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Weighing Matters
5’
Accurate weighing measurements matter in every industry
1946
1973:
5
Copyright 2009 Mettler-Toledo, Inc.
Accurate & Efficient Weighing
Weighing Matters
Dave Cirullo
GWP Consultant
Accurate weighing: Essential for your processes
Guaranteed Accuracy – Reduced Costs – Secure Audits
Problem source:
Prevent bad batches
Inaccurate weighing
and OOS*?
-QUALITY-
Testing is costly
Appropriate testing at and a lot of effort
appropriate intervals
-COST-
Good Manufacturing Practice
10
FDA Warning: Risk management
Risk management
Weighing Device is Calibrated; is it appropriate?
I have a Calibration
Report from my service
provider, but are my
balances and scales
appropriate for my
weighing process?
Capacity: 3'000kg
Readability: 1kg
± 80%
uncertainty
0.4 kg 1.5kg
Metrology
Quality management
Process
requirements
Life Cycle Management
The weighing community should have a science-based standard for
efficient life-cycle management of weighing equipment.
Clear answers should be available on: how you calibrate each device,
how you establish of limits, and sound scientific rationale covering
every step in the life cycle management of a weighing device
New Equipment Evaluation
- Accuracy requirements
The knowledge about the measurement uncertainty and the minimum weight is the
requirement for the selection of a suitable, accurate measurement instrument.
Installation by a trained technician
“Measurement uncertainty
[…] Parameter that describes the dispersion of the quantity values
that is assigned to a scale […].”
International Vocabulary Of Basic And General Terms In Metrology (VIM) JCGM
200:2008, entry 2.26
Water : 70 %
Oil: 20 %
Emulsifier: 5%
Moisturizer: 3%
Stabilizer: 1,5 %
Fragrance: 0,5 % 500 g
500 g ± 5 g
A scale is ACCURATE
if it satisfies the requirements of the user.
In other words:
OK Fair Not OK
m1 kg m2 kg m3 kg Display [kg]
“Measurement uncertainty
[…] Parameter that describes the dispersion of the quantity values
that is assigned to a scale […].”
International Vocabulary Of Basic And General Terms In Metrology (VIM) JCGM
200:2008, entry 2.26
Non-linearity NL
Corner load EC
Repeatability RP
2 2 2
U 2 v w
v r
v W
e
v W
a
v K
W
Measurement uncertainty U
Weight W
Measurement uncertainty %]
Accuracy limit:
Minimum weight
Measurement uncertainty %]
Accuracy limit:
Minimum weight
Measurement uncertainty %]
1%
0.5%
0.1%
Indication
Load
« 5% 5%
"In order to satisfy the required weighing tolerance, when samples are
weighed the amount of sample mass (i.e., the net weight) must be equal
to or larger than the minimum weight. The minimum weight applies to
the sample weight, not to the tare or gross weight."
Safety factor ≥ 2
(depends on risk)
Accuracy ensured over the long-term
Variability of the Minimum weight – safety factor
Minimum weight
Time
Initial calibration "As Found" calibration "As Left“ calibration
Traceable Documentation of Minimum Weight
Benefits
Evaluation of the overall performance of the
scale by testing all relevant weighing
parameters
Determination of the measurement uncertainty
and the minimum weight
Output of recognized and verifiable certificates
according to ISO 17025/USP/A2LA
Restrictions
Unknown status of the scale between several
calibrations if they were not frequently executed
High costs if they were frequently executed
Self-testing by Intelligent scales
FACT
Without
With
Benefits
Automatic adjustment compensates for
drafts and corrects temperature effects
Reduction of costs and effort, because on
scales having FACT fewer routine tests are
required.
Restrictions
Weights are formally not verifiable for national
or international standards and guidelines.
No determination of repeatability or corner load
errors
Functionality of Auto-Calibration / Adjustment
57
Copyright 2009 Mettler-Toledo, Inc.
Functionality of Auto-Calibration / Adjustment
Internal adjustment
mechanisms are a great
compliment to a weighing
quality process
They should not be used in
place of a routine testing
They should be used in
conjunction with routine testing
They should be challenged by
appropriate routine testing
performed by end users and
appropriate service providers
For most weighing equipment,
only OEM service technicians
have the ability to adjust these
58
mechanisms
Copyright 2009 Mettler-Toledo, Inc.
Routine testing by User
Benefits
Effortless and rapid checking of the required
accuracy
Immediate determination of deviations
Minimization of risks by testing at appropriate
intervals between the calibrations
Restrictions
Incomplete testing of the properties of the
scale
Weights must be recalibrated at regular
intervals
GWP: A risk-based Test strategy
Weighing
accuracy
Impact
Risk Management
Non-linearity NL
Eccentricity load EC
Repeatability RP
Repeatability
Dominant influence on samples with low mass
Non-linearity
Not dominant with samples having high mass; generally
not dominant over the entire sample mass range
Weight 1: Recommended
Incorrect
Weight 2: Permissible
Load
« 5% 5% Nominal capacity
Weight 2 for Testing the repeatability
Display
Weight 2: Recommended
With load
« 5% 5%
The assessment of the repeatability is much easier with weight 2 than with a
much lower weight (weight 2 is less prone to operating errors).
Test weights For user tests
XP205 PBA430x-60
200 g and 10 g 50 kg and 2 kg
Accurate & Efficient weighing processes
Questions to ask a quality manager…
4 Simple Questions to Answer
Am I performing too many or
Are my balances/scales accurate?
too few tests?
Recommendations for
measuring equipment
monitoring based on risk
analysis
Complete documentation
Training
GWP® - The Global Weighing Standard
Metrology
Quality management
Process
requirements