Quantachrome® ASiQwin™- Automated Gas Sorption Data

Acquisition and Reduction

© 1994-2012, Quantachrome Instruments
version 3.0

Analysis Report
Operator: Lab. Energi ITS Date:2019/10/02 Operator: Lab. Energi ITS Date:2019/10/04
Sample ID: EI-564 SAMPEL1 Filename: iq_phisy_st1_2019_10_02_09_04_29EI-564 SAMPEL1.qps
Sample Desc: Comment:
Sample Weight: 0.6912 g Instrument: Autosorb iQ Station 1
Approx. Outgas Time:12.2 hrs Final Outgas Temp.: 100 °C Extended info: Available
Analysis gas: Nitrogen Non-ideality: 6.58e-05 1/Torr CellType: 9mm w/o rod
Analysis Time: 2:10 hr:min Bath temp.: 77.35 K
Analysis Mode: Standard VoidVol Remeasure: off
VoidVol. Mode: He Measure Cold Zone V: 10.0004 cc Warm Zone V: 16.5658 cc
HK method : Volume
Data Reduction Parameters
Thermal Transpiration: on Eff. mol. diameter (D): 3.54 Å Eff. cell stem diam. (d): 4.0000 mm
HK method Tabulated data interval: 1
Adsorbate Nitrogen Temperature 77.350K
Molec. Wt.: 28.013 Cross Section: 16.200 Ų Liquid Density:
-24
0.808 g/cc
Avg. Diameter:0.300 nm 14
Polarizability: 1.460 (cc/molec) x 10 Magn. Suscept.: 2.000
Molec. Density6.700 (mol/cm²)x10
Adsorbent Carbon 14 -24
Atom Diameter: 0.340 nm Surf. Atom Dens.: 38.450 (mol/cm²)x10 -29Polarizability: 1.020 (cc/molec)x10
Magn. Susc.: 13.500 (cc/molec)x10

V dV

0.0840 0.0786
0.0800 0.0748
0.0760 0.0711
0.0720 0.0673
0.0680 0.0636
0.0640 0.0599
0.0600 0.0561
Cumulative Pore Volume (cc/g)

Pore Volume [dV(r)] (cc/Å/g)

0.0560 0.0524
0.0520 0.0486
0.0480 0.0449
0.0440 0.0411
0.0400 0.0374
0.0360 0.0337
0.0320 0.0299
0.0280 0.0262
0.0240 0.0224
0.0200 0.0187
0.0160 0.0150
0.0120 0.0112
0.0080 0.0075
0.0040 0.0037
0.0000 0.0000
0.00 4.00 8.00 10.70

Half pore width (Å)

HK method summary
Mode : 1.838 Å

Quantachrome® ASiQwin™- Automated Gas Sorption Data Acquisition and Reduction © 1994-2012, Quantachrome Instruments version 3.0 Report id:{909043898:20191004 100840968} Page 1 of 1