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Abstract: A laboratory study was undertaken to assess the effects of polymer treatment (PT) on the monotonic, cyclic, and postcyclic
behavior of a low plasticity slurry using a direct simple shear (DSS) apparatus. This study was conducted to extend the results of previous
testing that assessed the effects of PT on the same material’s consolidation behavior and critical state line. Consistent with previous tests
on this material, DSS testing indicated that PT resulted in lower consolidated densities at a given magnitude of effective stress, and higher
undrained shear strengths at a given density. PT appeared to increase the effects of strain rate on strength, whereas both PT and untreated
materials responded similarly to the effects of overconsolidation. Cyclic and postcyclic testing indicated essentially indistinguishable
results for the two materials. The effects of PT were seen to persist at vertical effective stresses up to 800 kPa. The potential implications
of these findings for tailings design are discussed. DOI: 10.1061/(ASCE)GT.1943-5606.0001660. © 2017 American Society of Civil
Engineers.
The material developed by Reid and Fourie (2016), and used in this Geotechnical Institute (SGI) type. The device consists of vertical
study was made from a combination of kaolin, silica 200G silt, and and horizontal electromechanical motors, load cells, and linear
silica fine (SF) sand, all produced by Sibelco Australia Ltd. A com- variable displacement transducers (LVDT). The samples were sur-
bination of 31% SF sand, 43% silica 200G, and 26% kaolin by dry rounded by a latex membrane and a series of Teflon rings to min-
mass was found to produce a material that met the requirements imize lateral strain. A schematic of the testing system is provided
previously outlined (i.e., to be susceptible to liquefaction, and ame- in Fig. 1.
nable to polymer treatment). The mixture had a specific gravity It is noted that although Teflon rings may be more common
(SG) of 2.62. The resulting gradation and plasticity of the material in commercial DSS testing, the majority of published data in
are generally consistent with examples of tailings from a variety of the geotechnical literature appears to be obtained using a steel-
mineral types, including iron ore, gold, mineral sands, and nickel wire reinforced rubber membrane, referred to as the Norwegian
tailings. Further information on the slurry constituents is provided Geotechnical Institute (NGI) type. However, a comparison of
by Reid and Fourie (2016). the two lateral restraint types undertaken by McGuire (2011) indi-
The PT process undertaken (discussed subsequently) was found cated negligible difference in the results obtained, provided that
to modify the material’s liquid limit, plastic limit and plasticity corrections for the influence of friction related to the lateral con-
index (PI) significantly, as outlined in Table 1. Liquid limit was finement components was made. The correction technique outlined
measured with the fall cone method. The variance of Atterberg lim- by McGuire (2011) was applied to test results outlined herein.
its following PT is consistent with previous experimental data The system used filter stones with protruding pins to reduce the
(Jeeravipoolvarn et al. 2009; Beier et al. 2013; Manzotti et al. 2014) potential for sliding between the soil and platen. A total of 18 pins
were placed on each of the top and bottom platens, with the pins
approximately 1 mm high and 1 mm in diameter. The use of this
Sample Preparation and Polymer Treatment
form of pins is consistent with the current state of practice for DSS
BASF Australia Pty Ltd (BASF) provided assistance to the authors testing (e.g., ASTM 2007). In test interpretations presented sub-
in selecting a polymer for use in the experimental study. Polymer sequently, shear strain γ was calculated based on a sample height
type and dosage were selected on the basis of a series of dewatering measured between the two filter stones, i.e., the length of the pins
tests where the treated materials were poured into geotextile-lined was not considered in strain calculations.
columns with base drainage, and increase in solids content was As noted previously, the initial specimen diameter after
tracked over time. The screening assessment undertaken by BASF extrusion from columns was approximately 63.6 mm. The internal
indicated that the high molecular weight polymer RHEOMAX diameter of the Teflon rings was 64.5 mm, and the triaxial mem-
ETD DPW 1687, at a dose of 500 g of dry polymer to ton of brane used was approximately 0.3–0.5 mm thick, depending on
dry solids was well suited to the treatment of the slurry developed pressure applied (i.e., with calipers when measuring). Thus, when
from this study with respect to increased dewatering rates. initially assembling the membrane and rings around the sample, it
The slurry material was initially mixed in a dry state to the mass was found to be a reasonably tight fit with no gaps apparent.
proportions previously outlined. Tap water was then added to make Because the likely slight reduction in thickness of the membrane
up a slurry at 122% gravimetric water content (GWC), and mixed as increasing horizontal pressure was applied during consolidation,
thoroughly in a 20 L bucket. During mixing, 2 g of sodium chloride
salt per liter of slurry was added, to increase the dissolved solids to
a range more typical of a tailings process fluid. After mixing, the
material was left for two days to allow the kaolin particles to hy-
drate. At this point, material that was to be used as UT slurry was
decanted, with sufficient clear water removed to produce a resulting
slurry with approximately 45% GWC. This decanting was under-
taken to produce a nonsegregating slurry.
For PT batches, polymer solution was made up one day prior to
use, at a mass concentration of 0.25% The settled slurry (without
decanting) was again thoroughly mixed, with the first half of the
polymer solution added once the material was remixed. The
material was then poured into another 20 L bucket, then back into
the original bucket. The second half of the polymer solution was
then added, followed by four additional pours between buckets.
To prepare the material for DSS testing, columns with 63.6 mm
internal diameter were prepared with a filter and drainage medium
Fig. 1. Schematic of DSS system with sample prepared for test
at the base. UT material was poured into the columns, whereas PT
tests to be completed within a 24 h period. Additional tests to assess ing. It is noted that this equivalence between reduction in total ver-
the effects of shear rate on the material were undertaken at approxi- tical stress and excess pore pressure in undrained tests implicitly
mate strain rates of 40 and 4,000%/h, respectively. It is noted that assumes that, when testing under constant-volume conditions,
4,000%/h is significantly higher than is typically applied in shear the material is sheared at a rate such that no excess pore pressure
rate studies. This high shear rate was selected as the primary in situ occurs within the constant-volume test, i.e., it is a drained constant-
parameter, and the test device used to assess material strength volume test. Constant-volume conditions can be achieved passively
during PT trials is often the hand shear vane (e.g., Cooling and (by clamping the system) or actively, through computer-control of
Beveridge 2015). This device is popular owing to its simplicity vertical load. Regardless of the method used, ASTM (2007) recom-
and low cost, and because many PT trials involve (at least initially) mends that for monotonic tests a maximum vertical strain of 0.05%
a relatively small thickness of material for which other in situ test occur during shearing to ensure constant-volume conditions. The
devices may not be suitable. However, the hand shear vane is typ- authors are unaware of any specific guidelines for cyclic testing.
ically sheared to failure rapidly, resulting in shear rates that may in As outlined in Tables 2 and 3, the recommended maximum vertical
some circumstances approach 4,000%=h. For this reason, an as- strain during shear was achieved for the majority of tests under-
sessment of the effects of such high strain rates on the strength taken. However, slightly higher vertical strains of 0.054–0.075%
of PT material, compared with UT material, is potentially important occurred in monotonic tests at 4,000% shear strain, and in two
when considering the frequent use of hand shear vane comparison of the cyclic tests. Although these strains are higher than recom-
testing in PT assessment trials. mended, the results for these tests are consistent with those for
Consolidated Densities
Normally Consolidated Monotonic Undrained
The consolidated void ratios for monotonic DSS tests are shown Strengths—Slow Shear Rate
in Fig. 2. The consolidation paths of K 0 triaxial tests undertaken
by Reid and Fourie (2016) are included for comparison. The results The behavior of normally consolidated samples under monotonic
indicate that PT material exhibits a consistently looser state when shear at approximately 4%=h. strain rate are presented in Figs. 3
compared with UT material at a given vertical effective stress. and 4, with a summary presented in Table 2. The materials exhibit
This was seen across the range of vertical effective stresses targeted contractive behavior in undrained shear, resulting in normally con-
in this study. PT material is also more compressible in one- solidated peak undrained strength ratios of 0.22–0.23 for UT
material, and 0.18–0.20 for PT material. These strength results
dimensional loading. Further, the consolidated void ratios, and
for UT material are generally consistent with published examples
general trends between materials, are consistent with those ob-
of materials of similar PI (e.g., Ladd 1991). However, the lower
served by Reid and Fourie (2016) in triaxial conditions. This result
strength ratios for PT, despite higher PI, are inconsistent with gen-
eral trends which typically indicate an increase in DSS strength
ratio with increasing PI. Furthermore, lower normalized peak un-
drained strength ratios were also seen for PT material in triaxial
compression (Reid and Fourie 2016). These results were previously
seen to be consistent with the preshear state parameter Ψ0 (Been
and Jefferies 1985) seen for PT material. Although Ψ0 cannot be
inferred from DSS tests of the kind reported here which lack lateral
stress measurement, the similarity between the K 0 triaxial consoli-
dation paths and DSS consolidated densities suggests a similar
range of Ψ0 may apply to the DSS tests. Therefore, lower normal-
ized peak undrained strength ratios exhibited for PT materials
may be a result of their being in a looser state, relevant to the
CSL for PT material.
PT materials exhibited considerably lower shear stiffness than
Fig. 2. DSS consolidated densities for UT and PT, compared with K0
UT material, with peak strengths achieved for PT material at up
triaxial densities (adapted from Reid and Fourie 2016)
to 25–30% strain in some cases, compared with 10–13% for UT
(a)
(b)
Fig. 3. UT monotonic DSS results: (a) stress strain; (b) stress path
(a)
(b)
Fig. 4. PT monotonic DSS results: (a) stress strain; (b) stress path
samples. Such strains are somewhat higher than typical for most tests for both materials, compared with triaxial compression at the
materials when measured in DSS loading. Indeed, at such strains same density, are consistent with typical observations regarding
the ability of the DSS system to provide accurate results may be anisotropic undrained strength (e.g., Ladd 1991). The triaxial tests
questionable (Wijewickreme et al. 2005). However, the softer re- were sheared at approximately 1%=h, and hence strain rate effects are
sponse seen in PT material is consistent with previous triaxial test- unlikely to significantly contribute to the differences seen in Fig. 5.
ing on the material. Further, the peak undrained strength ratios seen
for PT material are consistent across the range of vertical effective
Strain Rate Effects
stresses applied in this study, including a test at 800 kPa where peak
strength occurred at a lower strain of 19%. Stress strain results for monotonic tests at 4, 40, and 4,000%=h
The peak undrained shear strength for each DSS test sheared at are shown in Fig. 6 for UT and PT materials. Consistent with
approximately 4%=h are presented against void ratio in Fig. 5. Data typical behavior of cohesive soils, increasing strain rate results
for the same materials in CIU and CK 0 U tests reported by Reid and in an increased undrained shear strength. Further, the results indi-
Fourie (2016) are included for comparison. The results indicate cate that increasing strain rate generally increases the strain to
higher strengths for PT material at a given density, consistent with failure γ f . These results in terms of peak undrained strengths
previously cited studies. The lower peak strengths obtained in DSS are summarized in Fig. 7.
(a)
(b)
Fig. 6. Rate effects on peak undrained shear strength—stress strain: (a) UT; (b) PT
(a)
(b)
Fig. 8. OCR effects on peak undrained shear strength of UT material: (a) stress strain; (b) stress path
To quantify the effects of strain rate on strength, Sheahan et al. the literature. Although some early triaxial studies on rate effects
(1996) proposed the parameter ρε̇ a0: indicated that an increased strain rate could increase strain to failure
γ f (Bjerrum et al. 1958; Berre and Bjerrum 1973), as noted by
ρε̇ a0 ¼ ½ðΔsu =su0 Þ=Δ log ε̇a Sheahan et al. (1996) the early studies cited used frictional ends.
As such, nonuniform stresses and strains and resulting pore water
where su0 = peak undrained shear strength at a reference strain rate migration may have affected the results obtained. Alternatively, the
of ε̇a ¼ ε̇a0 ; and Δsu = change in undrained strength across an in- work of Sheahan et al., which used lubricated ends and tested at a
crement of strain rate. This expression for ρε̇ a0 outlined above has range of OCRs, did not indicate an effect of strain rate on strain to
primarily been used to interpret triaxial data in the literature, and failure. Further, available data for simple shear and triaxial exten-
hence is based on axial strain rates. In this study, the same expres- sion loading previously cited do not indicate an effect on strain to
sion is used, interchanging shear strain for axial strain. The values failure from strain rate.
of ρε̇ a0 for different increments of strain increase are included in The increased sensitivity of PT to strain rate, compared with UT,
Fig. 6 for each strain increment in brackets, based on a reference may agree in a general sense with some correction methods for
strain rate of 4%=h ρε̇ a0 calculated for each increment of strain rate vane shear testing, which show an increase in shear rate sensitivity
is included on Fig. 7 in brackets. The results indicate that the un- with increasing PI (Bjerrum 1972; Chandler 1988). It has been sug-
drained strength of PT material is more sensitive to an increase in gested that much of the vane shear testing correction relationships
strain rate than UT material. Further, UT material exhibits a similar based on PI are a result of strain rate effects (e.g., Ladd and
range of ρε̇ a0 compared with previously published data (Sheahan DeGroot 2003).
et al. 1996). However, the values of ρε̇ a0 for PT material are gen-
erally higher than most published examples.
Overconsolidation Effects
It is noted that no study as comprehensive as that of Sheahan
et al. (1996) to study rate effects has been undertaken with a The results of monotonic tests at overconsolidation ratios (OCR) of
DSS apparatus. However, some relevant examples of the effect 1, 2, and 4 are shown in Fig. 8 for UT and Fig. 9 for PT materials.
of strain rate in simple shear and triaxial extension loading include Consistent with typical soil behavior, increasing OCR is seen to
Zhu and Yin (2000) and Biscontin (2001), who observed strength increase peak undrained shear strength and reduce positive excess
increases of 5–10% per log cycle of strain rate, generally consistent pore pressure generation during shear.
with the findings of Sheahan et al. (1996) for triaxial compression The plots shown in Figs. 8 and 9 allow SHANSEP (stress
loading. history and normalized engineering properties) equation coeffi-
The increased strain to failure γ f with increasing strain rate ob- cients S and m to be developed. For reference, the SHANSEP equa-
tained in this study is somewhat contradictory to data available in tion (Ladd and Foott 1974) is of the following form:
(a)
(b)
Fig. 9. OCR effects on peak undrained shear strength of PT material: (a) stress strain; (b) stress path
Fig. 11. UT sample, cyclic DSS results, test UT-C-03 (CSR 0.107), stress strain
Fig. 12. PT sample, cyclic DSS results, test PT-C-03 (CSR 0.107), stress
(e.g., De Alba et al. 1976). However, CRR has also been shown to incorporated into some cyclic liquefaction assessment techniques
be significantly affected by material fabric (Mulilis et al. 1977). that extend to clayey materials (Robertson 2009). However, as
Therefore, the two effects of density and fabric may be counteract- noted by Boulanger and Idriss (2007), the ratio ðτ cyc: =su ÞN¼30
ing one another. Further, it is noted that cyclic resistance has been for young materials reconstituted in the laboratory is often lower
shown to be controlled by distance to the CSL (Jefferies and Been than for natural soils that have undergone ageing, and that are tested
2015). Therefore, the apparent modification to the CSL owing to from recovered samples. Therefore, it might be suggested that for
PT may result in both materials having similar states with respect to young artificial materials such as tailings, a lower assumed ratio of
the CSL, under the cyclic test conditions. τ cyc: =su be used when interpreting in situ test data.
Included in Table 5 are comparisons of CRR30 to the normalized
peak undrained strength for the two materials, indicating τ cyc: =su
ratios of approximately 0.50–0.65. This range of ratios is Postcyclic Results
lower than observed for many predominately clay soils, where The stress-strain results of postcyclic tests on UT material are
an average of 0.8 has been proposed for use in some assessment shown in Fig. 15, with PT tests shown in Fig. 16. Monotonic tests
methods (Boulanger and Idriss 2007). Indeed, this ratio has been undertaken from the same consolidated vertical effective stress are
and triaxial compression behavior. The results of the laboratory “Optimised season deposition for successful management of treated
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for financial support of this study, the mechanical, electronics, and Environmental Engineer, Univ. of California, Berkeley, Berkeley, CA.
laboratory staff at UWA for their support, and BASF for advice and Dyvik, R., Berre, T., Lacasse, S., and Raadim, B. (1987). “Comparison
assistance in polymer selection and preparation. The authors also of truly undrained and constant volume direct simple shear tests.”
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acknowledge the anonymous reviewers of this manuscript, whose
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