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a
DECivil-IST, Technical University of Lisbon, Av. Rovisco Pais, 1049-001, Lisbon, Portugal
b
Department of Buildings, National Laboratory of Civil Engineering – LNEC,
Av. do Brasil, 101, 1700-066, Lisbon, Portugal
This research assessed the performance of mortars in which recycled concrete aggregates (RCA)
was a component. It replaced natural sand but kept the same particle size distribution. Three mortars
were produced with replacement ratios of 20%, 50% and 100% as well as a reference mortar containing
no recycled aggregate. The compressive and flexural strength, water absorption by capillarity, drying
capacity and susceptibility to cracking of these mortars were analyzed first. Then, based on these results,
the most satisfactory replacement ratio was chosen and the following properties were analyzed: water
retentivity, shrinkage, adhesive strength, modulus of elasticity, and water vapor permeability. Somewhat
surprisingly the best results in the first stage occurred for 20% and 100% replacement ratios, leading
to a cautious choice of the 20% ratio for the second stage. Generally the mortar with 20% replacement
ratio performed better than the reference mortar, except for adhesive strength and dimensional stability.
1. Introduction
World population expansion has led to an exponential these characteristics and by comparison with a reference
increase in the consumption of natural resources and energy, conventional mortar, in order to verify their performance
and the amount of waste produced. Until quite recently, and as renderings.
despite years of experience in the field, the construction
industry has seemed quite oblivious to worries about 2. Literature Review
managing the waste produced.
Construction is not only one of greatest generators of Various studies on the use of recycled aggregate in
waste; it also consumes around 40% of all extracted natural concrete have been performed in the last few years, but for
resources1. It is thus essential to intervene to encourage more mortar such research is only just starting. Some interesting
sustainable construction practices. conclusions have nevertheless been reached.
Studies on the use of recycled aggregates have mostly It was generally found that mortars containing recycled
focused on their coarse fraction and ignored the fine fraction. aggregates need more mixing water to reach the same level
This is basically because the extreme porosity of fine of workability as conventional mortars because of the greater
porosity of the recycled aggregates. It is well established
recycled materials leads to reductions in the performance
that aggregates with greater porosity and surface area per
of any composites containing them2.
volume unit absorb more water and therefore they make
Our study focused on the viability of replacing sand with
the resulting mortar more consistent3. Bavaresco4 observed
fine recycled concrete aggregate in the production of mortar,
that mortars made with recycled aggregate consumed
i.e. composites made of cement, fine aggregates, water and
75% more water than that made with sand. Miranda5 and
eventually admixtures and additions, particularly for use as
Silva et al.6 obtained similar results, i.e. more mixing water
wall coatings and mixed on site for immediate application.
needed for modified mortars in order to obtain a satisfactory
This research intends to contribute to the management
workability. However, because the high water absorption of
and reuse of construction and demolition waste (CDW) in
these porous aggregates the effective content in the cement
order to reduce their impact, and simultaneously reducing
paste can be substantially lower than the total water content,
the extraction of sand from river beds, an activity with a
a distinction has to be drawn between total and effective w/c
great potential for degrad-ing the environment.
ratio in mortars containing recycled aggregate7.
The most important characteristics of hardened
The mortar’s density is also affected. According to the
mortar for wall covering are: mechanical strength,
literature there is a downward trend as recycled aggregates
modulus of elasticity, water permeability, adhesive
are incorporated into the mix because their particle density
strength and resistance to weathering, and those of fresh
is lower than that of conventional aggregates. In the
mortar are workability, and water retentivity3. Several
Hanžič et al.3 study the dry bulk density of the hardened
mortars with recycled aggregates are assessed based on
mortars containing recycled aggregate was 8% lower than
*e-mail: jb@civil.ist.utl.pt that of mortar made with natural sand only, and a similar
2014; 17(1) Using Fine Recycled Concrete Aggregate for Mortar Production 169
situation occurred in the Silva et al.6, Bavaresco4 and reference mix or mortars made with recycled aggregates of a
Pedrozo8 studies. different nature, such as ceramic materials. Moriconi et al.16
Most studies consulted found that water retentivity of and Corinaldesi and Moriconi17 found that mortars with
fresh mortar made with recycled aggregates was lower. recycled aggregates exhibited a stronger bond with the
Since they are made of porous materials (ceramic materials substrate (masonry). According to the authors the mortars
and crushed concrete) water retention capacity becomes an with recycled aggregates had higher w/c ratios for the same
important characteristic9. In the Hamassaki et al.10 study workability as the reference mix. Thus these mortars could
the mortar with the highest water retentivity was the one more effectively waterproof the brick surface and guarantee
containing ceramic bricks and the mortars made with a physical blockage and improved bonding.
concrete waste had a lower retentivity than the reference This is considered very positive since the mechanical
mix. This situation is corroborated by Miranda and Selmo11 performance of a coating mortar depends more on its
and Bavaresco4 where the mortars with the highest concrete connection to the substrate than on the compressive or
waste content had lower water retentivity than the one with flexural strength of the paste itself16.
ceramic material. Therefore it is concluded that a higher As for the modulus of elasticity, it is concluded that
content of concrete in the recycled aggregates leads to lower it is lower in mortars made with ceramic materials than
ability to retain the mixing water. in mortars containing concrete waste and the reference
In terms of water absorption by capillary action, results
mix. Topçu and Sengel15 obtained a maximum value and
from the studies consulted reveal greater water absorption
a minimum value for the modulus of elasticity at 20% and
and porosity, which are both typical of recycled aggregates.
90% replacement ratios, respectively. The author reports
In the Silva et al.6 and Pedrozo8 studies, however, replacing
that this was due to the porous nature and lower modulus
sand with recycled aggregate led to a decrease of 20% to
of elasticity of the recycled aggregates than natural sand.
30% in absorption by capillary ac-tion of the mortars made
Based on the literature review it can be concluded
with recycled aggregates.
that the incorporation of recycled aggregates in mortars
This better initial performance is explained by the
to replace conventional aggregate (sand) in small ratios
combination of the slight pozzolanic effect of the fine
ceramic aggregates incorporated with a filler effect, even (between 10% and 20%) can improve their performance.
though the content of ultrafine particles in the ceramics was After that the performance of mortars made with recycled
only slightly higher than that in sand. However, for higher aggregates tends to decline, particularly for ratios over
replacement ratios the overall effect switches to an increase 50%. Silva et al.6 concluded that the optimal replacement
of the capillary absorption approximately proportional to percentage in cementitious mortars (for aggregates made of
the ratio, probably because the ultrafine particles content crushed ceramic materials) would be 15%. This difference
exceeds the potential filling effect they allow. in performance may also depend on the type of recycled
Previous studies showed a poorer performance with aggregate used, and in the studies performed so far mortars
respect to dimensional stability. Because recycled aggregates with recycled ceramic aggregates gave better results than
have a relatively high water demand, shrinkage increases as those with concrete waste, as in the studies of Levy18,19 and
more are added12. Mortar shrinkage may depend on factors Bavaresco4, in which the authors compared mortars that
such as the w/c ratio, cement content, size grading of the incorporated various types of recycled aggregates.
sand, and setting time13. Thus, shrinkage depends on the As a conclusion from previous works, it seems to be
aggregates’ density, the porosity of the paste adhered to them possible to use recycled aggregates in mortars without loss
and their saturation6,14. In the Hamassaki et al.10 study it was of performance, but the limitations of use and the optimal
observed that the mortars with the highest drying shrinkage content to be adopted depend on the nature of the recycled
were those with the highest concrete waste content. material. Thus complete studies are needed for each type.
There is no consensus in the literature concerning
compressive and flexural strength, since some studies led 3. Sequence of Testing
to higher values in mortars with recycled aggregates and
vice-versa. Unlike concrete where compressive strength 3.1. Materials used
is a decisive factor for its application, the influence of this
property on the performance of coatings is weak3. This research was divided into two experimental stages
Pedrozo8 and Topçu and Sengel15 found that almost all to determine how replacing sand with fine recycled concrete
mixes with recycled aggregates had higher flexural strength aggregates, in various percentages but with the same particle
than the reference mix, whereas compressive strength tended size distribution, influences mortar’s performance.
to decrease. The two series of tests comprised:
When the recycled aggregate was crushed concrete • 1st stage - the characteristics of each mortar mix were
both the flexural and compressive strength improved. The compared through a set of relevant tests to find the
particles’ shape (sharper edges) has a positive effect on the best replacement ratio to be analyzed in the second
interface bond between the aggregate and the surrounding stage;
cement paste. • 2 nd stage - complementary tests on the mortar
Concerning the adherence to the substrate, it was mix selected in the first stage to characterize its
found in all studies cited that the performance of mortars performance more precisely and establish the viability
incorporating concrete waste performed better than the of using it in coating solutions.
170 Neno et al. Materials Research
The reason is the same as for the decrease of the cement paste of the mix is better. Furthermore, this waste
fresh bulk density. The small initial increase is linked to may contain some non-hydrated cement that completes its
a possible reduction of the voids due to the probable filler hydraulic reactions and sets when in contact with water,
effect stated in the Materials section concerning especially leading to greater cohesion between the particles and
the fraction below 0.063 mm (thus increasing the mass for strength25.
the same volume). This filler effect no longer prevails after Of those made with RCA the mortar with 100% has
the 20% replacement ratio because the volume of concrete the lowest water content in its composition, i.e. for the
waste increases and the influence of its lower particle same cement it has less water and lower voids volume,
density becomes more significant than the filler effect of creating greater cohesion and higher strength in the mortar.
the ultrafine fraction. Usually the addition of air (porosity) leads to a reduction
of around 3% to 5% in mechanical strength per 1% of air
5.1.4. Flexural and compressive strength of hardened incorporated26.
mortar These results agree with those of other authors such
These tests were performed according to European as Hamassaki et al.10, who obtained the best compressive
standard EN 1015-11[24] to determine the strength of the strength results for the mix with 100% incorporation of
mortars under a uniform compressive and flexural stress. concrete waste.
This is achieved by submitting the specimen to a flexural test Other studies report that the compressive strength
and then applying a compressive load to each half specimen decreased in the mortars with recycled aggregates, for
that leads to its failure. Ultimate loads are registered for both example Pedrozo8 used a volumetric proportion of 1:3
tests. The flexural test was performed on three prismatic (cement: sand) and the recycled aggregates were of various
specimens (40 mm × 40 mm × 160 mm) per mix after curing types, thus decreasing the bond between particles.
for 28 days. The compressive test was carried out on the six As for flexural strength, the results agree with previous
resulting half specimens. studies, especially the one by Pedrozo 8, in which the
Figures 3 and 4 indicate that there is a similar pattern in maximum flexural strength was obtained in the mortar
flexure and compression. The respective strengths show a containing 100% recycled aggregates. Even though the
growing trend until 20% replacement, a slight decrease for reference mix of the Corinaldesi and Moriconi17 study had
50% and reach a new maximum for 100%. higher strength than those containing recycled aggregates
This may be caused by various factors. The concrete made of bricks or a recycled aggregates mixture, the mix
particles have a higher specific surface and are sharper- with concrete waste was the strongest at 28 days.
edged and more porous than sand, so the bond with the In the Topçu and Sengel15 study where crushed tiles were
incorporated the reference mix had the lowest figures for
flexural strength while the maximum strength was achieved
for a recycled aggregates replacement ratio of 30%.
5.1.5. Water absorption due to capillary action of
hardened mortar
To determine the water absorption due to capillary
action the methodology and procedures set out in European
standard EN 1015-18[27] were followed. What was measured
is the increase in water mass that ascends by capillarity
through the prismatic specimen cross-section in contact with
a water surface. The test was performed on three specimens
(semi-prisms) per mix type after curing for 28 days. The
water absorption coefficient due to capillary action was
Figure 3. Compressive strength of hardened mortar relative to Figure 4. Flexural strength of hardened mortar relative to
replacement ratio. replacement ratio.
172 Neno et al. Materials Research
determined and the water absorption rate expressed over a Previous findings do not totally agree with these results.
period of between 10 and 90 min. Pedrozo8 also obtained an increase in capillary absorption as
In this test the mortars showed almost constant initial the incorporation rate of recycled aggregate went up, again
water absorption coefficient values that decreased after because of the nature of the recycled materials (various
a 50% replacement ratio (Figure 6). The mortar with types of recycled aggregates) that created more voids and
the highest capillarity coefficient was the reference mix less uniformity and cohesion in the mortar.
(A0) and the one with the lowest was A100 (Figure 6), 5.1.6. Drying test of hardened mortar
though it was also the one that absorbed most water at
To determine the drying capacity the three specimens
long term (Figure 5). This means that the open porosity
used in the water absorption by capillary action test were
of A100 is the highest, confirming the results of the other
removed from the water containers and left to dry at the same
tests, so the asymptotic water absorption is also the most temperature. They were then weighed 30, 60, 90, 270 and
significant; on the other hand, the average pores’ diameter 450 min after the first weighing and again at 24 h intervals
is possibly the lowest, due to best connection between until constant mass.
matrix and aggregates and probably also due to the filler The results are presented in Figure 7.
effect, explaining the lowest capillary rate expressed by the It was found that the mortars containing concrete
coefficient of capillarity28. waste (20%, 50% and 100%) exhibited behavior relatively
Given that the recycled aggregates are more porous similar to that of the reference mix (0%). The highest water
than natural sand they can absorb more water that later on evaporation rate for all mixes occurred between 400 and
can combine with cement leading to a positive effect on the 3600 min (6.7 h to 60 h).
mortar’s hydration process3.
5.1.7. Susceptibility to cracking
Another relevant factor is the fact that the mortar with
100% RCA is the one using least water in its composition This characteristic was qualitatively evaluated by
(of those made with RCA). The amount of free water in applying each mortar type to three bricks. The surface was
then checked at intervals during 28 days curing in a dry
the mix and the voids volume are thus reduced for this
conditioned room (23 °C/50% RH).
mortar, which increases the cohesion between particles and
None of the mortars showed any type of cracking
decreases the water absorption rate by capillarity (Figure 5).
(see Figure 8) after 7 months of observation. It is thus
concluded that none of the replacement ratios tested is very
susceptible to cracking and therefore concrete waste used
as fine aggregate in mortars did not significantly worsen
their short/medium-term performance in terms of cracking.
However, this application on relatively limited areas such
as a brick’s surface is no guarantee that there is no cracking
in larger areas and therefore this test is but a first approach
to this analysis.
5.1.8. Selection of mortars for the second stage
Analyzing and comparing the results from the first stage
for the three mortars with RCA (A20, A50 and A100) the
one with most consistent and satisfactory results was chosen.
Mortar A100 had better results than the others and would
Figure 5. Water absorption by capillarity action tests results of be the probable choice for the second stage. However it was
hardened mortar relative to replacement ratio. not chosen because the initial purpose of this mix was to
Figure 6. Water absorption coefficient by capillary action of Figure 7. Specimens’ water loss by evaporation relative to square
hardened mortar relative to replacement ratio. root of time.
2014; 17(1) Using Fine Recycled Concrete Aggregate for Mortar Production 173
quantify the asymptotic trend of the results (which was not This increase in dimensional variability may be because
achieved) and to check how the mortars would perform in a recycled aggregates such as concrete waste are made of
limit situation, i.e. total replacement of sand with recycled much more absorbent and porous particles than natural
aggregate. It was decided to be conservative and choose sand, leading to a reduction in stiffness that prevails over
mortar A20 for which every property studied improved the filler effect advantage.
relative to the reference mix, particularly compressive and This phenomenon is also associated with the higher
flexural strength where the results were better for A20 than cement (and cement paste) content, possibly incompletely
A50. Even though A100 returned even higher figures for stabilized, and very fine particles in the mortar made with
these properties they were not particularly advantageous concrete waste)13, which would both lead to increased
since a coating mortar needs minimal strength and some shrinkage.
elasticity in order to cope with the substrate movements 5.2.2. Water retentivity of fresh mortar
without cracking. This cautious appraisal of the situation
proved to be the most appropriate in the second stage. This test was performed according to European standard
In terms of capillary water absorption, mortar A20 prEN 1015-8[30] and is based on the evaluation of the water
retained through a suction procedure, thus determining
has a lower coefficient than A50 and A0, i.e. the mortar’s
the amount of water retained within the mortar after the
performance improved from this point of view, but the best
procedure is over. The result is presented as a percentage
result was again given by A100.
of the water initially retained within the mortar and is the
In the drying test and the susceptibility to cracking test
average of three specimens per mix type.
no differences were detected between the three mortars.
The results presented (Table 3) show that the mortar
Other important properties of the mortars were tested in
containing concrete waste (A20) has greater water retentivity
the second stage and these results allowed a better general
than the reference mortar (A0). This is a very positive
characterization of the advantages and drawbacks of the result because the more water the mortar retains the more
mortar with 20% incorporation of concrete waste compared probable the hydration of the cement within the mix is,
with the reference mix. which encourages the proper hardening of the paste and
5.2. Second stage improved mechanical strength and adherence31.
Cement hydration is a time-consuming process that
5.2.1. Dimensional stability (shrinkage) tends to slow down, but it occurs as long as the mix contains
enough water and the temperature range is favorable25. Once
This test was performed according to Cahier 2669-4[29] the water is lost hydration ceases and therefore, according
on three specimens per mix type (A20 and A0), immediately to Silva et al.6, water retention helps prevent rapid suction
after demolding. The shrinkage that occurs while the mortar from the substrate and evaporation, which both dries out
hardens and in the first months of curing may be called the mortar and hinders complete hydration of the cement,
drying shrinkage13. and so the function of part of the cement switches from
Figure 9 shows that the dimensional change results for binder to filler.
the reference mortar (A0) are substantially less pronounced According to Scherer 32 the existence of different
than those of mortar made with RCA (A20). It is thus capillary pressures within the mortar during curing may
concluded that the mortar containing concrete waste shrinks lead to cracking.
considerably more than the reference one, in accordance These results disagree with some of the previous studies
with Kikuchi et al.12. of mortars with recycled concrete aggregates, in particular
by Miranda and Selmo11 and Bavaresco4. But increased this value. The test was performed on three specimens per
water retentivity was found in studies of mortars containing mix type after curing for 28 days.
recycled ceramic aggregates (e.g. the Silva et al.6 study found Table 5 shows that the modulus of elasticity of the mortar
that the mortar with brick waste incorporation had the best with concrete waste incorporation (A20) is slightly higher
water retentivity). In the Hanžič et al.3 study the mortars than that of the reference mortar (A0). This increase is not
with recycled aggregates also gave the best results in terms necessarily favorable because the modulus of elasticity is
of water retention capacity. directly related to the cracking propensity of mortars, since
deformations give rise to higher internal stresses. These
5.2.3. Adhesive strength of hardened mortar results concur with those for compressive and flexural
This test was performed according to European standard strength, which were also higher in the mortar made with
EN 1015-12[33] and consisted of determining the tensile recycled aggregates.
force necessary (adhesive strength) to pull off a given area This trend is partly due to the greater dry bulk density
of mortar applied to a substrate. The test was performed (higher density and lower voids content) of the mortar with
on three specimens per mix type after curing for 28 days. concrete waste, which is linked to the filler effect mentioned
Table 4 shows that the adhesive strength of the mortar above that seems to prevail for this replacement ratio (20%).
made with RCA (A20) is lower than that of the reference The results of previous studies, particularly those by
mix (A0). But the difference is small, given the dispersion Silva et al.6 and Topçu and Sengel15, did not agree with the
of the results (high standard deviations). The scatter in current investigation. This may be because their recycled
the results of this test is explained by its execution, which aggregates came from more porous ceramic materials with
depends on various factors such as procedures to humidify higher voids content, which implies slower propagation
the brick (substrate), the manual application of the mortar velocity of the ultrasonic waves and thus a lower modulus
on the brick, and the way the manual pull-off equipment of elasticity36.
is handled. Groot34 concluded that the two water flows can 5.2.5. Water vapor permeability of hardened mortar
influence the mortars’ adhesive strength: from the mortar
to the brick (right after they are in contact) and from the This test was performed according to European standard
brick to the mortar (after compaction and initial hydration EN 1015-19[37] and was based on inducing different pressure
of the paste). levels in two opposing faces of a 20 mm circular specimen
Therefore it can be considered that the mixes showed a and measuring the amount of water vapor that circulates
similar performance without significant differences. between them. The test was performed on five specimens per
mix type after curing for 28 days. Water vapor permeability
5.2.4. Modulus of elasticity of hardened mortar is a factor in pathology associated with excess condensation
This test was performed according to the standard or dampness, usually linked with lack of permeability26.
NP EN 14146[35] and it consisted of using a fundamental The results in Table 6 show that the water vapor
frequencies measuring device to determine the resonance permeability of the mortar containing concrete waste (A20)
is slightly higher than that of the reference mix (A0). This
frequency of a prismatic specimen subjected to longitudinal
is again linked to the concrete waste particles being more
vibrations. The dynamic modulus of elasticity depends on
porous and having higher water absorption, thus allowing
freer permeability for water vapor to circulate. However, the
difference is small because the influence of particle porosity
Table 4. Results of the adhesive strength test.
was to some extent offset by a filler effect that hinders water
Mortar Adhesive strength Standard deviation Type of vapor circulation.
(MPa) (MPa) failure With these results it is concluded that the mortar with
A0 0.33 0.113 Adhesive RCA incorporation has a slightly improved performance
Adhesive/ in terms of capacity to release water vapor by comparison
A20 0.27 0.053
cohesive with conventional mortars, because it facilitates drying of
both the mortar and its substrate.
Table 5. Results of the determination of the module of elasticity. 5.2.6. Render cracking susceptibility - restrained
Mortar Module of elasticity Standard deviation shrinkage and tensile strength of hardened
(GPa) (GPa) mortar
A0 7.07 0.46 This test is based on a technique developed and validated
A20 8.25 0.38 by Veiga38 at the laboratory of wall coatings of LNEC
Table 9. Functional demands of mortar in current buildings and characteristics of the mortars to be used (adapted from)44.
Functional Characteristic Requirement or Results for the mortar with Requirement
requirement recommendation RCA basis
Modulus of elasticity E ≤ 10 000 MPa 8 250 MPa
Medium to weak
Susceptibility to Restrained shrinkage Moderate
susceptibility
cracking
No demand
Water retentivity Higher than the reference mix LNEC’s
(preferably high)
Complementary
Water vapor Thickness of the air diffusion layer requirements
Sd ≤ 0.15 m Sd = 0.15
permeability equivalent to 0.10 m of mortar Sd (m)
performance compared with the reference mix. All the comply with the criteria recommended by Veiga43,
results presented complied with the criteria proposed by as seen in Table 9.
Veiga43 (Table 9): Overall, the mortar with incorporated fine recycled
• Concerning water absorption by capillarity, the concrete aggregate proved to be a viable solution with
presence of concrete waste in mortars seems to have great potential for use in the construction industry. Its
a very positive effect since the water absorption rate mechanical performance is significantly superior regardless
decreased (by up to 25% for total replacement versus of the replacement ratio, and its permeability is also more
the reference mix); favourable. As for susceptibility to cracking, the performance
• In terms of compressive and flexural strength, obtained for 20% substitution is considered acceptable and
incorporating concrete waste in mortars (replacing comparable to that of a conventional cementitious mortar.
sand) led to a substantial improvement (35% in Based on the results of this study it is recommended to
flexural strength and 45% in compressive strength); use RCA partially replacing sand in mortars intended for
as for adhesive strength of the RCA mortar to the wall rendering, as long as the replacement ratio is limited
substrate there was a decrease (around 20%) from the to 20% by volume. The very complete test program allowed
reference mix figure, though it remained well within evaluating many properties that influence the performance
the limits set in Table 9; of mortars used for wall covering and that are not analysed
• The performance of the mortar with RCA incorporation in most studies, such as susceptibility to cracking, water
in terms of water vapor permeability was slightly vapour permeability and water retentivity. It must be
superior (approximately 5%) to the reference mix; stressed that, based on a smaller program (first stage), 100%
• The results for cracking susceptibility were generally replacement would seem favourable, while a more complete
a bit poorer than those of the reference mix; besides study showed the trend to increase susceptibility to cracking.
an increase of around 45% of shrinkage in the mortar However, the performance of these modified mortars
made with RCA, the modulus of elasticity was also needs to be fine-tuned in on site large-scale applications.
higher, which indicates this mortar has a higher
propensity to cracking; this slight loss of performance
was confirmed in the restrained shrinkage test
Acknowledgements
in which the susceptibility of the RCA mortar to The authors are grateful for the support of ICIST
cracking was classified as moderate whereas the Research Centre (Instituto de Engenharia de Estruturas,
reference mix was classed as low; even though these Território e Construção), IST, Technical University of
results are unfavorable in relative terms they still Lisbon and FCT (Fundação para a Ciência e Tecnologia).
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