Qualitative - Quantitative Chemistry (Laboratory)

Course Outline

Outcomes
 Demonstrate qualitative and quantitative laboratory analysis skills with precision and
accuracy following good laboratory practice guidelines to preserve, protect, and enhance
God’s creations

Approach:

 Perform series of qualitative and quantitative chemical analysis experiments with various
techniques and instruments
 Certify laboratory instruments and standards
 Maintain laboratory records in compliance with Good Laboratory Practice Guidelines

CRITERIA FOR GRADING

The grades reflected in the transcript is assigned by computing the average of the grades
obtained in the preliminary, midterm and final grading period in the whole semester. Grading
system per grading period is calculated according to the following criteria

LECTURE LABORATORY
Criteria Rate Percent Criteria Rate Percent
Equivalent Equivalent
TLA 30% 70% TLA 30% 70%
AT 70% AT 70%
Term Exam 30% Term Exam 30%

Total 100% Total 100%

Schedule of Learning Activities:

Weeks 1-6 (PRELIM)

 Perform Experiments 1-7 (Separation of Basic Cation Constituents Analysis)

 E-1 Separation of the Basic Constituents into Groups
 E-2 Reactions of the Silver Group
 E-3 Reactions of the Hydrogen Sulfide Group
 E-4 Reactions of the Ammonium Sulfide Group
 E-5 Reactions of the Alkaline Earth Groups
 E-6 Reactions of the Alkali Group
 E-7 Analysis of Cation in a Solution Containing Only One Inorganic Compound

Weeks 7-12 (MIDTERM)

 Perform Experiments 8-14

E-8 and E-9 (Separation of Basic Anion Constituents Analysis
E-9 -13 (Volumetric Analysis: Acid-Base Titration Neutralization Titrations)

AD MAJOREM DEI GLORIAM
 E-14 (Complexometric Titrations)
 E-8 The Chemistry of the Acidic Constituents
 E-9 Analysis of an Anion in a Solution Containing Only One Inorganic Compound
 E-10 Preparation and Standardization of Hydrochloric Acid Solution
 E-11 Preparation and Standardization of Sodium Hydroxide Solution
 E-12 Standardization of Sodium Hydroxide Solution with Potassium Acid
Phthalate
 E-13 Determination of Acetic Acid content in Vinegar

Week 13-18 (FINALS)

 Perform Experiments 14-20
E-14 Preparation and Standardization of EDTA
E-15 (Complexometric Titrations)
E-16-17 (Reduction-Oxidation Titrations)
E-18 (Gravimetric Analysis)
E-19 -20 (Separation Analysis Using Instrumentation Method)
 E-19 Introduction to Instrumentation
 E-20 Spectrophotometry

Learning References:

Bishop, Michael l. et al. (2010) “Clinical Chemistry Techniques, Principles, Correlations” 6th
Edition
Day, Jr R.A. and Underwood, A.L. Quantitative Analysis. 6 th edition. New Jersey: Prentice –
Hall, Inc. 1991.
Gilreath, Esmarch. Qualitative Analysis Using Semimicro Methods. New York: McGraw-Hill
Book Company, Inc., 1964.
Hargis, Larry. Analytical Chemistry Principles and Techniques. New Jersey: Prentice – Hall, Inc.
1988.
Knevel, A.M. and DiGangi, F.E. Jenkins’ Quantitative Pharmaceutical Chemistry. Philippines.
Merriam Webster Bookstore, Inc.,1977.
Linne and Ringsrud’s “The Basics and Routine Techniques” 6th Edition
McPherson, Richard A. et al. “HENRY’S CLINICAL DIAGNOSIS by LABORATORY METHODS”
Sorum, C.H. and Lagowski, J.J. Introduction to Semimicro Qualitaitive. 6 th edition. New Jersey.
Prentice – Hall, Inc., 1983.
Turgeon, Mary Louise (2007) “Clinical Laboratory Science” 5th Edition

AD MAJOREM DEI GLORIAM