Performance Report

System

System
Start time: 4/22/2020 1:26:09 PM
Instrument: iCAP Q
Operator: ICP-MS-PC\ICP-MS
Template: STD BHIOS 4
Instrument Serial Number: 03310R
Last Autotune: Autotune-KED Autotune Line 1-20200422-132020411.imatdat
Solution: No solution specified
Sensitivity & Stability Test

Sensitivity & Stability Test

Result Runs Sweeps
Passed 4 60

Sensitivity

Sensitivity
Analyte Result Value Condition Limit
Bkg4.5 Passed 0.13 CPS Less than 1.0 CPS
Bkg220.7 Passed 0.0 CPS Less than 2.0 CPS
7Li Passed 83,867.0 CPS Greater than 50,000.0 CPS
59Co Passed 203,306.0 CPS Greater than 100,000.0 CPS
238U Passed 495,699.0 CPS Greater than 300,000.0 CPS
140Ce.16O/140Ce Passed 0.0193 Less than 0.025
137Ba++/137Ba Passed 0.026 Less than 0.03
115In Passed 376,975.0 CPS Greater than 220,000.0 CPS

Stability

Stability
Analyte Value Limit
7Li 0.8 % 2
59Co 0.5 % 2
238U 0.4 % 2
115In 0.4 % 2

Mass Calibration Test

Mass Calibration Test

Result Channels Dwell MeasureWidth PointSpacing Sweeps
Passed 75 0.04 1.5 0.02 5

Analyte Result Centroid Mass [u] Offset Peak width [u] Peak width min [u] Peak width max [u]
7Li Passed 6.9946 0.0214 0.726 0.650 0.850
59Co Passed 58.9177 0.0155 0.711 0.650 0.850
115In Passed 114.8442 0.0597 0.768 0.650 0.850
238U Passed 237.9889 0.0619 0.777 0.650 0.850

4/29/2020 1:04:37 PM 1/3

Performance Report

Tunesettings

Tune Settings
Parameter Value
Additional Gas Flow 1 0.00
Additional Gas Flow 2 0.00
Additional Gas Flow 3 0.00
Angular Deflection -382.40
Auxilliary Flow 0.80
CCT Bias -2.01
CCT Entry Lens -94.00
CCT Exit Lens -160.01
CCT Focus Lens -1.92
CCT1 Flow 0.00
CCT1 Shut-Off Valve 0.00
CCT2 Flow 0.00
CCT2 Shut-Off Valve 0.00
Cool Flow 14.00
D1 Lens -198.39
D2 Lens -80.00
Deflection Entry Lens -35.00
Extraction Lens 1 Negative 0.00
Extraction Lens 1 Polarity 0.00
Extraction Lens 1 Positive 0.00
Extraction Lens 2 -144.33
Focus Lens 21.70
Nebulizer Flow 0.81
Peristaltic Pump Speed 40.00
Plasma Power 1350.00
Pole Bias -1.00
Quad Entry Lens -28.01
Sampling Depth 5.00
Spray Chamber Temperature 2.50
Torch Horizontal Position -0.50
Torch Vertical Position -0.77
Virtual CCT Mass Maximum Dac Limit Set 4095.00
Virtual CCT Mass parameter b 0.65
Virtual CCT Mass to Dac Factor 130.00
Virtual CCT Mass to Dac Offset -190.00

Vacuum Check

Vacuum Check
Parameter Result Value
Analyzer Pressure Vacuum ok 4.032e-7
Interface Pressure 1.581e+0

Detector Voltages

Detector Voltages
Analog Counting
-2125.00 1500.00

4/29/2020 1:04:37 PM 2/3

Performance Report

Mass Calibration Peaks

Mass Calibration Peaks

7Li

Analyte: 7Li

59Co

Analyte: 59Co

238U

Analyte: 238U

115In

Analyte: 115In

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