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Effects of Polymer Treatment on Undrained Strengths and

Cyclic Behavior of a Low-Plasticity Slurry


David Reid 1 and Andy Fourie 2
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Abstract: A laboratory study was undertaken to assess the effects of polymer treatment (PT) on the monotonic, cyclic, and postcyclic
behavior of a low plasticity slurry using a direct simple shear (DSS) apparatus. This study was conducted to extend the results of previous
testing that assessed the effects of PT on the same material’s consolidation behavior and critical state line. Consistent with previous tests
on this material, DSS testing indicated that PT resulted in lower consolidated densities at a given magnitude of effective stress, and higher
undrained shear strengths at a given density. PT appeared to increase the effects of strain rate on strength, whereas both PT and untreated
materials responded similarly to the effects of overconsolidation. Cyclic and postcyclic testing indicated essentially indistinguishable
results for the two materials. The effects of PT were seen to persist at vertical effective stresses up to 800 kPa. The potential implications
of these findings for tailings design are discussed. DOI: 10.1061/(ASCE)GT.1943-5606.0001660. © 2017 American Society of Civil
Engineers.

Introduction the geotechnical effects of PT (Jeeravipoolvarn et al. 2014; Reid


and Fourie 2015). There is thus clear evidence that PT of tailings
Over the past decade, the treatment of tailings with polyacrylamide- can have significant impacts on the resulting geotechnical proper-
based polymers at the point of slurry discharge to increase initial ties of a slurry, that therefore needs to be accounted for in design of
rates of dewatering, increase yield stress, reduce segregation, and tailings deposits that utilize PT. Additionally, PT has been shown to
improve return water clarity has found increasing application in the
significantly alter a deposited material’s fabric (Wells et al. 2011)
mining and oil sands industries (Wells et al. 2011; Caldwell et al.
which is consistent with many of the geotechnical effects observed.
2014; Riley and Utting 2014). In parallel with the increased appli-
Although the effects of PT on a number of geotechnical proper-
cation of polymer treatment (PT) to assist in the management of
slurries, research on the effects of PT on subsequent geotechnical ties have been assessed, there is still uncertainty as to how PT may
behavior of the material has been ongoing. Thus far, experimental affect cyclic resistance and postcyclic strength reduction, and the
and field investigations have indicated that PT can result in both effects of overconsolidation and shear rate on peak undrained
higher (Van Impe et al. 2009; Azam 2011; Manzotti et al. 2014) strengths. This paper presents the results of a laboratory investiga-
and lower (Jeeravipoolvarn et al. 2009; Yao 2012; Reid and tion utilizing a direct simple shear (DSS) system to assess the ef-
Fourie 2016) densities across a range of vertical effective stresses, fects of PT on undrained strengths, cyclic resistance, and postcyclic
can increase the shrinkage limit (Yao 2012), produce a strengths for a low plasticity slurry. This work extends previous
material with higher undrained shear strengths at a given density laboratory investigations on the effect of PT on the same low plas-
(Jeeravipoolvarn et al. 2009; Yao 2012; Beier et al. 2013; Manzotti ticity slurry, undertaken by means of slurry consolidometer and
et al. 2014; Cooling and Beveridge 2015; Gholami and triaxial testing (Reid and Fourie 2016).
Simms 2015; Reid and Fourie 2016), increase undrained brittleness
and sensitivity (Beier et al. 2013), increase liquid and/or
plastic limits (Jeeravipoolvarn et al. 2009; Beier et al. 2013; Previous Study
Manzotti et al. 2014; Reid and Fourie 2016), result in an increased
hydraulic conductivity at a given density (Jeeravipoolvarn Reid and Fourie (2016) undertook a study of the effects of PT
et al. 2009; Van Impe et al. 2009; Azam 2011; Reid and Fourie on a low plasticity slurry material developed from a combination
2016), can produce a different critical state line (Reid and Fourie of laboratory-standard soils. The slurry was developed such that it
2016) and may reduce cyclic resistance and postcyclic strengths would have a sufficient quantity of plastic fines to result in a
(Reid and Boshoff 2015). Subsequent shearing of PT slurries prior material amenable to PT, while having index properties such that
to consolidation has also been shown to reduce, but not eliminate,
the material was susceptible to liquefaction under current screening
techniques (Seed et al. 2003; Bray and Sancio 2006). A synthetic
1 material was used rather than an actual tailings, to prevent potential
Ph.D. Candidate, Univ. of Western Australia, 35 Stirling Hwy.,
Crawley, WA 6009, Australia; Senior Tailings Engineer, Golder Associates limitations on publication, and to enable essentially unlimited
Pty Ltd, 1 Havelock St., West Perth, WA 6005, Australia (corresponding quantities of material to be produced for subsequent geotechnical
author). E-mail: 20877398@student.uwa.edu.au beam centrifuge testing. The laboratory slurry consolidometer
2
Professor, Univ. of Western Australia, 35 Stirling Hwy., Crawley, and triaxial testing results indicated that for the material tested,
WA 6009, Australia. PT resulted in (1) lower densities at a given effective stress,
Note. This manuscript was submitted on April 23, 2016; approved on
(2) higher rates of consolidation and hydraulic conductivity at a
September 28, 2016; published online on February 2, 2017. Discussion
period open until July 2, 2017; separate discussions must be submitted given density, (3) an apparent increase in elevation and compress-
for individual papers. This paper is part of the Journal of Geotechnical ibility of the material’s critical state line (CSL), and (4) higher shear
and Geoenvironmental Engineering, © ASCE, ISSN 1090-0241. strengths at a given density.

© ASCE 04017007-1 J. Geotech. Geoenviron. Eng.

J. Geotech. Geoenviron. Eng., -1--1


Table 1. Atterberg Limits material was gently spooned in, while gently stirring the material to
Soil UT PT improve sample homogeneity. The material was then one dimen-
sionally loaded in increments to 40 kPa, and allowed to consolidate
Liquid limit (%) 24 49
for approximately 24 h. This resulted in a material of sufficient
Plastic limit (%) 15 25
Plasticity index (%) 9 24 strength and stiffness such that approximately 18–20 mm high
specimens could, after extrusion and trimming, freely stand on
the DSS base platen prior to membrane and ring placement.

Materials and Sample Preparation


Testing Methods
Materials
The simple shear device used in this study was of the Swedish
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The material developed by Reid and Fourie (2016), and used in this Geotechnical Institute (SGI) type. The device consists of vertical
study was made from a combination of kaolin, silica 200G silt, and and horizontal electromechanical motors, load cells, and linear
silica fine (SF) sand, all produced by Sibelco Australia Ltd. A com- variable displacement transducers (LVDT). The samples were sur-
bination of 31% SF sand, 43% silica 200G, and 26% kaolin by dry rounded by a latex membrane and a series of Teflon rings to min-
mass was found to produce a material that met the requirements imize lateral strain. A schematic of the testing system is provided
previously outlined (i.e., to be susceptible to liquefaction, and ame- in Fig. 1.
nable to polymer treatment). The mixture had a specific gravity It is noted that although Teflon rings may be more common
(SG) of 2.62. The resulting gradation and plasticity of the material in commercial DSS testing, the majority of published data in
are generally consistent with examples of tailings from a variety of the geotechnical literature appears to be obtained using a steel-
mineral types, including iron ore, gold, mineral sands, and nickel wire reinforced rubber membrane, referred to as the Norwegian
tailings. Further information on the slurry constituents is provided Geotechnical Institute (NGI) type. However, a comparison of
by Reid and Fourie (2016). the two lateral restraint types undertaken by McGuire (2011) indi-
The PT process undertaken (discussed subsequently) was found cated negligible difference in the results obtained, provided that
to modify the material’s liquid limit, plastic limit and plasticity corrections for the influence of friction related to the lateral con-
index (PI) significantly, as outlined in Table 1. Liquid limit was finement components was made. The correction technique outlined
measured with the fall cone method. The variance of Atterberg lim- by McGuire (2011) was applied to test results outlined herein.
its following PT is consistent with previous experimental data The system used filter stones with protruding pins to reduce the
(Jeeravipoolvarn et al. 2009; Beier et al. 2013; Manzotti et al. 2014) potential for sliding between the soil and platen. A total of 18 pins
were placed on each of the top and bottom platens, with the pins
approximately 1 mm high and 1 mm in diameter. The use of this
Sample Preparation and Polymer Treatment
form of pins is consistent with the current state of practice for DSS
BASF Australia Pty Ltd (BASF) provided assistance to the authors testing (e.g., ASTM 2007). In test interpretations presented sub-
in selecting a polymer for use in the experimental study. Polymer sequently, shear strain γ was calculated based on a sample height
type and dosage were selected on the basis of a series of dewatering measured between the two filter stones, i.e., the length of the pins
tests where the treated materials were poured into geotextile-lined was not considered in strain calculations.
columns with base drainage, and increase in solids content was As noted previously, the initial specimen diameter after
tracked over time. The screening assessment undertaken by BASF extrusion from columns was approximately 63.6 mm. The internal
indicated that the high molecular weight polymer RHEOMAX diameter of the Teflon rings was 64.5 mm, and the triaxial mem-
ETD DPW 1687, at a dose of 500 g of dry polymer to ton of brane used was approximately 0.3–0.5 mm thick, depending on
dry solids was well suited to the treatment of the slurry developed pressure applied (i.e., with calipers when measuring). Thus, when
from this study with respect to increased dewatering rates. initially assembling the membrane and rings around the sample, it
The slurry material was initially mixed in a dry state to the mass was found to be a reasonably tight fit with no gaps apparent.
proportions previously outlined. Tap water was then added to make Because the likely slight reduction in thickness of the membrane
up a slurry at 122% gravimetric water content (GWC), and mixed as increasing horizontal pressure was applied during consolidation,
thoroughly in a 20 L bucket. During mixing, 2 g of sodium chloride
salt per liter of slurry was added, to increase the dissolved solids to
a range more typical of a tailings process fluid. After mixing, the
material was left for two days to allow the kaolin particles to hy-
drate. At this point, material that was to be used as UT slurry was
decanted, with sufficient clear water removed to produce a resulting
slurry with approximately 45% GWC. This decanting was under-
taken to produce a nonsegregating slurry.
For PT batches, polymer solution was made up one day prior to
use, at a mass concentration of 0.25% The settled slurry (without
decanting) was again thoroughly mixed, with the first half of the
polymer solution added once the material was remixed. The
material was then poured into another 20 L bucket, then back into
the original bucket. The second half of the polymer solution was
then added, followed by four additional pours between buckets.
To prepare the material for DSS testing, columns with 63.6 mm
internal diameter were prepared with a filter and drainage medium
Fig. 1. Schematic of DSS system with sample prepared for test
at the base. UT material was poured into the columns, whereas PT

© ASCE 04017007-2 J. Geotech. Geoenviron. Eng.

J. Geotech. Geoenviron. Eng., -1--1


a specimen diameter of 63.8 mm was used for stress and density The test conditions for monotonic tests are outlined in Table 2.
calculations. It is likely that small lateral strains occurred during Monotonic tests were undertaken at 200, 400, and 800 kPa vertical
initial consolidation stages, because the sample slightly com- effective stress. Higher stresses were targeted in this study because
pressed the membrane adjacent to the Teflon rings. most previous testing on the effects of PT were focused on surficial
Monotonic shearing was undertaken at a rate of approximately samples through hand shear vane testing (as previously noted), or at
4%=h, and postcyclic shearing was at a rate of approximately lower stresses in the laboratory (Gholami and Simms 2015).
8%=h. As outlined subsequently, investigation of the effects of Monotonic and cyclic shearing were conducted under constant-
shear rate on undrained strength for the materials studies indicated volume conditions. Constant-volume conditions were enforced by
that increasing the rate from 4 to 8% was likely to have a negligible active computer-controlled variation to vertical load. It has previ-
effect on strength results. On this basis, the higher strain rate was ously been demonstrated (Finn 1985; Dyvik et al. 1987) that in
used for postcyclic testing as the DSS system used was under con- constant-volume conditions, changes to total stress are equivalent
sistently high demand, and the increased strain rate enabled two to increases or decreases of excess pore pressure in undrained test-
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tests to be completed within a 24 h period. Additional tests to assess ing. It is noted that this equivalence between reduction in total ver-
the effects of shear rate on the material were undertaken at approxi- tical stress and excess pore pressure in undrained tests implicitly
mate strain rates of 40 and 4,000%/h, respectively. It is noted that assumes that, when testing under constant-volume conditions,
4,000%/h is significantly higher than is typically applied in shear the material is sheared at a rate such that no excess pore pressure
rate studies. This high shear rate was selected as the primary in situ occurs within the constant-volume test, i.e., it is a drained constant-
parameter, and the test device used to assess material strength volume test. Constant-volume conditions can be achieved passively
during PT trials is often the hand shear vane (e.g., Cooling and (by clamping the system) or actively, through computer-control of
Beveridge 2015). This device is popular owing to its simplicity vertical load. Regardless of the method used, ASTM (2007) recom-
and low cost, and because many PT trials involve (at least initially) mends that for monotonic tests a maximum vertical strain of 0.05%
a relatively small thickness of material for which other in situ test occur during shearing to ensure constant-volume conditions. The
devices may not be suitable. However, the hand shear vane is typ- authors are unaware of any specific guidelines for cyclic testing.
ically sheared to failure rapidly, resulting in shear rates that may in As outlined in Tables 2 and 3, the recommended maximum vertical
some circumstances approach 4,000%=h. For this reason, an as- strain during shear was achieved for the majority of tests under-
sessment of the effects of such high strain rates on the strength taken. However, slightly higher vertical strains of 0.054–0.075%
of PT material, compared with UT material, is potentially important occurred in monotonic tests at 4,000% shear strain, and in two
when considering the frequent use of hand shear vane comparison of the cyclic tests. Although these strains are higher than recom-
testing in PT assessment trials. mended, the results for these tests are consistent with those for

Table 2. Monotonic Testing Summary


Approximate Shear stage Maximum axial
Test Sample 0
σvc shear rate Peak sample height strain during shear
number type (kPa) OCR (%=h) ec su (kPa) 0
su =σvc (mm) (%)
UT-M-01 UT 200 1 4 0.43 46.7 0.23 17.9 0.006
UT-M-02 UT 400 1 4 0.37 90.6 0.23 18.5 0.016
UT-M-03 UT 800 1 4 0.33 178.4 0.22 18.5 0.016
UT-M-04 UT 200 1 40 0.40 51.0 0.26 17.3 0.063
UT-M-05 UT 200 1 4,000 0.47 59.6 0.30 18.0 0.044
UT-M-06 UT 200 2 4 0.43 77.2 0.39 18.5 0.016
UT-M-07 UT 200 4 4 0.39 133.8 0.67 19.1 0.026
PT-M-01 PT 200 1 4 0.58 39.8 0.20 18.4 0.038
PT-M-02 PT 400 1 4 0.51 71.2 0.18 18.2 0.027
PT-M-03 PT 800 1 4 0.45 152.5 0.19 19.5 0.020
PT-M-04 PT 200 1 40 0.53 50.8 0.25 17.5 0.017
PT-M-05 PT 200 1 4,000 0.56 63.3 0.32 17.5 0.063
PT-M-06 PT 200 2 4 0.50 64.2 0.32 16.9 0.041
PT-M-07 PT 200 4 4 0.45 113.5 0.57 17.7 0.040

Table 3. Cyclic Testing Summary


Number of Number of Maximum axial strain
cycles to Maximum Shear stage cycles to during shear (%)
Test 0
Sample σvc CSR γ ¼ 3.75 cyclic strain Peak sample height γ ¼ 3.00
0 0
number type (kPa) ec (τ cyc =σvc ) (%) (%) sr (kPa) sr =σvc (mm) (%) Cyclic stage Postcyclic stage
UT-C-01 UT 200 0.41 0.120 22 10 38.0 0.19 18.9 21 0.048 0.011
UT-C-02 UT 200 0.41 0.151 9 17 31.2 0.16 19.0 9 0.042 0.005
UT-C-03 UT 200 0.39 0.107 59 30 21.0 0.11 18.7 57 0.032 0.027
UT-C-04 UT 200 0.42 0.166 5 5 38.4 0.19 18.2 4 0.044 0.022
PT-C-01 PT 200 0.57 0.160 7 6 38.8 0.19 18.6 6 0.054 0.005
PT-C-02 PT 200 0.57 0.121 22 14 31.7 0.16 17.9 21 0.073 0.022
PT-C-03 PT 200 0.59 0.107 73 19 29.3 0.15 17.7 69 0.034 0.011
PT-C-04 PT 200 0.59 0.138 11 21 25.0 0.13 18.4 9 0.065 0.022

© ASCE 04017007-3 J. Geotech. Geoenviron. Eng.

J. Geotech. Geoenviron. Eng., -1--1


the majority of tests where the requirement was achieved, as out- Table 4. Estimated Minimum Cyclic Load Time for Accurate Excess Pore
lined subsequently. Pressure Measurement
Cyclic loading consisted of a symmetric unidirectional sinusoi- Average t50 Required minimum
dal shear stress applied at a frequency of 0.1 Hz. Cyclic stress ratio Material at 200 kPa (s) cycle time (s)
(CSR) values ranging from 0.107 to 0.166 were applied. The onset UT 23 363
of cyclic liquefaction has been inferred as occurring at a shear PT 12 185
strain, γ cyc , of 3.75% (e.g., NRC 1985). All cyclic tests were there-
fore loaded until they exceeded this strain criterion. However,
rather than terminate cyclic testing at or slightly higher than this
value, cyclic loading was continued to a range of different strains is consistent with observations for a number of laboratory studies
for each test undertaken. This was conducted to provide an indi- on the effect of PT, as previously cited.
cation as to the effect of cyclic strain magnitude on resulting
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postcyclic strengths. All cyclic tests outlined in this study were


Inferring Excess Pore Pressure
undertaken at 200 kPa vertical effective stress.
Postcyclic testing of soil and tailings using a DSS apparatus to Donahue et al. (2008) discuss the required cyclic shear rates,
investigate material behavior following cyclic liquefaction on ele- with respect to the t50 relevant to the preceding consolidation stage,
ments of soil has become increasingly popular (Wijewickreme such that pore pressures within the sample remain at an equilibrium
et al. 2005; Al-Tarhouni et al. 2011; James et al. 2011; Sivathayalan level, i.e., zero, during shearing to enable accurate assessment of
and Yazdi 2014). However, as noted by previous workers excess pore pressure changes (and hence vertical effective stresses)
(Wijewickreme et al. 2005; James et al. 2011) it is unlikely that based on total stress changes in constant-volume DSS testing. They
cyclic testing on relatively small elements of soil will reproduce suggest that for inferred excess pore pressure changes to be accu-
the complex void ratio redistribution processes hypothesized rate in this manner, the time for one cycle of loading should be
(e.g., Kulasingam et al. 2004) to occur in full scale flow liquefac- greater than 16t50 of the material in the density and state relevant
tion events triggered by cyclic liquefaction. It is further noted that to cyclic loading.
the magnitude of cyclic straining of the sample appears to affect Estimates of t50 for tests at 200 kPa vertical effective stress were
resulting postcyclic strengths for some materials (Thiers and Seed made based on the log time method, as indicated in Table 4, along
1969; Castro 2003; Sivathayalan and Yazdi 2013; Dahl et al. 2014). with the estimated minimum cycle time such that excess pore pres-
On this basis, different cyclic strains were applied to the samples sures can be accurately measured. Comparison of these results with
tested, to assess the effect of PT and cyclic strain magnitude on the cycle time of 10 s (i.e., 0.1 Hz) used in this study suggests that
material behavior. The test conditions of cyclic and postcyclic tests excess pore pressures will not be accurately measured through
changes to vertical total stress for cyclic tests on this material at
are outlined in Table 3.
0.1 Hz. As such, these are not reported in the interpretation of cyclic
test results. Further, the interpretation undertaken indicates mono-
tonic tests at a strain rate of 4,000%=h are also unlikely to provide
Results and Discussion accurate excess pore pressure measurements during shear.

Consolidated Densities
Normally Consolidated Monotonic Undrained
The consolidated void ratios for monotonic DSS tests are shown Strengths—Slow Shear Rate
in Fig. 2. The consolidation paths of K 0 triaxial tests undertaken
by Reid and Fourie (2016) are included for comparison. The results The behavior of normally consolidated samples under monotonic
indicate that PT material exhibits a consistently looser state when shear at approximately 4%=h. strain rate are presented in Figs. 3
compared with UT material at a given vertical effective stress. and 4, with a summary presented in Table 2. The materials exhibit
This was seen across the range of vertical effective stresses targeted contractive behavior in undrained shear, resulting in normally con-
in this study. PT material is also more compressible in one- solidated peak undrained strength ratios of 0.22–0.23 for UT
material, and 0.18–0.20 for PT material. These strength results
dimensional loading. Further, the consolidated void ratios, and
for UT material are generally consistent with published examples
general trends between materials, are consistent with those ob-
of materials of similar PI (e.g., Ladd 1991). However, the lower
served by Reid and Fourie (2016) in triaxial conditions. This result
strength ratios for PT, despite higher PI, are inconsistent with gen-
eral trends which typically indicate an increase in DSS strength
ratio with increasing PI. Furthermore, lower normalized peak un-
drained strength ratios were also seen for PT material in triaxial
compression (Reid and Fourie 2016). These results were previously
seen to be consistent with the preshear state parameter Ψ0 (Been
and Jefferies 1985) seen for PT material. Although Ψ0 cannot be
inferred from DSS tests of the kind reported here which lack lateral
stress measurement, the similarity between the K 0 triaxial consoli-
dation paths and DSS consolidated densities suggests a similar
range of Ψ0 may apply to the DSS tests. Therefore, lower normal-
ized peak undrained strength ratios exhibited for PT materials
may be a result of their being in a looser state, relevant to the
CSL for PT material.
PT materials exhibited considerably lower shear stiffness than
Fig. 2. DSS consolidated densities for UT and PT, compared with K0
UT material, with peak strengths achieved for PT material at up
triaxial densities (adapted from Reid and Fourie 2016)
to 25–30% strain in some cases, compared with 10–13% for UT

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(a)

(b)

Fig. 3. UT monotonic DSS results: (a) stress strain; (b) stress path

(a)

(b)

Fig. 4. PT monotonic DSS results: (a) stress strain; (b) stress path

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Fig. 5. Peak undrained shear strengths versus void ratio, including


triaxial data (adapted from Reid and Fourie 2016) Fig. 7. Summary of rate effects on peak undrained shear strengths

samples. Such strains are somewhat higher than typical for most tests for both materials, compared with triaxial compression at the
materials when measured in DSS loading. Indeed, at such strains same density, are consistent with typical observations regarding
the ability of the DSS system to provide accurate results may be anisotropic undrained strength (e.g., Ladd 1991). The triaxial tests
questionable (Wijewickreme et al. 2005). However, the softer re- were sheared at approximately 1%=h, and hence strain rate effects are
sponse seen in PT material is consistent with previous triaxial test- unlikely to significantly contribute to the differences seen in Fig. 5.
ing on the material. Further, the peak undrained strength ratios seen
for PT material are consistent across the range of vertical effective
Strain Rate Effects
stresses applied in this study, including a test at 800 kPa where peak
strength occurred at a lower strain of 19%. Stress strain results for monotonic tests at 4, 40, and 4,000%=h
The peak undrained shear strength for each DSS test sheared at are shown in Fig. 6 for UT and PT materials. Consistent with
approximately 4%=h are presented against void ratio in Fig. 5. Data typical behavior of cohesive soils, increasing strain rate results
for the same materials in CIU and CK 0 U tests reported by Reid and in an increased undrained shear strength. Further, the results indi-
Fourie (2016) are included for comparison. The results indicate cate that increasing strain rate generally increases the strain to
higher strengths for PT material at a given density, consistent with failure γ f . These results in terms of peak undrained strengths
previously cited studies. The lower peak strengths obtained in DSS are summarized in Fig. 7.

(a)

(b)

Fig. 6. Rate effects on peak undrained shear strength—stress strain: (a) UT; (b) PT

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(a)

(b)

Fig. 8. OCR effects on peak undrained shear strength of UT material: (a) stress strain; (b) stress path

To quantify the effects of strain rate on strength, Sheahan et al. the literature. Although some early triaxial studies on rate effects
(1996) proposed the parameter ρε̇ a0: indicated that an increased strain rate could increase strain to failure
γ f (Bjerrum et al. 1958; Berre and Bjerrum 1973), as noted by
ρε̇ a0 ¼ ½ðΔsu =su0 Þ=Δ log ε̇a  Sheahan et al. (1996) the early studies cited used frictional ends.
As such, nonuniform stresses and strains and resulting pore water
where su0 = peak undrained shear strength at a reference strain rate migration may have affected the results obtained. Alternatively, the
of ε̇a ¼ ε̇a0 ; and Δsu = change in undrained strength across an in- work of Sheahan et al., which used lubricated ends and tested at a
crement of strain rate. This expression for ρε̇ a0 outlined above has range of OCRs, did not indicate an effect of strain rate on strain to
primarily been used to interpret triaxial data in the literature, and failure. Further, available data for simple shear and triaxial exten-
hence is based on axial strain rates. In this study, the same expres- sion loading previously cited do not indicate an effect on strain to
sion is used, interchanging shear strain for axial strain. The values failure from strain rate.
of ρε̇ a0 for different increments of strain increase are included in The increased sensitivity of PT to strain rate, compared with UT,
Fig. 6 for each strain increment in brackets, based on a reference may agree in a general sense with some correction methods for
strain rate of 4%=h ρε̇ a0 calculated for each increment of strain rate vane shear testing, which show an increase in shear rate sensitivity
is included on Fig. 7 in brackets. The results indicate that the un- with increasing PI (Bjerrum 1972; Chandler 1988). It has been sug-
drained strength of PT material is more sensitive to an increase in gested that much of the vane shear testing correction relationships
strain rate than UT material. Further, UT material exhibits a similar based on PI are a result of strain rate effects (e.g., Ladd and
range of ρε̇ a0 compared with previously published data (Sheahan DeGroot 2003).
et al. 1996). However, the values of ρε̇ a0 for PT material are gen-
erally higher than most published examples.
Overconsolidation Effects
It is noted that no study as comprehensive as that of Sheahan
et al. (1996) to study rate effects has been undertaken with a The results of monotonic tests at overconsolidation ratios (OCR) of
DSS apparatus. However, some relevant examples of the effect 1, 2, and 4 are shown in Fig. 8 for UT and Fig. 9 for PT materials.
of strain rate in simple shear and triaxial extension loading include Consistent with typical soil behavior, increasing OCR is seen to
Zhu and Yin (2000) and Biscontin (2001), who observed strength increase peak undrained shear strength and reduce positive excess
increases of 5–10% per log cycle of strain rate, generally consistent pore pressure generation during shear.
with the findings of Sheahan et al. (1996) for triaxial compression The plots shown in Figs. 8 and 9 allow SHANSEP (stress
loading. history and normalized engineering properties) equation coeffi-
The increased strain to failure γ f with increasing strain rate ob- cients S and m to be developed. For reference, the SHANSEP equa-
tained in this study is somewhat contradictory to data available in tion (Ladd and Foott 1974) is of the following form:

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(a)

(b)

Fig. 9. OCR effects on peak undrained shear strength of PT material: (a) stress strain; (b) stress path

su Cyclic Loading Results


¼ SðOCRÞm
σv0
The behavior of the materials under cyclic loading is shown in
where S = value of 0
su =σvc for OCR ¼ 1; and m = slope of the Figs. 11 and 12 for UT and PT materials, respectively, when loaded
0
su =σvc versus OCR relationship in log-log space. The results of by a CSR of 0.107. The results are truncated to a strain of 10%
OCR testing are summarized in Fig. 10, which indicate SHANSEP for clarity. Stress strain loops for the same tests are compared in
parameters of S ¼ 0.23 and m ¼ 0.76 for UT material, with S ¼ Fig. 13. The loops shown are those where the tests first reach
0.20 and m ¼ 0.76 for PT material. The identical m values suggest γ cyc: ¼ 3.75%. As each test had a slightly asymmetrical strain bias
the effects of overconsolidation on increased peak undrained (in opposite directions) at this point, in Fig. 13 the PT sample result
strength is similar for both materials. This may be of importance has been shifted by þ0.6% shear strain to enable a more direct
when considering the implications of air drying thin lifts of PT comparison of stress-strain loop shape. Qualitatively, the stress
material, as is currently considered a promising method for improv- strain behavior of either material does not develop the flat middle
ing mature fine tailings deposition behavior and strength increase portions of negligible stiffness often seen for sands. This is consis-
for the oil sands industry (e.g., Caldwell et al. 2014). tent for the PI of the materials, which on the basis of classification
systems proposed by Boulanger and Idriss (2006) would indicate
that PT is a clay-like material with respect to cyclic response,
whereas UT material is at the approximate boundary between
transition and clay-like soils.
A summary of the cyclic results, in terms of number of cycles to
achieve γ cyc: ¼ 3.75%, is shown in Fig. 14 and Table 5. The results
are seen to be indistinguishable, in the context of typical cyclic test-
ing repeatability. Table 5 includes both cyclic resistance ratio
(CRR15 ) results for a γ cyc: ¼ 3.75% criterion, and CRR30 results
for a γ cyc: ¼ 3.0% criterion as suggested for clay-like soils by
Boulanger and Idriss (2007). The CRR results under both criteria
are essentially indistinguishable for the two materials. Both
measures of CRR are compared in Table 5, owing to the range
of PI of the materials tested.
That the two materials exhibited essentially identical cyclic
Fig. 10. Summary of OCR effects on peak undrained shear strength,
resistances, despite the PT material being at a significantly lower
SHANSEP interpretation
density, is unusual because of the dependence of CRR on density

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Fig. 11. UT sample, cyclic DSS results, test UT-C-03 (CSR 0.107), stress strain

Fig. 12. PT sample, cyclic DSS results, test PT-C-03 (CSR 0.107), stress

(e.g., De Alba et al. 1976). However, CRR has also been shown to incorporated into some cyclic liquefaction assessment techniques
be significantly affected by material fabric (Mulilis et al. 1977). that extend to clayey materials (Robertson 2009). However, as
Therefore, the two effects of density and fabric may be counteract- noted by Boulanger and Idriss (2007), the ratio ðτ cyc: =su ÞN¼30
ing one another. Further, it is noted that cyclic resistance has been for young materials reconstituted in the laboratory is often lower
shown to be controlled by distance to the CSL (Jefferies and Been than for natural soils that have undergone ageing, and that are tested
2015). Therefore, the apparent modification to the CSL owing to from recovered samples. Therefore, it might be suggested that for
PT may result in both materials having similar states with respect to young artificial materials such as tailings, a lower assumed ratio of
the CSL, under the cyclic test conditions. τ cyc: =su be used when interpreting in situ test data.
Included in Table 5 are comparisons of CRR30 to the normalized
peak undrained strength for the two materials, indicating τ cyc: =su
ratios of approximately 0.50–0.65. This range of ratios is Postcyclic Results
lower than observed for many predominately clay soils, where The stress-strain results of postcyclic tests on UT material are
an average of 0.8 has been proposed for use in some assessment shown in Fig. 15, with PT tests shown in Fig. 16. Monotonic tests
methods (Boulanger and Idriss 2007). Indeed, this ratio has been undertaken from the same consolidated vertical effective stress are

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Fig. 13. Stress strain comparison at γcyc. approximately 3.75%

• Increasing cyclic strain magnitude reduces postcyclic peak


strength, and generally reduces the stiffness of the material in
postcyclic shearing. This decay in postcyclic strength with max-
imum cyclic strain γ cyc: during cyclic loading has been demon-
strated, in laboratory element tests, for a number of materials
(Thiers and Seed 1969; Castro 2003; Sivathayalan and Yazdi
2013; Dahl et al. 2014).
The normalized postcyclic strengths for all the tests undertaken
are summarized in Fig. 17, to enable a direct comparison of the
results. Aside from slight initial differences in monotonic strengths,
the decay of postcyclic strength with cyclic strain is nearly indis-
tinguishable for the two materials.
In some previous postcyclic test campaigns, the decay in post-
Fig. 14. Cyclic DSS test results for onset of cyclic liquefaction cyclic strengths with cyclic strain has been shown to be less for
(γ ¼ 3.75%) higher plasticity materials (Dahl et al. 2014). Further, in one exam-
ple (Reid and Boshoff 2015), PT of a lateritic nickel tailings was
shown to decrease postcyclic strengths compared with UT material.
Table 5. CRR Comparisons However, neither the increase in plasticity induced by PT in this
study, nor the PT process and resulting fabric and density changes
CRR15 CRR30 Average
0 significantly affected the results obtained.
Material (γ cyc: ¼ 3.75%) (γ cyc: ¼ 3.00%) su =σvc ðτ cyc: =su ÞN¼30
Typically, a cyclic strain target was set prior to testing. When
UT 0.135 0.12 0.23 0.52 prespecified in this manner, the device returned to an approximate
PT 0.135 0.12 0.19 0.63 zero stress/strain condition prior to commencing postcyclic shear-
ing. However, for two tests, the authors elected to override the
automatic termination, to achieve a different prespecified maxi-
included for comparison in both figures. The postcyclic testing mum cyclic strain magnitude. This resulted in postcyclic shearing
indicates the following: commencing from a nonzero stress/strain condition, as seen for
• The qualitative postcyclic response, wherein samples initially tests UT-C-03 and PT-C-03 in Figs. 15 and 16, respectively.
exhibit low stiffness which subsequently increases with further Despite the different initial stress conditions in postcyclic shearing
strain, has been observed in DSS postcyclic testing on for these two samples, similar postcyclic strength trends were ob-
many materials, including water-pluviated sands (Vaid and tained (Fig. 17).
Sivathayalan 1997) and mine tailings (Wijewickreme et al. The postcyclic results are generally inconsistent with some in
2005; James et al. 2011). situ vane shear data (Beier et al. 2013) which have suggested that
• Shear strains of approximately 40–60% to develop peak post- for some materials, PT can increase sensitivity. However, residual
cyclic undrained strength are consistent with other published vane shear and postcyclic testing are significantly different in terms
results (e.g., Wijewickreme et al. 2005; James et al. 2011; of strain magnitude (e.g., Poulos et al. 1985) and the loading
Sivathayalan and Yazdi 2013). However, as noted by mechanism—although residual shear strengths are often referenced
Wijewickreme et al. (2005), at this level of strain the reliability as the likely minimum postseismic undrained strength following
of test results may become questionable. high cyclic straining (Farrar 2010; Stark et al. 2012).

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Fig. 15. UT material, postcyclic stress strain summary

Fig. 16. PT material, postcyclic stress strain summary

• Whereas lower densities at a lower effective stress are consis-


tently observed for PT material, this does not appear to result in
lower strengths or increased brittleness or loss of strength when
compared with UT material;
• The results obtained here do not provide an indication of the
potential for ageing to negatively affect the behavior of PT
samples. Should the higher strengths observed (when refer-
enced to density) be a result of the polymer itself, then ageing
may reduce the available strength and/or increase contractive-
ness and sensitivity of a PT material. This is the subject of
ongoing research;
• Caution should be applied when interpreting hand shear vane
results in PT material, because a higher cv results in an increased
potential for partial drainage during shearing, whereas an in-
Fig. 17. Postcyclic summary, peak strength versus cyclic strain creased susceptibility to strain rate effects may indicate existing
magnitude vane shear correction procedures do not apply to PT material.
Both potential effects with respect to vane shear testing may
give higher, nonconservative undrained strength results, if not
recognized during a site investigation;
Implications for Tailings Storage Facility (TSF) Design
• The SHANSEP method for normalizing strength results based
The results obtained in this study are of relevance to the design of on stress history was successfully applied to PT material. This
potential TSFs with PT tailings deposition. Implications of this may be of benefit when accounting for the effect of air drying-
study for TSF design include the following: induced overconsolidation in PT tailings deposits; and

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• The variation in Atterberg limits following PT may obscure the Bjerrum, L., Simons, N., and Toblaa, I. (1958). “The effect of time on the
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A laboratory study was undertaken to assess the effects of PT on the
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and triaxial compression behavior. The results of the laboratory “Optimised season deposition for successful management of treated
testing indicate that, similar to previous slurry consolidometer mature fine tailings.” Paste 2014, Proc., 17th Int. Seminar on Paste
and triaxial consolidation results, PT results in lower densities at and Thickened Tailings, R. J. Jewell, A. B. Fourie, P. S. Wells, and
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Cooling, D., and Beveridge, A. (2015). “Use of Rheomax ETD technology
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for financial support of this study, the mechanical, electronics, and Environmental Engineer, Univ. of California, Berkeley, Berkeley, CA.
laboratory staff at UWA for their support, and BASF for advice and Dyvik, R., Berre, T., Lacasse, S., and Raadim, B. (1987). “Comparison
assistance in polymer selection and preparation. The authors also of truly undrained and constant volume direct simple shear tests.”
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acknowledge the anonymous reviewers of this manuscript, whose
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feedback improved this document’s clarity.
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