Ea MB Harsh Patel New

1 5
YELLOW FLOW RATES ARE ASSUMED VALUE AND OTHER ARE CAALCULATED WITH ASSUME VALUES
1 FEED ETHANOL
MASS FLOW MASS% MOLAR FLOW MOLE%
ACETIC ACID 0 0 0 0
ETHANOL 3267.0454545455 99 71.0227272727 97.483589
ETHYL ACETATE 0 0 0 0
WATER 33.0004591368 1 1.8333588409 2.5164114
TOTL 3300.0459136823 72.8560861137
ACTUAL CAPACITY 150 MTPD 6250 kg/hr
PLANT LOAD 100 % 6250 kg/hr
6250.0000002069
1 2 18
total in 3300.0459136823 4267.7653 5200 12767.811
31 49
total out 6250 6184.443101457 12434.443
3586 4456 4517 12559
6250 6135 12385

5
SSUME VALUES
2 FEED ACETIC ACID

MASS FLOW MASS% MOLAR FOW MOLE%
ACETIC ACID 4261.36363636 99.85 71.0227272727 99.501744
ETHANOL 0 0 0 0
WATER 6.4016479264 0.15 0.355647107 0.4982561
TOTAL 4267.76528429 71.3783743798
5 FEED MIXTURE
ACETIC ACID 4261.3636363636 56.309064 71.0227272727 49.241164
ETHANOL 3267.0454545455 43.170282 71.0227272727 49.241164
WATER 39.4021070633 0.5206539 2.189005948 1.5176719
TOTAL 7567.8111979724 144.2344604934
35328.8270734357
35485.8995979723
6
21
LIMITING REACTANT ETHANOL

CONVERSION 57.737324 %
6 PRODUCT VAPOUR 21 REACTIVE COLUMN BOTTO

MASS FLOWMASS% MOLAR FLO MOLE% MASS FLOW
ACETIC ACID 13501.937 38.048737 225.03228 35.588959 ACETIC ACID 13501.937
ETHANOL 2415.53 6.8070135 52.511521 8.3047214 ETHANOL 1012.1392
ETHYL ACETATE 16572.481 46.701594 188.32364 29.783472 ETHYL ACETA 9296.4983
WATER 2995.9524 8.4426559 166.4418 26.322848 WATER 1495.4356
TOTAL 35485.9 632.30924 TOTAL 25303.479
TOTAL INLET 21 REACTIVE COLUMN BOTTO
ETHANOL 5715.5159 16.106442 124.25035 19.65025 ETHANOL 1015.36
WATER 1704.6536 4.8037491 94.702976 14.97732 WATER 1500.1944
TOTAL 35485.9 632.30924 TOTAL 25384
DEVIATION
7
16
REACTIVE COLUMN BOTTOM 29 PRODUCT COLUMN RECYCLE

MASS% MOLAR FLO MOLE% MASS FLOWMASS % MOLAR FLO MOLE%
53.36 225.03228 51.641679 ACETIC ACID
4 22.003025 5.0493787 ETHANOL
36.74 105.64203 24.24333 ETHYL ACETATE
5.91 83.079757 19.065612 WATER
435.75708 TOTAL 0
53.36 225.74837 51.641679 ACETIC ACID
4 22.073043 5.0493787 ETHANOL
36.74 105.9782 24.24333 ETHYL ACETATE
5.91 83.344133 19.065612 WATER
437.14375 TOTAL 0
80.520707
19
14
15
46 RECOVERY DECANTOR TO REACTOR 7

MASS FLOWMASS % MOLAR FLO MOLE%
ACETIC ACID 0 0 0 0 ACETIC ACID
ETHANOL 1391.1377 56.607 30.242125 61.171805 ETHANOL
ETHYL ACETA 906.24018 36.875959 10.298184 20.830497 ETHYL ACETA
WATER 160.15867 6.517041 8.8977037 17.997697 WATER
TOTAL 2457.5366 49.438012 TOTAL
46 RECOVERY DECANTOR TO REACTOR
ACETIC ACID 0 0 0 0
ETHANOL 1433.1105 56.61 31.154575 61.170125
ETHYL ACETA 933.38249 36.87 10.606619 20.825455
WATER 165.05706 6.52 9.1698367 18.00442
TOTAL 2531.55 50.931031
DEVIATION -74.013418
17
D3604
18
WASH WATER
30
20
PRODUCT VAPOUR 14 CONDENSTE AFTER WASHING

MASS FLOWMASS % MOLAR FLO MOLE% MASS FLOWMASS % MOLAR FLO
0 0 0 0 ACETIC ACID 0 0 0
2543.4599 6.4042223 55.292607 9.2962392 ETHANOL 1417.8015 3.86 30.821771
34522.453 86.92469 392.30061 65.956743 ETHYL ACETA 33883.986 92.25 385.0453
2649.4466 6.6710879 147.19148 24.747018 WATER 1428.8207 3.89 79.378926
39715.36 594.78469 TOTAL 36730.608 100 495.24599
PERCENTAGE OF 14 STREAM GOES TO 16 IS
SPLIT PERCENTAGE
22
D3603
28
S3602
27
31
35
37
16 REFLUX TO D3601 15
MOLE% MASS FLOWMASS % MOLAR FLO MOLE%
0 ACETIC ACID 0 0 ACETIC ACID
6.2235276 ETHANOL 1105.8852 3.86 ETHANOL
77.748291 ETHYL ACETA 26429.509 92.25 ETHYL ACETA
16.028181 WATER 1114.4801 3.89 WATER
TOTAL 28649.874 TOTAL
78 %
16 REFLUX TO D3601
ACETIC ACID 0 0 0 0
ETHANOL 1140.0691 3.86 24.784112 6.2235276
ETHYL ACETA 27246.471 92.25 309.61899 77.748291
WATER 1148.9298 3.89 63.829432 16.028181
TOTAL 29535.47 398.23253
deviation 885.5956
29
39
49
TO ETP
FEED TO WASH COLUMN 20 BOTTOM

0 0 ACETIC ACID 0 0
311.91632 3.86 ETHANOL 1391.1377 16.72
7454.4769 92.25 ETHYL ACETA 886.93351 10.66
314.34055 3.89 WATER 6042.1305 72.62
8080.7338 TOTAL 8320.2018 100
46
45
44
48
19 WASH COLUMN OUTLET 17

ACETIC ACID 0 0 ACETIC ACID
ETHANOL 311.91632 5.16 ETHANOL
ETHYL ACETA 547.66704 9.06 ETHYL ACETA
WATER 5185.3067 85.78 WATER
TOTAL 6044.89 TOTAL
19 WASH COLUMN OUTLET
ACETIC ACID 0 0 0 0
ETHANOL 275.30922 5.16 5.984983 2.2521789
ETHYL ACETA 483.39177 9.06 5.4930883 2.0670764
WATER 4576.749 85.78 254.26383 95.680745
TOTAL 5335.45 265.74191
deviation -709.44002
1 2
18 31 49

0
0
6906.8099 96
287.78375 4
7194.5936
18 WASH WATER
MASS FLOWMASS % MOLAR FLO
ACETIC ACID 0 0
ETHANOL 0 0
ETHYL ACETA 0 0
WATER 5200 100
TOTAL 5200
30 27
ETHANOL 0 0 ETHANOL
ETHYL ACETA 0 0 ETHYL ACETA
WATER 41.250143 100 WATER
41.250143
41.250143
MOLE%
28
0 0 ACETIC ACID 0 0
0 0 ETHANOL 0 0
7549.5032 96 ETHYL ACETA 7549.5032 96
314.56263 4 WATER 314.56263 4
7864.0659 TOTAL 7864.0659
SPLIT RATIO OF 28 / 27
28
ACETIC ACID 0 0
ETHANOL 0 0
ETHYL ACETA 6912 96
WATER 288 4
TOTAL 7200
devaion 664.06586
13818.81
575.78375
29 35
ACETIC ACID ACETIC ACID
ETHANOL ETHANOL
ETHYL ACETATE ETHYL ACETA
WATER WATER
TOTAL 0 TOTAL
100 %
22 31
ETHANOL 0 0 ETHANOL
WATER 575.78375 7.0695208 WATER
37
MASS FLOWMASS % MOLAR FLO MOLE% MASS FLOWMASS %
0 0 ACETIC ACID 0 0
0 0 ETHANOL 1391.1377 16.097443
19.306676 6 ETHYL ACETA 906.24018 10.486488
302.47125 94 WATER 6344.6018 73.416069
321.77793 TOTAL 8641.9797
49
48
0 0 ACETIC ACID
0 0 ETHANOL
6250 100 ETHYL ACETATE
0 0 WATER
6250 TOTAL 0
48
ACETIC ACID
ETHANOL
ETHYL ACETATE
WATER
TOTAL 0
39
MOLAR FLO MOLE% MASS FLOWMASS % MOLAR FLO MOLE%
ACETIC ACID 0 0 0
ETHANOL 5523.2348 57.48 120.07032 64.197807
ETHYL ACETA 3620.2084 37.675309 41.138732 21.99558
WATER 464.80965 4.8372483 25.822758 13.806613
TOTAL 9608.968 99.992558 187.03181
REFLUX RATIO 2.91
44 46
ETHANOL 5523.2348 57.48 120.07032 64.197807 ETHANOL
WATER 464.80965 4.8372483 25.822758 13.806613 WATER
TOTAL 9608.968 99.992558 187.03181 TOTAL
MOLE%
45
ACETIC ACID 0 0
ETHANOL 4132.0971 57.78
ETHYL ACETA 2713.9682 37.95
WATER 304.65098 4.26
TOTAL 7151.4315
49
0 0 0 0 ACETIC ACID 0 0
1391.1377 56.607 30.242125 61.171805 ETHANOL 0 0
906.24018 36.875959 10.298184 20.830497 ETHYL ACETA 0 0
160.15867 6.517041 8.8977037 17.997697 WATER 6184.4431 100
2457.5366 49.438012 TOTAL 6184.4431
3708.0484
MOLE%
ACETIC ACID
ETHANOL
ETHYL ACETATE
WATER
TOTAL
1 5
YELLOW FLOW RATES ARE ASSUMED VALUE AND OTHER ARE CAALCULATED WITH ASSUME VALUES
1 FEED ETHANOL
ACETIC ACID 0 0 0 0
ETHANOL 4247.1590909091 99 92.3295454545 97.483589
WATER 42.9005968779 1 2.3833664932 2.5164114
TOTL 4290.059687787 94.7129119478
CP 0.663
LH
TEMP 50
Q 142215.47865014 0 0 0 0
ACTUAL CAPACITY 150 MTPD 6250 kg/hr

PLANT LOAD 130 % 8125 kg/hr
8124.9973757303
5
SSUME VALUES
2 FEED ACETIC ACID

MASS FLOW MASS% MOLAR FOW MOLE%
ACETIC ACID 5539.77272727 99.85 92.3295454545 99.501744
ETHANOL 0 0 0 0
WATER 8.3221423044 0.15 0.4623412391 0.4982561
TOTAL 5548.09486958 92.7918866937
CP 0.5213
LH
TEMP 50
Q 144611.092776 0 0 0 0
0.5280073462 0.6828424455
0.5227272727
5 FEED MIXTURE
ACETIC ACID 5539.7727272727 56.309064 92.3295454545 49.241164
ETHANOL 4247.1590909091 43.170282 92.3295454545 49.241164
WATER 51.2227391822 0.5206539 2.8457077323 1.5176719
TOTAL 9838.1545573641 187.5047986414
CP 0.5830901919
LH
TEMP 50
Q 286826.571425665 0 0 0 0
6
21
LIMITING REACTANT ETHANOL

CONVERSION 57.737324 %
6 PRODUCT VAPOUR 21 REACTIVE COLUMN BOTTO

ETHANOL 3142.9707 6.8121687 68.32545 8.3107071 ETHANOL 1315.4093
WATER 3896.2252 8.4447951 216.45696 26.328555 WATER 1943.5173
TOTAL 46137.593 822.13762 TOTAL 32885.234
CP 0.34124 CP 0.5731
LH 161.162 LH
TEMP 106 TEMP 97.52
Q 9104490 0 0 0 0Q 1837913.3
TOTAL INLET 21 REACTIVE COLUMN BOTTO

ETHANOL 7436.7527 16.11864 161.66854 19.664413 ETHANOL 1319.968
WATER 2216.0496 4.8031323 123.11387 14.974849 WATER 1950.2527
TOTAL 46137.593 822.13762 TOTAL 32999.2
CP CP 0.5731
LH LH
TEMP TEMP 97.52
Q 2210909.4 0 0 0 0Q 1844282.8
DEVIATION
CP 142.118 J/K
HEAT OF REACTION -7078 kJ/kmol
ethanol reacted 93.343087 kmol
HEAT OF REACTION -660682.37 Kj

-157793.74 kcal/hr
Qin 2210909.4 kcal/hr

Qout 9104490 kcal/hr
REBOILER DUTY 6735786.8 kcal/hr

LATENT HEAT 505 kcal/hr
steam flow 13338.192 kg/hr

7
16

53.36 292.45934 51.641679 ACETIC ACID
4 28.595855 5.0493787 ETHANOL
36.74 137.29585 24.24333 ETHYL ACETATE
5.91 107.97318 19.065612 WATER
566.32423 TOTAL 0
CP
LH
TEMP
0 0 0 0Q 0 0 0 0

53.36 293.47289 51.641679 ACETIC ACID
4 28.694957 5.0493787 ETHANOL
36.74 137.77166 24.24333 ETHYL ACETATE
5.91 108.34737 19.065612 WATER
568.28688 TOTAL 0
CP
LH
TEMP
0 0 0 0Q 0 0 0 0
-113.96646
E3601 E3603 E3601B

6 PRODUCT VAPOUR
MASS FLOW
ACETIC ACID 17547.561
ETHANOL 3142.9707
ETHYL ACETA 21550.837
WATER 3896.2252
TOTAL 46137.593
CP 0.34124
LH 161.162
TEMP 106
Q 9104490
INLET OUTLET
ETHANOL FE 4290.0597 ETHYL ACET 8124.9974
ACETIC ACID 5548.0949 WASTE WAT 8473.15
WASH WATE 6760
TOTAL 16598.155 16598.147

0
19
14
15
46 RECOVERY DECANTOR TO REACTOR 7

ETHANOL 1811.2878 56.607 39.375823 62.854424 ETHANOL
WATER 169.53677 5.2984222 9.4187093 15.034798 WATER
TOTAL 3199.7595 62.646064 TOTAL
CP 0.5386 CP
LH LH
TEMP 50 TEMP
0Q 86169.522 0 0 0 0 0Q
46 RECOVERY DECANTOR TO REACTOR

ACETIC ACID 0 0 0 0
ETHANOL 1869.6256 56.81 40.644035 61.260765
ETHYL ACETA 1212.739 36.85 13.781125 20.771616
WATER 214.57418 6.52 11.920788 17.96762
TOTAL 3291.015 66.345948
CP 0.5386
LH
TEMP 50
0Q 88627.034 0 0 0 0 0 0
DEVIATION -91.255539
D3601 D3603
Qin-Qout -42194.226 QIN
QOUT
13 QOUT-QIN
MASS FLOW COOLING WATER
ACETIC ACID 17547.561 LATENT HEA
ETHANOL 3142.9707 H20 802602.38 FLOW
ETHYL ACETA 21550.837 TOTAL 802602.38
WATER 3896.2252 CP 1
TOTAL 46137.593 TIN 33
CP 0.4675 TOUT 43
LH 0 Q 8026023.8
TEMP 50
Q 1078466.2
17
D3604
18
WASH WATER
30
20
PRODUCT VAPOUR 14 CONDENSTE AFTER WASHING

3309.6512 6.4084414 71.94894 9.301549 ETHANOL 1843.0808 3.86 40.066973
44889.214 86.918494 510.10471 65.946266 ETHYL ACETA 44047.72 92.25 500.54227
3446.3166 6.6730651 191.46203 24.752185 WATER 1857.4052 3.89 103.18918
51645.182 773.51568 TOTAL 47748.206 100 643.79842
0.3479 CP 0.4598
132.99 LH
73.339 TEMP 50
8186000.9 0 0 0 0Q 1097731.3 0 0
PERCENTAGE OF 14 STREAM GOES TO 16 IS
SPLIT PERCENTAGE
0 0 0 0 0 0 0 0 0
D3602
451683.26 kcal/hr QIN 1041677.4 kcal/hr
2387409.8 kcal/hr QOUT 3878245.9 kcal/hr
1935726.6 kcal/hr QOUT-QIN 2836568.5 kcal/hr
505 kcal/kg LATENT HEA 505 kcal/kg

3833.1219 kg/hr FLOW 5616.9674 kg/hr
22 26
MASS FLOW MASS FLOW
ACETIC ACID 0 ACETIC ACID 0
ETHANOL 0 ETHANOL 0
ETHYL ACETA 9022.9253 ETHYL ACETA 9022.9253
WATER 764.91717 WATER 764.91717
TOTAL 9787.8424 TOTAL 9787.8424
CP 0.3428 CP 0.520566
LH 124 LH
TEMP 70.9 TEMP 50
Q 1451581.3 Q 254760.9
22
D3603
28
S3602
27
31
35
38
16 REFLUX TO D3601 15
0 ACETIC ACID 0 0 0 0 ACETIC ACID
6.2235276 ETHANOL 1474.4646 3.86 32.053578 6.2235276 ETHANOL
77.748291 ETHYL ACETA 35238.176 92.25 400.43382 77.748291 ETHYL ACETA
16.028181 WATER 1485.9242 3.89 82.551343 16.028181 WATER
TOTAL 38198.565 515.03874 TOTAL
CP 0.4593 CP
LH LH
TEMP 50 TEMP
0 Q 877230.04 0 0 0 0Q
80 reflux ration 0.5287229 1.3877052
16 REFLUX TO D3601
ACETIC ACID 0 0 0 0
ETHANOL 1482.0899 3.86 32.219345 6.2235276
ETHYL ACETA 35420.412 92.25 402.50469 77.748291
WATER 1493.6087 3.89 82.978262 16.028181
TOTAL 38396.111 517.70229
CP 0.4593
LH
TEMP 50
0 0Q 881766.69 0 0 0 0 0
39
MASS FLOW
MASS FLOW COOLING WATER ACETIC ACID 0
ETHANOL 7191.357
H20 119682.04 ETHYL ACETA 4752.5732
TOTAL 119682.04 WATER 566.19815
CP 1 TOTAL 12511.059
TIN 33 CP 0.78
TOUT 43 LH 179.58
Q 1196820.4 TEMP 73.72
Q 2966142
29
39
49
TO ETP
FEED TO WASH COLUMN 20 BOTTOM

368.61615 3.86 8.0133946 6.2235276 ETHANOL 1811.2878 16.72 39.375823
8809.544 92.25 100.10845 77.748291 ETHYL ACETA 1154.8043 10.66 13.122776
371.48104 3.89 20.637836 16.028181 WATER 7866.9691 72.62 437.05384
9549.6412 128.75968 TOTAL 10833.061 100 489.55244
0.4598 CP 0.821
LH
50 TEMP 50
219546.25 0 0 0 0Q 444697.16 0 0
0 0 0 0 0 0 0 0 0
43
MASS FLOW
ACETIC ACID 0 COOLING WATER
ETHANOL 7191.357
ETHYL ACETA 4752.5732 H20 262919.41
WATER 566.19815 TOTAL 262919.41
TOTAL 12511.059 CP 1
CP 0.53864 TIN 33
LH TOUT 43
TEMP 50 Q 2629194.1
Q 336947.85
46
45
44
48
19 WASH COLUMN OUTLET 17

ACETIC ACID 0 0 0 ACETIC ACID
ETHANOL 368.61615 5.16 8.0133946 ETHANOL
ETHYL ACETA 647.22138 9.06 7.3547884 ETHYL ACETA
WATER 6127.8863 85.78 340.43813 WATER
TOTAL 7143.7238 355.80631 TOTAL
CP 0.97588 CP
LH LH
TEMP 50 TEMP
0 0Q 348570.86 0 0 0 0Q
19 WASH COLUMN OUTLET

ACETIC ACID 0 0 0 0
ETHANOL 357.90199 5.16 7.780478 2.2521789
ETHYL ACETA 628.4093 9.06 7.1410148 2.0670764
WATER 5949.7737 85.78 330.54298 95.680745
TOTAL 6936.085 345.46448
CP 0.9758
LH
TEMP 50
0 0Q 338411.59 0 0 0 0 0
deviation 207.63884
0
0
8162.3226 95.31
390.51717 4.56
8563.973
0.51
50
218381.31 0 0 0 0 0 0 0 0
18 WASH WATER
ACETIC ACID 0 0
ETHANOL 0 0
ETHYL ACETA 0 0
WATER 6760 100
TOTAL 6760
CP 1
LH
TEMP 40
0 0 0 0 0Q 270400
30 27
ETHANOL 0 0 ETHANOL
ETHYL ACETA 0 0 ETHYL ACETA
WATER 613.07756 100 WATER
CP 1 CP
LH LH
TEMP 40 TEMP
0 0Q 24523.102 0 0 0 0Q
MOLE%
28
0 0 ACETIC ACID 0 0
0 0 ETHANOL 0 0
8958.7947 96 ETHYL ACETA 8958.7947 96
373.28311 4 WATER 373.28311 4
9332.0778 TOTAL 9332.0778
0.5 CP 0.5
LH
50 TEMP 50
233301.95 0 0 0 0Q 233301.95 0 0
SPLIT RATIO OF 28 / 27
28
ACETIC ACID 0 0
ETHANOL 0 0
ETHYL ACETA 8985.6 96
WATER 374.4 4
TOTAL 9360
CP 0.5
LH
TEMP 50
Q 234000 0 0
29 35
ACETIC ACID ACETIC ACID
ETHANOL ETHANOL
ETHYL ACETATE ETHYL ACETA
WATER WATER
TOTAL 0 TOTAL
CP CP
LH LH
TEMP TEMP
0 0Q 0 0 0 0 0Q
100
22 31
ETHANOL 0 0 ETHANOL
WATER 764.91717 7.8149722 WATER
CP 0.3428 CP
LH 124 LH
TEMP 70.9 TEMP
0 0Q 1451581.3 0 0 0 0Q
38
MASS FLOWMASS % MOLAR FLO MOLE% MASS FLOWMASS %
0 0 ACETIC ACID 0 0
0 0 ETHANOL 1811.2878 15.218472
64.130529 6 ETHYL ACETA 1218.9349 10.241512
1004.7116 94 WATER 8871.6807 74.540016
1068.8421 TOTAL 11901.903
0.9737 CP 0.8979
LH
50 TEMP 74.01
52036.58 0 0 0 0 0Q 790924.08 0
48
0 0 ACETIC ACID
0 0 ETHANOL
8124.9974 100 ETHYL ACETATE
0 0 WATER
8124.9974 TOTAL 0
0.3416 CP
87.096 LH
82.21 TEMP
935828.55 0 0 0 0Q 0 0 0
ACETIC ACID
ETHANOL
ETHYL ACETATE
WATER
TOTAL 0
39
ACETIC ACID 0 0 0
ETHANOL 7191.357 57.48 156.33385 64.655316
ETHYL ACETA 4752.5732 37.986976 54.006514 22.335587
WATER 566.19815 4.5255811 31.455453 13.009097
TOTAL 12511.059 99.992558 241.79581
CP 0.78
REFLUX RATIO 2.91 LH 179.58
TEMP 73.72
0 0Q 2966142 0 0 0 0
44 46
ETHANOL 7191.357 57.48 156.33385 64.655316 ETHANOL
WATER 566.19815 4.5255811 31.455453 13.009097 WATER
TOTAL 12511.059 99.992558 241.79581 TOTAL
CP 0.5386 CP
LH LH
TEMP 50 TEMP
0 0Q 336922.83 0 0 0 0Q
45
ACETIC ACID 0 0 0 0
ETHANOL 5380.0692 57.78 116.95803 65.285061909
ETHYL ACETA 3533.6384 37.95 40.154981 22.414198955
WATER 396.66138 4.26 22.036743 12.300739137
TOTAL 9311.3 179.14975
CP 0.5386
LH
TEMP 50
Q 250753.31 0 0 0 0 0 0
49
0 0 0 0 ACETIC ACID 0 0
1811.2878 56.607 39.375823 62.854424 ETHANOL 0 0
1218.9349 38.094578 13.851532 22.110778 ETHYL ACETA 0 0
169.53677 5.2984222 9.4187093 15.034798 WATER 8702.1439 100
3199.7595 62.646064 TOTAL 8702.1439
0.5386 CP 1
LH
50 TEMP 104.8137
86169.522 0 0 0 0Q 912103.9 0 0
50
ACETIC ACID 0 0
ETHANOL 0 0
ETHYL ACETA 0 0
WATER 8702.1439 100
TOTAL 8702.1439 0
CP 1
LH
TEMP 77.728388
0 Q 676403.62
E36015
1A 1
FLOW 4290.0597 FLOW 4290.0597
CP 0.663 CP 0.794
LATENT HEA 0 LATENT HEAT
TEMP 50 TEMP 25
Q 142215.48 Q 85157.685
0
E60216
2A 1
FLOW 5548.0949 FLOW 5548.0949
CP 0.5213 CP 0.50733
LATENT HEA 0 LATENT HEAT
TEMP 50 TEMP 25
Q 144611.09 Q 70367.874
E3608
37
MASS FLOWMASS %
ACETIC ACID 0 0
ETHANOL 1811.2878 15.218472
ETHYL ACETA 1218.9349 10.241512
WATER 8871.6807 74.540016
TOTAL 11901.903
CP 0.933
LH
TEMP 50
Q 555223.79
51
FLOW 8702.1439
CP 1
LATENT HEAT
TEMP 71.171637
Q 619345.82
52
FLOW 8702.1439
CP 1
LATENT HEAT
TEMP 62.640036
Q 545102.61
38
ACETIC ACID 0 0
ETHANOL 1811.2878 15.218472
ETHYL ACETA 1218.9349 10.241512
WATER 8871.6807 74.540016
TOTAL 11901.903
CP 0.8979
LH 0
TEMP 74.01
Q 790924.08
46 29
1 5
MIXER
REACTOR
V3601
DIST.
D3601
14
ACTOR SPLITTER
601
21
15
S3601
19 D3604
20
22
D3603
17
28
18 S3602
WASH WATER
30
31
T3607 35
29
39
D3602
S3602
SPLITT
27 ER
49
TO ETP
37
46
45
S3603
SPLITTER
44
48

Ea MB Harsh Patel New

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1 5

3586 4456 4517 12559

6250 6135 12385

2 FEED ACETIC ACID

LIMITING REACTANT ETHANOL

6 PRODUCT VAPOUR 21 REACTIVE COLUMN BOTTO

REACTIVE COLUMN BOTTOM 29 PRODUCT COLUMN RECYCLE

46 RECOVERY DECANTOR TO REACTOR 7

PRODUCT VAPOUR 14 CONDENSTE AFTER WASHING

FEED TO WASH COLUMN 20 BOTTOM

19 WASH COLUMN OUTLET 17

MASS FLOWMASS % MOLAR FLO MOLE%

ACTUAL CAPACITY 150 MTPD 6250 kg/hr

2 FEED ACETIC ACID

LIMITING REACTANT ETHANOL

6 PRODUCT VAPOUR 21 REACTIVE COLUMN BOTTO

TOTAL INLET 21 REACTIVE COLUMN BOTTO

HEAT OF REACTION -660682.37 Kj

Qin 2210909.4 kcal/hr

REBOILER DUTY 6735786.8 kcal/hr

steam flow 13338.192 kg/hr

REACTIVE COLUMN BOTTOM 29 PRODUCT COLUMN RECYCLE

REACTIVE COLUMN BOTTOM 29 PRODUCT COLUMN RECYCLE

E3601 E3603 E3601B

ETHANOL FE 4290.0597 ETHYL ACET 8124.9974

ACETIC ACID 5548.0949 WASTE WAT 8473.15

WASH WATE 6760

TOTAL 16598.155 16598.147

46 RECOVERY DECANTOR TO REACTOR 7

46 RECOVERY DECANTOR TO REACTOR

PRODUCT VAPOUR 14 CONDENSTE AFTER WASHING

PERCENTAGE OF 14 STREAM GOES TO 16 IS

1935726.6 kcal/hr QOUT-QIN 2836568.5 kcal/hr

505 kcal/kg LATENT HEA 505 kcal/kg

80 reflux ration 0.5287229 1.3877052

FEED TO WASH COLUMN 20 BOTTOM

19 WASH COLUMN OUTLET 17

19 WASH COLUMN OUTLET

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