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Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
1. Sco
Scope
pe 2. Referenc
Referenced
ed Documents
1.1 Thi
Thiss test method
method cov
covers
ers the det
determ
ermina
inatio
tion
n of mat
materia
eriall 2.1 ASTM Standards: 3
loss by gas-entrained solid particle impingement erosion with E122 Practice
E122 Practice for Calculating Sample Size to Estimate, With
jetnozzle type erosion equipment. This test method may be Specified Precision, the Average for a Characteristic of a
used in the laboratory to measure the solid particle erosion of Lot or Process
different materials and has been used as a screening test for G40 Terminology
G40 Terminology Relating to Wear and Erosion
ranking solid particle erosion rates of materials in simulated 2.2 American National Standard:
service environments (1, 2).2 Actual erosion service involves B74.10 Grading of Abrasive Microgrits 4
ANSI B74.10 Grading
particle sizes, velocities, attack angles, environments, and so
3. Terminology
forth, that will vary over a wide range ( 3-5)). Hence, any single
(3-5
laborato
labo ratory
ry test may not be suf suffficie
icient
nt to evaevalua
luate
te exp
expecte
ected
d 3.1 Definitions:
service
service per
perfor
forman
mance.
ce. Thi
Thiss test meth
methodod des
describ
cribes
es one wel
welll 3.1.1 erosion— progressive
progressive loss of original material from a
characterized procedure for solid particle impingement erosion solid
solid susurf
rface
ace du
duee to mec
mecha
hani
nica
call in
inte
tera
racti
ction
on be
betw
twee
eenn th
that
at
measurement for which interlaboratory test results are avail- surface and a fluid, a multicomponent fluid, or impinging liquid
able. or solid particles.
3.1.2 impingement— a pr
proc
oces
esss re
resu
sulti
lting
ng in a co cont
ntin
inui
uing
ng
1.2 Units— The
The values stated in SI units are to be regarded
succession of impacts between (liquid or solid) particles and a
as standard. No other units of measurement are included in this solid surface.
standard (exceptions below).
3.2 Definitions of Terms Specific to This Standard:
1.2.1 Exceptions: Table 1 uses HRB hardness. Footnote 7
3.2.1 erosion value— the
the volume loss of specimen material
and 11.2
and 11.2 use
use abrasive grit designations.
divided by the total mass of abrasive particles that impacted the
1.3 This standar
standard d doe
doess not purport
purport to add
addre
ress
ss all of the specim en (mm3·g−1).
specimen
safetyy co
safet conc
ncer
erns
ns,, if an
anyy, as
asso
socia
ciate
ted
d wit
with
h its us
use.
e. It is th
thee erosion value (mm3·g−1) of
3.2.2 Normalized Erosion Rate— erosion
responsibility of the user of this standard to establish appro- specim
spe cimen
en mate
materia
riall div
divide
ided
d by ero
erosio
sion
n value (mm3·g−1) of
value
priate safety, health, and environmental practices and deter- reference material.
mine the applicability of regulatory limitations prior to use.
1.4 This int
intern
ernati
ationa
onall sta
standa
ndard
rd was dev
develo
eloped
ped in acc
accor
or-- 4. Summ
Summary
ary of Test
Test Method
dance with internationally recognized principles on standard- 4.1 Th
4.1 Thisis te
test
st me
meth
thod
od ut
utili
ilizes
zes a re
repe
peat
ated
ed im
impa
pact
ct er
eros
osio
ion
n
izatio
ization
n esesta
tabl
blis
ishe
hed
d in th
thee De
Decis
cisio
ion
n on Pr
Prin
incip
ciple
less fo
forr th
thee approach involving a small nozzle delivering a stream of gas
Development of International Standards, Guides and Recom- containing abrasive particles which impacts the surface of a
mendations issued by the World Trade Organization Technical test specimen. A standard set of test conditions is described.
Barriers to Trade (TBT) Committee. However
Howev er,, deviati
deviations
ons from some of the standard conditions
conditions are
permitted if described thoroughly. This allows for laboratory
scale erosion measurements under a range of conditions. Test
1
This test method is under the jurisdiction of ASTM Committee G02 on Wear
and Erosion and is the direct responsibility of Subcommittee G02.10
Subcommittee G02.10 on on Erosion by
3
Solids and Liquids. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Oct. 1, 2018. Published November 2018. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approv
app roved
ed in 198
1983.
3. Las
Lastt pre
previo
vious
us edi
editio
tion
n app
approv
roved
ed in 201
20133 as G76 – 13.13. DOI
DOI:: Standards volume information, refer to the standard’s Document Summary page on
10.1520/G0076-18. the ASTM website.
2 4
The boldface numbers in parentheses refer to a list of references at the end of Available from American National Standards Institute (ANSI), 25 W. 43rd St.,
this standard. 4th Floor, New York, NY 10036.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
G76 − 18
TABLE 1 Characteristics of Type 1020 Steel Reference Material
Annealed 900 s at 760°C, air cooled.
Hardness: HRB = 70 ± 2.
Chemical Composition:
C = 0.20 ± 0.01 wt %
Mn = 0.45 ± 0.10
S = 0.03 ± 0.01
Si = 0.1± 0.05
P = 0.01 ± 0.01
where:
a = gas jet nozzle,
b = nozzle length,
methods are described for preparing the specimens, conducting c = mixing chamber,
the erosion exposure, and reporting the results. d = abrasive hopper,
e = gas source,
5. Significance and Use f = test specimen,
5.1 The significance of this test method in any overall g = nozzle-to-specimen distance, and
measurements program to assess the erosion behavior of θ = impingement angle.
materials will depend on many factors concerning the condi-
tions of service applications. The users of this test method FIG. 1 Schematic of Test Rig
should determine the degree of correlation of the results
obtained with those from field performance or results using
other test systems and methods. This test method may be used shall be measured at the location to be occupied by the
to rank the erosion resistance of materials under the specified specimen and under the conditions of the test.
conditions of testing.
7. Test Materials and Sampling
6. Apparatus
7.1 This test method can be used over a range of specimen
6.1 The apparatus is capable of eroding material from a test sizes and configurations. One convenient specimen configura-
specimen under well controlled exposure conditions. A sche- tion is a rectangular strip approximately 10 by 30 by 2 mm
matic drawing of the exit nozzle and the particle-gas supply thick. Larger specimens and other shapes can be used where
system is shown in Fig. 1. Deviations from this design are necessary, but must be documented.
permitted; however, adequate system characterization and
control of critical parameters are required. Deviations in nozzle 7.2 The abrasive material to be used shall be uniform in
design and dimensions must be documented. Nozzle length to essential characteristics such as particle size, moisture, chemi-
diameter ratio should be 25:1 or greater in order to achieve an cal composition, and so forth.
acceptable particle velocity distribution in the stream. The 7.3 Sampling of material for the purpose of obtaining
recommended nozzle5 consists of a tube about 1.5 mm inner representative test specimens shall be done in accordance with
diameter, 50 mm long, manufactured from an erosion resistant acceptable statistical practice. Practice E122 shall be consulted.
material such as WC, A12O3, and so forth. Erosion of the
nozzle during service shall be monitored and shall not exceed 8. Calibration of Apparatus
10 % increase in the initial diameter. 8.1 Specimens fabricated from Type 1020 steel (see Table 1
6.2 Necessary features of the apparatus shall include a and Fig. 2) equivalent to that used in the interlaboratory test
means of controlling and adjusting the particle impact velocity, series6 shall be tested periodically using specified (see Section
particle flux, and the specimen location and orientation relative 9) 50 µm A12O3 particles to verify the satisfactory performance
to the impinging stream (impingement angle). of the apparatus. It is recommended that performance be
6.3 Various means can be provided for introducing particles verified using this reference material every 50 tests during a
measurement series, and also at the beginning of each new test
into the gas stream, including a vibrator-controlled hopper or a
series whenever the apparatus has been idle for some time. The
screw-feed system. It is required that the system provide a
uniform particle feed and that it be adjustable to accommodate recommended composition, heat treatment, and hardness range
for this steel are listed in Table 1. The use of a steel of different
desired particle flow values.
composition may lead to different erosion results. A photomi-
6.4 A method to measure the particle velocity shall be crograph of the specified A1 2O3 particles is shown in Fig. 3.
available for use with the erosion equipment (6-9). Examples The range of erosion results to be expected for this steel under
of accepted methods are high-speed photography (7), rotating the standard test conditions specified in Section 9 is shown in
double-disk (6), (8), and laser velocimeter (9). Particle velocity Table 2 and is based on interlaboratory test results. 6
8.2 Calibration at standard test conditions is recommended
5
The sole source of supply of the recommended nozzle (tungsten carbide) even if the apparatus is operated at other test conditions.
known to the committee at this time is Kennametal Inc., 1600 Technology Way, PO
Box 231, Latrobe, PA 15650-0231. If you are aware of alternative suppliers, please
provide this information to ASTM International Headquarters. Your comments will
receive careful consideration at a meeting of the responsible technical committee,1 6
Supporting data have been filed at ASTM International Headquarters and may
which you may attend. be obtained by requesting Research Report RR:G02-1003.
G76 − 18
APPENDIX
(Nonmandatory Information)
X1.1 This erosion test is usually applied to bulk materials. It For example, surface preparation of the coating, like mechani-
may also be applied to coatings upon bulk substrates, if care is cal polishing, before testing may not be appropriate. Cleaning
taken not to penetrate the coating during the test. The test of the surface may be constrained by the nature of the coating.
results from coated test specimens should apply to the material In such cases, the user shall ensure that the preparation steps
comprising the coating, and thus to the coated system, as long used for this test do not alter the characteristics of the coating
as the coating is not altered, fragmented, or dislodged during being tested. The procedures that are used shall be adequately
the test. described in the test report.
X1.2 The standard test conditions may penetrate a coating
making it difficult to rank various coatings. If this occurs, the X1.4 Normally, this test is conducted on numerous separate
impinging solid particle stream can be made less aggressive by specimens, each eroded for a given time and condition. While
reducing the angle of incidence. Testing at 45° or even 15° has not recommended, it is possible to conduct repeated erosion
been used by users. Some G76 users even employ a different tests (under the same conditions) on the same individual
abrasive (glass beads, 70 to 210 µm) and two times the specimen by carefully repositioning the specimen after eroding
impingement mass (20 g) at 15° impingement angle for coating it, removing it for cleaning, and weighing it. In such a case, the
comparisons. This test has shown to not penetrate many hard specimen must occupy the identical position for each test in the
coatings like PVD TiN and glass enamels. series; otherwise the accumulated erosion effect will not be
correct.
X1.3 In the case where this test is applied to coatings on
bulk substrates, some of the test steps may need to be modified.
REFERENCES
(1) Young, J. P., and Ruff, A. W., Journal of Engineering Materials and (8) Ninham, A. J., and Hutchins, I. M., Proceedings of the 6th Interna-
Technology, Transactions of ASME , Vol 99, 1977, pp. 121–125. tional Conference on Erosion by Liquid and Solid Impact (Univ. of
(2) Hansen, J. S., in Erosion: Prevention and Useful Applications , Adler, Cambridge, 1983) pp. 50-51.
W. F., ed., ASTM STP 664, 1979, pp. 148–162. (9) Barkalow, R. H., Goebel, J. A., and Pettit, F. S., in Erosion:
(3) Finnie, I., Levy, A., and McFadden, D. H., in Erosion: Prevention and Prevention and Useful Applications, Adler, W. F., ed., ASTM STP 664,
Useful Applications, Adler, W. F., ed., ASTM STP 664, 1979, pp. 1979, pp. 163–192.
36–58. (10) Allen, T., Particle Size Measurement , Chapman and Hall, London,
(4) Wood, F. W., Journal of Testing and Evaluation, 14 , 1986. 1974.
(5) Preece, C. M., ed., Erosion: Treatise on Materials Science and
(11) Ponnaganti, V., Stock, D. E., and Sheldon, G. L., Proceedings on
Technology, Vol 16 Academic Press, New York, NY, 1979.
Symposium Polyphase Flow and Transport Tech. (ASME) NY, 1980
(6) Ruff, A. W. and Ives, L. K., Wear , Vol 35, 1975, pp. 195-199.
pp 195-199.
(7) Finnie, I., Wolak, J., and Kabil, Y., Journal of Materials, Vol 2, 1967,
pp. 682–700.
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