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The Savvy Separator Series

UNDERPERFORMING
GAS SCRUBBERS
HOW TO FIX
THEM AND
HOW TO
AVOID THEM

Elizabeth Morillo, Victor van Asperen, and Sander


Baaren, FMC Technologies Separation Systems Inc.
I
n this sixth article of the Oil and Gas Facilities Savvy conditioning in the pipe upstream and inside gas scrubbers
Separator series, underperforming gas scrubbers are from day one to decommissioning. Otherwise, scrubbers
discussed. Introduced last June, the series presents become no more than expensive containers that can cause
helpful design know-how, lessons learned, and solutions for multiple operational problems, or even downtime, inside a
separation problems. production facility.
Traditionally, the main drivers for sizing gas scrubbers A systematic and holistic approach for scrubber design
in the oil and gas industry have been performance should be the result of an iterative process that begins by
requirements, process conditions, and project specifications. clearly defining the basis for design (relevant process data
Unfortunately, too often space limitation, deadlines, and conditions*) and the performance requirements for the
budgetary constraints seem to take priority over the sizing vessel. But it also must comprise the use of tools such as
task, leaving the fundamentals of phase separation as inlet flow regime analysis, empirical efficiency correlations,
just an afterthought in the design process. It is frequently and in some cases, computational fluid dynamics (CFD)
overlooked that optimizing cost, delivery times, and simulations to support the results. The method should also
weight is not the same as improving scrubber performance. consider the effects of high-pressure conditions and low
In reality, it is difficult to point out a single reason, interfacial tension on gas demisting and upstream piping on
as there are numerous ones, to explain why actual flow distribution when necessary. Mark Bothamley’s series
performance is so easily disregarded in the design process, of articles in the Oil and Gas Facilities magazine (2013a,
often leading to inadequate gas scrubber sizing. Just a few 2013b, 2013c) provides clear guidelines for the task of
worth mentioning follow: separator/scrubber design.
• Old-fashioned practices that rely on criteria-based This article uses a case study to illustrate how
design methodologies an inadequate sizing methodology hinders scrubber
• Lack of consideration of the system as a whole (effects performance. In this case, the scrubber was causing
on processing equipment downstream, and actual contamination of the downstream equipment due to
performance of upstream equipment) excessive liquid carry-over. The causes for the carry-over
• Compartmentalized design teams, piping engineers, are identified, and later in this article a potential solution
process engineers, project engineers, and contractors is presented for revamping this vessel. For illustration
working separately on their portion of the project purposes, a new scrubber is designed based on a systematic
• Overconfidence in process guarantees provided by design approach, and the newly designed vessel is compared
vendors without being able to validate them to the original design. The comparison is based on three
different aspects in order to highlight the benefits of
These common practices, however, have to be using a more consistent design methodology: the final
questioned when their shortcomings so often result in the
need for expensive fixes just after plant startup. Adequate *Startup, shutdown, and blowdown scenarios; normal, maximum, and minimum
phase separation has to be achieved through proper flow operating conditions; and correct fluid properties shall be included (Chin 2015).

Max Case
Operating Pressure barg 8.20

Gas Flow MMSCF/D 121.70 2

Gas Density kg/m3 8.41

Liquid Density kg/m3 674.90

Liquid Viscosity cP 0.39


1 Main Geometry
Interfacial Tension dyne/cm 17.01
Vessel ID 1920 mm
Liquid Volume Fraction % 0.10
Tan/Tan 4500 mm
Vessel k-value* m/s 0.18

Inlet Momentum kg/(m⋅s2) 6892

*Vessel k-value from the Souders-Brown equation (Bothamley 2013b).

Fig. 1—The original gas scrubber main geometry and basis for design. (1) Vane-type inlet device and (2) vane-type demister in vertical
orientation.

April 2016 ¥ Oil and Gas Facilities 17


Separation Performance

Demisting
Efficiency Correlation
• Liquid load • Gas momentum per tube • Surface tension

Agglomerator
Efficiency Correlation
• k-value • Liquid load factor (G/L ratio) • Surface tension

Gravity Separation
Droplet-size distribution in inlet pipe and
theoretical cut size

Inlet Arrangement
Separation of bulk liquid
flow regime and entrainment of droplets in the pipe
Upstream Piping
Flow regime and
entrainment of droplets in the pipe

Fig. 2—Factors used in the analysis of key components of a gas scrubber to evaluate separation performance.

configuration of the equipment, estimated carry-over, and Fig. 2 was used as a guide to perform the design
flow distribution through the vessel based on CFD analysis. evaluation. It is a diagram for a separation performance
evaluation showing some of the factors that must be
Case Study: First-Stage Suction considered when designing and assessing gas scrubbers.
Scrubber An inherently important aspect for all separation stages
The case study comes from an underperforming gas is the flow distribution, which strongly depends on the
scrubber that was sized using criteria-based design configuration of internals, vessel layout, and inlet piping.
methodologies. The separation performance requirement This will be demonstrated in the analysis below.
specified for the vessel was 0.1 USG/MMSCF (maximum
allowable liquid carry-over in the gas), as expected for this Upstream piping. Layout of the upstream piping can have
type of application. However, high levels of liquid carry- a positive or negative influence on the separation efficiency
over were detected when the vessel was operated at the of a vessel, and these effects are usually underevaluated.
higher end of the flow rate envelope (max design case). Unfavorable piping arrangements may, for example, lead to
Crude oil contamination of downstream compressors swirling flow, slugging behavior, liquid re-entrainment, and
caused by excessive liquid carry-over prompted the reduction in droplet size distribution affecting the overall
separation performance evaluation presented below. performance of the scrubber. (Heijckers 2012).
Fig. 1 shows the main geometry of the gas scrubber Upstream piping layout and geometry of this vessel
and the basis for design. The following process internals complies with general inlet piping requirements: there are
were originally installed in the first-stage suction scrubber: no out-of-plane bends with a straight pipe length equivalent
(1) a vane-type inlet device, and (2) a vane-type demister in to 10 times the inlet nozzle inside diameter (ID) in front of
vertical orientation. the vessel.
However, an important aspect was possibly overlooked,
Scrubber Performance Evaluation perhaps not even calculated: the entrainment of droplets
The aim of this analysis was to demonstrate how partial in the pipe. Depending on the flow regime, liquids can be
understanding of the fundamentals of phase separation when found in both bulk and droplet form and their proportion
sizing a scrubber can lead to operational problems (e.g., can vary depending on the actual momentum and the
excessive liquid carry-over). The conclusions drawn from the liquid volume fraction of the system. That is why the first
analysis will be used for the following. tool needed when designing a gas scrubber is one that can
• The redesign of a new version of this gas scrubber approximate the theoretical amount of entrained liquid in
that would work properly under the stated the form of droplets inside the inlet pipe so appropriate
conditions. measures can be taken regarding the size of the inlet pipe or
• The recommendation of modifications to improve inside the vessel, if required.
the performance of the existing vessel for a retrofit In this case, it was found that a high proportion of
scenario. droplets (approximately 65% of the total liquid) were

18 Oil and Gas Facilities • April 2016


formed within the upstream piping of this vessel, preventing type of vessel (gas scrubber). However, it is still only a rule
the removal of liquid within the gravity settling section and of thumb that, when applied without further analysis, could
allowing only a portion of liquid to be separated by the inlet hinder the final performance of the vessel.
device. Therefore, one of the first issues observed in this The gravity settling section plays an important role
original design was that the majority of the incoming liquid in defining the separation efficiency of a scrubber since it
was expected to reach the demister device. provides an opportunity for some of the entrained liquid
(mist) to be removed from the gas stream. The effectiveness
Inlet Arrangement. The use of a vane-type inlet device was of the gravity section in removing droplets will be a
expected to be appropriate. The calculated inlet momentum function of gas velocity and physical properties. It can be
for the max case [6892 kg/(m⋅s2)] was relatively high but estimated by the use of Stokes’, Intermediate, or Newton’s
still inside the acceptable range for this type of inlet device. laws, depending upon the Reynolds number around the
The calculated inlet momentum number (ρv2) is droplet. A table with these correlations can be found in
widely used for the selection of inlet devices in our Bothamley (2013b).
industry; nevertheless it should not be used blindly. The Gravity-based separation calculated for this design
main functions of an inlet device are to minimize droplet was negligible due to the poor distribution resulting in
shearing, dissipate the momentum, and improve the high gas velocities and the small size of the liquid droplets.
distribution of gas over the scrubber’s cross-sectional Consequently, a high mist loading was expected to reach
area. Attaining an even distribution of the gas (and the demister, reducing the demister’s overall droplet
entrained liquids) requires that high gas velocities inside removal efficiency.
the inlet device must be avoided when possible, or that
additional measures must be taken to minimize the Demisting Device. The original design was found to have a
effect of unpreventable high gas velocities. There are vane-type demister in vertical orientation, with a properly
many different effects influencing the overall efficiency sized open area for the service (2.18 m2) assuming even gas
of the inlet device. A CFD simulation is required in distribution across the vane pack flow area.
order to predict the gas distribution across the originally However, the geometry of the horizontal-flow vane
installed demisting device illustrated in Fig. 1. Uneven gas pack mist eliminator in this vertical vessel creates the
distribution is expected across the upstream face of the vane potential for uneven gas distribution over the device’s open
pack demister. This will lead to premature flooding of the area (Fig. 1). Gas entering the vessel must change direction
equipment due to a combination of localized high gas and multiple times before reaching the demister, making an
liquid loadings. even distribution over the total vane area difficult. It is
important to realize that this mist eliminator device only
Gravity Separation. The vessel k-factor was approximately operates properly when the gas flow is evenly distributed
0.18 m/s. Again, this value is considered adequate for this over the vane pack’s total open area. Another potential

New design includes


• Two horizontal vane pack
mist eliminators
• Vane-type inlet device

Original design includes


• Vertical vane pack
c mist eliminator
• Vane-type inlet device
a

Fig. 3—A schematic of the original and new designs of the gas scrubber.

April 2016 • Oil and Gas Facilities 19


(a) (b) (c) (d)

CFD Results Description

(a) Gas Velocity Streamlines Visualized gas-flow field throughout the scrubber, colored by gas velocity

Red: Velocity too high


(b) Effective Area Vane Pack Demister Yellow: Velocity too low
Green: Velocity within requirements (62% of vane pack area)

(c) Gas Velocity Streamlines Visualized gas-flow field throughout the scrubber, colored by gas velocity

Red: Velocity too high


(d) Effective Area Vane Pack Demister Yellow: Velocity too low
Green: Velocity within requirements (99% of vane pack area)

Fig. 4—A comparison of CFD analysis of the original ([a] and [b]) and the new scrubber designs ([c] and [d]).

drawback to the geometry in Fig. 1 is the suction effect of • Gas distribution and velocity profiles over the
the gas outlet nozzle. The close proximity to the vane pack open area of the vertically oriented vane-type mist
leads to preferential flow through the vane pack’s center, eliminator
increasing the chance for gas maldistribution and higher
k-values. Because of these issues, it was anticipated that the
In this case, the combination of very small droplet total liquid load entering the demister would prove to
formation and large mist fraction in the vapor phase in the be excessive, especially at the higher end of the gas flow
inlet line, and the orientation of the demisting device, is rate envelope for which the vessel was designed. At these
expected to lead to excessive liquid carry-over. conditions, the demister was expected to be overloaded,
A CFD study was done to determine the gas flow which would explain the high levels of liquid carry-over
path through the vessel and gas velocity profiles across the observed by operations.
original vane pack open area. The results of the study are Based on the findings, the following recommendations
shown in Fig. 4 as a part of the final comparison between were made to build a new gas scrubber for the same
the original design and new scrubber design (which also process conditions.
contains a vane pack demister) and are discussed later in
the article. Recommendations for Scrubber
In summary, after the analytical evaluation was New Vessel Design
completed, the main areas of concern in this vessel were Fig. 3 shows the basic differences between the final
as follows: equipment configuration in the original design and a
• Feed characteristics (higher mist load in gas phase) newly designed gas scrubber The letters a, b, c, and d
• Bulk and gravity separation (velocity was too in the figure correspond to the recommendations
high to separate incoming drops by gravity) that follow.
• Location of the gas outlet nozzle (poor flow a) To avoid the detrimental effect of excessive liquid
distribution over the demisting device) droplets in the new vessel, it was determined using

20 Oil and Gas Facilities • April 2016


Revamped design includes
:
• Cyclonic-type demisting b
device
• Vane pack agglomerator
• Vane-type inlet device
c

Fig. 5—The schematic for the internal design and gas flow path through the retrofitted vessel modeled by CFD.

engineering models that it was necessary to increase the • Gas flow field through the scrubber. The streamlines
inlet piping size from 18 in. (original design) to 20 in. in Fig. 4a show a turbulent and chaotic flow pattern,
This will significantly reduce the entrainment of liquid indicating that the original internals configuration led
droplets into the gas phase from approximately 65% to to a maldistribution of gas flow.
45%, improving the “bulk” separation. Although the mean • Gas velocity (k-value) through the vane pack.
droplet size at the inlet was also increased due to the larger When the gas velocity through the vane pack
inlet pipe diameter, this had a negligible impact on the demister is too high, liquid carry-over will occur.
“gravity” separation. A critical velocity can be computed based on fluid
b) To improve the gas flow distribution over the properties, interfacial tension, and liquid load.
mist eliminator device, based on CFD results it was When this critical velocity is exceeded, carry-over
recommended to change the location of the outlet nozzle, is expected. The separation performance of the vane
shifting the gas flow through the mist eliminator device pack also diminishes if the velocity is too low and
from horizontal to vertical. liquid load too high.
c) To meet the specified performance requirement
of 0.1 USG/MMSCF, it was determined using CFD The maldistribution of gas flow means that certain
simulations and performance estimation tools that areas of the vane pack may be overloaded (gas velocity and/
two demisting steps were necessary. Two vane packs or liquid load too high) while in other areas the velocity
were selected in this case. The first vane pack will is too low. The area where the velocity through the vane
bring the additional benefits of improving the gas pack is too high is highlighted in red in Fig. 4b. The area
flow distribution over the cross-sectional area of the where the velocity is too low is highlighted in yellow. This
vessel and the second vane pack. Another option leaves just 62% of the vane pack area where the velocity was
would have been to use a cyclone deck instead of the considered to be within acceptable limits.
second vane pack; the former was mainly preferred for The CFD analysis of the new design shows the
comparison purposes. following.
d) To enable the vane packs to operate in nonflooding • Gas flow field through the scrubber. The streamlines
regime, it was necessary to increase the vessel ID from in Fig. 4c also show a turbulent and chaotic flow
1920 mm (original design) to 2223 mm. This also increases pattern below the vane pack agglomerator in which
gravity-based separation inside the vessel. the flow is straightened. Downstream of the vane
pack agglomerator, the gas flow is equally distributed
Comparisons of the CFD Analysis across the vessel cross-sectional area.
for Original and New Designs • Gas velocity (k-value) through the vane pack. There
The CFD analysis of the original and new designs is is no gas flow maldistribution coming into the vane
illustrated in Fig. 4. pack mist eliminator as shown in Fig. 4d. Therefore,
The CFD analysis of the original design shows the the velocity is considered to be within acceptable
following. limits for 99% of the open area available.

April 2016 • Oil and Gas Facilities 21


Before After New
Estimated Performance Retrofit Retrofit Design Good Design Matters
• The downsides of bad designs can range from
Separation Efficiency (%) 67.0 98.0 99.0% damages to downstream equipment and disruption
of operations to safety concerns.
Liquid Carry-over 25.0 1.5 0.1 • There are many options to fix underperforming
(USG/MMSCF) scrubbers, but this approach always will come with
restrictions and extra expenditure.
TABLE 1—Comparison of the vessel performance before • Saving money upfront may be a bad trade-off when
and after retrofit.
compared to the required expenses in the future.

To improve the performance of the existing


vessel, recommendations were made based on
the evaluation. used specifications for liquid carry-over in production
separators (Chin 2015); it is also a very stringent one. It can
Recommendations for only be attained when vessels are specifically designed with
Scrubber Revamp that purpose in mind, or if the liquid/gas ratio at the inlet is
Fig. 5 illustrates the modifications proposed for the already very low. In addition, this requirement is not always
retrofitting of the gas scrubber (indicated as a, b, and c needed when looking at the downstream equipment, as this
in the diagram) and a CFD simulation that was done to example has shown.
validate the design. Commonly used scrubber design practices in the
a) To include an additional separation stage, a vane- industry are in need of serious reviewing. Many criteria-
pack agglomerator, in order to reduce the liquid loading based design methodologies that are still in use today
to the demisting device. Gravity separation and bulk lack the support of representative test data, and rely on
separation in this vessel are negligible. Most of the incoming incorrect assumptions regarding flow distribution. All
liquid in the original design was reaching the vane-type of this leads to undersized and/or poorly designed gas
demister and overloading the device. The added stage will scrubbers that in turn could cause multiple operational
prevent this in the retrofitted design. It will also improve gas problems (equipment damage, disruption of operations,
distribution and gas velocity profile over the mist eliminator and safety concerns).
device, while reducing the liquid load and increasing Application of proper design methodologies and setting
droplet size distribution of the liquid coming into the mist of realistic performance requirements are crucial. These
eliminator device. The vane-pack agglomerator was selected important steps, many times ignored or oversimplified, can
due to the fouling nature of the service. mean the difference between underperforming facilities
b) To modify the gas outlet arrangement in order to in need of costly post-startup vessel upgrades and full
mitigate suction effects and gas maldistribution in the mist operational plants that are able to attain the required
elimination section. separation performance and throughput from day one
c) To use a cyclonic-type demisting device, instead to decommissioning.
of the vane-type demister selected previously. The limited A well-conceived scrubber design that is able to achieve
cross-sectional area available now that the gas outlet has the required separation performance from day one is always
been corrected requires the use of a high-capacity mist the best option, both from a technical and economical point
elimination device. This type of device also creates a bigger of view.
pressure drop, dampening the effect of gas maldistribution.
The placement of the cyclones will change gas flow from The authors would like to thank members of the
horizontal to vertical through the demisting device. SPE Separations Technology Technical Section Ed Grave,
Table 1 presents the estimated performance of the Cris Heijckers, Richard Arntzen, Jimmie Riesenberg, and
gas scrubber before and after the retrofit as well as for Robert Chin for their valuable review and contributions
the newly designed gas scrubber. Notice that the estimated to this article.
liquid carry-over for the revamp design is still higher Introduced in the June 2015 issue of Oil and Gas
than 0.1 USG/MMSCF, the separation performance Facilities, The Savvy Separator series was conceptualized by
requirement specified for the vessel by the engineering Robert Chin, Padden Engineering LLC, and developed in
contractors. However, in this case, the downstream conjunction with the SPE Separations Technology Technical
equipment was able to function properly after the Section (STTS). Chin, a cofounder and past chair of the
retrofitting of the scrubber. STTS, serves as the editor of the series and works with STTS
This table also reveals that for these process conditions members to present helpful design approaches and solutions
a separation efficiency of at least 99.9% is required in order for separation problems. He may be reached at r.w.chin@
to achieve 0.1 USG/MMSCF. This is one of the most poorly sbcglobal.net. OGF

22 Oil and Gas Facilities • April 2016


treatments). She holds two US patents and has a degree in
References
chemical engineering from Universidad Simón Bolívar.
Bothamley, M. 2013a. Qualifying Separation Performance
Morillo may be reached at elizabeth.morillo@fmcti.com.
in Gas/Liquid Separators. Oil and Gas Fac 2 (4): 21–29.
Bothamley, M. 2013b. Qualifying Separation Performance
Victor van Asperen has several years
in Gas/Liquid Separators—Part 2. Oil and Gas Fac 2 (5):
of experience in separation, including
35–47.
the process design of more than 150
Bothamley, M. 2013c. Gas/Liquid Separators—Part 3: separator projects. He has worked at
Quantifying Separation Performance. Oil and Gas Fac 2 FMC Technologies Separation Systems
(6): 34–47. (formerly CDS Engineering) for the
Chin, R. 2015. The Savvy Separator Series: Part 4—The past 16 years in different geographical
Ghosts of Separators Past, Present, and Future. Oil and areas: The Netherlands, United Arab
Gas Fac 4 (6): 18–23. Emirates, and the US. He has worked in research and
Heijckers, C. 2012. Flow Conditioning Impact on development, computational fluid dynamics (CFD), process
Separations, SPE Separations Technology Technical engineering, and sales and management. Van Asperen
Section webinar, https://webevents.spe.org/products/ holds an MSc in chemical and biochemical engineering and
flow-conditioning-impact-on-separations. a professional doctor of engineering degree in process and
systems design from the Delft University of Technology.
Elizabeth Morillo is a process
engineer at FMC Technologies based Sander Baaren has worked at FMC
in Houston. In her current role, she Technologies Separation Systems
oversees the design of separation (formerly CDS Engineering) in The
systems for the Americas. During her Netherlands and US since 2012 in
9 years of experience in the oil and CFD, process engineering, and
gas industry, she has held various research and development, and was
positions in operations, engineering, responsible for the CFD evaluation of
and research and development, focusing on pressure separation equipment for more than 50
pumping services and hydrocarbon processing (crude oil projects. Baaren holds an MSc in mechanical engineering
dehydration and stabilization and gas and water from the University of Twente in The Netherlands.

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