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12 Paper No.

98-1216 TRANSPORTATION RESEARCH RECORD 1609

Probabilistic Method of Asphalt Binder


Selection Based on Pavement Temperature
ERLAND O. LUKANEN, CHUNHUA HAN, AND EUGENE L. SKOK, JR.

The Strategic Highway Research Program, conducted in the United States sonal monitoring program (SMP), consisting of a number of sites
and Canada from 1987 to 1992, included a significant asphaltic concrete around the United States and Canada, to evaluate the seasonal
study. The study included a new grading method for asphalt binders, per- response of pavements. These sites include air and pavement tem-
formance grading, resulting in what is termed PG asphalt. The grade selec-
tion process is based on air temperature distribution. Since 1994, the perature sensors and a data logger that records the air and pavement
Long-Term Pavement Performance program has established a seasonal temperatures hourly. These data now are available and can be used
monitoring program that consists of a number of sites with air and pave- to refine the heat flow models to predict more accurately the
ment temperature sensors and a data logger that records the air and pave- extreme temperatures that are needed for Superpave and the selec-
ment temperatures hourly. These data are now available for prediction of tion of the appropriate PG asphalt, or they can be used to develop
the extreme temperatures that are needed for the selection of the appro-
simple regression equations that relate the 7-day average high
priate PG asphalt binder. On the basis of the review of the recent pave-
ment temperature studies and statistical analysis of the pavement (maximum) air temperature to the 7-day average high (maximum)
temperature data available, an empirical prediction model has been devel- pavement temperature and relate the minimum air temperatures to
oped from the original data set and validated from the expanded data set. the minimum pavement temperatures.
The model is compared with existing prediction relationships including Many state departments of transportation are in the process of imple-
the heat flow model. Pavement prediction data and climatic data on high menting the Superpave mix design. Cost is one of the concerns regard-
and low temperature from weather stations are used to calculate the prob-
ability that a specific asphalt temperature will be exceeded. Variations ing the implementation. Both asphaltic cement and the aggregate costs
both in prediction and in annual maximum or minimum air temperature may be higher for Superpave than for the normal agency mix designs
are assumed to be independent and considered in the calculation. The reli- because the specifications may limit the sources or increase process-
ability contours for a given PG grade are presented as a convenient tool to ing costs. In the case of the binder, the PG requirements may either
the asphalt binder selection. require that the asphalt be modified or limit the crude oil sources. In
either case, the asphalt cost may increase. Preliminary estimates in
The Strategic Highway Research Program (SHRP) included a sig- Minnesota indicate that the increase may be as much as 30 percent
nificant asphaltic concrete study (1). That study resulted in a new (personal communication). The Minnesota Asphalt Pavement Associ-
approach to asphalt mix design called Superpave. This included a ation (MAPA) has noted that previously there were 13 crude sources
new grading method for asphalt binders (2). The asphalt binders, from which asphalt could be made; however, only 3 sources can meet
under Superpave, are graded by a method that is called performance the specifications without modifiers.
grading (PG), resulting in what is termed PG asphalt. PG is a two- Implementation of Superpave has raised questions regarding
number system intended to ensure that the proper binder is used to pavement temperatures among agencies, including Minnesota’s.
resist rutting under hot temperatures and to resist thermal cracking Minnesota adapted the PG method of grading asphalt binders
at cold temperatures. Local climatic data are used to determine the effective January 1, 1997. The new criteria required PG 52-34
expected temperatures of the asphalt for the hottest and coldest north and east of I-94 and PG 58-28 south and west of I-94, includ-
times of the year. A PG asphalt binder is selected to span these two ing I-94. Generally it was thought that neither of these two grades
values. The work performed to date on grade selection is based on would require the use of modifiers. However, as described, after
air temperature distribution. The air temperatures, in turn, are used the PG criteria were adapted, concerns developed regarding the
to estimate the high temperature at 20 mm below the pavement sur- availability of asphalt that meets the specifications; not all asphalt
face and the low surface temperature. Because limited data were previously supplied would meet the new PG criteria, limiting the
available regarding the pavement temperatures, the relationship supply.
between air and pavement temperatures was developed from heat Given the adaptation of the new grading procedure, other questions
flow models. arose, including:
In the past 3 years, the Long-Term Pavement Performance
(LTPP) program, developed under SHRP and continued by the • What would be the appropriate PG requirement for underlying
Federal Highway Administration (FHWA), has established a sea-
asphalt layers, including binder and base courses?
• What is the appropriate binder to use for hot mix asphalt
recycling?

E. O. Lukanen and C. Han, Braun Intertec Corporation, 6875 Washington Neither of these issues has been actively investigated during the
Avenue South, Minneapolis, MN 55439. E. L. Skok, Minnesota Asphalt
Pavement Association, 900 Long Lake Road, Suite 202, New Brighton, development of the Superpave system of asphalt mix design. The
MN 55112. present study was intended to answer these questions.
Lukanen et al. Paper No. 98-1216 13

SUPERPAVE PAVEMENT TEMPERATURE • The announcement by many agencies that they were planning
OR HEAT FLOW MODEL to implement Superpave over the next few years, including the
adoption of the PG asphalt binders.
A mix design computer program, Superpave Software, was developed • A general concern in the frost-belt area that the minimum air
for Superpave. Superpave Software uses heat flow models to calcu- temperature was not a realistic expression of the minimum pavement
late the pavement temperatures from a weather database that has been temperature.
developed for Superpave. The software is being evaluated and is not • Economics. The adaptation of the PG selection criteria would
available for general release; some flaws have been identified in the require modified asphalt or would restrict the overall supply of un-
temperature routines in the program. modified asphalt that could meet the grading criteria. The need for
The selection of PG asphalt without the benefit of Superpave modifiers can significantly increase the cost of the binder and a
Software requires a transfer model to calculate typical pavement restricted supply also would result in some increase, although not
temperatures from the air temperature data. A SHRP report pre- as much as expected for a modified asphalt.
sents regression equations to predict the pavement temperatures
from air temperatures, based on results obtained from the heat flow Several years had passed since the SMP data became available
model (2). and there was no indication that the data were being used to evalu-
The equations include a model to predict the maximum surface ate the pavement temperature models for the selection of PG asphalt.
temperature from the air temperature and the latitude as follows: MAPA decided to proceed with such a study when indications
developed that the new Minnesota PG criteria may result in an
Ts (max) = Ta (max) − 0.00618Φ 2 + 0.2289Φ + 24.4 (1) increase in asphalt prices (3).
Soon after this project began, the authors discovered two studies
where that were underway to address these issues, one by Warren D.
Robertson in Canada (4) and one by Alaeddin Mohseni in Maryland
Ts(max) = maximum surface temperature (°C), (5). Robertson used data from Canadian sites at which temperature
Ta(max) = maximum air temperature (°C), and instrumentation was installed. In Robertson’s study, the LTPP SMP
Φ = latitude (degrees). sites were not selected because he was not aware that suitable data
A second equation was developed for the maximum temperature were being collected. Mohseni was performing a study for FHWA
for calculating the temperature at depth, as follows: using the SMP data. His study was for an expert task group that had
been formed by the FHWA to provide input into the binder selec-
Td (max) = [Ts (max) + 17.8][1 − 2.48 E10 −3 d tion process. Mohseni had the same basic database that the authors
had from the first round seasonal testing. Because Mohseni’s efforts
+ 1.1E10 −5 d 2 − 2.4 E10 −8 d 3 ] − 17.8 (2) were independent from those of the authors, the authors developed
an analysis data set different from Mohseni’s. In the authors’ study,
where only single maximum and minimum values were selected for each
Td(max) = maximum temperature at depth (°C), season available, whereas Mohseni selected several for each season
Ts(max) = maximum surface temperature (°C), and to increase the size of the data.
d = depth from surface (mm). The benefit of three independent temperature studies is that
these studies serve as checks on each other. All three studies had
Because the high temperature of the PG asphalt is based on the similar results and all three represented significant changes from
temperature at a 20-mm depth, the equation simplifies to the Superpave temperature selection criteria.

T20(max) = 0.955Ts (max) − 0.8 (3)


PAVEMENT TEMPERATURE DATA
The minimum surface temperature was defined as the minimum
air temperature. Since the completion of the temperature selection work for Super-
pave, the LTPP program developed the SMP. The SMP was estab-
Ts (min) = Ta (min) (4) lished to monitor environmental effects on about 48 asphalt
sections located throughout the United States and Canada. The geo-
An additional equation was offered to calculate the minimum graphical distribution of the SMP sites, shown in Figure 1, results
temperature at depth as follows: in a good representation of the range of environmental conditions
in the United States and Canada. Each SMP site is instrumented to
Td (min) = Ts (min) + 5.1E10 −2 d − 6.3E10 −5 d 2 (5) record, among other things, weather data and pavement and soil
temperature data. The temperature data is read every minute and
The idea of determining the appropriate temperature for underly- the average hourly temperature is recorded on a data logger. The
ing asphalt layers has been presented (2) but has not received much temperature data that are of interest are the air temperature and the
attention. temperatures within the asphalt. A temperature probe containing
three temperature sensors is installed in the asphalt so that the top
sensor is about 25 mm below the surface and the bottom sensor is
NEW PAVEMENT TEMPERATURE STUDIES 25 mm above the bottom of the asphalt. A sensor at the center of
the probe records the mid-depth asphalt temperature. The probe is
Three key factors contributed to the new interest in pavement a thin cylindrical rod that is placed in a saw cut at the instrumenta-
temperatures: tion location. The probe is 305 mm long to meet the placement
14 Paper No. 98-1216 TRANSPORTATION RESEARCH RECORD 1609

ment temperatures, as expected. The 25 sites and one summer season


and two winter seasons did not provide enough data to significantly
separate the role of air temperature and latitude in the prediction of
pavement temperatures. It is expected that as the data set grows, there
will be sufficient data to develop better models. Sixteen additional
SMP sites were monitored the second summer and following winter,
and three more are yet to be instrumented. The final number of asphalt
SMP sites will be 44. Of the 16 additional sites, 15 have been used to
validate the models developed based on the original 25 sites. If other
sites, such as Mn/ROAD and the sites used by Robertson, are added,
the data set should be fully adequate for the development of predic-
tion models. This does not mean that the models developed to date are
not adequate; in fact, they represent a significant improvement over
the models used previously. Nevertheless, further improvement is
possible. The model sets developed by Han, Mohseni, and Robertson
are described below.

Han’s Models
FIGURE 1 Location of LTPP SMP sites included in original
analyzed data. The data used by Mohseni were analyzed by Chunhua Han to develop
and evaluate models that relate the 7-day average high (maximum)
criteria for the thickest asphalt in the study. For thin pavements, the air temperatures to the 7-day average high (maximum) temperature
probe is placed at an angle so that the ends are 25 mm from the within the asphalt concrete and the coldest (minimum) air tempera-
asphalt surface and bottom. ture to the temperature within the asphalt concrete pavement (3).
Two data sets were developed from the SMP data. The data used These models were slightly different from those developed by
in the study were taken from the original field data files created by the Mohseni but they provided similar results. The temperatures pre-
monthly downloads from the data loggers at each of the SMP sites dicted by Mohseni and Han result in essentially the same PG. Han’s
(personal communication). QuickBASIC filter programs were writ- equations are as follows:
ten to scan the data and extract the 7-day average high (maximum)
air temperature and the corresponding pavement temperatures for Td (max) = 0.52 + 6.225Φ − 0.15Φ 2 + 0.0011Φ 3
each of the thermistors in the asphalt. A scan also was made to extract
+ 0.28Ta (max) − 8.37 LN ( d + 40) (6)
the minimum air temperature at the site and the corresponding mini-
mum pavement temperatures for each of the thermistors. The pave-
The R-squared for this equation is 0.875 on 70 data points and
ment temperature response typically lagged behind the air temperature
the standard error of the estimate is 2.2°C. It is interesting to note
by several hours.
that the temperature is so strongly correlated to latitude and depth
that the air temperature is the least significant of the independent
variables.
TEMPERATURE PREDICTION OF ASPHALT
Td (min) = − 0.14 − 1.7Φ + 0.06Φ 2 − 0.0007Φ 3
LAYER WITH SMP DATA
+ 0.69 * Ta (min) + 4.12 LN ( d + 100) (7)
The two data sets developed consist of the maximum or minimum air
temperature, corresponding pavement temperatures and thermistor The R-squared for this above equation is 0.948 on 71 data points
depths, and latitude. Initial correlation matrices developed from the and the standard error of the estimate is 2.6°C. For the minimum
data sets as shown in Tables 1 and 2 showed very high correlation pavement temperature, the air is the most significant independent
between the latitude and the maximum and minimum air and pave- variable.

TABLE 1 Correlation Matrix for Maximum Air Temperature Data Set


Lukanen et al. Paper No. 98-1216 15

TABLE 2 Correlation Matrix for Minimum Air Temperature Data Set

Mohseni’s Models Robertson’s equation has a very good fit with a standard error
of the estimate of 1.5°C. No other independent variables were
Part of the SHRP asphalt study was the collection of historic weather included. Latitude was not a factor because the sites generally were
data from all the reporting stations in the United States and Canada. above 45 degrees latitude and the results are less sensitive at those
These data were distributed in 1994 with the SHRP Superpave latitudes. His equation corresponds to about 47 degrees latitude on
Binder Selection Program, Version 1.0 (6). Mohseni also has devel- Han’s equation, as shown in Figure 2, which perhaps is somewhat
oped a database of the SMP temperature data and, from that data, south of the average latitude of his sites. Note that the positions of
has developed models to predict the high and low temperatures as the lines are most appropriate in the −40°C to −50°C range because
a function of air temperature, depth, and latitude. Mohseni pre- the higher minimum temperatures are not common between 45 and
sented his findings at the January 1997 Data Analysis Working 50 degrees latitude in North America. Northern latitudes in Europe,
Group meeting in Washington, D.C. The equations presented by particularly those affected by the Gulf Stream, may have a different
Mohseni are as follows: temperature response.

Td (max) = 54.32 + 0.77585Ta (max) − 0.002468Φ 2


− 15.137 Log( d + 25) (8) VALIDATION AND COMPARISON
OF PREDICTION MODELS
The R-squared for this equation is 0.76 on 309 data points and the
standard error of the estimate is 3.0°C. As discussed, 15 additional SMP sites have become available and
have been used to validate the models developed based on the orig-
Td (min) = −1.56 + 0.71819Ta (min) − 0.003966Φ 2 inal data sets. The new data set is from a monitoring period of two
+ 6.264 Log( d + 25) (9) summers and one winter. The annual maximum of 7-day daily max-
imum averages and the annual minimum of daily minimums for air
The R-squared for this equation is 0.96 on 411 data points and the
standard error of the estimate is 2.1°C.

Robertson’s Models

Robertson undertook a study to investigate the relationship between


the minimum air temperatures and the minimum pavement surface
temperatures. The Canadian Strategic Research Program (C-SHRP)
considered the low air temperature originally proposed by SHRP to
be much too severe. Earlier research by C-SHRP prompted FHWA
to modify the low temperature requirements in an interim guideline
for determining the low temperature requirements.
Robertson reviewed the LTPP SMP data for the study but found
only daily high and low temperatures for the air and pavement,
which was inadequate for his work. As described earlier, hourly data
exist but probably were not made available to Robertson at the time
of the request. Data from eight non-LTPP sites within Canada were
available that had hourly air and pavement temperatures. Robertson
collected that data and developed a simple relationship between
the minimum air temperature and minimum surface temperature as
follows:

TS = 0.749TA (10)

where TS is the minimum pavement surface temperature (°C) and TA


is the minimum air temperature (°C). FIGURE 2 Comparison of Han and Robertson data.
16 Paper No. 98-1216 TRANSPORTATION RESEARCH RECORD 1609

and pavement were determined. For each site only one annual max-
imum and minimum are selected to expand the original data set. The
resulting new equations follow.

Td (max) = 0.47 + 5.717Φ − 0.1276Φ 2 + 0.0008121Φ 3


+ 0.3078Ta (max) − 8.602 LN ( d + 40) (11)

The R-squared for this equation is 0.81 on 113 data points and the
standard error of the estimate is 2.7°C. It is interesting to note that the
temperature still is correlated strongly to latitude and depth and that
the air temperature is the least significant of the independent variables.

Td (min) = − 0.15 − 1.9Φ + 0.06Φ 2 − 0.0007Φ 3


+ 0.59 p Ta (min) + 5.2 LN ( d + 100) (12)

The R-squared for this equation is 0.946 on 113 data points and the
standard error of the estimate is 2.4°C. For the minimum pavement
temperature, the air is the most significant independent variable.
The model developed based on the expanded data set is slightly
different from that of the original data set in functional form
and fitting statistics. The model is compared with Mohseni’s and FIGURE 4 Maximum pavement temperature at 25-mm depth
SHRP’s in the prediction of the maximum pavement temperature as function of maximum air temperature for 40-degree latitude.
because the predictions from all the models are similar. In Figures
3 and 4, the maximum pavement temperatures at the depth of 25 mm
from three models are plotted against the maximum air temperature air temperature typical of the latitude) is presented in Figure 6, as
for 35- and 40-degree latitude, respectively. Han’s shows the flat- predicted by three models. Han’s is lower than the other two at the
test slope and SHRP’s, the steepest. Because air temperature and lower latitudes.
latitude are so strongly related in the data used in Han’s and Mohseni’s
models, only temperatures that are typical of the latitude should
be used. SELECTION OF PAVEMENT TEMPERATURE
In Figure 5, the pavement temperature profiles from three models ON BASIS OF LTPP SMP
are presented with a given latitude of 40 degrees and maximum air
temperature of 35°C. Again, Han’s predicts the coldest profile and The development of the models on the basis of the SMP provides a
Mohseni’s and SHRP’s are warmer. The variation of the maximum means of estimating pavement temperatures based on temperature
pavement temperature at the depth of 25 mm with the latitude (and measurements of in-service pavements. The pavement temperatures
then can be used to select the appropriate PG asphalt. The models
also can provide a means of selecting a PG asphalt for non-wear
courses including the binder and the base. The majority of the ton-
nage on high-volume projects is in the asphalt base. The selection
of a performance graded asphalt, based on current criteria that do
not consider temperatures at depth, may result in the use of asphalt
that is more costly than needed for binder and base layers.

APPLICATION OF MODELS TO MINNESOTA


WEATHER STATION DATA

The data from the Minnesota weather stations were loaded into a
spreadsheet and an estimate of the PG required, based on the predicted
maximum and minimum temperatures, was calculated. The maxi-
mum pavement temperature at a 20-mm depth and the minimum
pavement surface temperatures are predicted by the various models
(3). Mohseni’s models currently are the preferred models because
they have been presented to the FHWA’s expert task group on PG
binders.
Temperatures at depth also were calculated on the basis of the
models. Applying Mohseni’s relationships indicates that there is a
FIGURE 3 Maximum pavement temperature at 25-mm depth substantial temperature change with depth. For each of the weather
as function of maximum air temperature for 35-degree latitude. stations in Minnesota, the temperatures were calculated for 50-mm,
FIGURE 5 Profile of maximum pavement temperatures.

FIGURE 6 Maximum pavement temperature at 25-mm depth as function of


latitude.
18 Paper No. 98-1216 TRANSPORTATION RESEARCH RECORD 1609

100-mm, and 150-mm depths on the basis of the average air tem- An average maximum air temperature of 37°C with a standard devi-
perature and the 98th percentile. Table 3 shows the statewide aver- ation of 3°C results in the air and pavement temperature distributions
age of the in-depth temperatures. Han’s model, as discussed above, and the reliability of a PG 58 is shown in Figure 7.
provided similar results. This reliability analysis resulted in four tables (surface and depths
The 50-mm depth is 13 mm below the surface of a typical binder of 50 mm, 100 mm, and 150 mm) of reliability for maximum tem-
course in Minnesota (37-mm wear course). As shown in Table 3, perature grades of 46°C, 52°C, 58°C, and 64°C and for the mini-
depth has a greater impact on the maximum pavement temperature mum temperature grades of −22°C, −28°C, −34°C, and −40°C. To
than on the minimum pavement temperature. These data indicate illustrate the reliability distributions throughout the state, contour
that the potential for rutting diminishes with depth, even without maps were generated from the data in some of these tables. Contour
accounting for the lower stress at depth. maps were generated for the wear course requirements and for sev-
eral PG binders at various depths. Two of the contour maps are pre-
sented in Figures 8 and 9 and clearly show the effect of pavement
EVALUATING RELIABILITY OF PG BINDERS depth on reliability. Different PG grades may be selected for asphalt
in different depths to meet the required reliability level.
The established grading for PG binders steps at 6-degree increments
for the maximum and minimum temperatures. Climatic conditions
may result in large areas that are marginal for a particular grading
CONCLUSIONS
but do not quite meet the selection criteria at 98 percent reliability.
To develop a better understanding of how the climatic variations
An empirical model is a statistical solution that provides practi-
within Minnesota affect reliability, calculations were made to deter-
cal predictions of pavement temperature. The empirical model
mine the reliability of a specific maximum or minimum temperature
developed focuses on three main factors—extreme air temperatures,
at all of the weather stations.
temperature profiles in the pavement, and latitude—and is practically
To handle the reliability issue, Robertson adds the 0.749nσ and
nSEE to the equation to determine the surface temperature at the simple in use. The wide data range from the LTPP SMP sites used
chosen reliability and its corresponding n. For instance, for 98 per- for model development makes the model applicable in much of North
cent, the n is equal to 2.06. If the standard deviation of the minimum America.
air temperature is 3 degrees, then the 98th percentile would be The distribution of the annual maximum and minimum temper-
2.06(0.749 × 3 + 1.5) = 7.7 degrees colder than the 50th percentile atures over many years is independent of the errors associated with
temperature. A more appropriate approach, as discussed below, to predicting the maximum and minimum pavement temperatures.
calculate the reliability is to use the following calculation process: The combined standard deviation of the maximum or minimum
2.06[(0.749 × 3)2 + 1.52]1/2 = 5.6 degrees. A 2-degree difference pavement temperature is the square root of the sum of squares of
would make a difference on about a third (2°/6°) of the projects. maximum or minimum air temperature standard deviation and the
Robertson’s equation that includes reliability actually is equivalent standard error of the estimate of the model.
to an n of 2.86 or a reliability of 99.8 percent. The regional reliability contour for a given PG grade selection is
The calculation of the reliability of a certain PG asphalt binder a direct and convenient tool for asphalt binder selection. There is a
first assumes that the maximum and minimum air temperatures are great potential for the application of reliability contours based on the
normally distributed and that the residuals of the prediction model probabilistic method at the state and regional levels.
also are distributed normally. It also is assumed that the variation The pavement temperatures within the base and binder layers do
in annual maxima is independent of the variation in predication. The not require the same PG grade of asphalt. It may be possible to select
combined standard deviation of the pavement temperatures calcu- lower-cost asphalt binders for binder and base layers.
lated with one of the models discussed is calculated by the following
equation:

σ pvm't = σ air
2
+ σ 2reg (13) ACKNOWLEDGMENTS

The authors gratefully acknowledge financial support from the Min-


where
nesota Asphalt Pavement Association. The authors also thank David
σpvm’t = standard deviation of pavement temperature, S. Holt for providing valuable guidance and comments. Permission
σair = standard deviation of air temperature, and from the Minnesota Asphalt Pavement Association to allow the
σreg = standard error of estimate of model. authors to publish the results is appreciated.

TABLE 3 Average Pavement Temperatures, Based on Mohseni’s Models


FIGURE 7 Distribution of maximum air and pavement temperatures and
probability temperature will not exceed 58°C.

FIGURE 8 PG 52 reliability contours in Minnesota.


20 Paper No. 98-1216 TRANSPORTATION RESEARCH RECORD 1609

FIGURE 9 PG 52 reliability contours at 50-mm depth in Minnesota.

REFERENCES 4. Robertson, W. D. Determining the Winter Design Temperature for


Asphalt Pavements. Presented at Annual Meeting of the Association of
Asphalt Pavement Technologists, St. Paul, Minn., 1997.
1. Strategic Highway Research Program Research Plans. TRB, National
5. Mohseni, A. Seasonal AC Pavement Temperature (SAPT) Database. Pre-
Research Council, Washington, D.C., 1986.
sented at meeting of the Transportation Research Board Data Analysis
2. Superior Performing Asphalt Pavements (Superpave): The Product of
Working Group Meeting, Washington, D.C., January 1997.
the SHRP Asphalt Research Program. SHRP-A-410, Strategic High-
6. Mohseni, A. SHRP Superpave Binder Selection Program, Version 1.0.
way Research Program, National Research Council, Washington,
FHWA, U.S. Department of Transportation, October 1994.
D.C., 1994.
3. Lukanen, E. O., and C. Han. Performance Grade Selection for Asphalt
Binder and Base. Report prepared for Minnesota Asphalt Pavement Publication of this paper sponsored by Committee on Characteristics of
Association. Braun Intertec Corporation, St. Paul, Minn., March 1997. Bituminous Materials.

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