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a b s t r a c t
In the last decades, Information and Communications Technologies (ICT) have been promoting the creation and
adoption of new learning and teaching styles. Virtual laboratories, by overcoming some limitations of conventional
hands-on experiments, have been adopted as a complement or in substitution of laboratory sessions.
This paper describes the design and implementation of two virtual labs for biochemical engineering education
intended for students at the BSc degree.
One of the virtual labs is intended to fully replace the hands-on experiment and consists on the determination of
the correlation between oxygen transfer rate, aeration rate and agitation power in a reactor. The other virtual lab
consists on the determination of the residence time distribution (RTD) in continuous stirred tanks series and was
implemented to support the physical experiments rather than replacing them.
The virtual labs provide the students a learning platform covering the fundamentals underlying the experiment,
its pre-visualization and simulation. The effectiveness of the implemented system was evaluated through direct
experimentation and survey (through questionnaires) with students taking the chemical technology lab course. For
the RTD virtual Lab, and based on specific learning outcomes, teachers could assess significant improvement in
students’ performance in the lab and also a more thorough discussion of the results in the reports. The survey
results show that, in average, considering the two virtual labs and several classes, 93% of the students consider the
virtual labs of great utility.
© 2010 The Institution of Chemical Engineers. Published by Elsevier B.V. All rights reserved.
∗
Corresponding author. Tel.: +351 253 604400; fax: +351 253 678986.
E-mail address: luciliad@deb.uminho.pt (L. Domingues).
Received 3 April 2009; Received in revised form 11 November 2009; Accepted 4 February 2010
1749-7728/$ – see front matter © 2010 The Institution of Chemical Engineers. Published by Elsevier B.V. All rights reserved.
doi:10.1016/j.ece.2010.02.001
education for chemical engineers 5 ( 2 0 1 0 ) e22–e27 e23
Fig. 1 – Web platform structure of the “Determination of the Residence Time Distribution in Continuous Tank Series” virtual
lab.
ities. The portal http://vlabs.uminho.pt allows access to the spreadsheet (Ferreira et al., 2004) to determine the model
virtual laboratories where animations, videos and control of parameters—the Peclet number (for the dispersion model) and
virtual experiments can be handled, providing extra digital the number of tanks (for the tanks in series model) from the
content for laboratory classes and for curricular units with- best fits of their experimental data. The experimental RTD is
out an assigned laboratory schedule. Contents and didactic obtained using methylene blue as tracer. After a pulse injec-
material are currently being developed for the virtual labora- tion, its concentration profile is followed at the tanks’ outlet by
tories, in which the students can explore details on various spectrophotometry. This experiment has been implemented
laboratory-scale equipments like microscopes and reactors, in the CTL course for many years, as a traditional lab experi-
as well as come in contact with intangible realities like the ment. It was adapted for the VLabs because, even though it is
mechanisms behind catalytic reactions. very easy and safe to perform in the laboratory, the students’
The Biological Engineering Department is engaged in this written reports generally showed a insufficient knowledge of
VLabs Project. The adoption of these tools in teaching activ- the RTD concepts, as well as strong limitations in the discus-
ities and their offering over the Internet will permit a better sion of the results obtained from their experiments.
preparation of the students before attending the laboratory
classes or the simulation and observation of certain key- 2.1.2. Virtual lab goals and gains
experiments. The main goal with this virtual lab was to provide a web
This paper describes the design and implementation of two support to the traditional lab experiment, thus improving stu-
virtual labs for biochemical engineering education: dent’s effectiveness and autonomy in the laboratory class, in
data analysis and report writing.
- “Determination of the Residence Time Distribution in Con- Even though this virtual lab was not designed to replace the
tinuous Tank Series—RTD”; hands-on experiment, it reduced costs as it allowed decreas-
- “Determination of the Correlation between oxygen transfer ing the time needed to conduct the experiment, decreasing
rate, aeration rate and agitation power—A&A”. the number of repetitions (due to errors), and also eliminating
the need for full-time supervision.
These virtual labs were designed for the course “Chem-
ical Technology Laboratory” (CTL), taught to the third year 2.1.3. Web platform description
students of the Biological Engineering five-years integrated The web platform structure is presented in Fig. 1 and is divided
Master degree and were first implemented in 2006. The two into three main sections: theory fundamentals, experiment
virtual labs have distinct goals: while A&A aims at replac- and simulation.
ing the hands-on experiment, RTD will support the hands-on In the theory fundamentals section, the theory underlying
experiment. the experiment is presented with animations and illustra-
tions. Also, a self-evaluation test can be done and some
2. Implementation and results exercises are proposed.
In the experiment section, the safety procedures that stu-
2.1. Determination of the residence time distribution dents must learn and practice once in the lab are given. Also,
(RTD) in continuous tank series a detailed description of the experimental set-up is provided
through an interactive platform, where the students can view
2.1.1. Experiment description details on specific equipment just by placing the computer
This experiment aims at the experimental determination of mouse on top of the corresponding picture. To enhance the
the residence time distribution in a cascade of 1, 2, 3, and 4 visual experience, parts of the experimental procedure are
stirred tanks (see for example Fogler, 1986; Levenspiel, 1972 detailed in videos that show some relevant aspects of the
for the fundamentals of this work) and the application of experimental assay, accompanied by written text and sound,
the “Tanks in Series Model” to a series of continuous stirred explaining what is being executed. In this section, the exper-
tank reactors. Students are also encouraged to apply the “Dis- imental protocol and a template for lab data registration are
persion Model” and to use the Solver feature of the Excel® also available for download, so that students can take it to the
e24 education for chemical engineers 5 ( 2 0 1 0 ) e22–e27
Fig. 2 – Web platform structure of the “Determination of the correlation between oxygen transfer rate, aeration rate and
agitation power” virtual lab.
lab. Also, there is a calculation procedure implemented in a In the simulation section the students can perform RTD
questionnaire format so that the students can think by them- experiments using either the tanks in series model or the dis-
selves before the answer is provided by the software. Finally, persion model. They can set the volumetric flow rate, the tank
a test-quiz has to be answered by the students. This test is volume and model parameters (the number of tanks for the
meant to evaluate if the students are prepared to do the lab- tanks in series model and the Peclet number for the disper-
oratory experiment. Once the students complete the test, the sion model). Students can also use the simulation section to
results are sent automatically to the teacher by email. If a score determine the most suitable time interval for sample collec-
above the 50% threshold is obtained, the student is authorized tion, a relevant parameter for performing the RTD laboratory
to do the experiment. experiments.
Fig. 3 – Experiment platform for the “Determination of the correlation between oxygen transfer rate, aeration rate and
agitation power” virtual lab.
education for chemical engineers 5 ( 2 0 1 0 ) e22–e27 e25
Fig. 4 – Students’ survey results for the RTD virtual lab (2006/2007; 2007/2008 and 2008/2009 results). Question 1: The RTD
virtual Lab contents have led to a better understanding of the concepts necessary for the execution of the experimental
work; 2: the RTD virtual Lab contents have made the execution of the experimental work easier; 3: the RTD virtual Lab
contents have made the calculation procedure easier; 4: the RTD virtual Lab contents have helped in the analysis and
interpretation of the results; 5: the RTD virtual Lab portal is easy to use?; 6: the RTD virtual Lab portal is well organized; 7:
the RTD virtual Lab portal is complete; 8: in general, I consider the RTD virtual Lab portal of great utility.
2.2. Determination of correlations between oxygen are more than adequate to perform the simulations using any
transfer rate, aeration rate and agitation power (A&A) computer with an Internet connection.
Fig. 5 – Students survey results in aeration and agitation virtual lab (2006/2007 results). Question 1: The A&A virtual Lab
contents have led to a better understanding of the concepts necessary for the execution of the experimental work; 2: the
virtual experiment replaces the hands-on experiment completely, there is no need to do the experiment on the lab.; 3: the
A&A virtual Lab contents have made the calculation procedure easier; 4: the A&A virtual Lab contents have helped in the
analysis and interpretation of the results; 5: the A&A virtual Lab portal is easy to use; 6: the A&A virtual Lab portal is well
organized; 7: the A&A virtual Lab portal is complete; 8: in general, I consider the A&A virtual Lab portal of great utility.
(turn on/off water, nitrogen, air supplies and stirrer). On the In terms of organization and skills at the laboratory ses-
right-hand side a real-time graphical illustration of dissolved sion, it was possible to assess an increase from 60 to 90% in the
oxygen versus time is shown. A new experiment with a dif- number of students that attained the following learning out-
ferent air flow rate can only be performed after the dissolved come: “to plan and execute an experiment applying Chemical
oxygen concentration had dropped to zero (after turning on Reaction Engineering Concepts of RTD”. This evaluation was
again the nitrogen supply). The results can be downloaded in based on the comparison of the average marks obtained by the
an Excel® worksheet and a report template is also available for students during the laboratory session, before (average of five
download. years) and after the virtual lab implementation. The advan-
tages of using virtual labs as preparation tools for laboratory
sessions have also been noticed by others (Martinez-Jimenez
3. Assessment/students feedback
et al., 2003; Woodfield et al., 2005; Dalgarno et al., 2009). Con-
cerning the results interpretation analysis and discussion, it
Both virtual labs (RTD and A&A) were first implemented in
was possible to quantify an increase from 55 to 80% in the
the CTL course in 2005/2006. In this first year implemen-
number of students that attained the following learning out-
tation of the virtual labs platform, instructors could assess
come: “to interpret, analyze and discuss experimental results
the improvement of student’s performance at three levels: (i)
in a quantitative way”. This evaluation was based on the com-
preparation of laboratory session assessed through a written
parison of the average marks obtained by the students on the
questionnaire; (ii) organization and experimental skills at the
discussion section of the written report, before (average of
laboratory session; and (iii) results interpretation analysis and
five years) and after the virtual labs implementation. In the
discussion. These evaluations were quantitatively compared
first year of implementation (2005/2006), students feedback
with the learning outcomes obtained in the previous five years.
was very positive but no assessment was made. Students per-
In terms of preparation of laboratory sessions, a com-
ception was evaluated by a survey (through questionnaires)
parison between the former and the actual method is not
performed with students taking the CTL course in 2006/2007,
straightforward. The former method was based on oral exam-
and 2007/2008 and 2008/2009 for the RTD virtual lab and in
inations in the laboratory class, before starting the session,
2006/2007 for the A&A virtual lab. Due to Bologna implemen-
whereas now the students have to answer a questionnaire on
tation in the curriculum reform, this virtual lab has not been
the web. The fundamental difference is the actual possibility
used in CTL classes after 2006/2007.
of accessing all kind of information sources while answering
Data from the survey performed in 2006/2007, 2007/2008
the questionnaire. Considering the inherent advantages and
and 2008/2009 for the RTD virtual lab, in a total of 121 students,
disadvantages of both approaches, it is still not evident which
are presented in Fig. 4.
one is better for learning purposes.
education for chemical engineers 5 ( 2 0 1 0 ) e22–e27 e27
The students have considered that the virtual lab portal Acknowledgments
is easy to use (95% agreed or completely agreed) and well
organized (93% agreed or completely agreed), and 79% have This project is being supported by strategic funds from “Pro-
considered that it is complete. The majority of the students grama Qualidade” of the University of Minho. The students
have agreed that the RTD virtual Lab contents led to a bet- Cristiana Mota and Helena Venda are acknowledged for their
ter understanding of the concepts necessary for the execution contribution in the design of the A&A virtual lab platform.
of the experimental work (97%) and that it made easier the Doctor Anthony Danko is acknowledged for English proofread-
execution of the experimental work (94%). They have also con- ing of the manuscript.
sidered (88%) that the virtual lab portal helped in the analysis
and interpretation of the results. Only 83% have agreed that References
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