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Journal of Materials Processing Technology 238 (2016) 73–80

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Journal of Materials Processing Technology


journal homepage: www.elsevier.com/locate/jmatprotec

Tool assisted friction welding: A FSW related technique for the linear
lap welding of very thin steel plates
T. Mira-Aguiar a , D. Verdera b , C. Leitão a , D.M. Rodrigues a,c,∗
a
CEMUC, Department of Mechanical Engineering, University of Coimbra, Rua Luís Reis Santos, 3030-788 Coimbra, Portugal
b
AIMEN, Relva 27A Torneiros, 36410 Porriño, Spain
c
ISISE, Department of Mechanical Engineering, University of Coimbra, Rua Luís Reis Santos, 3030-788 Coimbra, Portugal

a r t i c l e i n f o a b s t r a c t

Article history: A Friction Stir Welding (FSW) related technique, which will be labelled Tool Assisted Friction Welding
Received 4 March 2016 (TAFW), is presented in the current paper. Using this technique, linear lap welding of very thin steel plates
Received in revised form 14 June 2016 is obtained by using a non-consumable columnar tool, with a featureless shoulder, to generate heat by
Accepted 3 July 2016
friction with the components to be welded, as in FSW, and also to promote the joining of the plates,
Available online 5 July 2016
under pressure, as in Friction Welding (FW). The joining mechanisms, as well as the thermomechanical
conditions developed during welding, will be discussed based on the metallurgical analysis of similar
Keywords:
welds produced in two steels: a galvanised low carbon steel (DX51D) and a mild steel (DC01). Mechanical
FSW
Steel
testing, using Digital Image Correlation (DIC) for strain data acquisition, enabled to assess welds strength
Lap joining and plastic properties. The results obtained prove that the TAFW technique enables to obtain very good
Microstructure quality welds, for both base materials, at a very high welding speed and low tool wear/damage. An
Pinless tool important influence of the galvanised coating of the DX51D steel on the welding conditions and weld
microstructure was also observed.
© 2016 Elsevier B.V. All rights reserved.

1. Introduction labelled as Tool Assisted Friction Welding (TAFW) by the current


authors.
In the present paper a Friction Stir Welding (FSW) related tech- The use of tools without pin, in lap and butt joining, has been
nique, for the lap joining of very thin steel plates, is presented. The previously studied by other authors. Zhang et al. (2010) performed
main operation principles of this technique are very similar to that friction stir lap welding of 1.8 mm thick aluminium plates using
of the FSW technology, i.e., a non-consumable cylindrical tool, ani- a simple columnar tool without a pin. The microstructural analy-
mated of rotation and translation speeds, is used to generate heat sis revealed a black bond line, at the central region of the weld,
by friction with the upper surface of the plates to be welded. How- and traces of vertical base materials intermixing resulting in the
ever, while in FSW, the tool has a pin to promote base materials formation of multiple bonded micro-zones. The black line disap-
stirring/mixing during welding, in the current technique, a pinless peared at the advancing side (AS) of the weld, where ring structures
tool, with a flat featureless surface, is used. The absence of a pin, were observed together with a hooking defect. In spite of this, the
or non-flat shoulder features, leads to completely different joining authors found that the lap welds failed at the retreating side (RS),
mechanism between the overlapped plates. In fact, instead of the in tensile-shear testing, due to top sheet thinning. It was concluded
base materials stirring, characteristic of FSW, no mixture of base that the formation of a vertical intermixed ring, at the advancing
materials is observed to take place when using the pinless tool, side, was the main joining mechanism.
with the connection being achieved through a combination of heat In order to improve base materials stirring during the welding
and pressure, in the same way as it happens in forging and fric- with pinless tools, Tozaki et al. (2010) and Bakavos et al. (2011)
tion welding. Based on this knowledge, this joining technique was tested pinless tools with grooved surfaces in friction stir spot weld-
ing of aluminium alloys. Tozaki et al. (2010) concluded that the
grooves on the pinless tool surface played an important role in the
material stirring. The welds obtained with the grooved surface tool
revealed to have higher tensile-shear strength than those obtained
∗ Corresponding author at: Department of Mechanical Engineering, University of
with the tool with a pin. The use of a plain pinless tool resulted
Coimbra, Rua Luís Reis Santos, 3030-788 Coimbra, Portugal.
E-mail address: dulce.rodrigues@dem.uc.pt (D.M. Rodrigues).
in low strength welds. Bakavos et al. (2011), who tested several

http://dx.doi.org/10.1016/j.jmatprotec.2016.07.006
0924-0136/© 2016 Elsevier B.V. All rights reserved.
74 T. Mira-Aguiar et al. / Journal of Materials Processing Technology 238 (2016) 73–80

pinless tools, with and without grooved surfaces, concluded that Table 1
Nominal chemical composition of the base materials (wt-%).
the grooved surface tools promoted material flow between the
overlapped plates, giving rise to hooking defects. On the other hand, Fe C Si Mn S P
for the welds obtained with the featureless surface tool, the orig- DC01 Bal. 0.078 0.004 0.314 0.016 0.012
inal interface line remained intact and no traces of material flow DX51D Bal. 0.05 0.02 0.35 0.01 0.008
were seen by the authors. The authors concluded that the strength
of the welds was dependent on the surface groove configuration,
and that the welds produced with the feature and featureless sur- ing interface (Van der Rest et al., 2014), were pointed as the main
face tools could display similar strength values, depending on the mechanisms promoting the joining. This paper demonstrates that
welding parameters. excellent quality steel lap welds can be performed using a fea-
Zhang et al. (2011) also used a pinless tool for the dissimilar lap tureless pinless tool with no interlayer material melting, dissimilar
joining of 1. 8 mm thick aluminium and low carbon steel plates. material reactions nor vertical material intermixing. As shown in
However, these authors used a zinc foil (0.1 mm thick) in between the following sections, the TAFW technique, which is based in very
the two overlapped plates. The zinc foil melted during the process simple thermo-mechanical principles, allows for the creating of
and the connection between the plates resulted from an Al-Zn-Fe high strength steel welds at much higher welding speeds than that
metallurgical reaction, instead of the mechanical mixing between used in current friction stir lap welding literature.
the overlapped materials. Based on this conclusion the authors Since no base materials stirring takes place during TAFW, this
labelled this technique as friction stir brazing. technique enables to overcome some lap welding defects typical
Kuang et al. (2015) and Khorrami et al. (2015) also used friction of the FSW process, such as the hooking, at one or both sides of
stir brazing related techniques for the lap welding of aluminium- the weld, and the keyhole left by the tool at the end of the weld.
copper and copper–copper joints, respectively. Kuang et al. (2015) According to Rai et al. (2011), another important FSW limitation
used a zinc foil insert (0.2 mm thick) in between the 2 mm thick consists in the tool destruction due to the pin wear/rupture dur-
aluminium and copper plates, identifying zinc melting as the main ing the welding of high melting point materials, such as steels and
bonding mechanism. Khorrami et al. (2015) inserted a Pb-Sn foil in titanium alloys. By supressing the pin, in TAFW, tool life is maxi-
between the 3 mm thick copper overlapped plates. Since the Pb- mized since the only failure mechanism becomes the tool wear at
Sn foil melting was found to promote the joining of the copper the shoulder/base materials contact surface.
sheets, the authors labelled the technique as friction stir soldering.
The authors tested the friction stir soldering technique with pin and 2. Experimental procedure
pin-free tools, concluding that higher weld strengths were obtained
when welding with tools with a pin, i.e. FSW. In this work, similar lap welds in a galvanised low carbon steel
Finally, Van der Rest et al. (2014) performed dissimilar lap weld- DX51D (0.11%C) and a mild steel DC01 (0.078%C), both 1 mm thick,
ing between a microalloyed ultralow carbon steel (0.8 mm thick) were performed. The nominal chemical compositions of the base
and aluminium alloys 1050 and 2024 using a pinless tool. The materials are shown in Table 1. The welds were performed in posi-
higher-melting point material was placed at the top of the joint. tion control, using a carbide tungsten pinless tool with 16 mm
According to the authors, the heat generated at the contact inter- diameter and a flat featureless surface (Fig. 1b). The tool was tilted
face between the pinless tool and the high melting point material is backwards by 2◦ , and the sheets were welded at a rotational speed
transmitted to the bottom sheet, which is partially melted in con- (ω) of 1000 rpm and a travel speed (v) of 600 mm/min, as shown in
tact with the upper sheet, promoting joining by the formation of Fig. 1a. For comparative analysis, a tool with a conical non-threaded
Al-Fe intermetallics. The authors labelled this technique as friction pin was used to join the two different steels in a dissimilar lap joint
melt bonding process. configuration (Fig. 1c). This weld was performed under force con-
According to the literature review, pinless tools can be success- trol, with a tool rotation speed of 1000 rpm, a traverse speed of
fully used in similar and dissimilar lap joining of several metallic 100 mm/min and an axial force of 12 kN.
alloys. Base materials stirring (Zhang et al., 2010), melting of Weld specimens were prepared for metallographic analysis
an interlayer material (Zhang et al., 2011; Kuang et al., 2015; following standard practices. The transverse cross-section of the
Khorrami et al., 2015) and metallurgical reactions at the bond- welds was etched, using Nital (49 ml ethyl alcohol; 1 ml HNO3),
and observed using an optical microscope Leica DM 4000 M LED.

Fig. 1. Scheme of the TAFW process (a), TAFW tool (b) and FSW tool (c).
T. Mira-Aguiar et al. / Journal of Materials Processing Technology 238 (2016) 73–80 75

Fig. 2. Transverse cross-sections: DX51D (a) and DC01 (b) welds.

SEM/EDS analysis was also performed in order to determine the rial flow of the lower plate base material (Cederqvist and Reynolds,
chemical composition in localised areas of the welds using a Philips 2001), in both sides of the friction stir weld. No hooking can be
XL30 SE microscope. detected in the cross-sections of the welds in Fig. 2, which is another
Tensile-shear advancing and retreating side samples, with indicator of the absence of material flow across the faying interface.
16 mm width, were extracted from the welds following the pro- Figs. 4 and 5 show magnifications of the through-thickness
cedures described in Costa et al. (2015a). An optical system microstructural evolution, from the centre of the weld, as marked
(Aramis 3D 5 M) was used for strain data acquisition during the in Fig. 2, for the DX51D and DC01 welds, respectively. Both fig-
tensile-shear testing. All the procedures used for the specimen’s ures show an evident microstructural gradient across the thickness,
preparation and strain data analysis are described in Leitão et al. characterized by structures with decreasing grain size, from the
(2012, 2013). top to the bottom of the welds. Another common feature between
the two welds is the presence of a very thin dark region, at the
3. Results and discussion very top of both welds, which, according to the magnifications in
Figs. 4b and 5b, has a layered morphology. An SEM/EDS analysis
3.1. Microstructural analysis in these regions allowed the detection, for both welds, of the pres-
ence of tungsten (Figs. 4g and 5g). For the DX51D weld, in addition
Transverse cross-sections of the similar welds produced with to tungsten, Zinc was also detected (Fig. 4g) in the dark top layer.
the pinless tool, for the DX51D and DC01 steels, are shown in Meanwhile, the presence of tungsten has to result from the con-
Figs. 2a and b, respectively. A large process affected region, with tact with the WC welding tool. The zinc element, in the top layer
the microstructure contrasting with that of the base material, of the DX51D weld, are remnants of the galvanised coating of this
is clearly visible in both cross-sections. The shape of the trans- base material. As a result of the tungsten content, very high hard-
formed region reveals that, despite the welding tool having no ness values were registered at the top of both welds, reaching peak
pin, the thermo-mechanical conditions developed during welding, values around 800 Hv, for the DX51D weld (Fig. 4h), and around
promoted through-thickness metallurgical transformations in both 900 Hv, for the DX51D weld (Fig. 5h). No vestiges of tungsten or
plates. A continuous dark line aligned with the abutting plate’s zinc, nor any brittle particles were detected inside any of the welds,
initial interface is also visible in both images, corresponding to in the area under this top dark layer, which again points for the
remnants of the base metals surface oxides. The presence of this inexistence of vertical material stirring. Zinc was only found at the
continuous line, in both cross-sections, indicates that no vertical borders of the weld, where remnants of the galvanised coating,
material flow took place from the upper to the lower plate, or which was expelled from the interface by the compression load,
vice-versa, proving that the weld does not result from base mate- remained trapped (Fig. 2a).
rials stirring as in FSW. To better illustrate this assumption, Fig. 3 In spite of all the similarities in morphology between the DX51D
shows the cross-section of the dissimilar DC01-DX51D weld, made and DC01welds, as stressed previously, important differences in the
by FSW, using a tool with a conical pin and conical flat shoulder. microstructural evolution, from the top to the bottom of the weld,
The presence of the typical onion ring structure, resulting from base can also be easily depicted by comparing Figs. 4 and 5. Meanwhile,
materials stirring during welding, is clearly visible in the image, in for the DC01 weld, a clear change in microstructure between the
opposition to that observed for the welds in Fig. 2. It is also possible upper and lower plates, can be seen by comparing Fig. 5b–f. For
to see the presence of the hooking defect, due to the upward mate- the DX51D weld, no important changes in microstructure can be

Fig. 3. Transverse cross-section of the dissimilar friction stir weld using a tool with pin.
76 T. Mira-Aguiar et al. / Journal of Materials Processing Technology 238 (2016) 73–80

Fig. 4. Magnifications of the microstructure of the DX51D weld, in the areas marked in the transverse cross-section in Fig. 2a, EDS analysis (g) and micro-hardness
measurements in the dark layer at the top of the weld (h).

depicted by comparing Fig. 4b–f. In fact, the DX51D weld displays a weld. The microstructural evolution registered for the DX51D weld
ferritic structure, very similar to that of the base material (Fig. 4k). is actually very similar to the traditional HAZ microstructure in car-
The main difference relative to the base material is that the grain bon steel fusion welds: a coarse grained zone, near the top of the
size decreases from the top to the bottom of the weld, as shown in weld, where the peak temperatures reached may be in the super-
Fig. 6a, where the grain size distribution for the base material and critical domain, and a fine grained structure, near to the bottom
for the weld zones in Figs. 4c and f are plotted. The results show that of the weld, where the temperatures may not exceed that charac-
at the top of the weld the grain is coarser than that of the base mate- teristic of the intercritical domain (Easterling, 2013). The ferritic
rial. At the bottom of the weld, despite the average grain size being structure, all across the weld thickness, also indicates that slow
similar to that of the base material, the grain size distribution is cooling took place after welding.
different, showing that some microstructural transformations also Similarly to what was registered for the DX51D weld, a fer-
took place in this zone of the weld. ritic fine grained structure, characteristic of “low” heating and slow
The through-thickness microstructural gradient, registered for cooling rates was registered at the bottom of the DC01 weld (Fig. 5f).
the DX51D weld, can be easily related to the thermal gradient devel- Analysing Fig. 6b, where the grain size distribution for this region
oped across the thickness during welding. In TAFW, the friction and for the DC01 base material is plotted, enables the conclusion
between the flat tool and the surface of the top plate constitutes that no grain refinement or coarsening occurred in the lower part of
the heat source for the process. The heat generated at the tool- the weld. On the other hand, at the top of the DC01 weld (Fig. 5c),
workpiece interface is dissipated, through the plates, in a process a microstructure with a large percentage of acicular ferrite nee-
very similar to that registered in the heat affected zone (HAZ) of any dles, randomly oriented, completely different from that of the base
T. Mira-Aguiar et al. / Journal of Materials Processing Technology 238 (2016) 73–80 77

Fig. 5. Magnifications of the microstructure of the DC01 weld, in the areas marked in the transverse cross-section in Fig. 2b, EDS analysis (g) and micro-hardness measurements
in the dark layer at the top of the weld (h).

Fig. 6. Grain size distribution in the base material (BM), (Fig. 4f and c) for DX51D weld (a); in BM and Fig. 5f) for DC01 weld.
78 T. Mira-Aguiar et al. / Journal of Materials Processing Technology 238 (2016) 73–80

Fig. 7. DC01 weld microstructure at the interface level: AS (a) and RS (b).

Fig. 8. Transverse cross-section of the DX51D weld performed at 200 mm/min (a); details of the microstructure at the central region (b, c) and at the base material (d).

material (Fig. 5k) and DX51D weld (Fig. 4c), can be seen. Acicu- it is plausible to assume that plastic deformation taking place dur-
lar ferrite is usually associated with low carbon and micro-alloyed ing DC01 base material welding promoted ferrite nucleation inside
steels, being nucleated inside the austenite grains, at non-metallic the austenite grains, conducting to acicular ferrite formation upon
inclusions (Krauss and Thompson, 1995). Since both base materi- cooling.
als analysed in the current work are low carbon steels, with similar Strain induced transformation happens when two precondi-
alloy content, subjected to similar welding procedures, the acic- tions are met, a critical strain and temperatures above Ar3 , the
ular ferrite formation, in the DC01 weld, could not be driven by austenite transformation temperature (Sun et al., 2014). Since the
nucleation at non-metallic inclusions. Otherwise, the same type of coarse grained structure, at the top of the DX51D weld, is a clear
structures would have to be present at the bottom of the weld and evidence that the base material was in the austenitic domain, the
in the DX51D weld. However, ferrite nucleation inside austenite absence of acicular ferrite is indicative that no intense plastic defor-
grains can also be promoted by plastic deformation, in a process mation took place during the welding of this base material. The
which can be labelled Strain Induced Transformation, or Dynamic tool was in contact with the surface of the plates, generating heat
Strain Induced Transformation, when the ferrite grains are formed by friction, but the material under the tool was not stirred by it,
dynamically during austenite deformation (Sun et al., 2014). Recent i.e., sliding was the predominant contact condition at the tool-
studies proved that plastic deformation augments, in large scale, workpiece interface. On the other hand, the presence of acicular
the ferrite nucleation sites, contributing towards activating non- ferrite in the DC01 weld, is indicative that base material stirring
equilibrium transformations (Zhang et al., 2014, 2015). This way, took place under the tool, which implies that sticking was the pre-
T. Mira-Aguiar et al. / Journal of Materials Processing Technology 238 (2016) 73–80 79

Fig. 9. DX51D weld shear-tensile test curves (a), specimen rupture (b) and strain maps (c).

dominant contact condition at the tool-workpiece interface. The speed, there was time for the melted/vaporized galvanised coating
acicular ferritic structure extends to the lower plate, in a thin layer, to be expelled from the tool-workpiece contacting area giving rise
few microns thin, located immediately below the interface line in to sticking contacting conditions and base materials stirring under
the middle of the weld (Fig. 5d). This observation enables to con- the tool. This microstructure corroborates the previous assump-
clude that the joining of the plates is assisted by a combination of tion of strain induced phase transformation taking place during
plastic deformation, at the interface, as in friction welding, and dif- welding.
fusion across the overlapped base materials interface. The acicular
ferritic structure is not visible near the unconnected interface, at the
advancing (Fig. 7a) and retreating (Fig. 7b) extremities of the weld, 3.2. Tensile tests
where no deformation could have taken place. In spite of this, a clear
HAZ, characterized by a refined grain structure, can be seen above The load-displacement curves obtained in the tensile-shear test-
and under the unconnected interface. The refined microstructure ing of advancing and retreating side samples of the DX51D and
is a result of thermal induced metallurgical transformations. DC01welds are shown in Figs. 9a and 10a, respectively, together
For the DX51D weld, no evidence of plastic deformation near with the load-displacement curve obtained in the tensile testing
the interface can be perceived from Fig. 4d. For this base mate- of base material samples with the same width of the tensile-shear
rial, the joining of the plates results only from diffusion across the samples. Figs. 9c and 10c, show strain distribution maps, at max-
contacting surfaces under compression. The microstructure of the imum load, for the two welds. Analysing the results it is possible
HAZ, above and below the interface is similar, which confirms the to conclude that both welds displayed excellent mechanical per-
hypothesis that no severe plastic deformation took place at the formance reaching tensile-shear strength values very close to the
interface, in the middle of the weld. As already reported when tensile strength of the respective base material. Actually, the strain
analysing Fig. 4, the SEM/EDS analysis revealed the presence of distributions maps in Figs. 9c and 10c and the specimens in Figs.
the zinc element at the top layer of the weld. This way, the slid- 9b and 10b clearly show that the failure of the tensile-shear sam-
ing contacting conditions at the tool/workpiece interface may be ples occurred in the base material, far from the welded interface,
attributed to the melting/vaporization of the galvanised coating, after significant plastic deformation took place. No plastic strain
which acts as a lubricant during welding. By reducing the welding was registered in the weld area, for any of the base materials.
speed from 600 mm/min to 200 mm/min, the microstructure of the Finally, it is also important to remark that no significant differences
DX51D weld changed drastically, as shown in Fig. 8, where an aci- in advancing and the retreating sides strength were registered for
cular ferritic rich structure is shown all across the weld thickness these welds, in contrast to that registered for traditional friction
(Figs. 8b and c). It can be concluded that at this very slow welding stir lap welds (Costa et al., 2015a,b).

Fig. 10. DC01 weld shear-tensile test curves (a), specimen rupture (b) and strain maps (c).
80 T. Mira-Aguiar et al. / Journal of Materials Processing Technology 238 (2016) 73–80

4. Conclusions Costa, M.I., Verdera, D., Costa, J.D., Leitao, C., Rodrigues, D.M., 2015a. Influence of
pin geometry and process parameters on friction stir lap welding of
AA5754-H22 thin sheets. J. Mater. Process. Technol. 225, 385–392.
A new FSW related technique, labelled tool assisted friction Costa, M.I., Verdera, D., Leitão, C., Rodrigues, D.M., 2015b. Dissimilar friction stir lap
welding (TAFW), is proposed for the welding of very thin steel welding of AA 5754-H22/AA 6082-T6 aluminium alloys: influence of material
plates. Taking into account the results displayed in the paper, the properties and tool geometry on weld strength. Mater. Des. 87, 721–731.
Easterling, K., 2013. Introduction to the Physical Metallurgy of Welding. Elsevier.
following conclusions can be drawn: Khorrami, M.S., Kokabi, A.H., Movahedi, M., 2015. Study on joint interface and
mechanical properties of Cu/Pb-Sn/Cu lap joint produced by friction stir
- Non-defective steel welds, with tensile-shear strength similar to soldering process. J. Mater. Eng. Perform. 24, 2158–2169.
Krauss, G., Thompson, S.W., 1995. Ferritic microstructures in continuously cooled
the tensile strength of the base material, may be obtained for
low-and ultralow-carbon steels. ISIJ Int. 35, 937–945.
galvanised and non-galvanised low carbon steels. Kuang, B., Shen, Y., Chen, W., Yao, X., Xu, H., Gao, J., Zhang, J., 2015. The dissimilar
- Weld microstructure is influenced by the thermo-mechanical friction stir lap welding of 1A99 Al to pure Cu using Zn as filler metal with
“pinless” tool configuration. Mater. Des. 68, 54–62.
conditions developed during welding, which in turn depends
Leitão, C., Galvão, I., Leal, R.M., Rodrigues, D.M., 2012. Determination of local
on the base materials surface condition, i.e., on the presence or constitutive properties of aluminium friction stir welds using digital image
absence of a galvanised coating, and on the welding speed. correlation. Mater. Des. 33, 69–74.
- The main joining mechanisms responsible for the welding are Leitão, C., Costa, M.I., Khanijomdi, K., Rodrigues, D.M., 2013. Assessing strength and
local plastic behaviour of welds by shear testing. Mater. Des. 51, 968–974.
plastic deformation, at the abutting plates interface, and atomic Rai, R., De, A., Bhadeshia, H.K.D.H., DebRoy, T., 2011. Review: friction stir welding
diffusion at high temperature and pressure. No base materials tools. Sci. Technol. Weld. Join. 16, 325–342.
inter-mixing takes place during welding, as is the case for FSW. Sun, L., Muszka, K., Wynne, B.P., Palmiere, E.J., 2014. Effect of strain path on
dynamic strain-induced transformation in a microalloyed steel. Acta Mater. 66,
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Acknowledgments Tozaki, Y., Uematsu, Y., Tokaji, K., 2010. A newly developed tool without probe for
friction stir spot welding and its performance. J. Mater. Process. Technol. 210,
844–851.
This work was supported by FCT (Portuguese Foundation for Sci- Van der Rest, C., Jacques, P.J., Simar, A., 2014. On the joining of steel and aluminium
ence and Technology), within ISISE, project UID/ECI/04029/2013, by means of a new friction melt bonding process. Scr. Mater. 77, 25–28.
and CEMUC, project Pest-C/EME/UI0285/2013. The author C. Leitão Zhang, G.-f., Su, W., Zhang, J., Wei, Z.-x., Zhang, J.-x., 2010. Effects of shoulder on
interfacial bonding during friction stir lap welding of aluminum thin sheets
is supported by FCT through SFRH/BPD/93685/2013 fellowship. All using tool without pin. Trans. Nonferrous Met. Soc. China 20, 2223–2228.
supports are gratefully acknowledged. Zhang, G., Su, W., Zhang, J., Wei, Z., 2011. Friction stir brazing: a novel process for
fabricating Al/Steel layered composite and for dissimilar joining of Al to steel.
Metall. Mater. Trans. A. 42A, 2850–2861.
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