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Titration

level 1
Sarah

Aims
In level 1, you'll analyse samples from a river that has been contaminated with acid. You'll perform titration
experiments to work out the concentration of acid in the samples.

In each activity you'll be able to collect points. At the end of the level you can restart to improve your skills.

Video 100 Points

Comprehension 90 Points 2 Attempts


Hydrochloric acid fully dissociates when dissolved in water.

The pH of water is approximately 7 which means it is neutral.

When an acid and alkali react to form water and salt it is called neutralisation.

A titration experiment can be used to determine the unknown concentration of acid using a known concentration of
base.

An indicator helps us to see the point of neutralisation during a titration experiment by causing a colour change.

Acids and alkalis 90 Points 1 Attempt

pH 0-2 pH 7 pH 12-14

hydrochloric acid distilled water sodium hydroxide

sulfuric acid potassium hydroxide

nitric acid calcium hydroxide

Phenolphthalein is an indicator which changes colour close to the point of neutralisation and is used to show the end-
point of this titration. When adding a strong acid to a strong base the phenolphthalein indicator changes colour from
pink to colourless.

Weighing 90 Points 1 Attempt


You correctly used the balance to accurately weigh:

Mass of sodium hydroxide = 1.00 g

This was transferred to a beaker for you ready for the next step of the experiment.

Standard solution 70 Points 3 Attempts


First the sodium hydroxide powder was dissolved in distilled water.

Next you transferred to solution to a 250.0 cm3 volumetric flask and rinsed the beaker with more water.

Finally you made up the standard solution to the to the 250.0 cm3 level using a dropping pipette

Alkali concentration 80 Points 2 Attempts


You calculated the molar mass for sodium hydroxide as 40 g mol-1.

Then you worked out the amount of sodium hydroxide you used was0.0250 mol.

Finally you calculated the concentration of your stock solution as being 0.10 mol dm-3.

Preparing for titration 100 Points 1 Attempt


First you rinsed a pipette with your sodium hydroxide solution.

Next you used the pipette to transfer exactly 25.00 3 of the solution into a conical flask and added 3 drops of
phenolphthalein indicator.

Burette setup 100 Points 1 Attempt


First you rinsed a burette with distilled water.

Next you rinsed the burette with your acidic contaminated river sample.

Then you filled the burette with the river sample and ensured the eye level was good for reading the burette level

Then you removed the funnel.

Finally the burette was filled below the tap by running out some solution.
Titration experiment 70 Points
You performed titration experiments on contaminated river water from two sites B and C.

1st 2nd
Sample site
B Trial accurate accurate
titration titration

Final reading
27.35 25.00 25.05
(cm3)

Initial reading
10.35 8.60 8.65
(cm3)

Volume added
17.00 16.40 16.40
(cm3)

Average
volume added 16.40
(cm3)

Sample site 1st 2nd


Trial accurate accurate
C
titration titration

Final reading
36.75 38.75 39.60
(cm3)

Initial reading
8.65 10.70 11.50
(cm3)

Volume added
28.10 28.05 28.10
(cm3)

Average
volume added 28.08
(cm3)

Number of times
that sample B 1
was tested

Average volume
added for all 16.40
samples (cm3)

Number of times
that sample C 1
was tested

Average volume
added for all 28.08
samples (cm3)

Titration analysis 100 Points


You correctly determined the concentration of acid in the river at sites B and C.

Amount of sodium hydroxide = 0.0025 mol.

Amount of hydrochloric acid = 0.0025 mol.

Concentration of hydrochloric acid at site B = 0.15 mol dm-3.

Concentration of hydrochloric acid at site C = 0.09 mol dm-3.


The pH of the river is normally neutral.

The pH values increase as the concentration of HCl decreases.

The pH at the site of special scientific interest is bad.

The pH of the river returns to a moderate level by the time it reaches site D.

Review
Things I did well on:

Things I could improve on:

Your titrations and quick response helped protect some of the wildlife at the site of special scientific interest. Three
days later you sample the river at all the sites again. What do you predict your results would be?

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