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1
J A S 0 M 346-93
gas is sealed and cooled by water or air (1) The lamp power can be adjusted manu-
forcibly. ally so that irradiance may be kept at a
(b) The filter is used to obtain required spectral constant.
characteristics and to cool the xenon-arc (2) The lamp power can be adjusted automati-
lamp. A glass filter for cutting off ultra- cally so that irradiance may be kept at a
violet region, flowing water, etc. is used constant.
for it. (3) The lamp power can be adjusted manu-
The other materials excellent in weath- ally and progressively according to use
erability, corrosion resistance, moisture time.
resistance, or electrical insulationare used
properly. 4.3 Black panel thermometer
Spectral characteristics of light emit- The black panel thermometer shall have a
ting part construction in which a heat sensitive element
The xenon-arc lamp should give prefer- such as bimetal, platinum resistance, ther-
ably continuous spectrum over a wave mistor, thermocouple, etc. is installed Co-axially
length of at least 250 to 1200 nm, and a with thezenter of the metal plate, and the
construction of light similar to sun light heat sensitive element protective tube is fit-
through glass window by combining with ted closely on it.
the filter. The construction and dimensions of it shall
Irradiance on test piece be in accordance with Item 5.7 (2) of JIS B
The irradiance on test piece shall be set 7754 and Attached fig. 1, Type A.
between 48 w/m2and 162 w/m2over a wave
length of 300 to 400 nm. 4.4 Test chamber
Also a spectral irradiance on test piece The devices not specified in the above item
over a wave length of at least 300 to 400 such as the xenon-arc starting and stabiliz-
nm shall be indicatedfor each type of tester. ing device, temperature adjusting device,
By mutual agreement between two par- humidity adjusting device, test piece holding
ties concerned, irradiance in other range device, cooling device, instrument, etc. shall
of wave length or spectral irradiance at be in accordance with JIS B 7754.
particular wave length may be indicated
and used. 4.5 Temperature and humidity
The measurement method shall be in ac- The temperature and humidity in the test cham-
cordance with the attachment of JIS B 7754. ber shall be as follows
Permissible variation range of irradi- B.P.T. at test piece and its adjustment
ance on operating period accuracy
+lo% of the set irradiance can be main- The black panel temperature at test piece
tained. and its adjustment accuracy shall be 89
Permissible range of irradianceon each Ie3"C.
surface of test piece By mutual agreement between two par-
A difference in irradiance between posi- ties concerned, the other temperature and
tions on test piece shall not exceed 10% its adjustment accuracy may be used.
of the set value. Remark: The temperature depends on the type of
xenon-arc lamp and its combination with
Irradiation method the filter. Also, th8 black panel thermom-
In general, a specified irradiance shall be eter used shall be in accordance with JIS
B 7754, Type A.
irradiated continuously.
Relative humidity and its adjustment
accuracy
4.2 Irradiance adjusting device
Relative humidity should be preferably ad-
The irradiance adjusting device is a device justed to (50*5)'/0 for the indicated tem-
to correct the damping of radiation energy ac-
perature stipulated in (1). It shall be
companied by the use of xenon-arc lamp and measured near the outlet of air in the test
filter, and measures irradiance over a wave
chamber.
length of 300 to 400 nm. It shall be provided
By mutual agreement between two par-
with either of the following conditions.
ties concerned, the other relative humid-
2
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variation in colour and gloss, etc. of test piece.
is lined on the back surface of the test piece,
Variation in colour shall be measured for judg-
it shall be made in contact closely with the
ment in accordance with JIS 2 8722, and that
back surface of the test piece as far as prac-
in gloss shall be in accordance with JIS Z 8741.
ticable, and the surface of the test piece shall
For variation such as in choking, crazing, bloom-
be free from slackness.
ing, crack, stain contamination, etc., measure-
ment shall be made in accordance with JIS
6.2 Sample holder with test piece
D 0205, 7.
The sample holder with test piece shall be
installed on the rack or disk so that any clear-
9. Marking
ance in not left. If any sample holder without
The marking of variation in colour shall be
test piece is present, white thick paper, alu-
made in accordance with JIS Z 8730 or by
minium plate, stainless steel plate, etc. shall
mutual agreement between two parties con-
be attached on all the holders to keep a ther-
cerned. The making of variation in gloss shall
mal equilibrium state in the test chamber.
be in accordance with JIS 2 8741 or by mu-
6.3 Irradiance
tual agreement between two parties concerned.
The other markings shall be made in accor-
The irradiance shall be selected from a range
dance with JIS D 0205.
of 48 to 162 W/m2 over a wave length of 300
to 400 nm, and the selected irradiance shall
be adjusted so that it is kept at a constant
during the exposure.
The amount of radiant exposure can be cal-
culated by the following equation.
E= I Xtx C
Where E : Amount of radiant exposure
(kJ/m2/nm)
I : Irradiance (W/m2/nm)
t : Exposure time (h)
C : Constant 3600 (s/h)
3
JASO M 346-93
Explanatory note
on
JASO M 346-93 Light-exposure test method by xenon-arc lamp
for automotive interior part
This explanatory note simply explains the items quirement. Accordingly, the test method has
stipulated in the text of the standard and the been standardized by JASO.
related items and not a part of the standard.
3. Content of investigation and
1. Introduction supplementary explanation
Activities of investigation for standardization Based on the investigation results up to Step
of the above subject were started in 1990 for 3, the following content was discussed pri-
the purpose of internationalizingthe test method marily, and the standardized test method has
and improving its accuracy. The activities from been established as follows.
preparation to establishment of the standard
were planned first such that, in preparatory 3.1 Test apparatus
step, a consistency of fundamental conditions For convenience of use by users and to cope
(settings on temperature and light) of devices with internationalization, three types of ap-
to be used was maintained, in step 1, devices paratuses were selected as a base so that,
to obtain the re-producibility of test and the in Japan, the U.S., and the European coun-
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management method of the test were inves-
tigated, in step 2, test conditions to maintain
a correlation with the outdoor exposure test
(underglass) were investigated and, in step
tries, at least one can be purchased easily
by users and also maintained, and adding a
high strength type to them to cope with in-
creased acceleration, the specifications in
3, the results in steps 1 and 2 were finally Attached table have been established.
summarized. Then the investigation was pro-
ceeded in accordance with that plan and the 3.2 Type of test and test conditions
standard has been established. Deterioration of polymeric materiais depends
on a combination of light, heat, water, etc.
2. Purpose However, the investigation was proceeded on
The accelerated exposure test method is used the assumption that the test for automotive
to evaluate, in a laboratory, polymeric mate- interior parts shall be made in one condition.
rials such as plastics, fibre, etc. deteriorated A correlation between the results of the out-
due to solar radiation. The method in which door exposure test and those in various con-
carbon-arc is used as light source was stan- ditions (Step 1 to 3) has been analyzed, and
dardized and has been used in Japan. In the the standardized test conditions have been
U.S.and European countries, on the other established as in Text 3.
hand, the xenon-arc lamp type is predomi-
nant from before and, also in ISO, the test 3.3 Validity of standardized test
method in which xenon-arc lamp is used as conditions for each material
light source is the leading part. In such cir- Polymeric materials äeteriorate due to light,
cumstances, some exposure test methods heat, water, etc., and the degree of deterio
(hereinafter referred to as "test method")inwhich ration depends on a combination of them. The
xenon-arc lamp is used as light source, which validity of the standardized test conditions to
its light is mostly similar to solar light in wave market environment is assumed from the test
length distribution, are sometimes studied and results in this investigation,deterioration factors,
adopted by automotive companies, with the and deteriorating mechanism of polymeric
increasedJapan's overseas corporate activities materials as follows.
in recent years and the increased quality re- The test conditions used in each step are as
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5
J A S 0 M 346-93
~ ~~ ~
Explanatory table 1 Correlation of accelerated test conditions for outdoor exposure test
1OOw/mZ (R0.93) (R:0.84) (R0.67) (Fk0.82) tions except for Step 1, Series 3, the Step 1, Series 1
was judged to be appropriate by the following reasons.
* Onset wave length (Series 3): A correlation between
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and dark cycle requires a long time and causes ex-
A A C A cessive contamination on the test piece.
*
Temperature control: Though there is no decisive dif-
53wlm2 (R0.97) (R:O.90) (R:0.55) (R:0.87)
ference between B.P.T. and B.S.T. in correlation, a
correlation in B.P.T. is rather better.
2. Validity of Test Conditions Based on Deterioration Mecha-
nism
The ABS resin is deteriorated by heat and light, re-
markably at a wave length of 320 nrn or below. The
~
ering accuracy and acceleration.
d. A A C A 3. Cautions on Use
Irradiance gives effect on acceleration, and also on
162w/m2 (R:0.80) (R0.84) ( R :O. 68) (R0.82)
sample temperature and heat history.
Accordingly, it is required to set the irradiance con-
sidering the degree of effect by humidity.
Step 1, Step 2
Series 1 Series 2 Series 3
1 00w/m2 (R:0.72) (R0.96) (K0.99) (Fc0.97) (temporary conditions) was judged to be equiva-
lent to Step 1-2.
@ The numerical value for gloss and haze is more
in which the contamination on
reliable in Step i-i,
surface of sample due to adhesion of water drop is
less, than in Step 1-2.
2. Validity of Test Conditions Based on Deterioration Mecha-
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A A A A nism
* In the UV irradiation (300 to 500 nm) at low tempera-
53wlm2 (Ft0.94) (R0.96) (R :O .99) (R0.95)
tures (35 to 40%) , only lowering of molecular weight
occurs, and deterioration due to oxidation and
crosslinking does not occur.
Though it is generally said that, depolymerization oc-
curs at high temperature region, effect of heat dete-
rioration is small at 100 "C or less.
d. A A A A
7
J A S 0 M 346-93
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A A A A be explained by the processes of radical forma-
tion, peroxide formation, breakage and crosslinking
53wlm2 (R:0.94) (R:0.94) ( R0.89) (R0.94)
of principal chain, and variation in chemical con-
stitution of principal chain in that order. It shows
a characteristic absorption of ultraviolet ray in a
wave length region of 320 nm or less (large dete-
rioration). Also most engineering plastics hardly
absorbs moisture and, therefore, deterioration due
to moisture will not be accelerated. (Even polyamid
~~ ~~
Step 1, Step 2
Series 1 Series 2 Series 3
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Based on the following considerations on deterioration
A A A A mechanism made in additionto a correlationwith the outdoor
exposure, the standard test condition (StepllSeries 1)
can be said to be appropriate.
53wlm2 (R:0.91) (Fk0.90) (R0.88) (R:0.89) (1) Continuous Irradiation including Short Wave Length
Region
Since Step IlSeries 3 includes short wave length re-
gion, the deterioration acceleration is increased, and
evaluation can be made in short period. However,
for evaluation of interior parts, light ray through win-
dow glass does not match the actual circumstances
because it does not include short wave length.
(2) Light and dark Cycle (Step 2) Containing Humidify-
ing Conditions
The deterioration phenomenon is considered to be
caused primarily by deterioration of polymer itself.
A A A B Though the deterioration is started and continued by
C. radical reaction due to thermal oxidation and light
energy mainly, humidification is not necessarily the
48wlm2 (R:0.99) (R0.81) (W0.95) (R0.73) condition indispensable to accelerate the deteriora-
tion in the PP which is low in hygroscopicity.
Also, for other physical variation which causes ther-
mal effect, there is crystallization.
However, initial history is dominant at a constant tem-
perature, and effect by repeated intermittent heating
can be neglected.
3. Cautions on Test
(i) Relationship between Exposure Amount and Test Time
Because the acceleration tests were compared with
each other based on the amount of exposure this time.
the larger the illuminance of test apparatus is given,
the smaller the test time is required when the amount
of exposure is the same, and also the smaller the
d. A C C heat history on a sample is given. In such appara-
tus, it is required to set an evaluation standard con-
sidering not only the amount of exposure but also
162w/m2 (R0.83) (R:0.28) (R0.69) deterioration due to heat.
(2) Relationship between Exposure Site and Accelera-
tion Test
In the table on the left, the data in the other sites
were omitted because a correlation between the ex-
posure result in Florida and that in each accelera-
tion test was maximum in comparison at the same
amount of exposure. If analyzing by other factors
(such as test time, etc.) than the amount of expo-
sure, it is not conducted this time, but a different re-
sults may be obtained.
9
J A S 0 M 346-93
80wlm2 (R0.82) (R:0.86) (FC0.78) (R:0.88) Moquette comprising polyester and ny-
lon, fabric tricot (model sample)
Colour: Blue, Red, Gray, Brown (Colours used
generally for automotive interior parts)
1. Validity of Test Conditions Based on Outdoor Expo-
sure Results
The table on the left shows the ranking of correlation
coefficients which are combined with the amounts of
irradiant exposure in each outdoor exposure results
b. A A 6 A and each accelerationtest results ( A E * for both) nearest
each other and averaged. From these results, it can
1 00w/m2 (R:0.90) (R:0.90) (R:0.75) (R0.86)
be found that, because a correlation of Step 1, Series
3 (short wave length onset condition) is low, effect of
short wave length in ultraviolet ray region is large, and
also light in this wave length region to be cut by win-
dow glass is harmful for automotive interior parts.
In the other test conditions, the same level of results
are obtained. and Step 1, Series 1 test condition was
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A A B A judged to be more appropriate rather than Step 1. Se-
ries 2 (B.S.T. control).
53wlm2 (R0.82) (R:0.84) (R:0.72) (Fk0.87)
2. Validity of Test Conditions Based on Deterioration Mecha-
nism
Most of fibres now used for automotive seats are poly-
ester, and its deterioration due to light is primarily caused
by light in 320 nm or less. For humidity, synthetic
fibre is generally less in hygroscopicity, and difficult
to be affected by humidity particularly at temperatures
A A A A of 100C or less.
C.
Accordingly, Step 1, Series 3 is not preferable in ac-
48w/m2 (R:0.92) (R:0.87) (R:0.83) (R:0.86)
curacy for automotive interior parts and, based on ac-
celeration, Step 1, Series I is considered to be ap-
propriate mostly. This also matches the test results.
3. Cautions on Use
Because irradiance affects sample humidity and heat
history, in the condition of high irradiance, a correla-
tion with exposure may be lowered due to effect by
heat reserve, depending on samples. Accordingly,
adjustment of conditions such as selection of a proper
d. A C C B
irradiance or release of polyurethane foam from the
162wlm2 (Fk0.70) (Fk0.79) (R:0.54) (k0.72) back surface is required.
NOTE (1): Step 3, Series 2 (R:0.91)
The same condition as Step 1, Series 1,
and polyurethane foam is not installed on
- Step 3 - the back surface.
A (R:0.91)
10
Step 1, Step 2
Series 1 Series 2 Series 3
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The major deterioration mechanism of polyvinylchloride
A A C B is such that dehydrochlorination reaction is produced
by heat and light to form polyene constitution, and com-
53wlm2 (k0.93) (K0.84) (k0.67) (R:0.76)
pound other than polyene may be formed due to light
and discolouring may occur simultaneously due to bleach-
ing effect in presence of oxygen, etc., and a balance
of heat and light is considered to be important. From
this point of view, the test conditions of Step 1, Se-
ries l were judged to be appropriate.
3. Cautions on Test
Vinyl chloride leather and sheet are generally covered
C. A A A C with urethane form on the back surface for testing.
Due to heat insulation effect by this, the sample tem-
48wlm2 (R:O.90) (Ft0.89) (R:0.85) (R:0.59) perature becomes higher than that on the black panel
thermometer. Especially, in high irradiance, this ef-
fect is large, and the deterioration of the sample some-
times does not match the actual deterioration condi-
tion, and breaching effect is observed occasionally.
Therefore, the test conditions should be preferably ad-
justed by comparing the deterioration of the sample
with the actual deterioration conditions beforehand.
NOTE (1) The temperature setting in the test condi-
tions is 94°C in B.S.T. Because this is
3. C C B
equivalent to 70 OC in B.P.T. which is dif-
1 62wlm2 (k0.22) (k0.57) :R:0.66) ferent from the temperature setting in the
other tests, it is not evaluated.
(2) This was conducted in the conditions of
Step 1, Series 1 and at a low amount of
irradiant exposure of 17 to 25 MJI m2, and
- Step 3(2) -
a good correlation could be obtained.
A (R:0.81)
11
J A S 0 M 346-93
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A A C A A correlation in Step 1. Series 1 was mostly excellent
and it was judged to be appropriate considering the
53wlm2 (R:0.88) (Fk0.84) (R0.68) (k0.80)
shortening of test time.
2. Validity of Test Conditions Based on Dterioration Mecha-
nism
Polyvinyl chloride is said that it forms polyene due to
dehydrochlorination by mainly compound action of heat
and light, and also forms carbonyl group in presence
of oxygen, to discolour and deteriorate. In this test,
discolouration occurred earlier as predicted before on
C. A C B B the test piece in which less amount of ultraviolet ray
absorbing agent is contained.
48wlm2 (R:0.89) (k0.67) (R0.71) (Fk0.79) For PVC material, deterioration due to moisture was
less and the accelerated deterioration test conditions
by light and heat in Step 1, Series 1 were judged to
be appropriate.
3. Cautions on Test
A correlation between the test on a highly strong en-
ergy type (irradiance of 162 w/m2 ) apparatus and the
exposure in Florida was investigated in the condition
of Step 3 where the exposure for acceleration test is
approximately half the amount in Step 1, Series 1, and
d. C C B C the result was excellent. Because, in the highly strong
162wlm2 (R:0.56) (R:0.52) (R :O. 77) energy type apparatus, the temperature on both sides
(w0.49)
of the test piece rises 20 "C higher than that in the
standard apparatus, however, effect of deterioration
due to heat becomes larger. It is required for evalua-
tion in the test on the highly strong energy type appa-
- Step 3 - ratus to add that point.
B (R:0.74)
12
3.4 Consistency with other standards automobiles that passes through a light
Many standards on xenon-arc light-exposure of 320 nm or below.
test are found in ISO, and US, German, and Accordingly, the conditions under which
Japanese Standards as shown in Explana- a short wave length of 320 nm or below
tory table 2. can be cut were considered mostly pref-
For major standards on "Light-Exposure Test erable for practical use, correlation with
Method by Xenon-Arc Lamp for Automotive the outdoors, and internationalization, etc.,
Interior Part", I S 0 105-B06, DIN-75202 and and adopted as a standard.
SAE J 1885 are well known. A comparison (4) Irradiance
of test conditions for these test methods is The irradiance is set in I S 0 and DIN with
shown in Explanatory table 3 in which a con- an average of solar radiation in subtropi-
sistency with these standards is shown for cal region as a reference and, in SAE, it
each item. is increased approximately 1.5 times that
(1) Temperature in I S 0 and DIN. Because, in SAE, the
For indicationof representative temperature onset wave length is 275 nm, some fac-
of a sample, two kings of temperatures tors which will increase acceleration may
of black panel temperature (B.P.T.) and be produced in the short wave length re-
black standard temperature (B.S.T.) are gion. Therefore, the irradiance in these
in use. In Japan and the US, the B.P.T. standards cannot be compared simply by
is generally used, and the B.S.T. is used the level of irradiance only. The level of
primarily in Europe and investigated by irradiance may be a direct cause to af-
ISO. The B.S.T. shows rather higher than fect photochemical reaction speed and heat
the B.P.T., and its difference depends on history, and its amplitude affects largely
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an irradiance of light source and the type on the correlation and acceleration of the
of filter. In this standard, the B.P.T. has material. Accordingly, particularly a limit
been adopted as a standard based on the to which a sample is affected by temperature
test results and considering a difference must be taken into consideration when
between models, correlation with the out- irradiance is selected. In this standard,
doors, consistency with the standards in an irradianceof 300 to 400 nm over a range
and outside Japan, etc. B.P.T. of 89°C of 48 to 162 w/m2 has been adopted to
has been judged appropriate and adopted make various tests for a variety of mate-
as a standard because, in the outdoor light- rials used for automotive internal parts,
exposure test conducted during this ex- taking correlation and acceleration into
periment, the surface temperature of sample consideration.
rose to 1 1O to 116°C in Okinawa (August), For indication of irradiance, the narrow
88 to 104°C in Florida (September), and band (Ex. point indication such as 340 nm,
88 to 110°C in Arizona (November) in mea- 420 nm, etc.) method and wide band (Ex.
surement by thermo label, and also the band indication such as 300 to 400 nm,
B.P.T. of 89°C in SAE and the B.S.T. of etc.) method are available worldwide. The
100°C in DIN were already standardized. former is adopted in SAE, and a part of
(2) Humidity IS0 and DIN, and the latter is being studied
Because humidity of 20% in I S 0 and DIN to adopt in ISO, etc. In this standard, an
is too low as compared with actual one irradiance of 300 to 400 nm has been
and also a correlation with the conditions adopted as a standard for international-
in SAE and outdoor light-exposure in this ization and common use in the conven-
experiment could be obtained, 50% RH tional apparatuses.
has been adopted as a standard. Light and dark
(3)Onset wave length of irradiation light Though the light and dark cycle is adopted
Though the onset wave length of light pass- in SAE and as a part of ISO, its effect
ing through window glass is not a con- could not be noticed in this test results.
stant because the type and thickness of This cycle may cause water-drop due to
the window glass differ according to ve- high humidity to adhere on the surface of
hicle model, there is no window glass for sample, and make the estimation difficult.
13
J A S 0 M 346-93
Considering the efficiency of test time and Explanatory fig. 3 The amount of radiant ex-
the I S 0 and DIN standards, the light and posure and exposure time are shown in the
dark cycle was not adopted, and the con- form of comparison drawing so that they can
tinuous irradiation has been adopted as be used as a standard for the test time when
a standard. managed by the amount of radiant exposure
3.5 Supplementary explanation of tester in actual testing.
The permissible variation range of irradiance (1) Explanatory table 4
during the test is stipulated at within f 10% List of Specifications of Testers
in ISO, JIS, ASTM, etc. Considering a con- (2) Explanatory table 5
sistency with them, a variation range off 10% a and b Structure of Light Used in Test
has been adopted in this standard. However, (3) Explanatory fig. 1
it is f 5% in the tester of automatic irradi- Spectral Distributionof Solar Light (Through
ance control system now widely used and, Window Glass)
therefore, this control system should be pref- (4) Explanatory fig. 2
erably used. Example of Spectral Distribution of Light
Though a tester is stipulated in JIS 6 7754 Emitting Part
which is applicable to this standard, a par- ( 5 ) Explanatory fig. 3
ticular tester with which this preliminary test Radiant Exposure Amount and Irradiation
was conducted for standardization will be in- Time
troduced.
object
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Explanatory Table 2 List of reference standards
IS0 us Germany Japan
ASTM/D4355
Plastics I S 0 4892 ACTMID2565 DIN153386
ASTM1D4459 DIN153387
ASTMID5071 DIN175202
Paint ISOIDIS 2809 ASTMID4303 DIN153321
I S 0 787-15
Automobile ISO1DIS 105-806* CAE1J1885' DIN175020'
ISO/TC22/SCll SAE/J 1960
Others IS0 4665 ASTMIG26 ACTMIE765 DIN154004 JIS B 7754
ASTM/E781 ASTM1D4434
ACTMID4637 ACTMID4798
ASTMIC732
14
Explanatory table 3 List of test conditions for standards relating to internal parts
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wave length No.1-No.4 -320 nm 320nm 275 nm
N0.5 -275 nm
~~
15
J A S 0 M 346-93
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16
Type a b (') C d
Wave
Length I I I I i i i
Range
l l n l l l n l l l n I 1 l n
290-300
300-31 O
310-320
320-330
330-340
-
34O 35O
390-400
290-400
Note
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(I):
13.80
80.00
I 17.20
100.00
I 11.60
53.80
I 21.54
100.00
I 10.90
48.00
I 22.70
100.00
I 36.70
162.00
I 23.70
100.00
This is value (initial value) obtained from a new xenon-arc lamp and filter combined with each other and aged for
approx. 20 hours.
(2): A spectral irradiance of 100 W/m2 is equal to the values in column U.
300 or less
300-320
I 0
<O.l
320-360 3.020.5
360-400 6.0+1.O
17
J A S 0 M 346-93
E
c
2-
2
0
c
O
m
.-
U
L
.-
L
-
L
*
U
0
(1
v)
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Explanatory fig. 2 Spectral distribution of light emitting part
18
I I I I I
8 50 1O0 150 200 250
Amount of irradiant Exposure (MJ/ m2)
- Irradiance 150 W/m2 ---- Irradiance 100 W/m2 --- Irradiance 50 W/m2
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19
J A S 0 M 346-93
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a : THIRD PHASED STANDARD
(The standard where SI units and newly values are given and do not using customary units, but it is excepted
that the standards are represented in only accustomed metric units as rn, A, Hz etc.)
Published by
The Society of Automotive Engineers of Japan, Inc.
10-2, Goban-Cho, Chiyoda-ku, Tokyo 102, Japan