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Moisture Analyzer
〖Operation Instruction〗
for HBD5 MS2100 Series Humidity/Water Activity/Moisture Analyzer
Ref:HMS2100_Me
Instrument Version:4.6
Revision:2.2
Date:2002-12-10
Contents
1. General
2. Test Routine
3. Function Operation
4. System Arrangement
4.1 Components to be combined
4.2 Instrument
5. Preparation for Operation
6. Setup Operation
7. Maintenance
7.1 Detector cleaning
7.2 Battery replacement
8. Troubles and remedies
8.1. Troubles finding procedure
8.2. Confirming temperature compensation
8.4 Confirming probe output
8.5 Troubles shooting
9 Adjustment after detector replacement
Appendix 1 Measurement theory
Appendix 2 Standard specifications
Appendix 3 Difference Correction Method
Appendix 61 2DC Calibration Table
Product List
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MS2100 Moisture Analyzer Instruction Manual
1. General Description
Hand held MS2100 Moisture analyzer is one modest full function industrial instrument. Equipped with
different series sensor for diverse applications for both of industry and laboratory.
MS2100 is general for air, gas, liquid and solids moisture analysis with suitable accessories.
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MS2100 Moisture Analyzer Instruction Manual
2. Test Routine
2.1. Parameters Test for Gas
Absolute moisture, Volume ratio, %volume, Partial pressure, Saturation moisture, Relative humidity, Specific
quantity, Dew point, Humidity Ratio
calculation
Wa calculation
No Is it the end?
Yes
Smart: Hour/Mins/Sec
Aw:x.xxx T25.1 °COK
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MS2100 Moisture Analyzer Instruction Manual
Aw:x.xxx C#
lMS: x.xxU T25.1 °C
Aw:x.xxx C#
lMS: x.xxU T25.1 °COK
Note:
1) To measure the moisture by this way, users must calibrate the instrument first, to establish the pertinence
chart quantificationally between water activity and moisture against user sample. Once calibrated, you just
need to select the right channel each time to test the relavant samples(need not to calibrate every time).
2) After Direct Insertion test, clear the residential solvents.Using suitable mild solvents, such as gasoline,
benzine, toluence etc, to wash the sensor if the liquid sample is erosive to the sensor before storage;
Aw:x.xxx C#
sMS: x.xxU T25.1 °C
Aw:x.xxx C#
sMS: x.xxU T25.1 °COK
Note:
To measure the moisture by this way, users must calibrate the instrument first, to establish the pertinence chart
quantificationally between water activity and moisture against user sample. Once calibrated, you just need to
select the right channel each time to test the relavant samples(need not to calibrate every time).
For clean solid particles test, you can directly insert the sensor into sample stack. Otherwise use indirect way to
test. Be aware, you must keep the same way to calibrate and test.
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MS2100 Moisture Analyzer Instruction Manual
The record interval is equal to the interval set when you started calibration. So that each calibration chart has it’s
own interval.
You can read out the stored data by press <MEMO>. Data will be displayed sequentially by order. This time you
can press <ENTER> print out the current data.
If the stored data pass over 200, the old one would be deleted automatically if you restore a new one.
3.3 Printer
And also you can print out the current LCD data, by press <QUIT> or<ESC>.
Made by BDp
Key <3>, then key<ENTER>, the information would be appeared on the LCD:
Version number: H MS2123 V2.1
Manufacture Date: year: month:data
Product Number(SeriesNum):
Sensor Number(SensorNum):
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MS2100 Moisture Analyzer Instruction Manual
4. System Configuration
4.1. Configuration for Normal Test
4.1.1. Gas or Direct Liquid Insertion Sensor System
Basic Parts
Items Introduction References
Analyzer Data processor
H-MS2100N Probe should be connected to analyzer
Connection
Special Accessories
Items Model Type Remarks
N-P Fit ST1 Fitter ZG1”,NPT1” Screw Fixing to pipe line
For temporary on-line pipe continuous test usage
N-B Fit B25 Fitter Dia.25 Fixing to glass instruments
For temporary continuously test usage
Special Accessories
Items Introduction
DSC Kit Accessory for Clamp Kit and Vap Kit. Each pack consists of 100 disposable sample
cups (14mm deep and or 40mm)
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MS2100 Moisture Analyzer Instruction Manual
Special Accessories
Items Introduction
DSC Kit Accessory for Clamp Kit and Vap Kit. Each pack consists of 100 disposable sample
cups (14mm deep and or 40mm)
4.3.Common Consumes
Calibration Kit 1 EA35 (35 %RH)and 1 EA80 MS2123 is long time stable.
(80%RH) Standards If found any err, you can get chemicals to make
samples. Refer to Appendix 2
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MS2100 Moisture Analyzer Instruction Manual
4.5.Spare Sensors
MS2123M12T85 Spare sensor for HMS2123N probe replacement
MS2123pM12T85 Spare sensor for HMS2123N probe replacement, with pressure connector
MS2123M12T100 Spare sensor for HMS2123N probe replacement
MS2123pM12T100 Spare sensor for HMS2123N probe replacement, with pressure connector
MS2123M12T180 Spare sensor for MS2123N probe replacement
MS2123pM12T180 Spare sensor for MS2123N probe replacement, with pressure connector
MS2110M12T300 Spare sensor for MS2110N probe replacement
MS2110pM12T300 Spare sensor for MS2110N probe replacement, with pressure connector
*Refer to HMS2100_DS_E for details
If you found the trouble that you can not solve however, please contact with our engineer for help.
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MS2100 Moisture Analyzer Instruction Manual
6.Setup Routine
Version 2.1
SETUP Select:
No:12345 6-0
Use <PgDn> key to choose the right set item. Or <clear> to goback toward left.
Also you can direct select by number if you remember the function code.
Once <ENTER> to set your select
Using key value to index the functions:
There are 4 valid functional setup routine here involved
1) Calibrate: there is the entrance to buildup the user favored data convert program. 2DC insertion table is
employed in the MS2100 program. For further comprehension please refer to Appendix 6.1. Refer to 6.1.
Calibrate for details of operation procedure.
2) Chart Initialize: this is to zero the selected channel before calibration. The data established via initialization
is not assured to be correct. Refer to 6.4. Initialize the Chart..
3) System Information: this is to flush the EEProm memory for available, must executed at startup in plant.
User can use alterable “Delete” function in Calibration program instead of this operation. Some time
experienced or user defined data might be initialized
4) System Setup: Functions to setup alarm point and output range, refer to “Alarm&output”; to input sensor
basic data or device control parameters, refer to "DeviceCtrlSetup"; main sensor calibration,refer to
“PrimarySensorCal"; Temperature sensor calibration, refer to "TempSensorCal"; Pressure sensor calibration,
refer to "PresureSensorCal"; Power saving mode setup, refer to "PowerManage";
For procedure details, refer to 6.4. System Control.
Select the channel you want to setup:
Chart Select::
Ch:12345
It would automatically change to new window, the first line would remind information of current channel.
Such as it was set to Water Activity parameter before, the window is like this
Chart Select::
Ch:12345
6.1. Calibrate
Step Operation Outline:
z If first time to calibrate, you need to setup some necessary parameters for your application to current
channel;
z Then you can execute calibration with samples according the guide of LCD clew. Refer to step instructions
following
Utility Direction
z When you want to start to use or give up one Calibration chart, you need to <Delete> the old chart data at
first.
z You need 2 samples and implement twice times to calibrate one new chart at least to start one new channel.
The more samples calibration pint to be established, the higher accuracy were expected. But always to keep
it as simple as possible. It means, only if 2 points calibration could not satisfy your test, then insert one more
point again. The exact valued standard sample calibration results might be overlaid after repeated.
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MS2100 Moisture Analyzer Instruction Manual
Set Parameter:
Para:12345678 61-1
Use <PgDn> key to choose the right set item. Or <clear> to goback toward left.
Also you can direct select by number if you remember the parameter code.
If current number >8, then you have to key the new number(the <PgDn> and <Clear> not work in this case)
Once <ENTER> to set your select
If you want to change parameter existed in this channel, you should delete chart data first;
Refer to “6..1.5. Test Method Selection Routine” for further operation instructions. When first time to
calibrate.
After finished first time setup(Return from “Set Parameter”), LCD prompts
3>UseInitialData
1>GoOn Calibrate 61-2
Select <1> to start first sample calibration; refer to “1.1. Calibrate with Sample”
Key<3 > to give up first calibration this time, and use the initial data.
Note:
z As to gMoisture configuration, the initial data is very exact, do not calibrate it unless obvious errors found.
z If you test water activity, also not to calibrate here, unless you can not correct the humidity sensor itself.
Case 2:
If second time afterward to calibrate the same table chart, system would clew to
Case 3:
If third times later to calibrate the same table chart, system would clew to
1>Append C%d
2>Del 3>Zerooffset 61-4
If you want complement the last chart with new samples, please key <1>
If you want clear the old chart, please key <2> to delete it
If you only want to zero the existed chart with one standard “Zero” sample, key <3>
Also, if you want to change the paramter of calibration chart in current channel, u need to delete the table first, then
reentrant from normal ‘SETUP’ to setup the test mode.
Attention:
1) Zero function is not recommend to startup, unless you are dealing very complex curve calibration convert for
moisture of special materials. For most case 2DC is more easy to start, 2 points calibration can get quiet
good accuracy, especially for MS2123 sensor.
2) But convert from water activity to moisture needs more point to be exact.
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MS2100 Moisture Analyzer Instruction Manual
Now, please input the standard value of the Standard Sample this time you are used to calibrate with keypad.
You can input float data currently. Such as “1.0123” alike.
The click <ENTER> to finish your inputing.
Then System remind you to insert the sensor into the sample, or fill the sample into the sensor holder of clamp.
LCD cheers
Calibrating...C# 611-3
When the sample condition fixed, the ADC data should be more and more being close to stable. Then you can
click <ENTER> to finish the calibrate.
CH#STD#: OK
Sx.xxx; Ay.yyy 611-5
If it is correct as you memory, that you have done well of one sample point calibration.
Then short time of routine check, it will return to normal test state.
Attention:
z Generally speaking, the more points you calibrated, the more accuracy you might get. But you must use
reliable and accurate sample. Once wrong sample will absolutely ruin the accuracy of the chart.
z for more times of sample calibration, just repeat the calibration routine.
z At least you need 2 samples points to start this chat to working correctly.
z You can stop operation anytime by turn off the power for urgent cases.
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MS2100 Moisture Analyzer Instruction Manual
to name C#dest
the New Chart 612-3
LCD alrm
Chart C# 613-2
Deleted!
SampleNameSele
ct 614-1
Use <PgDn> key to choose the right set item. Or <clear> to goback toward left.
Also you can direct select by number if you remember the name order.
There are always fixed 12 names for user’s convenience to distinguish samples
This is just a symbol, none of relations to any virtual operation, but display flips.
Use <PgDn> key to choose the right set item. Or <clear> to goback toward left.
Also you can direct select by number if you remember the parameter code.
If current number >8, then you have to key the new number(the <PgDn> and <Clear> not work in this case)
Once <ENTER> to set your select
Now select the paramter you want to test by the following order code
1) RelativeHumidity
2) WpartialPressure
3) VolumeRatio
4) HumidityRatio
5) VolumePercent
6) SpecificHumidity
7) AbsoluteHumidity
8) Dew Point
9) Enthalpy
10) gMoisture
11) WaterActivity
12) sMoisture
13) lMoisture
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MS2100 Moisture Analyzer Instruction Manual
*if possibly some err in relations, you first accept the remind of LCD memo displayed.
IF you water activity, ERH method was selected, the system would guide you to setup test mode
1>Normal Method 615-2
2>Smart 3>Prof
*Important
If you are not professional , or you do not want to change these following parameters for bassic function. You just
need to <ENTER> each step LCD stoped and reminded to select or setup, so that the old defaulted data would be
kept available.
Select test mode by key number
Following choices are available:
1) Conventional_Method;
2) Smart_Method;
3) Extrapolate _Method;
4) Professional_Method;
Key <1> to run the pump when it should run by the program control.
Key<2> to stop it. (Choose this if your instrument not has pump, to avoid EM interferences)
In case you directly test moisture of liquids, for sure you need not the pump in present version. Choose “2”.
If you indirect test moisture by ERH, you usually need to start pump. So choose “1”.
Otherwise to test gas parameters, always you need not pump.
Then system guided to setup control parameters for water activity test mode. Refer to 1.7. Water Activity Test
Control for further setup.
isPressureSensor
Instaled?1>Y,0>N 615-4
if key <0> to negate, input Sea Level in meters of you local area, so that gas parameters can be solidly
compensated.
you can key float number here for high accuracy convert.
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MS2100 Moisture Analyzer Instruction Manual
Use <PgDn> key to choose the right set item. Or <clear> to go back toward left.
Also you can direct select by number if you remember the name order.
Then <ENTER> to choose the current one.
Available units includes: "V", "%RH" ,"ppmv", "ppmw", "g/kg","kg/kg", "%", "g/m3", "g/Nm3", "\337C", "\337K",
"\337F", "kcal/kg","Btu/lb","aw","atm"
1)Goon Calibrate
2)Keep BasicTest 615-7
6.1.6. Zero
You need one real “Zero” sample to implement this routine
Attention:
z the calculation is based on the converted data from relative 2DC chart.
z Once zero finished, 2DC chart can not be modified again.
z Only after the 2DC chart has been calibrated for 2 points up, zero could be executed.
TestInterval
= sec 617-1
Use <PgDn> key to choose the right set item. Or <clear> to go back toward left.
Also you can direct select by number if you remember the code.
Then <ENTER> to choose the current one.
Attention:
z User calibrated data would be deleted by this operation.
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MS2100 Moisture Analyzer Instruction Manual
SystemControl 64-1
Set::========
Note:
a) The calibration from 3)to 5)is to establish a formulae as Z=zerooffset+slope*variable relation for
relative sensors. The RH sensor needs also to setup “Supply voltage” as well, it is about 5.00V(this
is hardware related, can not change the value attached to each special instrument).
b) Don’t calibrate these sensors unless required.
Input a pair of suitable concentration data for the application from the first bit in rear of the indication of TopLimit
and BotomLimit separately. Each time you needed to finish data input by key of <ENTER>.
Note
z The data here is identical to the data in current channel.
z Each channel has different limit data.
The analog output was digitalized according to [20mA * (current data-BottomLimit)/( TopLimit - BottomLimit)]
Cal by 1)Setup
643-1
2)by Sample?
Set SensorSupply
=5.00 V 643-2
Following the guide of LCD to setup SensorSupply, Zero Offset, and SensorSlope correctly here.
LCD display
STD Sample RH
=?? %RH
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MS2100 Moisture Analyzer Instruction Manual
7. Maintenance
7.1. Detector cleaning
If you found abnormal response or slow reaction happened, might be the sensor was wrapped with some dirst.
Then you can clear it with mild solvents that can dissolve the contaminants if you know what they are. Such as
Ethanol, toluene, acetone, gas, kerosene, diesel oil etc can be used.
You can use cotton soaked of the solvents to scrub the surface of sensor softly.
If you have to use severe solvents. Do not be immerged for long time. Better use Ethanol to wash it after
clearance. And dry it as soon as possible.
Afterwards, you can blow it to be dry, but assure that the temperature would not be higher than 80 ºC.
Pay attention to the polarity of the socket, especially when you use another local standard adapter. Before you
use another adapter that not from BDTI, please verify the polarity with multi-meter, and judge if it matched. If
reversed, please cut the wire and swap the line. Then test and start to use.
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MS2100 Moisture Analyzer Instruction Manual
Water activity reflects the active part of moisture content or the part which, under normal circumstances, can be
exchanged between the product and its environment.
Water activity is usually defined under static conditions of equilibrium. Under such conditions, the partial pressure
of water vapor (p) at the surface of the product is equal to the partial pressure of water vapor in the immediate
environment of the product. Any exchange of moisture between the product and its environment is driven by a
difference between these two partial pressures.
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MS2100 Moisture Analyzer Instruction Manual
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