Spectro Oil Analysis PDF

Solutions for Power Generation and Industrial Plants
Maximize
machine
uptime
Extend
oil drains
Prevent
premature
failures
In-service Oil Analysis for Machine Condition Monitoring
Since the reliable operation of high value, fixed assets is critical to all industrial plants,
predictive maintenance programs are implemented to manage machinery uptime.
In-service oil analysis is a key machine condition monitoring technique for Condition
Based Maintenance (CBM) and Reliability programs. It complements vibration
analysis, thermography and other predictive maintenance technologies. In the time
it takes external laboratories to return oil sample results, machinery condition can
change significantly. On-site oil analysis eliminates this wait and enables immediate
decision making.
Corrosion and wear cause surface degradation of the lubricated surfaces in
machinery and are the root causes of most mechanically-induced equipment
downtime. Corrosion is caused by water or other fluids reacting with metal surfaces,
while wear is caused by surface abrasion, adhesion and fatigue.
Oil analysis provides early indications of equipment wear and identifies the root
causes of corrosion.
ONSET OF
FAILURE
OPTIMAL
WORKING
The P-F Curve (Potential- CONDITION
Failure Curve) illustrates
EQUIPMENT
how in-service oil analysis
EQUIPMENT CONDITION
FAILS
provides critical information
on machine condition in both
Proactive and Predictive PROACTIVE PREDICTIVE
Maintenance periods. MAINTENANCE MAINTENANCE
Monitor Oil Condition Monitor for
& Contamination: Abnormal Wear:
In the Proactive period, oil
• Viscosity, oil chemistry, water • Total ferrous
condition and contamination
• Particle count with ISO codes • Wear particle analysis
monitoring help prevent the • Elemental analysis of • Elemental analysis
onset of the root causes normal wear particles
of machine failure. In the • Total ferrous
Predictive period, monitoring FAILURE
COST TO REPAIR
the increasing severity

of wear particles allows
maintenance work orders to
be executed for component
replacement or repair before
catastrophic failure.
OPERATING HOURS
2 | Industrial Solutions
As part of a proactive maintenance program, on-site oil analysis
delivers rapid results with immediate decision making to:
n Lower operating costs
n Reduce unscheduled downtime
n Increase machine availability
n Extend equipment life
n Decrease total lifecycle equipment costs
n Provide immediate retest capability
Trivector™ – oil and machine health simplified

The TriVector™ is a simple representation of the integrity of the lubrication system and the
health of the machine itself. The Trivector indicates the degree of health in each vector.
Each vector is a representation of Alarm Limits based on underlying parameters, such as
viscosity, water contamination, acid number, oxidation, total ferrous, particle count and ISO
code, large ferrous particle count, etc.
The following questions can be answered:
 Is the machine healthy?

 Can I predict when the
machinery will fail?
 Is the oil dry?

 Is the oil clean/
free of dirt?
 Is it the right oil?

 Is the oil fit for use?
*Trivector is a trademark of Emerson Process Systems Industrial Solutions | 3

MiniLab Series
4 simple tests and less than 15 minutes
to comprehensive oil analysis
Can be operated on-site by plant staff; no chemist required.
ELEMENTAL ANALYSIS
The elemental analyzer provides
measurement of 24 elements to
identify individual contaminants,
wear metals and the elemental
composition of additives.
PARTICLE COUNT
AND FERROUS MONITOR
The direct imaging particle counter and
ferrous monitor provides particle counts
and ISO codes, wear classification,
ferrous particle counts & size distribution,
and total ferrous measurement.
VISCOSITY
The portable viscometer provides
high accuracy 40°C kinematic
viscosity measurements.
Trivector reports on
machinery health
Easy to interpret results with Trivector sample
and trend reports.
CHEMICAL ANALYSIS
The infrared spectrometer
measures Total Acid Number
(TAN), oxidation and water for
machinery oils and hydraulics.
Industrial Solutions | 5
MiniLab Series Software
The MiniLab Series software suite consists of the TruVu 360 Enterprise Software – a browser
based software platform, and the TruVu 360 Device Console for MiniLab operation.
It delivers best practice for the on-site oil analysis process and provides performance
dashboards at the asset, plant, and corporate level.
It unifies asset trending of oil condition, chemistry and machinery wear with automated
diagnostics and recommended maintenance actions, and provides maintenance and oil
savings tracking for assets.
The rules engine can be adapted to users’ unique asset requirements, including both
automatic diagnostics or user editable functions at the individual asset level.
TruVu 360 Enterprise cloud software
ASSET & TOOL BAR SAMPLE ANALYSIS PROCESS DASHBOARD

n Create asset database with provided n Track samples that are planned, in Dashboards bring visibility of lubricant
templates of component types. process and tested. management and savings at the asset,
n Customize your own or import existing n Review results and software-generated plant and corporate level:
asset structure. observations and recommendations. n Oil analysis results by category
n Assign pre-configured alarm limits n Add additional notes and observations
n Total repair savings
that can be adjusted at the component before sample report is released. n Total oil consumption
level based upon operating history.
n Assess alarm trends to refine alarm
limits.
1 Sample list 2 Test 3 Upload 4 Trivector chart
from TruVu 360 test results from rules engine
Instrument Results
Control Display
TruVu 360 Device Console
Reports
Trend reports are automatically generated including
observations and recommended actions based upon
alarm limit sets employed. Manual review and edits can
be made before report release and automatic distribution.
TruVu 360 report

TruVu 360 trending chart and historical sample data
MiniLab Evolution
5200 MiniLab vs MiniLab 153
The MiniLab Series is the next generation of Trivector on-site oil analyzers replacing the 5200 MiniLab.
5200 MINILAB MINILAB 153

Wear Large Ferrous content, trending only Total ferrous particle content (ppm)
Wear Debris Analysis (WDA) (Optional) Wear Debris Analysis (WDA) (Optional)
Automatic wear particle shape classification, count & distribution
Ferrous particle count & distribution (> 25 µm)
Wear elements: Fe, Cu, Pb, Mg, Ag, Sn
Contamination Particle count & distribution, ISO codes Particle count & distribution, ISO codes
Emulsified water only Dissolved water (ppm)
Free water (ppm)
Glycol contamination for engine oils
Contaminate elements: Si, Na
Chemistry Dynamic viscosity @ room temperature Kinematic viscosity @ 40°C
Dielectric, trending only Oxidation
Total Acid Number (TAN)
Nitration, Sulfation, Anti-wear additive,
Total Base Number (TBN), and soot for engine oils
Additive elements: Ca, P, Zn, Mg, Ba, Mo
Application Typical mineral and synthetic lubricant and hydraulics oils Mineral and synthetic lubricant and hydraulics for industrial rotating
for industrial rotating machinery. machinery, plus engine oil for backup generators and ground fleet,
Not suitable for backup generators. and special lubricants such as phosphate esters and PAG.
Oil library database

The MiniLab Series includes an extensive industrial oil library database to analyze in-service oils as a variety of
lubricants and fluids are used in industrial equipment. The following fluid categories can be tested:
PARTICLE COUNT
FLUIDS ELEMENTAL CHEMISTRY & FERROUS VISCOSITY
Mineral oil based Hydraulic fluids and lubricants Y Y Y Y
Synthetic hydrocarbon based hydraulic fluids and lubricants Y Y Y Y
Ester-based Lubricant blends Y Y Y Y
Oil Soluble Polyglycols (OSP) Y Y Y Y
Organic Esters (OE) Y Y Y Y
Phosphate Esters (Fyrquel/Skydrol) Y Y Y 1
Y
Polyalkylene Glycols (PAG) Y Y Y 1
Y
Poly Alpha Olefins (PAO) Y Y Y Y
Polyinternal Olefins Y Y Y Y
Polyol Esters (POE) Y Y Y Y
Grease Y Y2 N N
Mineral Transformer Oil Y N Y Y
1: Require factory installed Skydrol tube and fitting kits and compatible solvent 2: Oxidation and water (absorbance units) for trending
Typical limits for machinery
Factory libraries of component types, reference oils and alarm limits are provided and additional items can be added by the user.
TruVu 360 limit table grouped by Trivector parameters
Particle analysis and wearing mechanism

With total ppm, ferrous particles, LaserNet total particles and the wear classifier results, users can make informative actionable decisions by
identifying oil drain points, corrosive wear and the onset of a serious abnormal machine wear mechanism.
FERROUS PARTICLES LASERNET LARGE

MONITORING TOTAL Fe PPM >20 µm PARTICLES >20 µm LASERNET CLASSIFIER
Establish constant wear rate Dynamic equilibrium levels Dynamic equilibrium levels Dynamic equilibrium levels
Oil change interval Reaches limit level NA NA NA
Onset of corrossive wear Increase in rate No change No change No change
Transition into abnormal wear mode Increase in rate Increase Increase Increase – cutting/sliding/fatigue
Ongoing severe wear mechanism Same or decrease in rate Increase Increase Increase – cutting /sliding/ fatigue
(breakdown shear mixed layer)
Temporary wear rate change due Increase in rate No change No change No change
to increased load and speed
Onset of external contamination No change No change Increase Increase – non-metallic
3 Body abrasive mechanism iron No change Increase Increase Increase – cutting/sliding
3 Body abrasive mechanism No change No change Increase Increase – cutting/sliding

non-ferrous (copper, aluminum)
Onset of rolling contact failure No change Increase Increase Increase – fatigue
› Wear particle
Elemental Analysis
by metal type
› Contamination The SpectrOil 100 Series analyzes small particulate wear, lubricant additives and
ID by source contaminants for trace quantities of elements dissolved or suspended as fine particles.
› Oil additive Using the proven rotating disc electrode (RDE) technique, the SpectrOil 100 Series has
levels become the workhorse of industrial, commercial and military oil analysis laboratories
requiring rapid analysis of wear metals, contaminants and additives in lubricants.
Coolant, wash-down water and JOAP calibrations are available in addition to in-
service lubricating oil and hydraulic fluid analysis.
n Measures ppm levels of up to 32 elements in less than 30 seconds
n Easy to operate – no sample preparation, gases, coolants or solvents needed
n Compliant with ASTM D6595 for used oil analysis
Grating
On-site oil analysis provides greater
Exit Slits
insight into contaminant sources by
linking elemental parameters with the
probable source:
ELEMENT Oil Chemistry – metallic CCDs
additives possible sources Fixed

Electrode
Sodium Corrosion inhibitor additive, Entrance
also indicates coolant leak into Slit
Optics & diffraction
oil, can also be road salt, sea AC Arc grating produce
SpectrOil 100 Series instrument water, ingested dirt a spectrum
can be purchased separately. Boron Corrosion inhibitor additive, Rotating

Fiber Optic
Cable
Electrode
antiwear/antioxidant additive;
can indicate coolant leak,
Sample
grease contamination Cup
Magnesium Detergent/dispersive additive,

can also be alloying element
in steels SpectrOil 100 Series rotating disc electrode optical
Calcium Detergent/dispersant additive, emission spectrometer schematic
alkaline reserve additive for
high sulfur fueled engines, can
be grease contamination,
Molybdenum Solid/liquid antiwear additive,
alloy in bearing and piston
rings
Barium Corrosion inhibitors,
detergents, rust inhibitors Emission spectrum of hydrogen
Zinc Antiwear, corrosion inhibitors,
anti-oxidants, alloying element
for bearings, thrust washers,
galvanized cases
Emission spectrum of iron
Sample consumed using RDE
Phosphorus Antiwear, corrosion inhibitors,
technology is optically analyzed with anti-oxidants additives, EP
AE spectroscopy to detect elements. additives
Particle Count and Ferrous Monitor
› Ferrous content
The LaserNet 200 Series provides particle counts and codes, large wear particle › Wear particle shape
classification and ferrous wear monitoring. › Particle count
and codes
n Particle count, size distribution and codes (ISO 4406, NAS 1638, NAVAIR 01-1A-17,
SAE AS 4059, GOST, ASTM D6786, HAL, and user defined bins).
n Differentiates contaminants (silica and fibers from machine wear metal)
n Classifies wear particles, stores images, and reports particle count and size
distribution for each wear type of Cutting, Sliding, Fatigue, Fibers and Nonmetallics
n Ferrous Monitor measures total ferrous content in the sample and provides Ferrous
particle count and size distribution

n Widest range up to 5,000,000 particles/ml
n Test oil viscosity up to ISO320 without dilution
n Images through dark fluids containing up to 2% soot
n Error corrections for water and air bubbles
Options include an autosampler for high throughput sample processing as well as

configurations without the ferrous monitor and wear classification.
LaserNet 200 Series instrument can

be purchased separately.
Ferrous Particle
Count & Size FILTER SCREEN
SMALL COIL SET SLIDING WEAR

CUTTING WEAR
CCD CAMERA
640 x 480 resolution
100 frames/s • Particle size distribution
• ISO 4406 cleanliness codes
FLOW • Particle shape classification
CELL
CUTTING
FATIGUE WEAR NONMETALLIC
SLIDING
FATIGUE
x4 Lens Actual Pixel NON METALLIC
Resoluion WATER
LARGE COIL SET

WASTE
Ferrous PPM PUMP
LaserNet 230 flow diagram
› Water Chemical Analysis
› TAN
› TBN The FluidScan® 1000 Series oil chemistry analyzer determines when in-service oil is no
› Oxidation longer fit for use due to oil degradation or the ingress of water or glycol. It is fast and easy to
› Nitration use, with just one drop of oil needed for the sample and less than one minute for test results.
› Sulfation
› Soot The analyzer includes an extensive oil library; additional oils can be added by the user.
› Additive depletion n Compliant to ASTM D7889 “Standard Test Method for Field Determination of In-service
› Glycol
Fluid Properties Using IR Spectroscopy”
n High correlation to TAN and TBN laboratory tests conducted with ASTM D664 and D4739
n Patented, Comprehensive Water Measurement option extends range to 6.5%. (Included
with all MiniLab systems.)
FluidScan 1000 Series handheld

infrared spectrometer can be
purchased separately.
The oil library contains various categories

of fluids. The industrial library provided
with the MiniLab series includes the
Comprehensive Water Solution and the
Industrial Fluid Oil Library.
Industrial
CATEGORY Fluid Library
ASTM EP Gear/Hydro ✔
ASTM Petroleum Crankcase ✔
ASTM Polyol Ester ✔
BIODIESEL FEEDSTOCK
CHILLER ✔
ENGINE ✔ FluidScan operating principle
ENGINE-HEAVY DUTY
ENGINE-HFO
ENGINE-NAT GAS
ETHANOL IN GASOLINE
FAME
FAME in DIESEL
COMPREHENSIVE 6.5%
GEAR-PRESSURE ✔
WATER SOLUTION
GEAR-SPLASH ✔ Dissolved and
HEAT TRANSFER ✔ Free Water Measurement –
Up to 6.5% water
HYDRAULIC ✔
HYDRAULIC-FIRE RESISTANT ✔
SLIDEWAY ✔
STANDARD RANGE
TRANSMISSION 0.03%
Saturation Dissolved Water
Limit Measurement –
TURBINE-AERO ✔ (Oil Specific)
Up to saturation limit
TURBINE-CCGT ✔
TURBINE-STEAM ✔
Water measurement range
Viscosity › Viscosity
The MiniVisc 3000 Series provides fast, accurate 40°C kinematic viscosity measurements for
easy detection of viscosity variations caused by contamination, mix-up and oil degradation.
n Solvent free, portable, and easy to use
n Viscosity range 1-700 cSt @40°C
n Accuracy +/- 3% to NIST viscosity standards
n Fast results: ISO 15 ~10 seconds, ISO 320 ~ 3 minutes
For machinery oils, the 40°C kinematic

viscosity is used as the reference value.
Engine oils operate at higher temperatures
than rotating machinery, so they require
V100°C kinematic viscosity. The Viscosity
Index of an oil is a parameter that relates
the V40°C measurement value to the V100°C
value. A reference Viscosity Index value can
be entered in the viscometer and both the MiniVisc 3000 Series portable viscometer can
measured V40°C viscosity and the calculated be purchased separately.
V100°C viscosity values are displayed.
Positive displacement pipette
Open the two parallel plates for easy cleaning. MiniVisc 3000 Series kinematic viscometer schematic
Total Ferrous
The MiniLab 33 includes the FerroCheck, a portable ferrous analyzer that measures the
total ferrous content of a sample. It is easy to operate; simply insert the sample vial with
fluid sample to measure.
n Small sample requirement with results in 30 seconds
n No sample preparation and no solvents required to clean
n Measurement range 0-10,000 ppm for oil, 10-150,000 ppm for grease
FerroCheck 2000 Series portable ferrous

analyzer can be purchased separately.
Grease boat and sample introduction vials
Four MiniLab Options. Which One is for You?
MiniLab 153 – provides a complete oil analysis report
with elemental analysis, comprehensive wear particle
analysis, solid and water contamination, fluid chemistry
and viscosity. It is ideal for large power plants and
manufacturing plants with many assets.
MiniLab 153 – 4 tests
MiniLab 53 – provides a Trivector report with
comprehensive wear particle analysis, solid and water
contamination, fluid chemistry and viscosity.
MiniLab 33 – provides a basic Trivector report with total
ferrous wear, fluid chemistry, water in oil and viscosity.
MiniLab 23 – provides basic oil condition information
including viscosity, chemistry and water in oil.
PARAMETER Elemental Particle Count Ferrous Viscosity Chemical

and Ferrous
ASTM METHOD D6595 ASTM METHOD D7596 ASTM METHOD D8120 ASTM METHOD D8092 ASTM METHOD D7889
Contamination Particle count and ISO codes ✔

Non-metallic particle count, distribution and images ✔
Sodium and Silicon ✔
Total Water ✔
Chemistry Viscosity ✔
Total Acid Number (TAN) ✔
Oxidation ✔
Total Base Number (TBN), Oxidation, Nitration, and ✔
Sulfation for engine oils
Magnesium, Calcium, Barium, Zinc, Molybdenum, and ✔

Phosphorus
Wear Wear particle images, counts and distribution ✔

Total Ferrous content, ppm ✔ ✔
Ferrous particle count and size distribution ✔
Copper, Silver, Chromium, Titanium, Aluminum, Nickel, ✔
Iron, Manganese, Lead, Tin, Cadmium, and Vanadium
Accessories & Consumables
Sample Preparation Equipment Consumables
Sample preparation equipment such as the Homogenizer, Ultrasonic Deaerator, Electrode Spectro Scientific consumables are
Sharpener and Consumables for 100 samples is included with each MiniLab 153 system. selected and carefully tested with all
Spectro Scientific instruments to ensure
SAMPLE PREPARATION – 3 SIMPLE STEPS consistent, repeatable results. Always use
1. Sharpen electrode Spectro Scientific certified consumables
2. Homogenize the sample for better water for best results.
measurement
3. Ultrasonically degas the sample for
particle analysis
Validation Standards and ASTM Standards

Validation standards are supplied for all MiniLab Series instrumentation. These NIST
traceable standards support internal quality programs and compare current instrument
performance against factory calibration.
All instruments in the MiniLab Series have an associated ASTM Standard Test Method.
• PARTICLE COUNTER STANDARD • FERROUS PARTICLE ANALYZER • FLUIDSCAN IR CHECK FLUID

LNF-509 calibration checkfluid LNF-545 Ferrous Validation FL310 FluidScan CheckFluid
Standard for Magnetometer
• SPECTROMETER STANDARDS – Total Ferrous Content, • VISCOSITY STANDARDS
CS-24 100 ppm, 900ppm, baseoil nominal 100 ppm PV1025 Visc 30 standard
– Large Ferrous particle count, PV1026 Visc120 standard
nominal 42 µm particles
Service Contracts and Repair

Spectro Scientific’s service offerings for the MiniLab Series include:
System Installation & Training for instrument operation and routine maintenance.
Service Contracts for extended warranty and preventive maintenance.
Field Repair by certified customer service engineers on site.
In-house Instrument Calibration, Maintenance, Repair, and Upgrades
performed at our facility near Boston, MA.
MiniLab Series Product Information
PART NUMBER USER INTERFACE SPECIFICATIONS
800-00161 MiniLab 153 with Win 10 Pro Workstation, TruVu 360 Software/Operating Personal computer with Windows 10 Pro or Windows 7 Pro,
Software Suite and one Site User License, 115VAC,60 Hz System 32 or 64 bit, US English version. Quad core microprocessor
800-00162 MiniLab 153 with Win 10 Pro Workstation, TruVu 360 speed 2.6 GHz or higher and 8 GB RAM minimum.
Software Suite and one Site User License, 115VAC,50 Hz POWER REQUIREMENTS
800-00163 MiniLab 153 with Win 10 Pro Workstation, TruVu 360 Power MiniLab 153: 1 Phase power, 1200 W (max)
Software Suite and one Site User License, 220 VAC, 60 Hz MiniLab 53/33/23: 1 Phase power, 110 W (max)
800-00164 MiniLab 153 with Win 10 Pro Workstation, TruVu 360
MECHANICAL SPECIFICATIONS
Software Suite and one Site User License, 220 VAC, 50 Hz
800-00165 MiniLab 53 with TruVu 360 Software Suite Dimensions MiniLab 153: 71 cm x 214 cm x 66 cm (28” x 84” x 26”)
and one Site User License, 115VAC, 50/60 Hz (H x W x D) MiniLab 53: 35 cm x 50 cm x 53 cm (13.8” x 19.7” x 21”)
Minilab 33: 14 cm x 69 cm x 48 cm (5.5 x 27” x 19”)
800-00166 MiniLab 53 with TruVu 360 Software Suite Minilab 23: 10 cm x 51 cm x 48 cm (4” x 20” x 19”)
and one Site User License, 220 VAC, 50/60 Hz
Weight MiniLab 153: 84 kg (185 lbs)
800-00167 MiniLab 33 with TruVu 360 Software Suite MiniLab 53: 14 kg (31 lbs)
and one Site User License, 115VAC, 50/60 Hz MiniLab 33: 9 kg (22 lbs)
800-00168 MiniLab 33 with TruVu 360 Software Suite MiniLab 23: 6 kg (14 lbs)
and one Site User License, 220 VAC, 50/60 Hz
COMPLIANCE
800-00169 MiniLab 23 with TruVu 360 Software Suite
and one Site User License, 115VAC, 50/60 Hz CE Mark-EMC directive, RoHS
800-00170 MiniLab 23 with TruVu 360 Software Suite ANALYTICAL RANGE AND REPEATABILITY
and one Site User License, 220 VAC, 50/60 Hz Output Analytical Range Repeatability
ACCESSORIES AND CONSUMABLES Particle count and size distribution Particle count ≤ 6% RSD
800-00073 MiniLab 153 Standard Accessories Kit ISO codes per 4402/4406, 4-100 µm
800-00032 MiniLab 153 Consumables Kit for 500 samples other codes selectable
800-00072 MiniLab 53 Standard Accessories Kit Ferrous particle count and size 25-100 µm ≤ 5% RSD
distribution
400-00088 MiniLab 53 Consumables Kit for 500 samples
Total Ferrous, ppm 10-2,000 ppm ≤ 5% RSD
800-00063 MiniLab 33 Standard Accessories Kit
Wear particle counts and size 20-100 µm
800-00064 MiniLab 33 Consumables Kit for 500 samples distribution by wear mode : fatique,
800-00039 MiniLab 23 Standard Accessories Kit sliding, cutting,non-metallic, fibers
800-00040 MiniLab 23 Consumables Kit for 500 samples 40°C Kinematic viscosity, cSt 1-320 cSt at 40°C ≤ 3% RSD
600-00123 Minilab 153 Validation Standards Kit 320-700 cSt at 40°C ≤ 5% RSD
600-00122 Minilab 53 Validation Standards Kit Total Acid Number (TAN), mg KOH/g 0-6 mg KOH/g ≤ 3% RSD
600-00120 Minilab 33 Validation Standards Kit Total Base Number (TBN), mg KOH/g 0-70 mg KOH/g ≤ 3% RSD
600-00119 Minilab 23 Validation Standards Kit Oxidation, abs/0.1 mm 5-32 ≤ 3% RSD
FL360 All Libraries License for Fluidscan Nitration, abs/cm 0.5-18 ≤ 3% RSD
800-00171 Windows 10 Pro Workstation, with TruVu 360 Device Sulfation, abs/0.1 mm 16-39 ≤ 3% RSD
Console installed. 115/220 VAC, 50/60 Hz, 150W Water, dissolved ppm 100 ppm-saturation* ≤ 3% RSD
PRODUCT INFORMATION Water, free, ppm 0.03-6.5% (300- ≤ 25% RSD
Applications Mineral and synthetic lubricants including gear, engine, 65,000 ppm)
hydraulic, turbine and distillate fuels Elemental concentration of 23 Elemental analysis range and
Methodology ASTM D7596, ASTM D7889, ASTM 40831 ASTM D6595 elements, ppm repeatability vary with element
Calibration Factory calibrated, field calibration not required. Validation *Oil specific. RSD = Relative Standard Deviation.
and standardization fluids supplied.
SUPPORT RESOURCES
OPERATIONAL SPECIFICATIONS
Support Agreement Global one year support agreement
Environmental 5-40°C ambient temperature, 10-80% RH non-condensing,
Extended Warranty Global 1 year extended warranty, return to depot, part &
Requirements 2000 m maximum altitude
labor only
Sample Volume 30-50 ml, varies with viscosity
EDC303 Online live training, 3 hours
Solvents Lamp oil, odorless kerosene, or Electron 22
Factory PM Factory preventive maintenance & calibration
In Field PM In field (continental US) preventive maintenance & calibration
Spectro Scientific offers On- and Off-site Product Training, Field Repair, In-house
Instrument Calibration, Maintenance, Repair, and Upgrades and Service Contracts.
See previous page for more information about service and customer support.
To learn more about Spectro Scientific products please call 978-431-1120 or visit us online at www.spectrosci.com.
Call/WA: 085799742411 (Fathoni)

Email : fathoniputrawijaya@gmail.com
Email : fathoniputranata@gmail.com
MicroLab
ALL-IN-ONE, AUTOMATED LUBRICANT ANALYSIS SYSTEM
Comprehensive, on-location oil testing
The MicroLab delivers comprehensive on-site oil analysis, providing

MicroLab® Applications
immediate actionable results, saving time and reducing costs.
The MicroLab is used in virtually every
industry that operates equipment Reduce maintenance costs
powered by engines including: Extend component lifetime through preventative maintenance
■ Automotive
Proactively schedule maintenance based on predictive analysis
■ Trucking
Extend oil drain intervals based on oil condition rather than time, allowing savings in
■ Energy
■ Mining
labor, oil and waste disposal
■ Heavy Equipment
Increase equipment availability
■ Government (Military, Municipal)
Early identification and trending of component wear and failure modes for preventative
The two MicroLab models are: maintenance before catastrophic failure occurs
MicroLab 30 – Provides automated Analyzer provides a complete analysis of the oil and equipment health
comprehensive diagnostic analysis LubeTrak® software makes it easy to track and trend the key oil parameters necessary
of engine, generator, gear box, power for optimizing asset health and utilization
steering, and transmission fluids.
Fast and easy to use
MicroLab 40 – Provides automated
Comprehensive oil analysis in 15 minutes instead of waiting days or weeks for outside
comprehensive diagnostic analysis
of engine, generator, gear box,
lab results
hydraulics, power steering, and Minimal disruption to workflow with fully automated measurement, diagnostics and
transmission fluids. Recommended cleaning
if particle count is needed for Can be operated by maintenance or support staff, no chemist required
hydraulics. Easy to interpret results with expert system; recommended maintenance actions and
color coded alarm limits
MicroLab
FULLY AUTOMATED OIL ANALYSIS
The MicroLab combines automation and
artificial intelligence in a simplified oil
analysis tool. The user inputs sample
information on the touchscreen and the
automated fluidics system moves the sample
through the analysis and self-cleaning
processes. The embedded expert system
then provides a complete data analysis with
diagnostics and recommendations.
CHEMISTRY
The MicroLab Infrared Spectrometer measures six key

parameters which indicate potential oil degradation and
contamination.
Both the MicroLab 30 and 40 provide:
Oil degradation: oxidation, nitration, total base number
ELEMENTAL ANALYSIS
Oil contamination: soot, water, glycol
The MicroLab Optical Emission Spectrometer quantifies
wear metals cause from mechanical components, as
VISCOSITY
well as other elements from oil additives or sources of
The MicroLab Dual Temperature Viscometer (DTV) provides contamination.
kinematic viscosity analysis which can help identify MicroLab 40 analyzes 20 elements including wear,
potential oil degradation or contamination. contamination and additives
Both the MicroLab 30 and 40 provide: MicroLab 30 analyzes 10 elements (wear and
Kinematic viscosity at 40C and 100C contamination) and is upgradable to include all
Viscosity Index (VI) 20 elements
Expert System & Reports
The MicroLab has an embedded expert system which translates
all of the analytical data into maintenance actions specific to your
equipment. The artificial intelligence of the system is built from
over 20 years of industry knowledge and more than 10,000 rules
statements to generate the diagnostic statements that are specific
to each application, the type of equipment and the type of oil.
Saves time – compiles and analyzes all test data
Takes the guess work out of interpreting results – provides
suggested maintenance actions
Saves money – no need to hire an analytical resource
Comprehensive MicroLab report includes color-coded alarm limits,

diagnostic statements and trending history.
LubeTrak – Data Management

Online subscription service to track and
trend equipment sample results and
identify maintenance issues across all
sites and assets. All maintenance and
management personnel can access fleet
and equipment information from any web
device around the world.
Synchronized asset oil analysis history
across multiple locations
– Optimized for assets moving from
one location to another
PARTICLE COUNT Centralized asset condition based on
oil analysis results
The MicroLab 40 model is equipped with a particle counter – Corporate asset dashboard
to measure particle contamination which is crucial for – Multiple asset condition displays with one
maintaining hydraulic systems, compressors and turbines. display per site
The MicroLab 40 measures: Streamline communication between headquarters
Gross particle count and remote site operation, maximize the benefit of
ISO particle size oil analysis for the company.
MicroLab Information
PRODUCT INFORMATION USER INTERFACE SPECIFICATIONS
Part Numbers MicroLab 30: 800-00033800-00033 (115VAC) Computer OS Windows 7 32-bit; SQL Server database
800-00034 (220VAC)
Display 15” (diag.) touchscreen
MicroLab 40: 800-00035 (115VAC)
800-00036 (220VAC) Data Entry touchscreen / keyboard / USB port for computer mouse
Accessories UPS backup power supply/surge protector Data Storage (2) 250 GB hard drives (one as unconnected spare
(Included) drive); 4GB USB drive for database backups
Applications OnRoad, OffRoad/Mining, Marine, and Industrial Data Transfer FTP (for online reporting)
Equipment
Security AVG 2015
Operating Mode Single or multi-parameter tests
Communication Network port 25 (Email of reports) ; Port 21 (online
OUTPUT reporting); Remote access software (LogMeIn) for
support/training
Elemental analysis Basic Metals – MicroLab 30 and 40:
(ppm) Aluminum(Al), Chromium(Cr), Copper(Cu), Iron(Fe), POWER REQUIREMENTS
Lead(Pb), Molybdenum(Mo), Potassium(K), Silicon(Si),
Sodium(Na), Tin(Sn) Power 115/230V 50/60 Hz (single-phase) - Spec. by Part
Number (top)
Extended Metals – MicroLab 30 (option), MicroLab 40:
Barium(Ba), Boron(B), Calcium(Ca), Magnesium(Mg), Power Consumption 1100 Watts continuous; 1700 Watts instantaneous max.
Manganese(Mn), Nickel(Ni), Phosphorous(P),
MECHANICAL SPECIFICATIONS
Titanium(Ti), Vanadium(V), Zinc(Zn)
Fluid Chemistry Soot (% by weight), Water (% by weight), Glycol (% Dimensions 29” (L) x 30” (W) x 26” (H) (74cm x 76cm x 66cm)
by weight), Oxidation (Abs./cm), Nitration (Abs./cm), Weight 130 lbs. (59 kg)
TBN (mg KOH/g)
CONSUMABLES
Viscosity Kinematic Viscosity (up to 680 cSt) at 40C and 100C
29002-05-ABS 5 oz. ABS high-temp sample bottle (200)
Particle Count Particle counts > 4um [per mL]
(MicroLab 40) (7 particle size ranges, plus ISO Code) 29033-00 Cleaning Swabs (100)
Methodology Per ASTM D7417 29823-00 Sample Straws (Long) – 350 per pk.
Repeatability Per ASTM D7417 29824-00 Kimwipes (280)
OPERATIONAL SPECIFICATIONS 29088-01 Check Flush fluid (1 Gal)
Sample Volume 1-5 oz. depending on analyses performed 29087-01 Test Standard fluid (32 oz.)
Required
29089-01 Low-Viscosity Standard fluid (32 oz.)
Sample Time Required 5-15 minutes, depending on analyses selected
29090-01 High-Viscosity Standard fluid (32 oz.)
Oil range specs Up to 680 cSt at 40C
Particle counter limited to 320cSt at 40C 22194-00 Filter Screen (1/2”, #60 x 60 mesh)
Calibration Standardization (analyzer metals detection) 23042-00 Upper Electrode

dependent on application – Typically required every 23076-00 Lower Electrode
50 samples (software-changeable)
COMPLIANCE
Ambient Operating 0 to 25 deg. C
Temperature CE Mark / RoHS
Operational Humidity 0-85% non-condensing
Ambient Altitude up to 3000 meters
To keep your MicroLab running in top condition, it is important to use the recommended
cleaning and standardization fluids.
CheckFlush is specially designed to clean the lines in the MicroLab between samples. This prevents
cross-over contamination and keeps your instrument running its best.
The standardization fluids are designed for calibration of the instrument. Your maintenance
practices should follow the prescribed standardization process to ensure your results are accurate.
› TBN
FluidScan 1210 ®
HANDHELD INFRARED BN ANALYZER

Base Number Test for Marine Cylinder Lube Oils
The FluidScan® 1210 provides direct quantitative

Marine engine suppliers recommend
BN measurement of cylinder lube oil for two-stroke
daily monitoring of the Base Number
(BN) to optimize cylinder lubrication engines – in less than a minute.
feed rate and determine the residual
Reduce lubrication oil costs
BN of the piston underside oil.
Recent changes in vessel operation Optimize feed rate to the cylinders, eliminating wasteful
are driving innovation in engine over-lubrication.
monitoring including: Allows ship engineers to quickly comply with manufacturer
■ Shift to “slow steaming” and the recommendations for BN in new and residual cylinder oils.
resulting “cold corrosion” affecting Increase component lifetime
every vessel in operation.
Reduce “cold corrosion” due to the effects of slow steaming.
■ Increases in early failure due to
Reduce cylinder scuffing due to insufficient lubrication.
cylinder scuffing & scaling from
Prevent scaling which results from over-lubrication.
improper lubrication in constantly
changing conditions. The FluidScan brings innovation to ship-board BN tests
■ New sulfur emissions requirements
Fast and easy to use…needs just one drop of oil and one
impacting some vessels. Running minute to test, plus color-coded alarm limits for easy results
with multiple fuel types means
interpretation. Cylinder oil and inlet oil BN
major changes in lubrication BN to measurement
Reduced testing costs…fewer consumables and solvent-free.
compensate for high fluctuations in
Eliminates need for hazardous chemicals onboard.
acidic conditions in the cylinders.
More accurate…avoids the operator error of traditional
According to Wärtsilä Services
onboard tests and correlates with lab methods (ASTM D2896).
Technical Bulletin RT-161, daily
control of the cylinder oil BN is
the most effective way to prevent
“cold corrosion.” The FluidScan 1210 1210 BN Analyzer vs Onshore Lab
meets this challenge with a handheld 120
R² = 0.9461
BN analyzer. 100
1210 BN mg KOH/g)
80
60
40
20
0
5 15 25 35 45 55 65 75 85 95
BN by Laboratory Titration, mg KOH/g (ASTM D2896)
Correlation of 1210 BN analyzer to laboratory titration

FluidScan 1210 Ordering Information
The FluidScan® 1210 includes the FluidScan device, battery The FluidScan 1210
charger, USB cable, USB flash drive, and the Fluid Manager Suite, enables ship managers
to keep optimal residual
which contains the Fluid Manager desktop application, user
BN values to avoid cold
manuals, and a backup copy of the FluidScan device software. corrosion and scuffing
The FluidScan standard accessories kit includes cleaning pads without wasting cylinder
and pipettes for 100 samples and the IR check fluid. oil to over lubrication.
PART NUMBER MECHANICAL SPECIFICATIONS

FluidScan-Q1210 1210 marine cylinder lubrication oil BN analyzer. Dimensions 240 mm (H) x 140 mm (W) x 70 mm (D)
Requires SA1001 accessory kit. (9.5 in x 5.5 in x 2.75 in)
SA1001 FluidScan standard accessory kit Weight 1.4 kg (3 lbs)
PRODUCT INFORMATION Shipping package 17.1 cm (H) x 6.3 cm (W) x 5.5 cm (L);
dimensions (18 in x 16 in x 14 in)
Application Marine cylinder oil (MCL) BN (Base Number)
Shipping package 8.1 kg, (18 lbs)
Unit mg KOH/g
weight
Methodology ASTM D7889, ASTM E1655
COMPLIANCE
Range 5-100 BN
CE Mark: EMC Directive (2004/108/EC); RoHS
Accuracy ± 5% of measured value, typical
ACCESSORIES & CONSUMABLES
Repeatability ± 5% of measured value, typical
FL310 IR Check Fluid 5 mL
Calibration Factory calibrated to wet chemistry methods ASTM
D2896 for TBN. Use Check Fluid for instrument PV1011 Disposable non-abrasive cleaning pads;
validation. package of 500
OPERATIONAL SPECIFICATIONS P-11052 60 µL disposable pipettes, package of 500
Sample Volume 100 μL (about 1 drop) PV1012 60 µL disposable pipettes & non-abrasive cleaning
pad kit; pkg. of 100 each
Solvents/Reagents None
Ambient Operating 10°C to 50°C (14°F to 122°F) Note: System includes data logging on device and export capability to
Temperature spreadsheet. System is upgradeable with additional lubricant library and
Relative Humidity 0 to 100%, non-condensing parameters for other shipboard equipment.
Ambient Altitude up to 5,000 meters (16,404 feet)

USER INTERFACE SPECFICATIONS
Software/Operating Device: Microsoft Windows CE
System PC System: Windows 7 Pro, 32/64 bit, English US
version (for Fluid Manager software)
Display 320 x 320 transflective color screen
Data Storage Up to 5,000 analyses
Data Transfer USB for data updates and synchronization
Data Entry Directional pad and soft buttons
POWER REQUIREMENTS
Battery Power Source Built in rechargeable lithium ion battery
Power AC 110/240 V, 50/60 Hz, 10 Watts
Typical Runtime 6-8 hours
Recharge Time 6.5 hours
FluidScan 1210 and FerroCheck 2000
combination kit provides BN and total ferrous
content for marine engine oil analysis.


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Solutions for Power Generation and Industrial Plants

the increasing severity

n Extend equipment life

n Decrease total lifecycle equipment costs

n Provide immediate retest capability

Trivector™ – oil and machine health simplified

 Is the machine healthy?

 Is the oil dry?

 Is it the right oil?

*Trivector is a trademark of Emerson Process Systems Industrial Solutions | 3

TruVu 360 Enterprise cloud software

ASSET & TOOL BAR SAMPLE ANALYSIS PROCESS DASHBOARD

TruVu 360 Device Console

TruVu 360 report

5200 MINILAB MINILAB 153

Oil library database

TruVu 360 limit table grouped by Trivector parameters

Particle analysis and wearing mechanism

FERROUS PARTICLES LASERNET LARGE

3 Body abrasive mechanism No change No change Increase Increase – cutting/sliding

ELEMENT Oil Chemistry – metallic CCDs

additives possible sources Fixed

can be purchased separately. Boron Corrosion inhibitor additive, Rotating

Magnesium Detergent/dispersive additive,

particle count and size distribution

n Test oil viscosity up to ISO320 without dilution

n Images through dark fluids containing up to 2% soot

n Error corrections for water and air bubbles

Options include an autosampler for high throughput sample processing as well as

LaserNet 200 Series instrument can

SMALL COIL SET SLIDING WEAR

LARGE COIL SET

n Patented, Comprehensive Water Measurement option extends range to 6.5%. (Included

with all MiniLab systems.)

FluidScan 1000 Series handheld

The oil library contains various categories

n Fast results: ISO 15 ~10 seconds, ISO 320 ~ 3 minutes

For machinery oils, the 40°C kinematic

FerroCheck 2000 Series portable ferrous

Grease boat and sample introduction vials

PARAMETER Elemental Particle Count Ferrous Viscosity Chemical

Contamination Particle count and ISO codes ✔

Magnesium, Calcium, Barium, Zinc, Molybdenum, and ✔

Wear Wear particle images, counts and distribution ✔

Validation Standards and ASTM Standards

• PARTICLE COUNTER STANDARD • FERROUS PARTICLE ANALYZER • FLUIDSCAN IR CHECK FLUID

Service Contracts and Repair

Call/WA: 085799742411 (Fathoni)

The MicroLab delivers comprehensive on-site oil analysis, providing

The MicroLab combines automation and

artificial intelligence in a simplified oil

analysis tool. The user inputs sample

information on the touchscreen and the

automated fluidics system moves the sample

through the analysis and self-cleaning

processes. The embedded expert system

then provides a complete data analysis with

diagnostics and recommendations.

The MicroLab Infrared Spectrometer measures six key

Comprehensive MicroLab report includes color-coded alarm limits,

LubeTrak – Data Management

Calibration Standardization (analyzer metals detection) 23042-00 Upper Electrode

HANDHELD INFRARED BN ANALYZER