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Extrudability Properties
decrease increase 6063 “high strength” -T54, -T65
6005A
6082
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 3
Excellence
Fair
Basics
Surface critical
Roughness critical
Mill Finish
• PRINTER COPIER TUBE
• SUNROOF RAILS
• CRASH SYSTEM • COMPUTER
• SIDE TRIMS
• ABS HOUSING • MOBILE DEVICE CASE
• HEAT EXCHANGERS
• TRAILOR • LUGGAGE COVER
Roller aluminum tube
• HEAT & FLUID TRANSFER
images courtesy of • PLATFORM • DECORATIVE PARTS
Constellium • HEAT SINKS
• SUPERSTRUCTURE
• INDUSTRIAL
COMPONENT
• ENGINE PARTS
• ENGINE HOUSING
MgSi at
Coarse Atmos. Acid
Pick-up Blister grain
MgSi corrosion corrosion
boundary
Coarse
Speed Orange Alkali Rinse water
Tearing grain
Cracking peel corrosion corrosion
banding
Coloring
Corrosion
Die streak Snap mark Water stain Dull finish due to
fretting
MgSi
Inclusion
Longit. Inclusion Inadequate Castle and
Hot spots extrusion
weld cast-in rinse moat
© 2017 Rio Tinto. All rights reserved. process
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 5
Pick-up Blister
Speed
Tearing
Cracking
Micro die
Die line
line
Front-end Back-end
TW Coring
Longit.
Hot spots
weld
© 2017 Rio Tinto. All rights reserved.
Pick-up
During Extrusion / Mill Finish
Pick-up Blister
Speed
Tearing
Cracking
Micro die
Die line
line
Front-end Back-end
TW Coring
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 7
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 9
Pick-up – Mechanisms
Extrusion direction
Coating of aluminum oxide on the
die bearing exit
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 11
− Correct die preheating to prevent excessive oxidation of the die bearing (no overheating)
• Extrusion environment
Nitrogen shrouding reduces oxidation and
therefore pick-up
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 13
The Energy Dispersive X-Ray analysis (EDX) on the painted longitudinal section across the
defect revealed the presence of foreign material composed of Al, Mg, Ca, O. This is likely a
particle of clay, chalk or other pigment used to color the coating.
O Fe
C Fe
Mg Si Cr Fe
Cr
0 1 2 3 4 5 6 7 8
Pleine échelle 768 cps Curseur : 10.094 (0 cps )
Al
Mg Cl
O Na Cl K K
0 1 2 3 4
Pleine échelle 731 cps Curseur : 10.094 (0 cps )
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 15
Si Spectrum 2
Longitudinal polished
section.
Blister
During Extrusion / Mill Finish
Pick-up Blister
Speed
Tearing
Cracking
Micro die
Die line
line
Front-end Back-end
TW Coring
Longit.
Hot spots
weld
© 2017 Rio Tinto. All rights reserved.
8
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 17
Blister
Blow hole
• Entrapment of volatile liquid via back end of billet (minimum use of lubricants)
• Extrusion of billet skin
• Billet temperature too high (front-end should be hotter than back-end)
© 2017 Rio Tinto. All rights reserved.
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 19
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 21
Pick-up Blister
Speed
Tearing
Cracking
Micro die
Die line
line
Front-end Back-end
TW Coring
Longit.
Hot spots
weld
© 2017 Rio Tinto. All rights reserved.
Delamination
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 23
Temperature (oF)
SOLIDUS 600
Temperature (oC)
1000 550
Solid solution 500
800 450
400
350
600
300
SOLVUS 250
400 200
6360 6060 6063 6061
150
200 100
0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6
© 2017 Rio Tinto. All rights reserved. % Mg2Si
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 25
• Fragments (chips) of tool steel originated from die or cutting tool (scalping,
shear, dummy block…)
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 27
• Fragments (chips) of tool steel originating from die or cutting tool (if billet scalping is
used)
Nitride layer, die condition, container liner, dummy block…
Die lines
During Extrusion / Mill Finish
Pick-up Blister
Speed
Tearing
Cracking
Micro die
Die line
line
Front-end Back-end
TW Coring
Longit.
Hot spots
weld
© 2017 Rio Tinto. All rights reserved.
14
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 29
A
Mounting media
Aluminum
Mounting media B
Aluminum
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 31
• Countermeasures:
‒ Remove die from press for cleaning and bearing polishing
‒ Improve die preparation, die preheating, die nitriding and re-nitriding practices;
‒ Prevent inflow of billet skin;
‒ Review and adjust extrusion conditions;
‒ Use high quality billet;
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 33
• Countermeasures:
‒ Prevent inflow of billet skin;
‒ Improve die design, die correction and die maintenance;
‒ Use high quality billet;
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 35
Streaks – Mechanisms
TYPE II
Caused by die or
profile design
TYPE I
Caused by
contaminants
TYPE III
Caused by
extrusion process
© 2017 Rio Tinto. All rights reserved.
Streaks – Mechanisms
Textural streak anodized
Surface topography 0.2µm
Variable grain size and attack
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 37
Streaks – Mechanisms
Difference in
Grain Orientation or Grain Size
Difference in Difference in
Light Reflection Light Reflection
‒ Bearing shape:
No rounded edge at entrance
Square in respect to the die face
Bearing Bearing
X
© 2017 Rio Tinto. All rights reserved.
19
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 39
Zone 2
Web
intersection Zone 3
Solution: not over-restrict the flow of the vertical part near the intersection
4 4
5 4 5 4
3 5
5 5 5< 3 5.5
5 .2 5 2
4 4 5 4
5 5 4
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 41
Impact of bearing
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 43
Impact of billet
• Press misalignment
NOT BAD
BAD But not perfect
© 2017 Rio Tinto. All rights reserved.
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 45
MgSi at
Coarse
grain
MgSi
boundary
Coarse
Orange
grain
peel
banding
Corrosion Corrosion
pitting fingerprint
Corrosion
Water stain
fretting
Spacer Excess
marking lubricant
Inclusion
Inclusion
extrusion
cast-in
© 2017 Rio Tinto. All rights reserved.
process
MgSi
After Extrusion - Metallurgical
MgSi at
Coarse
grain
MgSi
boundary
Coarse
Orange
grain
peel
banding
Corrosion Corrosion
pitting fingerprint
Corrosion
Water stain
fretting
Spacer Excess
marking lubricant
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 47
Time
Casting Homogenization Ageing
Preheating
Extrusion
Cooling
© 2017 Rio Tinto. All rights reserved.
24
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 49
i.e. Low hardness: Presence of undissolved MgSi particles oriented in the extrusion direction
© 2017 Rio Tinto. All rights reserved.
20m
0.001”
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 51
MgSi
After Extrusion - Metallurgical
MgSi at
Coarse
grain
MgSi
boundary
Coarse
Orange
grain
peel
banding
Corrosion Corrosion
pitting fingerprint
Corrosion
Water stain
fretting
Spacer Excess
marking lubricant 1 nm
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 53
MgSi
After Extrusion - Metallurgical
MgSi at
Coarse
grain
MgSi
boundary
Coarse
Orange
grain
peel
banding
Corrosion Corrosion
pitting fingerprint
Corrosion
Water stain
fretting
Spacer Excess
marking lubricant
Inclusion
Inclusion
extrusion
cast-in
© 2017 Rio Tinto. All rights reserved.
process
27
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 55
Bad part
Appearance of the PCG area
Good part
uniform grain
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 57
• Die conditions
– Bearing length and choke angle influence the PCG thickness in quenched profiles
– Extrusion speeds with acceptable PCG thickness can be several times higher with
long choked bearings and in addition the onset of speed cracking can be delayed.
MgSi
After Extrusion - Metallurgical
MgSi at
Coarse
grain
MgSi
boundary
Coarse
Orange
grain
peel
banding
Corrosion Corrosion
pitting fingerprint
Corrosion
Water stain
fretting
Spacer Excess
marking lubricant
Inclusion
Inclusion
extrusion
cast-in
© 2017 Rio Tinto. All rights reserved.
process
29
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 59
• Extrusion conditions
– Slow billet preheating
– Exit temperature not high enough to dissolve MgSi
– Exit temperature too high favours re-crystallized outer-band
– Insufficient press quenching and avoid delay into the quench box
– Over stretching
– Ensure billet to container temperature differential more than 50oF
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 61
Atmos. Acid
corrosion corrosion
Spacer Chloride
marking contami.
Coloring
Dull finish due to
MgSi
White etch
Spangle
bloom
Spacer mark
After Anodization
Atmos. Acid
corrosion corrosion
Spacer Chloride
marking contami.
Coloring
Dull finish due to
MgSi
White etch
Spangle
bloom
31
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 63
Spacer mark
Also known as hot spots, dull spots, or black spotting.
• Typically visible after anodization
• Cool and reheat section creates the environment for a rapid precipitation of MgSi
Dull finish
After Anodization
Atmos. Acid
corrosion corrosion
Spacer Chloride
marking contami.
Coloring
Dull finish due to
MgSi
White etch
Spangle
bloom
32
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 65
Dullness Appearance
Dullness Appearance
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 67
Dullness Appearance
Color finish
After Anodization
Atmos. Acid
corrosion corrosion
Spacer Chloride
marking contami.
Coloring
Dull finish due to
MgSi
White etch
Spangle
bloom
34
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 69
Color finish
good
Low MgSi precipitates concentration in
the “good” light sample
35
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 71
20 film
30
Anodised Gloss 60°
Commercial
10 Caustic -10
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Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 73
Pits - Dissolution of Pits & grooves formed during alkaline etching Grooves - Dissolution of
aluminium matrix MgSi precipitates in grain
surrounding AlFeSi boundary
intermetallic particles
Pits in grain interior Grooves in grain boundaries
Grain
Fe intermetallic MgSi MgSi Grain size
orientation
Whole process
© 2017 Rio Tinto. All rights reserved.
37
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 75
Spangle
After Anodization
Atmos. Acid
corrosion corrosion
Spacer Chloride
marking contami.
Coloring
Dull finish due to
MgSi
White etch
Spangle
bloom
Irregular surface
Anodic layer thickness 6μm
SEM - Step
Spangle surface
Coarse grain size
Irregular surface
Anodic layer thickness 14μm
38
Extrusion Defects: Fundamentals & Solutions AEC – Finishing Workshop 2017 77
Extrusion Defects
Fundamentals & Solutions
for Optimum Finish
Columbus, Ohio – May 16-17, 2017
Jerome Fourmann
39