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Natural Gas Dehydration using Desiccant and

Sizing (Bonus Free Spreadsheet)
 November 22, 2018  Rifka Aisyah  Gas Processing Plant

In this post, I want to share you about natural gas dehydration using desiccant using
adsorption principle and how to size it.
In common commercial use, desiccant can be classified into three categories, which are gels
(alumina or silica gels), alumina, and molecular sieves.
When used for natural gas dehydration, silica gel will give outlet dewpoints of approximately
-70o to -80oF. As for alumina, outlet dewpoint is appoximately -100oF. Molecular sieves
produced the lowest water dewpoints, as low as -150oF. For gas going into cryogenic
processing, the only adsorbent that can obtain the required dehydration is a molecular sieve.
Table below shows characteristics of several type of desiccants [1].

Typical desiccant properties [1]Figure below shows a schematic of two-bed adsorber system.
Schematic of a two-bed adsorption unit [2]
[Read more: Several Natural Gas Dehydration Methods and Range of
Application]
Adsorber A dries natural gas, while the other bed, Adsorber B, goes through a regeneration
cycle. The wet gas enters inlet gas pre-filter or separator that will catch entrained liquids before
entering the active beds. Gas flow is top-down to avoid bed fluidization. The dried gas then
goes through solid after filter that catch fines adsorbent before exiting the unit.
A small amount of gas is used for regeneration. Sales gas is sometimes used because it has
advantage of being free of heavier hydrocarbon that can cause coking. This gas is usually 5%-
10% of gas throughput.
Regeneration involves heating the bed, regeneration (removing the water), and cooling.
During heating and regeneration, gas is heated to about 600 oF to heat the bed and removed
adsorbed water from the adsorbent. Regeneration gas enters from the bottom of the bed
(counter-current to flow during adsorption) to ensure that the lower part of the bed is the driest.
During adsorption cycle, the bed can be thought of operating with three zones.

1. The top zone is called the saturation or equilibrium zone, where the adsorbate on the
adsorbent is in equal with adsorbate in the inlet gas phase and no additional adsorption
occurs.
2. The middle zone is called mass transfer zone (MTZ), where mass transfer and
adsorption take place.
3. The bottom zone is unused desiccant and is often called the active zone, where no
adsorption has yet taken place.
 Three zones of adsorption
[3]Table below lists guidelines for typical molecular sieves dehydration units.

Typical operating
conditions for molecular sieve dehydration units [4]Sizing
Below is step-by-step process of sizing or design of natural gas dehydration unit using
desiccants.
Sizing method of natural gas dehydration using desiccant
The first step is to define operating condition of the system, such as gas flow rate, pressure,
temperature, gas density, gas viscosity, and gas molecular weight.
The second step is to determine desiccant type used.
After that, by using several equations and basis design, such as allowable pressure drop
accross the bed, we can estimate geometry of adsorber. We can also estimate how much
molecular sieve desiccant we need and how much gas we need during regeneration.
I prepared this free spreadsheet of natural gas dehydration using desiccant for you. This
spreadsheet is prepared based on GPSA engineering data books. This is preview of the
spreadsheet.
Screenshoot of spreadsheet of solid desiccant dryer sizing
Download the spreadsheet of natural gas dehydration sizing using
desiccant.
I hope this post is useful. Please spread it to the world!
 
References:
[1] GPSA Engineering Data Books
[2] Solid Desiccant-based Dehydration Technology (http://www.frames-group.com/)
[3] Natural Gas Dehydration by Desiccant Materials
(https://www.researchgate.net/publication/251659746_Natural_gas_dehydration_by_desiccant
_materials)
[4] Fundamentals of Natural Gas Processing