During analysis, it is
automatically raised and lowered. The elevator can be manipulated by the user when the
system is in manual mode.
Dewar
The Dewar for the TriStar 3000 carried over to the TriStar 3020 has a capacity of 2.75-L.
Sample Tubes
The TriStar has the ability to test up to three samples at a time The tubes are made out of
borosilicate glass to withstand the temperatures reached inside the Dewar or during degassing.
A green LED indicator is located on the front of the TriStar’s top panel to indicate the
instrument has power.
Instrument Back
Gas entrance
manifold
Vacuum pump
connector
Power switch
The back area of the TriStar is where the gas entrance manifold, the vacuum pump connection
and the power connection are located.
2-4 Jul 09
TriStar II 3020 Service Cabinetry/Sample Chamber
Vacuum Pump
A new feature of the TriStar II 3020 is that the vacuum system is outside the instrument
cabinet. Wet and dry pumps are available for nitrogen systems, while the krypton option must
use a dry pump.
Side Panels
The left panel of the TriStar is plain. The right panel, however, provides access to the unit’s
card cage, ethernet, and RS-232 connection.
Jul 09 2-5
Interior Modules TriStar II 3020Service
Interior Modules
Transducer
Servo valve Solenoid valves
Vacuum pump
connector
The Gas Entrance Manifold provides four gas inlet ports, that face the rear of the instrument.
The inlets have dust filters (frits) to prevent dirt from gas lines getting into the system. This
manifold also has the vacuum connection.
The servo valve sets dosing pressures in the manifold and regulates the rate of pressure
decrease during gas evacuation.The manifold transducer is also located on the gas entrance
manifold. All other valves are solenoid valves.
The Dosing Chamber or Volume Chamber is an aluminum chamber that has a capacity of 18
mL of volume. The volume chamber does not have any valves attached to it in order to prevent
2-6 Jul 09
TriStar II 3020 Service Interior Modules
local fluctuations of temperature, which would reduce the precision of gas measurements.
There is a temperature sensing device (RTD) mounted to the chamber.
Dosing volume
manifold
Solenoid valve
Transducer
The Sample Manifold contains the three sample ports and a P0 port for the instrument. Each of
the TriStar’s three ports has a 20-µm frit to prevent sample from entering and clogging the
system, a small-orifice solenoid valve for dosing, a large-orifice solenoid valve for evacuation,
1000-Torr transducer, and a pressure relief valve to protect against excess pressure build up
caused by too rapid desorption. The relief valves vent at 10 to 20 psig, even if there is no
power applied to the instrument and protect the sample transducers, sample tubes and dewar.
The P0 port is used for continuous saturation pressure measurement.
Jul 09 2-7
Schematic Board & Software TriStar II 3020Service
The schematic diagram of the 3020 is displayed on the computer screen by the TriStar
software. The schematic shows:
The software is designed to work on computers running Windows XP or Windows Vista. The
software also supports importing data from the TriStar 3000 and Gemini for analysis and
comparison with TriStar II 3020 plots. For more instructions on how to use the software and
run the TriStar analyzer, refer to Chapter 3 - Operational Procedures in the Operator’s
Manual.
2 12
4
5
1 9 8 7 6
3
10
11
2-8 Jul 09
TriStar II 3020 Service Printed Circuit Boards (PCBs)
The Analysis Transducer Interface PCB is responsible for controlling most functions
throughout the analysis module. This includes actions performed by the gas inlet, dosing, and
sample manifolds. The analysis transducer interface board is partially enclosed by a metal
barrier to protect its components from radio frequency interference.
Card Cage
1 - Backplane PB
1
3
2
Card Cage Photo Card Cage CAD
Jul 09 2-9
Printed Circuit Boards (PCBs) TriStar II 3020Service
The card cage is the main assembly of electrical systems and the connection between those
systems and other components inside and outside of the instrument. The card cage is
comprised of three boards: Backplane, CPU, and Digital Interface PCBs.
DSP-ISA CPU
The DSP-ISA CPU PCB provides control of the instrument. Application software is loaded
into this PCB. This board is in the first slot from right to left.
Digital Interface
The digital interface board generates control signals for valve drivers and the elevator
interface. This board also stores all PCB IDs, and instrument calibration information. Finally,
it has the necessary RS-232 channels for serial communications and connections for ethernet.
The digital interface board is in the second slot from right to left.
Backplane
The backplane carries the necessary signals and DC power to and from the boards in the card
cage.
2-10 Jul 09
TriStar II 3020 Service Power Module
Power Module
Power supply (from rear of instrument) Power switch (from rear of instrument)
The TriStar’s power supply assembly is the same model as used in the SediGraph 5120. The
power supply is mounted at the rear of the instrument providing access to the power switch.
Jul 09 2-11
Power Module TriStar II 3020Service
2-12 Jul 09
TriStar II 3020 Service Analysis Sequence
The analysis sequence describes what is taking place throughout the instrument during an analysis.The
instrument schematic, shown below, will be used to show the state of the system components during the
various phases of an analysis.
1000 mmHg
transducer
Temperature
Gas
inlet Sample
ports transducers
Elevator
Green = open
White = closed
(when in Manual Mode, yellow = closed)
Jul 09 3-1
Analysis Sequence TriStar II 3020 Service
Valve(s) Description
1 through 3 Sample ports
4 Po port
5 Isolation valve
6 Isolation valve
7 Helium port
8 and 9 Analysis gas ports
10 Vacuum
11 through 13 Unrestricted vacuum for sample ports
14 Analysis gas port
15 10-mmHg isolation valve (displays
only if the Krypton option is installed).
Unmarked Servo
Analysis Technique
The TriStar II 3020 Analyzer uses physical adsorption and capillary condensation principles to
obtain information about the surface area and porosity of a solid material. The analytical
technique is simple: a sample contained in an evacuated sample tube is cooled (typically) to
cryogenic temperature, then is exposed to analysis gas at a series of precisely controlled
pressures. With each incremental pressure increase, the number of gas molecules adsorbed on
the surface increases. The equilibrated pressure (P) is compared to the saturation pressure (Po)
and their relative pressure ratio (P/Po) is recorded along with the quantity of gas adsorbed by
the sample at each equilibrated pressure.
As adsorption proceeds, the thickness of the adsorbed film increases. Any micropores in the
surface are filled first, then the free surface becomes completely covered, and finally the larger
pores are filled by capillary condensation. The process may continue to the point of bulk
condensation of the analysis gas. Then, the desorption process may begin in which pressure
systematically is reduced resulting in liberation of the adsorbed molecules. As with the
adsorption process, the changing quantity of gas on the solid surface at each decreasing
equilibrium pressure is quantified. These two sets of data describe the adsorption and
desorption isotherms. Analysis of the shape of the isotherms yields information about the
surface and internal pore characteristics of the material.
3-2 Jul 09
TriStar II 3020 Service Analysis Sequence
Analysis Sequence
1. Create and save up to three sample files for use during an analysis.
2. Place a plug in any port that is not being used for analysis.
3. Prepare samples to be analyzed. This may include weighing the sample and degassing the
sample.
4. Load sample tubes in their respective ports and fill the Dewar.
5. Select Unit n > Sample Analysis > Browse to load the newly created sample file for each
port.
Jul 09 3-3
Analysis Sequence TriStar II 3020 Service
7. The system begins to evacuate the manifold at a rate and time specified in the sample file.
8. All valves close, then the N2 valve opens and the Po tube is filled to the target pressure.
9. The manifold is evacuated and helium is purged from the gas line.
3-4 Jul 09
TriStar II 3020 Service Analysis Sequence
10. A series of manifold dosings and port equilibrations begin to take place on each port to
prepare for analysis under cryogenic conditions. Helium warm free space is measured.
Then the elevator is raised to measure cold freespace.
Jul 09 3-5
Analysis Sequence TriStar II 3020 Service
11. Helium is evacuated from the samples and the Dewar is lowered if specified in the sample
file.
12. Samples are evacuated for the amount of time specified in the sample file.
3-6 Jul 09
TriStar II 3020 Service Analysis Sequence
1000.00
14. If the pressure does not change measurably, the Psat measurement is taken. If the pressure
changes measurably, another dose may be required.
Jul 09 3-7
Analysis Sequence TriStar II 3020 Service
15. After evacuation, the analysis phase begins. The instrument starts dosing to the set point
specified in the sample file and continues until the specified number of data points have
been collected. Data points are displayed in a graph as they are collected.
16. You can view the instrument schematic by selecting Instrument Schematic from the
View drop-down list.
3-8 Jul 09
TriStar II 3020 Service Preinstallation
4. PREINSTALLATION
This chapter contains the Preinstallation Instructions and Checklist for the TriStar II 3020.
This document helps to ensure that the customer has prepared the laboratory for installation of
the instrument and that the supplies, equipment, and personnel are available for installation.
Double-click on the following link to access the preinstallation instructions and checklist.
Jul 09 4-1
Preinstallation TriStar II 3020 Service
4-2 Jul 09
TriStar II 3020 Service Installation
5. INSTALLATION
Typically, the TriStar analyzers are customer-installed, except for the Confirm version which
usually is installed by a qualified Micromeritics service representative.
Jul 09 5-1
Installation TriStar II 3020 Service
5-2 Jul 09
TriStar II 3020 Service Operator Training
6. OPERATOR TRAINING
The Operator Training Checklist is used in conjunction with the operator’s manual and soft-
ware to train the person(s) who will be operating the analyzer. Click below to access the
Operator Training Checklist.
Jul 09 6-1
Operator Training TriStar II 3020 Service
6-2 Jul 09
TriStar II 3020 Service Maintenance Documents
7. MAINTENANCE DOCUMENTS
The documents listed below are included in Service PM kits, which may be purchased by the
user for proper maintenance of his analyzer. Use of these PM plans also help to prolong the
life of the analyzer.
Jul 09 7-1
Maintenance Documents TriStar II 3020 Service
7-2 Jul 09
TriStar II 3020 Service Calibration Procedure
8. CALIBRATION PROCEDURE
This chapter contains the calibration and test procedure used in Micromeritics’ Final Assem-
bly Department. It is provided as a reference so that you will be familiar with the calibration
procedures and instrument tests that are performed on the instrument during manufacture.
The methods used at the factory may differ from the methods documented in Chapter 7, Main-
tenance Documents. Use the established service calibration and test procedure unless
otherwise directed by a Micromeritics Service Managers or Service Specialist.
Jul 09 8-1
Calibration Procedure TriStar II 3020 Service
8-2 Jul 09
TriStar II 3020 Service Mechanical
This section contains mechanical and electrical drawings for the TriStar II 3020. These draw-
ings show assemblies in great detail. Some parts listed in these prints may be available only as
an assembly or in a kit. Do not provide copies of these drawings to a customer.
Mechanical
Refer to the following table for a list of the mechanical prints. Double-click on the part number
to view the print.
Electrical
Refer to the following table for a list of the electrical drawings. Double-click on the part num-
ber to view the print.
Jul 09 9-1
Electrical TriStar II 3020 Service
9-2 Jul 09
TriStar II 3020 Service Service Parts
This section contains a list of approved repair parts for this instrument. The items with an
asterisk (*) are included in the Service Parts Kit, P/N: 302-33680-00.
Jul 09 10-1
Service Parts TriStar II 3020 Service
10-2 Jul 09
TriStar II 3020 Service Service Parts
Jul 09 10-3
Service Parts TriStar II 3020 Service
10-4 Jul 09
TriStar II 3020 Service Software
11. SOFTWARE
A demo version of the software for is available for either the standard version or the Confirm
version of the TriStar II 3020 system. Double-click the demo software version you wish to
view.
Jul 09 11-1
TriStar II 3020 Service Operator’s Manual
A printed operator’s manual is shipped with every Gemini analyzer. Analyzers operated in a
Windows environment also have an electronic copy accessible from the Help menu.
Listed below are the operator manuals available for the Gemini II 2390 series analyzers. Click
the document you wish to view:
Jul 09 12-1
TriStar II 3020 Service Service Training
Service Training is provided to service personnel so that they can become familiar with the
TriStar system. Click Service Training below to view a syllabus of the training class.
• Service Training
Jul 09 13-1
Service Training TriStar II 3020 Service
13-2 Jul 09