PE Pressure Pipes Made From PE 100-RC: Hessel

HESSEL
Ingenieurtechnik
PE pressure pipes made from PE 100-RC

Design and calculation of gas- or water pipelines
for a minimum service life of 100 years
Dipl.-Ing. Sven Nonhoff

Dr.-Ing. Joachim Hessel
HESSEL Ingenieurtechnik GmbH
PE pressure pipes made from PE100-RC 1

Plastic Pressure Pipes 05.-07.October 2009 | HESSEL-Ingenieurtechnik GmbH
HESSEL
Ingenieurtechnik
HESSEL Ingenieurtechnik GmbH

We offer SOLUTIONS
Ł for engineering applications of thermoplastics,
Ł by quick and comprehensive tests of raw materials,
Ł to matters concerning design and fabrication.
We are an officially approved testing, inspection and certification

facility (NRW 37). raw materials / pipes / shafts
Accredited Testing Laboratory according to
DIN EN ISO/IEC 17025 by DAP GmbH (DAP-PL-3760.00)
Am Vennstein 1a ■ D-52159 Roetgen

Phone: +49-2471-92022-0 ■ Fax: +49-2471 - 92022 -19
E-Mail:info@hessel-ingtech.de ■ Internet: www.hessel-ingtech.de

HESSEL
Ingenieurtechnik
Contents
1. Overview on Failure Modes

2. Progress in raw material development
3. Requirements of PAS 1075
4. Thermal Ageing
5. New creep rupture curves for PE 100-RC
6. Conclusion

1. Overview on Failure Modes HESSEL
Ingenieurtechnik
Failure Modes
ductile
log σ [N/mm²]
flat ‘bran
ch’ brittle
failures through
2 nd
stretching of material ‘b r
an
ch’
thermal ageing
failures through failures independent of
stress cracking stress level
Relevant for Onset of thermal ageing
service life at 80 °C after 1 year*
log t [h]
* DVS directive DVS 2205-1, sup. sheet 19

1. Overview on Failure Modes HESSEL
Ingenieurtechnik
Test to detect stress cracking resistance: FNCT

Full-Notch Creep Test
rupture record
Advantage:
The results out of FNCT
correlate with results out of
pipes under internal pressure
Test time reduction by using dead load
surface active solutions
Test fluid – e.g. ARKOPAL N-100
F
FNCT
constant fluid F circumferential

notch
(VA 2.1-4, ISO 16770; DIN EN 12814-3 temperature
(2005-10), Anhang A.1; DVS 2203-4)
2. Progress in raw material development HESSEL
Ingenieurtechnik
Influence of medium
log σ [N/mm²]
su
rf a
(e ce wa ga
.g
.2 ac te s
% t r
AR ive
KO so
PA lu
L
N- ti o
1 00 n
)
Same slope but different rupture times
log t [h]

2. Progress in raw material development HESSEL
Ingenieurtechnik
Increasing rupture times

Rupture Time in Hours 14460 14835
10462
Test temperature 80 °C F
10.000 FNCT
tensile load 4 N/mm²
2 % Arkopal N-100 PE 100-RC
F circumferential
2.041
notch
832
1.000 643
491
338 359
259
100
51
Specimens show brittle failure
31
PE 63
11
10
4
PE 100
PE 80
1960 1980 1999
3. Requirements of PAS 1075 HESSEL
Ingenieurtechnik
Requirements to PE 100-RC raw material (PAS 1075)
Test Requirement
Stress cracking test > 8760 h (> 1 year) at 80 °C

(FNCT) 4 N/mm², in 2 % Arkopal N-100
Point loading test on > 8760 h (> 1 year) at 80 °C

full walled piping 4 N/mm², in 2 % Arkopal N-100
Thermal ageing test > 100 years @ 20 °C
Notch Test on full

walled piping > 8760 h
(DIN EN ISO 13479)

Ingenieurtechnik
> 8760 h (> 1 year) at 80 °C

FNCT
4 N/mm², in 2 % Arkopal N-100
⇒ no brittle failure until 1 year
⇒
onset of thermal ageing after
1 year at 80°C in water *
log σ [N/mm²]
4 N/mm²
F
FNCT
F circumferential
notch thermal ageing
> 1 year log t [h]

Ingenieurtechnik
Test Requirement
Stress cracking test > 8760 h (> 1 year) at 80 °C

(FNCT) 4 N/mm², in 2 % Arkopal N-100
Point loading test on > 8760 h (> 1 year) at 80 °C

full walled piping 4 N/mm², in 2 % Arkopal N-100
Thermal ageing test > 100 years @ 20 °C
Notch Test on full

walled piping > 8760 h
(DIN EN ISO 13479)

4. Thermal ageing HESSEL
Ingenieurtechnik
Influencing variables for thermal ageing
weekly exchange
Oxygen concentration of medium
Temperature
Circulating
Flow rate of medium
medium
Stabilization package
Point loads
Local strain situation
NOT taken into account in ISO 9080

⇒ values are too optimistic
⇒ For PE 100-RC materials thermal

ageing has to be tested additionally
Ingenieurtechnik
Extrapolation of results Arrhenius-Diagram
reciprocal slope of regression curve is

proportional to activation energy EA for
thermal ageing
Reciprocal absolute temperature [1/K]
20 °C
~ EA
80 °C
90 °C
100 °C
> 100 years log t [h]

Ingenieurtechnik
Minimum required activation energy for thermal ageing
1. Requirement: no failure until 100 years @ 20°C

Reciprocal absolute temperature [1/K]
20 °C
~ EA 80 °C
90 °C
Minimum required activation
energy for thermal ageing:
100 °C
EA ≥ 67 kJ/mol
> 1 year > 100 years log t [h]
2. no failure until 1 year @ 80°C *

5. New creep rupture curves for PE 100-RC HESSEL
Ingenieurtechnik
PE 100-RC exceeds standard creep rupture curves

log σ [N/mm²]
flat ‘bran PE 100-RC

ch’
5 N/mm²
s te
ep
PE 100 according to DIN 8075 ‘b ran
ch’
thermal ageing
1000 h
1 year at 80 °C ? log t [h]

5. New creep rupture curves for PE 100-RC HESSEL
Ingenieurtechnik
New creep rupture curves for PE 100-RC in PAS 1075

15
14
13 20°C
12
11
10
Hoop stress [N/mm²]

40°C
9
60°C
7
6
80°C
Creep rupture curves Creep rupture curves

according to DIN 8075 3
according to PAS 1075
1 10 100 Jahre
2,5
1 100 10.000 1.000.000
10 1.000 100.000
Rupture time [h]

6. Conclusion HESSEL
Ingenieurtechnik
Conclusion
• PE 100-RC - thermal ageing becomes the relevant failure mechanism

• PE 100-RC exceeds standard creep-rupture curves
• PE 100-RC are raw materials with very high stress crack resistance
⇒ High chemical resistance
⇒ Extended application alternative installation techniques

• PE 100-RC - New creep rupture curves have been established in
PAS 1075

HESSEL
Ingenieurtechnik
Thank you for your attention !


PE Pressure Pipes Made From PE 100-RC: Hessel

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HESSEL

PE pressure pipes made from PE 100-RC

Dipl.-Ing. Sven Nonhoff

PE pressure pipes made from PE100-RC 1

HESSEL Ingenieurtechnik GmbH

We are an officially approved testing, inspection and certification

Am Vennstein 1a ■ D-52159 Roetgen

PE pressure pipes made from PE100-RC 2

1. Overview on Failure Modes

PE pressure pipes made from PE100-RC 3

* DVS directive DVS 2205-1, sup. sheet 19

Test to detect stress cracking resistance: FNCT

Test fluid – e.g. ARKOPAL N-100

constant fluid F circumferential

PE pressure pipes made from PE100-RC 6

Increasing rupture times

Requirements to PE 100-RC raw material (PAS 1075)

Stress cracking test > 8760 h (> 1 year) at 80 °C

Point loading test on > 8760 h (> 1 year) at 80 °C

Thermal ageing test > 100 years @ 20 °C

Notch Test on full

PE pressure pipes made from PE100-RC 8

Requirements to PE 100-RC raw material (PAS 1075)

> 8760 h (> 1 year) at 80 °C

> 1 year log t [h]

Requirements to PE 100-RC raw material (PAS 1075)

Stress cracking test > 8760 h (> 1 year) at 80 °C

Point loading test on > 8760 h (> 1 year) at 80 °C

Thermal ageing test > 100 years @ 20 °C

Notch Test on full

PE pressure pipes made from PE100-RC 10

Influencing variables for thermal ageing

NOT taken into account in ISO 9080

⇒ For PE 100-RC materials thermal

Extrapolation of results Arrhenius-Diagram

reciprocal slope of regression curve is

> 100 years log t [h]

PE pressure pipes made from PE100-RC 12

Minimum required activation energy for thermal ageing

1. Requirement: no failure until 100 years @ 20°C

> 1 year > 100 years log t [h]

2. no failure until 1 year @ 80°C *

PE 100-RC exceeds standard creep rupture curves

flat ‘bran PE 100-RC

PE pressure pipes made from PE100-RC 14

New creep rupture curves for PE 100-RC in PAS 1075

Hoop stress [N/mm²]

Creep rupture curves Creep rupture curves

Rupture time [h]

• PE 100-RC - thermal ageing becomes the relevant failure mechanism

⇒ Extended application alternative installation techniques

PE pressure pipes made from PE100-RC 16

Thank you for your attention !

PE pressure pipes made from PE100-RC 17

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