Checked by: John D. Roberts and Stanley L.

Manatt
Published in Org. Synth. 1959, 39, 1
Org. Synth. 1963, Coll. Vol. 4, 6
ABIETIC ACID

Submitted by: G. C. Harris and T. F. Sanderson

Checked by: R. T. Arnold and K. L. Lindsay
Published in Org. Synth. 1952, 32, 1
Org. Synth. 1963, Coll. Vol. 4, 1

9-ACETYLANTHRACENE

Submitted by: Charles Merritt, Jr and Charles E.

Braun
Checked by: William S. Johnson and Ralph F.
Hirschmann
Published in Org. Synth. 1950, 30, 1
Org. Synth. 1963, Coll. Vol. 4, 8

3-ACETAMIDO-2-BUTANONE

Submitted by: Richard H. Wiley and O. H. Borum

Checked by: R. S. Schreiber and B. D. Aspergren
Published in Org. Synth. 1953, 33, 1
Org. Synth. 1963, Coll. Vol. 4, 5
α-ACETYL-δ-CHLORO-γ-
VALEROLACTONE
Submitted by: G. D. Zuidema, Eugene E. van
Tamelen, and G. Van Zyl
Checked by: William S. Johnson and Herbert I.
Hadler
Published in Org. Synth. 1951, 31, 1
Org. Synth. 1963, Coll. Vol. 4, 10

N-(p-
ACETYLAMINOPHENYL)RHODANINE

Submitted by: R. E. Strube

1|Page
 1-ACETYLCYCLOHEXANOL

Submitted by: Gardner W. Stacy and Richard A.

Mikulec
Checked by: John C. Sheehan, George A.
Mortimer, and Norman A. Nelson
Published in Org. Synth. 1955, 35, 1
Org. Synth. 1963, Coll. Vol. 4, 13

δ-ACETYL-n-VALERIC ACID

Submitted by: J. R. Schaeffer and A. O. Snoddy

Checked by: Richard T. Arnold and H. W. Turner
Published in Org. Synth. 1951, 31, 3
2-p-ACETYLPHENYLHYDROQUINONE Org. Synth. 1963, Coll. Vol. 4, 19

Submitted by: George A. Reynolds and J. A.

VanAllan
Checked by: R. S. Schreiber and A. H. Nathan
Published in Org. Synth. 1954, 34, 1
Org. Synth. 1963, Coll. Vol. 4, 15

ACROLEIN ACETAL

Submitted by: J. A. VanAllan

Checked by: T. L. Cairns and R. E. Benson
Published in Org. Synth. 1952, 32, 5
Org. Synth. 1963, Coll. Vol. 4, 21

2|Page
 Michelotti
Checked by: B. C. McKusick and F. W. Stacey
Published in Org. Synth. 1958, 38, 1
Org. Synth. 1963, Coll. Vol. 4, 29

ALLOXAN MONOHYDRATE

Submitted by: A. V. Holmgren and Wilhelm

Wenner
Checked by: T. L. Cairns and R. W. Upson
Published in Org. Synth. 1952, 32, 6
Org. Synth. 1963, Coll. Vol. 4, 23

p-AMINOBENZALDEHYDE

Submitted by: E. Campaigne, W. M. Budde, and

G. F. Schaefer
Checked by: Cliff S. Hamilton and R. C. Rupert
Published in Org. Synth. 1951, 31, 6
Org. Synth. 1963, Coll. Vol. 4, 31

ALLOXANTIN DIHYDRATE

Submitted by: R. Stuart Tipson

Checked by: T. L. Cairns and F. S. Fawcett
Published in Org. Synth. 1953, 33, 3
Org. Synth. 1963, Coll. Vol. 4, 25

2-AMINOBENZOPHENONE

Submitted by: H. J. Scheifele, Jr and D. F. DeTar

Checked by: R. T. Arnold and John D. Jones
Published in Org. Synth. 1952, 32, 8
Org. Synth. 1963, Coll. Vol. 4, 34

2-AMINO-4-ANILINO-6-
(CHLOROMETHYL)-s-TRIAZINE

Submitted by: C. G. Overberger and Francis W.

3|Page
 2-AMINO-3-NITROTOLUENE

Submitted by: John C. Howard

Checked by: Charles C. Price and Joseph D.
Berman
Published in Org. Synth. 1955, 35, 3
Org. Synth. 1963, Coll. Vol. 4, 42

ε-AMINOCAPROIC ACID

Submitted by: Cal Y. Meyers and Leonard E.

Miller
Checked by: Richard T. Arnold and William R.
Hasek
Published in Org. Synth. 1952, 32, 13 3-AMINOPYRIDINE
Org. Synth. 1963, Coll. Vol. 4, 39
Submitted by: C. F. H. Allen and Calvin N. Wolf
4|Page
Checked by: Cliff S. Hamilton and Marjorie
Debrunner
Published in Org. Synth. 1950, 30, 3
Org. Synth. 1963, Coll. Vol. 4, 45

ARYLUREAS
II. UREA METHOD
p-ETHOXYPHENYLUREA

Submitted by:
Checked by:
Published in Org. Synth. 1951, 31, 11
p-AMINOTETRAPHENYLMETHANE Org. Synth. 1963, Coll. Vol. 4, 52

Submitted by: Benjamin Witten and E. Emmet

Reid
Checked by: Richard T. Arnold and Jerome J.
Rosenbaum
Published in Org. Synth. 1950, 30, 5
Org. Synth. 1963, Coll. Vol. 4, 47

DL-ASPARTIC ACID

Submitted by: M. S. Dunn and B. W. Smart

Checked by: H. T. Clarke and W. Pearlman
Published in Org. Synth. 1950, 30, 7
Org. Synth. 1963, Coll. Vol. 4, 55

ARYLUREAS
I. CYANATE METHOD
p-BROMOPHENYLUREA

Submitted by: Frederick Kurzer

Checked by: Richard T. Arnold and Lester C.
Krogh
Published in Org. Synth. 1951, 31, 8
Org. Synth. 1963, Coll. Vol. 4, 49

ATROLACTIC ACID

5|Page
Submitted by: Ernest L. Eliel and Jeremiah P. Published in Org. Synth. 1952, 32, 16
Freeman Org. Synth. 1963, Coll. Vol. 4, 66
Checked by: Arthur C. Cope, William F. Gorham,
and Roscoe A. Pike
Published in Org. Synth. 1953, 33, 7
Org. Synth. 1963, Coll. Vol. 4, 58

BENZENEBORONIC ANHYDRIDE

Submitted by: Robert M. Washburn, Ernest

Levens, Charles F. Albright, and Franklin A. Billig

Checked by: B. C. McKusick and H. C. Miller

Published in Org. Synth. 1959, 39, 3
Org. Synth. 1963, Coll. Vol. 4, 68

AZELANITRILE

Submitted by: Arthur C. Cope, Robert J. Cotter,

and Leland L. Estes
Checked by: N. J. Leonard and R. W. Fulmer
Published in Org. Synth. 1954, 34, 4
Org. Synth. 1963, Coll. Vol. 4, 62
BENZHYDRYL β-CHLOROETHYL ETHER
Submitted by: Shigehiko Sugasawa and Kunio
Fujiwara
Checked by: N. J. Leonard, P. D. Thomas, and L.
A. Miller
Published in Org. Synth. 1953, 33, 11
Org. Synth. 1963, Coll. Vol. 4, 72

1,1'-AZO-bis-1-CYCLOHEXANENITRILE

Submitted by: C. G. Overberger, Pao-tung Huang,

and M. B. Berenbaum
Checked by: N. J. Leonard and E. H. Mottus

6|Page

BENZOFURAZAN OXIDE
Submitted by: F. B. Mallory, P. A. S. Smith, and J.
H. Boyer
Checked by: T. L. Cairns, H. E. Simmons, Arthur
C. Cope, David J. Marshall, and Douglas S. Smith
Published in Org. Synth. 1957, 37, 1
Org. Synth. 1963, Coll. Vol. 4, 74
BENZOYLCHOLINE IODIDE AND
CHLORIDE
Submitted by: A. H. Ford-Moore
Checked by: R. L. Shriner and Calvin N. Wolf
Published in Org. Synth. 1950, 30, 10
Org. Synth. 1963, Coll. Vol. 4, 84

BENZOGUANAMINE

Submitted by: J. K. Simons and M. R. Saxton

Checked by: T. L. Cairns and A. K. Schneider
Published in Org. Synth. 1953, 33, 13
Org. Synth. 1963, Coll. Vol. 4, 78

3-BENZOYLPYRIDINE

Submitted by: Frank J. Villani and Mary S. King

Checked by: Max Tishler and Matthew A.
Kozlowski
Published in Org. Synth. 1957, 37, 6
Org. Synth. 1963, Coll. Vol. 4, 88

BENZOYLACETANILIDE

Submitted by: C. F. H. Allen and W. J. Humphlett

Checked by: Max Tishler and R. Connell
Published in Org. Synth. 1957, 37, 2
Org. Synth. 1963, Coll. Vol. 4, 80

7|Page

2-BENZYLAMINOPYRIDINE
Submitted by: Yaïr Sprinzak
Checked by: Max Tishler and Matthew A.
Kozlowski
Published in Org. Synth. 1958, 38, 3
Org. Synth. 1963, Coll. Vol. 4, 91
3-BENZYL-3-METHYLPENTANOIC ACID
Submitted by: F. S. Prout, R. J. Hartman, E. P.-Y.
Huang, C. J. Korpics, and G. R. Tichelaar
Checked by: James Cason, K. C. Dewhirst, E. J.
Gauglitz, Jr, and William G. Dauben
Published in Org. Synth. 1955, 35, 6
Org. Synth. 1963, Coll. Vol. 4, 93
BENZYLTRIMETHYLAMMONIUM
ETHOXIDE
Submitted by: W. J. Croxall, Marion F. Fegley,
and H. J. Schneider
Checked by: John C. Sheehan and M. Gertrude
Howell
Published in Org. Synth. 1958, 38, 5
Org. Synth. 1963, Coll. Vol. 4, 98
BISCHLOROMETHYL ETHER
Submitted by: Saul R. Buc
Checked by: Charles C. Price, Frederick V.
Brutcher, and Jerome Cohen
Published in Org. Synth. 1956, 36, 1
Org. Synth. 1963, Coll. Vol. 4, 101
N-BROMOACETAMIDE
Submitted by: Eugene P. Oliveto and Corinne
Gerold
Checked by: Richard T. Arnold and Carl G.
Krespan
Published in Org. Synth. 1951, 31, 17
Org. Synth. 1963, Coll. Vol. 4, 104
8|Page
 β-BROMOETHYLPHTHALIMIDE

Submitted by: T. O. Soine and M. R. Buchdahl

Checked by: Cliff S. Hamilton and John D.
Sculley
Published in Org. Synth. 1952, 32, 18
Org. Synth. 1963, Coll. Vol. 4, 106

2-BROMO-3-METHYLBENZOIC ACID

Submitted by: J. F. Bunnett and M. M. Rauhut

Checked by: John D. Roberts and Marc S. Silver
Published in Org. Synth. 1958, 38, 11
Org. Synth. 1963, Coll. Vol. 4, 114

4-BROMO-2-HEPTENE

Submitted by: F. L. Greenwood, M. D. Kellert,

and J. Sedlak
Checked by: John D. Roberts and A. T. Bottini
Published in Org. Synth. 1958, 38, 8
Org. Synth. 1963, Coll. Vol. 4, 108

n-BUTYLACETYLENE

Submitted by: Kenneth N. Campbell and Barbara

K. Campbell
Checked by: R. S. Schreiber, M. F. Murray, and A.
C. Ott
p-BROMOMANDELIC ACID
Published in Org. Synth. 1950, 30, 15
Org. Synth. 1963, Coll. Vol. 4, 117
Submitted by: J. J. Klingenberg
Checked by: R. T. Arnold and C. D. Wright
Published in Org. Synth. 1955, 35, 11
Org. Synth. 1963, Coll. Vol. 4, 110

9|Page
 sec-BUTYL α-n-CAPROYLPROPIONATE 2-BUTYN-1-OL

Submitted by: Kenneth L. Rinehart Submitted by: P. J. Ashworth, G. H. Mansfield,

Checked by: John C. Sheehan and J. Iannicelli
Published in Org. Synth. 1955, 35, 15
Org. Synth. 1963, Coll. Vol. 4, 120
and M. C. Whiting
Checked by: John C. Sheehan, George Buchi, and
Walfred S. Saari
Published in Org. Synth. 1955, 35, 20
Org. Synth. 1963, Coll. Vol. 4, 128

BUTYRCHLORAL
n-BUTYL GLYOXYLATE
Submitted by: Gus A. Ropp, W. E. Craig, and
Submitted by: Frank J. Wolf and John Weijlard
Vernon Raaen
Checked by: N. J. Leonard and L. A. Miller
Checked by: T. L. Cairns and H. N. Cripps
Published in Org. Synth. 1955, 35, 18
Published in Org. Synth. 1953, 33, 15
Org. Synth. 1963, Coll. Vol. 4, 124
Org. Synth. 1963, Coll. Vol. 4, 130

tert-BUTYL HYPOCHLORITE

Submitted by: H. M. Teeter and E. W. Bell

Checked by: Charles C. Price and T. C. Schwann
Published in Org. Synth. 1952, 32, 20
Org. Synth. 1963, Coll. Vol. 4, 125

10 | P a g e
 β-CARBETHOXY-γ,γ- Org. Synth. 1963, Coll. Vol. 4, 141
DIPHENYLVINYLACETIC ACID

Submitted by: William S. Johnson and William P.

Schneider
Checked by: Arthur C. Cope and Malcolm
Chamberlain
Published in Org. Synth. 1950, 30, 18
Org. Synth. 1963, Coll. Vol. 4, 132

CHLOROACETONITRILE

Submitted by: D. B. Reisner and E. C. Horning

Checked by: R. L. Shriner and Calvin N. Wolf
Published in Org. Synth. 1950, 30, 22
Org. Synth. 1963, Coll. Vol. 4, 144

β-(o-CARBOXYPHENYL)PROPIONIC ACID

Submitted by: G. A. Page and D. S. Tarbell

Checked by: William S. Johnson, Shirley
Rosenberg, and Robert D. Eberhardt
Published in Org. Synth. 1954, 34, 8
Org. Synth. 1963, Coll. Vol. 4, 136
3-(o-CHLOROANILINO)PROPIONITRILE
Submitted by: S. A. Heininger
Checked by: John C. Sheehan and Alma M.
Boston
Published in Org. Synth. 1958, 38, 14
Org. Synth. 1963, Coll. Vol. 4, 146

CETYLMALONIC ESTER
Submitted by: Don E. Floyd and Sidney E. Miller
Checked by: James Cason and George A. Gillies
Published in Org. Synth. 1954, 34, 13
CHLORO-p-BENZOQUINONE
Submitted by: R. E. Harman
Checked by: N. J. Leonard and R. W. Fulmer
Published in Org. Synth. 1955, 35, 22
11 | P a g e
Org. Synth. 1963, Coll. Vol. 4, 148

1-CHLORO-2,6-DINITROBENZENE

Submitted by: F. D. Gunstone and S. Horwood

Tucker
Checked by: Arthur C. Cope, David J. Marshall,
and Ronald M. Pike
Published in Org. Synth. 1952, 32, 23
N-CHLOROBETAINYL CHLORIDE
Org. Synth. 1963, Coll. Vol. 4, 160
Submitted by: B. Vassel and W. G. Skelly
Checked by: John C. Sheehan and J. Iannicelli
Published in Org. Synth. 1955, 35, 28
Org. Synth. 1963, Coll. Vol. 4, 154

trans-2-CHLOROCYCLOPENTANOL

Submitted by: Hugh B. Donahoe and Calvin A.

Vanderwerf
Checked by: Arthur C. Cope and Elbert C. Herrick
Published in Org. Synth. 1950, 30, 24
Org. Synth. 1963, Coll. Vol. 4, 157 2-CHLORO-2-METHYLCYCLOHEXANONE
and 2-METHYL-2-CYCLOHEXENONE

Submitted by: E. W. Warnhoff, D. G. Martin, and

William S. Johnson
Checked by: M. S. Newman, G. R. Kahle, and D.
E. Reid
Published in Org. Synth. 1957, 37, 8
12 | P a g e
Org. Synth. 1963, Coll. Vol. 4, 162

o-CHLOROPHENYLCYANAMIDE

2-CHLORONICOTINONITRILE Submitted by: Frederick Kurzer

Checked by: Cliff S. Hamilton and David B.
Submitted by: E. C. Taylor, Jr and Aldo J. Crovetti Capps
Published in Org. Synth. 1951, 31, 19
Checked by: Charles C. Price and Walter A. Org. Synth. 1963, Coll. Vol. 4, 172
Schroeder
Published in Org. Synth. 1957, 37, 12
Org. Synth. 1963, Coll. Vol. 4, 166

α-(4-CHLOROPHENYL)-γ-
PHENYLACETOACETONITRILE

Submitted by: Stephen B. Coan and Ernest I.

Becker
Checked by: Charles C. Price and G. Venkat Rao
α-CHLOROPHENYLACETIC ACID Published in Org. Synth. 1955, 35, 30
Org. Synth. 1963, Coll. Vol. 4, 174
Submitted by: Ernest L. Eliel, Milton T. Fisk, and
Thomas Prosser
Checked by: James Cason, Lois J. Durham, and
Gerhard J. Fonken
Published in Org. Synth. 1956, 36, 3
Org. Synth. 1963, Coll. Vol. 4, 169

13 | P a g e

1-(p-CHLOROPHENYL)-3-PHENYL-2-
PROPANONE
Submitted by: Stephen B. Coan and Ernest I.
Becker
Checked by: Charles C. Price and G. Venkat Rao
Published in Org. Synth. 1955, 35, 32
Org. Synth. 1963, Coll. Vol. 4, 176
p-CHLOROPHENYL SALICYLATE
Submitted by: Norman G. Gaylord and P. M.
Kamath
Checked by: R. T. Arnold and J. John Brezinski
Published in Org. Synth. 1952, 32, 25
Org. Synth. 1963, Coll. Vol. 4, 178
o-CHLOROPHENYLTHIOUREA
Submitted by: Frederick Kurzer
Checked by: Cliff S. Hamilton and David B.
Capps
Org. Synth. 1963, Coll. Vol. 4, 180
2-CHLOROPYRIMIDINE
Submitted by: Irving C. Kogon, Ronald Minin, and
C. G. Overberger
Checked by: Charles C. Price and T. L. V. Ulbricht
Published in Org. Synth. 1955, 35, 34
Org. Synth. 1963, Coll. Vol. 4, 182
2-CHLORO-1,1,2-TRIFLUOROETHYL
ETHYL ETHER
Submitted by: Bruce Englund
Checked by: R. S. Schreiber and Burris D. Tiffany
Published in Org. Synth. 1954, 34, 16
Org. Synth. 1963, Coll. Vol. 4, 184
β-CHLOROVINYL ISOAMYL KETONE
14 | P a g e
Submitted by: Charles C. Price and Joseph A.
Pappalardo
Checked by: R. S. Schreiber, Wm. Bradley Reid,
Jr, and R. W. Jackson
Published in Org. Synth. 1952, 32, 27
Org. Synth. 1963, Coll. Vol. 4, 186
CHOLESTEROL, Δ5-CHOLESTEN-3-ONE,
AND Δ4-CHOLESTEN-3-ONE
Submitted by: Louis F. Fieser
Checked by: William S. Johnson and David G.
Martin
Published in Org. Synth. 1955, 35, 43
Org. Synth. 1963, Coll. Vol. 4, 195

Δ4-CHOLESTEN-3,6-DIONE

Submitted by: Louis F. Fieser

Checked by: William S. Johnson and David G.
Martin
Published in Org. Synth. 1955, 35, 36
Org. Synth. 1963, Coll. Vol. 4, 189

Δ4-CHOLESTEN-3-ONE

Submitted by: Jerome F. Eastham and Roy

Teranishi
Checked by: James Cason, James Jiu, and Elmer J.
Reist
Published in Org. Synth. 1955, 35, 39
Org. Synth. 1963, Coll. Vol. 4, 192

COUMALIC ACID

15 | P a g e
Submitted by: Richard H. Wiley and Newton R. Published in Org. Synth. 1952, 32, 29
Smith Org. Synth. 1963, Coll. Vol. 4, 207
Checked by: C. F. H. Allen and George A.
Reynolds
Published in Org. Synth. 1951, 31, 23
Org. Synth. 1963, Coll. Vol. 4, 201

3-CYANO-6-METHYL-2(1)-PYRIDONE

Submitted by: Raymond P. Mariella

Checked by: Arthur C. Cope, James E. Krueger,
and David J. Marshall
Published in Org. Synth. 1952, 32, 32
CREOSOL Org. Synth. 1963, Coll. Vol. 4, 210
Submitted by: R. Schwarz and H. Hering
Checked by: R. L. Shriner and C. L. Furrow, Jr
Published in Org. Synth. 1953, 33, 17
Org. Synth. 1963, Coll. Vol. 4, 203

N-2-CYANOETHYLANILINE
Submitted by: J. Cymerman-Craig and M. Moyle
Checked by: William S. Johnson and Duff S.
Allen, Jr
Published in Org. Synth. 1956, 36, 6
Org. Synth. 1963, Coll. Vol. 4, 205
1-CYANO-3-PHENYLUREA
Submitted by: Frederick Kurzer and J. Roy Powell
Checked by: John C. Sheehan and Ernest R.
Gilmont
Published in Org. Synth. 1956, 36, 8
Org. Synth. 1963, Coll. Vol. 4, 213

CYANOGEN IODIDE

Submitted by: B. Bak and A. Hillebert

Checked by: R. T. Arnold and H. E. Fritz
16 | P a g e
Top of Form

1,2-CYCLODECANEDIOL

Submitted by: A. T. Blomquist and Albert

Goldstein
Checked by: N. J. Leonard and F. H. Owens
Published in Org. Synth. 1956, 36, 12
Org. Synth. 1963, Coll. Vol. 4, 216

1,2-CYCLOHEXANEDIONE DIOXIME

Submitted by: Clifford C. Hach, Charles V. Banks,

and Harvey Diehl
Checked by: R. T. Arnold and Philip N. Gordon
Published in Org. Synth. 1952, 32, 35
CYCLODECANONE Org. Synth. 1963, Coll. Vol. 4, 229

Submitted by: Arthur C. Cope, John W. Barthel,

and Ronald Dean Smith
Checked by: N. J. Leonard and J. C. Little
Published in Org. Synth. 1956, 36, 14
Org. Synth. 1963, Coll. Vol. 4, 218

CYCLOHEPTANONE

Submitted by: Hyp J. Dauben, Jr, Howard J.

Ringold, Robert H. Wade, David L. Pearson,
Arthur G. Anderson, Jr, Th. J. de Boer, and H. J.
Backer
Checked by: Arthur C. Cope, Warren N. Baxter,
Robert J. Cotter, James Cason, John B. Rogan, and
Wm. G. Dauben
Published in Org. Synth. 1954, 34, 19
Org. Synth. 1963, Coll. Vol. 4, 221
CYCLOHEXENE SULFIDE
Submitted by: Eugene E. van Tamelen
Checked by: Charles C. Price and Paul F. Kirk
Published in Org. Synth. 1952, 32, 39
Org. Synth. 1963, Coll. Vol. 4, 232
17 | P a g e
 CYCLOHEXYLIDENECYANOACETIC
ACID AND 1-
CYCLOHEXENYLACETONITRILE DIACETYL-d-TARTARIC ANHYDRIDE
Submitted by: Arthur C. Cope, Alfred A. Submitted by: R. L. Shriner and C. L. Furrow, Jr
D'Addieco, Donald Edward Whyte, and Samuel A. Checked by: N. J. Leonard and R. R. Sauers
Glickman Published in Org. Synth. 1955, 35, 49
Checked by: T. L. Cairns and R. E. Heckert Org. Synth. 1963, Coll. Vol. 4, 242
Published in Org. Synth. 1951, 31, 25
Org. Synth. 1963, Coll. Vol. 4, 234

2,5-DIAMINO-3,4-DICYANOTHIOPHENE

Submitted by: W. J. Middleton

Checked by: James Cason and Ralph J. Fessenden
Published in Org. Synth. 1959, 39, 8
Org. Synth. 1963, Coll. Vol. 4, 243

CYCLOPENTADIENE AND 3-
CHLOROCYCLOPENTENE

Submitted by: Robert Bruce Moffett

Checked by: R. T. Arnold and George P. Scott
Published in Org. Synth. 1952, 32, 41
Org. Synth. 1963, Coll. Vol. 4, 238
2,4-DIAMINO-6-HYDROXYPYRIMIDINE

Submitted by: J. A. VanAllan

Checked by: Cliff S. Hamilton and John D.
Sculley
18 | P a g e
Published in Org. Synth. 1952, 32, 45
Org. Synth. 1963, Coll. Vol. 4, 245
DIAMINOURACIL HYDROCHLORIDE
Submitted by: Wm. R. Sherman and E. C. Taylor,
Jr
Checked by: T. L. Cairns and D. S. Acker
Published in Org. Synth. 1957, 37, 15
Org. Synth. 1963, Coll. Vol. 4, 247
DIAZOMETHANE
Submitted by: Th. J. de Boer and H. J. Backer
Checked by: James Cason, Max J. Kalm, and R. F.
Porter
Published in Org. Synth. 1956, 36, 16
Org. Synth. 1963, Coll. Vol. 4, 250
DIBROMOACETONITRILE
Submitted by: James W. Wilt and James L.
Diebold
Checked by: B. C. McKusick and H. E.
Knipmeyer
Published in Org. Synth. 1958, 38, 16
Org. Synth. 1963, Coll. Vol. 4, 254
4,4'-DIBROMOBIPHENYL
Submitted by: Robert E. Buckles and Norris G.
Wheeler
Checked by: R. S. Schreiber, Wm. Bradley Reid,
Jr, and Robert W. Jackson
Published in Org. Synth. 1951, 31, 29
Org. Synth. 1963, Coll. Vol. 4, 256
DI-n-BUTYLDIVINYLTIN
Submitted by: Dietmar Seyferth
Checked by: Melvin S. Newman and S.
Ramachandran
Published in Org. Synth. 1959, 39, 10
Org. Synth. 1963, Coll. Vol. 4, 258
19 | P a g e

DI-tert-BUTYL MALONATE
Submitted by: Allen L. McCloskey, Gunther S.
Fonken, Rudolph W. Kluiber, William S. Johnson,
and Chittaranjan Raha
Checked by: James Cason, Gerhard J. Fonken,
William G. Dauben, William S. Johnson, and
Rudolph W. Kluiber
Published in Org. Synth. 1954, 34, 26
Org. Synth. 1963, Coll. Vol. 4, 261
4,4'-DICHLORODIBUTYL ETHER
Submitted by: Kliem Alexander and H. V. Towles
Checked by: Arthur C. Cope, Malcolm
Chamberlain, and Mark R. Kinter
Published in Org. Synth. 1950, 30, 27
Org. Synth. 1963, Coll. Vol. 4, 266
1,1-DICHLORO-2,2-DIFLUOROETHYLENE
Submitted by: J. C. Sauer
Checked by: Charles C. Price and Maseh Osgan
Published in Org. Synth. 1956, 36, 19
Org. Synth. 1963, Coll. Vol. 4, 268
2,2-DICHLOROETHANOL
Submitted by: C. E. Sroog and H. M. Woodburn
Checked by: R. S. Schreiber and C. J. Lintner, Jr
Published in Org. Synth. 1952, 32, 46
Org. Synth. 1963, Coll. Vol. 4, 271
1,1'-DICYANO-1,1'-BICYCLOHEXYL
Submitted by: C. G. Overberger and M. B.
Berenbaum
Checked by: N. J. Leonard and E. H. Mottus
Published in Org. Synth. 1952, 32, 48
Org. Synth. 1963, Coll. Vol. 4, 273
1,2-DI-1-(1-
CYANO)CYCLOHEXYLHYDRAZINE
Submitted by: C. G. Overberger, Pao-tung Huang,
and M. B. Berenbaum
Checked by: N. J. Leonard and E. H. Mottus
20 | P a g e
Published in Org. Synth. 1952, 32, 50
Org. Synth. 1963, Coll. Vol. 4, 274

DICYANOKETENE ETHYLENE ACETAL

Submitted by: C. L. Dickinson and L. R. Melby
Checked by: James Cason, Edwin R. Harris, and
William T. Miller
Published in Org. Synth. 1959, 39, 13
Org. Synth. 1963, Coll. Vol. 4, 276
1-DIETHYLAMINO-3-BUTANONE
Submitted by: Alfred L. Wilds, Robert M. Nowak,
and Kirtland E. McCaleb
Checked by: William S. Johnson and Duane
Zinkel
Published in Org. Synth. 1957, 37, 18
Org. Synth. 1963, Coll. Vol. 4, 281

DICYCLOPROPYL KETONE

Submitted by: Omer E. Curtis, Jr, Joseph M.

Sandri, Richard E. Crocker, and Harold Hart
Checked by: V. Boekelheide, R. Taber, and D. S.
Tarbell
Published in Org. Synth. 1958, 38, 19
Org. Synth. 1963, Coll. Vol. 4, 278
N,N'-DIETHYLBENZIDINE

Submitted by: Rip G. Rice and Earl J. Kohn

Checked by: Max Tishler, W. H. Jones, and W. F.
Benning
Published in Org. Synth. 1956, 36, 21
Org. Synth. 1963, Coll. Vol. 4, 283

21 | P a g e

DIETHYL BENZOYLMALONATE
Submitted by: John A. Price and D. S. Tarbell
Checked by: T. L. Cairns and C. L. Dickinson
Published in Org. Synth. 1957, 37, 20
Org. Synth. 1963, Coll. Vol. 4, 285
DIETHYL 1,1-
CYCLOBUTANEDICARBOXYLATE
Submitted by: Raymond P. Mariella and Richard
Raube
Checked by: William S. Johnson, William
DeAcetis, and Herbert Title
Published in Org. Synth. 1953, 33, 23
Org. Synth. 1963, Coll. Vol. 4, 288
DIETHYL Δ2-
CYCLOPENTENYLMALONATE
Submitted by: Robert Bruce Moffett
Checked by: R. T. Arnold and George P. Scott
Published in Org. Synth. 1952, 32, 52
Org. Synth. 1963, Coll. Vol. 4, 291
DIETHYL ETHYLIDENEMALONATE
Submitted by: William S. Fones
Checked by: Arthur C. Cope, Harris E. Petree, and
E. R. Trumbull
Published in Org. Synth. 1952, 32, 54
Org. Synth. 1963, Coll. Vol. 4, 293
DIETHYL MERCAPTOACETAL
Submitted by: William E. Parham and Hans
Wynberg
Checked by: Max Tishler and George Purdue
Published in Org. Synth. 1955, 35, 51
Org. Synth. 1963, Coll. Vol. 4, 295
22 | P a g e
 DIETHYL cis-Δ4-
TETRAHYDROPHTHALATE AND DIETHYL
cis-HEXAHYDROPHTHALATE

Submitted by: Arthur C. Cope and Elbert C.

Herrick
Checked by: Charles C. Price and George A.
Cypher
Published in Org. Synth. 1950, 30, 29
Org. Synth. 1963, Coll. Vol. 4, 304

DIETHYL METHYLENEMALONATE

Submitted by: Wayne Feely and V. Boekelheide

Checked by: Max Tishler, Barbara P. Birt, and
Arthur A. Patchett
Published in Org. Synth. 1958, 38, 22
Org. Synth. 1963, Coll. Vol. 4, 298

DIETHYLTHIOCARBAMYL CHLORIDE

Submitted by: R. H. Goshorn, W. W. Levis, Jr, E.

Jaul, and E. J. Ritter
Checked by: T. L. Cairns and H. E. Cupery
Published in Org. Synth. 1955, 35, 55
Org. Synth. 1963, Coll. Vol. 4, 307
DIETHYL γ-OXOPIMELATE

Submitted by: W. S. Emerson and R. I. Longley, Jr

Checked by: William S. Johnson and I. A. David

Published in Org. Synth. 1953, 33, 25
Org. Synth. 1963, Coll. Vol. 4, 302

3,4-DIHYDRO-2-METHOXY-4-METHYL-
2H-PYRAN

Submitted by: Raymond I. Longley, Jr, William S.

Emerson, and Albert J. Blardinelli
23 | P a g e
Checked by: T. L. Cairns and T. E. Young
Published in Org. Synth. 1954, 34, 29
Org. Synth. 1963, Coll. Vol. 4, 311
9,10-DIHYDROPHENANTHRENE
Submitted by: Donald D. Phillips
Checked by: William S. Johnson and David C.
Remy
Published in Org. Synth. 1954, 34, 31
Org. Synth. 1963, Coll. Vol. 4, 313
9,10-DIHYDROXYSTEARIC ACID
Submitted by: Daniel Swern, John T. Scanlan, and
Geraldine B. Dickel
Checked by: John D. Roberts and Edgar F. Kiefer
Published in Org. Synth. 1959, 39, 15
Org. Synth. 1963, Coll. Vol. 4, 317
1,4-DIIODOBUTANE
Submitted by: Herman Stone and Harold Shechter
Checked by: Cliff S. Hamilton and R. C. Rupert
Published in Org. Synth. 1950, 30, 33
Org. Synth. 1963, Coll. Vol. 4, 321
1,6-DIIODOHEXANE
Submitted by: Herman Stone and Harold Shechter
Checked by: T. L. Cairns, B. C. McKusick, and G.
V. Mock
Published in Org. Synth. 1951, 31, 31
Org. Synth. 1963, Coll. Vol. 4, 323
DIISOPROPYL METHYLPHOSPHONATE
Submitted by: A. H. Ford-Moore and B. J. Perry
Checked by: William S. Johnson and James
Ackerman
Published in Org. Synth. 1951, 31, 33
Org. Synth. 1963, Coll. Vol. 4, 325
2,3-DIMETHOXYCINNAMIC ACID
Submitted by: J. Koo, M. S. Fish, G. N. Walker,
and J. Blake
24 | P a g e
Checked by: T. L. Cairns and A. E. Barkdoll
Published in Org. Synth. 1951, 31, 35
Org. Synth. 1963, Coll. Vol. 4, 327
DIMETHYL
ACETYLENEDICARBOXYLATE
Submitted by: E. H. Huntress, T. E. Lesslie, and J.
Bornstein
Checked by: T. L. Cairns and M. J. Hogsed
Published in Org. Synth. 1952, 32, 55
Org. Synth. 1963, Coll. Vol. 4, 329
p-DIMETHYLAMINOBENZALDEHYDE
Submitted by: E. Campaigne and W. L. Archer
Checked by: N. J. Leonard and R. W. Fulmer
Published in Org. Synth. 1953, 33, 27
Org. Synth. 1963, Coll. Vol. 4, 331
β-DIMETHYLAMINOETHYL CHLORIDE
HYDROCHLORIDE
Submitted by: Luther A. R. Hall, Verlin C.
Stephens, and J. H. Burckhalter
Checked by: Richard T. Arnold and William Lee
Published in Org. Synth. 1951, 31, 37
Org. Synth. 1963, Coll. Vol. 4, 333
2-(DIMETHYLAMINO)PYRIMIDINE
Submitted by: C. G. Overberger, Irving C. Kogon,
and Ronald Minin
Checked by: Charles C. Price and T. L. V. Ulbricht
Published in Org. Synth. 1955, 35, 58
Org. Synth. 1963, Coll. Vol. 4, 336
25 | P a g e
 4,6-DIMETHYLCOUMALIN
Submitted by: Newton R. Smith and Richard H.
Wiley
Checked by: R. S. Schreiber and H. H. Fall
Published in Org. Synth. 1952, 32, 57
Org. Synth. 1963, Coll. Vol. 4, 337
N,N-
DIMETHYLCYCLOHEXYLMETHYLAMINE
Submitted by: Arthur C. Cope and Engelbert
Ciganek
Checked by: William E. Parham and Robert
Koncos
Published in Org. Synth. 1959, 39, 19
Org. Synth. 1963, Coll. Vol. 4, 339
DIMETHYLFURAZAN
Submitted by: Lyell C. Behr and John T. Brent
Checked by: T. L. Cairns and J. E. Carnahan
Published in Org. Synth. 1954, 34, 40
Org. Synth. 1963, Coll. Vol. 4, 342
β,β-DIMETHYLGLUTARIC ACID
Submitted by: Walter T. Smith and Gerald L.
McLeod
Checked by: William S. Johnson and Donald D.
Cameron
Published in Org. Synth. 1951, 31, 40
Org. Synth. 1963, Coll. Vol. 4, 345
DIMETHYLKETENE
Submitted by: C. W. Smith and D. G. Norton
Checked by: T. L. Cairns and J. C. Sauer
Published in Org. Synth. 1953, 33, 29
Org. Synth. 1963, Coll. Vol. 4, 348
26 | P a g e
 Published in Org. Synth. 1953, 33, 32
Org. Synth. 1963, Coll. Vol. 4, 354

5,5-DIMETHYL-2-n-
PENTYLTETRAHYDROFURAN

Submitted by: J. Colonge and R. Marey

Checked by: V. Boekelheide and H. Kaempfen
Published in Org. Synth. 1958, 38, 25
Org. Synth. 1963, Coll. Vol. 4, 350

5,5-DIMETHYL-2-PYRROLIDONE

Submitted by: R. B. Moffett

Checked by: N. J. Leonard, W. E. Smith, and B. L.
3,5-DIMETHYLPYRAZOLE Ryder
Published in Org. Synth. 1952, 32, 59
Submitted by: Richard H. Wiley and Peter E. Org. Synth. 1963, Coll. Vol. 4, 357
Hexner
Checked by: William S. Johnson and Robert J.
Highet
Published in Org. Synth. 1951, 31, 43
Org. Synth. 1963, Coll. Vol. 4, 351

2,2-DIMETHYLPYRROLIDINE N,N-DIMETHYLSELENOUREA

Submitted by: Robert Bruce Moffett Submitted by: Frank Bennett and Ralph Zingaro
Checked by: N. J. Leonard and J. W. Curry Checked by: C. F. H. Allen and K. C. Kennard
Published in Org. Synth. 1956, 36, 23
27 | P a g e
Org. Synth. 1963, Coll. Vol. 4, 359

asym-DIMETHYLUREA

Submitted by: Frederick Kurzer

Checked by: William S. Johnson and William T.
Tsatsos
Published in Org. Synth. 1952, 32, 61
Org. Synth. 1963, Coll. Vol. 4, 361

2,6-DINITROANILINE
Submitted by: Harry P. Schultz
Checked by: Arthur C. Cope and Douglas S. Smith
Published in Org. Synth. 1951, 31, 45
Org. Synth. 1963, Coll. Vol. 4, 364
p,p'-DINITROBIBENZYL
Submitted by: Herbert O. House
Checked by: John C. Sheehan and J. Iannicelli
Published in Org. Synth. 1954, 34, 35
Org. Synth. 1963, Coll. Vol. 4, 367

1,4-DINITROBUTANE

Submitted by: Henry Feuer and Gerd Leston

Checked by: John C. Sheehan and J. Iannicelli
Published in Org. Synth. 1954, 34, 37
Org. Synth. 1963, Coll. Vol. 4, 368

28 | P a g e
 3,4-DINITRO-3-HEXENE

Submitted by: D. E. Bisgrove, J. F. Brown, Jr, and

L. B. Clapp
Checked by: John C. Sheehan, Richard L. Wasson,
and Herbert O. House
Published in Org. Synth. 1957, 37, 23
Org. Synth. 1963, Coll. Vol. 4, 372

1,4-DIPHENYL-5-AMINO-1,2,3-TRIAZOLE
AND 4-PHENYL-5-ANILINO-1,2,3-TRIAZOLE

Submitted by: Eugene Lieber, Tai Siang Chao, and

C. N. Ramachandra Rao
DIPHENYLACETALDEHYDE Checked by: T. L. Cairns and E. L. Martin
Published in Org. Synth. 1957, 37, 26
Submitted by: Donald J. Reif and Herbert O. Org. Synth. 1963, Coll. Vol. 4, 380
House
Checked by: M. S. Newman and W. H. Powell
Published in Org. Synth. 1958, 38, 26
Org. Synth. 1963, Coll. Vol. 4, 375

DIPHENYLACETYLENE

Submitted by: Arthur C. Cope, Douglas S. Smith,

and Robert J. Cotter
Checked by: Charles C. Price and Thomas F.
McKeon, Jr
Published in Org. Synth. 1954, 34, 42
Org. Synth. 1963, Coll. Vol. 4, 377
N,N'-DIPHENYLBENZAMIDINE
Submitted by: Arthur C. Hontz and E. C. Wagner
Checked by: R. S. Schreiber and Wm. Bradley
Reid, Jr
Published in Org. Synth. 1951, 31, 48
Org. Synth. 1963, Coll. Vol. 4, 383

29 | P a g e
 2,3-DIPHENYLSUCCINONITRILE

Submitted by: R. B. Davis, J. A. Ward, Jr, J. A.

McRae, and R. A. B. Bannard
Checked by: B. C. McKusick, R. L. Morgan, R. T.
α,β-DIPHENYLCINNAMONITRILE Arnold, and Stuart W. Fenton
Published in Org. Synth. 1952, 32, 63
Submitted by: Stanley Wawzonek and Edwin M. Org. Synth. 1963, Coll. Vol. 4, 392
Smolin
Checked by: Arthur C. Cope and Malcolm
Chamberlain
Published in Org. Synth. 1951, 31, 52
Org. Synth. 1963, Coll. Vol. 4, 387

p-DITHIANE

Submitted by: Richard G. Gillis and A. B. Lacey

Checked by: B. C. McKusick and R. J. Harder
Published in Org. Synth. 1959, 39, 23
Org. Synth. 1963, Coll. Vol. 4, 396

DIPHENYL SUCCINATE

Submitted by: Guido H. Daub and William S.

Johnson
Checked by: James Cason, Robert A. Wessman,
and William G. Dauben
Published in Org. Synth. 1954, 34, 44 trans-2-DODECENOIC ACID
Org. Synth. 1963, Coll. Vol. 4, 390
Submitted by: C. Freeman Allen and Max J. Kalm
Checked by: William S. Johnson and Alan D.
Lourie
30 | P a g e
Published in Org. Synth. 1957, 37, 29
Org. Synth. 1963, Coll. Vol. 4, 398

ETHOXYACETYLENE
ETHANEDITHIOL
Submitted by: E. R. H. Jones, Geoffrey Eglinton,
M. C. Whiting, and B. L. Shaw
Submitted by: A. John Speziale
Checked by: Arthur C. Cope and Ronald M. Pike
Checked by: R. S. Schreiber and R. W. Kratz
Published in Org. Synth. 1954, 34, 46
Published in Org. Synth. 1950, 30, 35
Org. Synth. 1963, Coll. Vol. 4, 404
Org. Synth. 1963, Coll. Vol. 4, 401

ETHYL α-ACETYL-β-(2,3-
DIMETHOXYPHENYL)-PROPIONATE

Submitted by: E. C. Horning, J. Koo, M. S. Fish,

and G. N. Walker
Checked by: T. L. Cairns and Charles W. Todd
Published in Org. Synth. 1951, 31, 56
Org. Synth. 1963, Coll. Vol. 4, 408

31 | P a g e

ETHYL AZODICARBOXYLATE
Submitted by: J. C. Kauer
Checked by: William G. Dauben and Robert L.
Cargill
Org. Synth. 1963, Coll. Vol. 4, 411
ETHYL BENZOYLACETATE
Submitted by: J. M. Straley and A. C. Adams
Checked by: Max Tishler and M. A. Kozlowski
Published in Org. Synth. 1957, 37, 32
Org. Synth. 1963, Coll. Vol. 4, 415
ETHYL tert-BUTYL MALONATE
Submitted by: R. E. Strube
Checked by: William S. Johnson and Duff S.
Allen, Jr
Published in Org. Synth. 1957, 37, 34
Org. Synth. 1963, Coll. Vol. 4, 417
Bottom of Form
Top of Form
Bottom of Form
Top of Form
N-ETHYL-p-CHLOROANILINE
Submitted by: Royston M. Roberts and Paul J.
Vogt
Checked by: James Cason and Milton Finger
Published in Org. Synth. 1958, 38, 29
Org. Synth. 1963, Coll. Vol. 4, 420
32 | P a g e
 Submitted by: Robert Bruce Moffett
Checked by: Charles C. Price and Charles E. Scott
Published in Org. Synth. 1955, 35, 59
Org. Synth. 1963, Coll. Vol. 4, 427

ETHYL CHLOROFLUOROACETATE

Submitted by: Bruce Englund

Checked by: R. S. Schreiber and Burris D. Tiffany
Published in Org. Synth. 1954, 34, 49
Org. Synth. 1963, Coll. Vol. 4, 423

ETHYL ENANTHYLSUCCINATE

Submitted by: Tracy M. Patrick, Jr and Floyd B.

Erickson
Checked by: T. L. Cairns and R. D. Cramer
Published in Org. Synth. 1954, 34, 51
Org. Synth. 1963, Coll. Vol. 4, 430

ETHYL DIAZOACETATE

Submitted by: N. E. Searle

Checked by: Melvin S. Newman, G. F. Ottmann,
and C. F. Grundmann
Published in Org. Synth. 1956, 36, 25
Org. Synth. 1963, Coll. Vol. 4, 424

ETHYLENIMINE

Submitted by: C. F. H. Allen, F. W. Spangler, and

E. R. Webster
Checked by: R. S. Schreiber, A. C. Ott, and M. F.
Murray
ETHYL DIETHOXYACETATE Published in Org. Synth. 1950, 30, 38
33 | P a g e
Org. Synth. 1963, Coll. Vol. 4, 433

2-ETHYLHEXANONITRILE

Submitted by: John A. Krynitsky and Homer W.

Carhart
Checked by: H. R. Snyder and Richard S.
Colgrove
Published in Org. Synth. 1952, 32, 65
Org. Synth. 1963, Coll. Vol. 4, 436

ETHYL ISOCYANIDE

Submitted by: H. L. Jackson and B. C. McKusick

Checked by: N. J. Leonard and L. E. Coleman, Jr

Published in Org. Synth. 1955, 35, 62
Org. Synth. 1963, Coll. Vol. 4, 438

4-ETHYL-2-METHYL-2-OCTENOIC ACID

Submitted by: Kenneth L. Rinehart and Edward G.

Perkins
Checked by: Melvin S. Newman and Joseph H.
Manhart
Published in Org. Synth. 1957, 37, 37
Org. Synth. 1963, Coll. Vol. 4, 444

β-ETHYL-β-METHYLGLUTARIC ACID

Submitted by: H. H. Farmer and Norman Rabjohn

Checked by: Melvin S. Newman and Robert
Harper
Published in Org. Synth. 1956, 36, 28
Org. Synth. 1963, Coll. Vol. 4, 441
34 | P a g e

5-ETHYL-2-METHYLPYRIDINE
Submitted by: Robert L. Frank, Frederick J.
Pilgrim, and Edward F. Riener
Checked by: R. S. Schreiber and T. L. Alderson
Published in Org. Synth. 1950, 30, 41
Org. Synth. 1963, Coll. Vol. 4, 451
ETHYL α-NITROBUTYRATE
Submitted by: Nathan Kornblum and Robert K.
Blackwood
Checked by: James Cason, Joanne Facaros, and
William G. Dauben
Published in Org. Synth. 1957, 37, 44
Org. Synth. 1963, Coll. Vol. 4, 454
ETHYL ORTHOCARBONATE
Submitted by: John D. Roberts and Robert E.
McMahon
Checked by: William S. Johnson and William E.
Loeb
Published in Org. Synth. 1952, 32, 68
Org. Synth. 1963, Coll. Vol. 4, 457
ETHYL β,β-
PENTAMETHYLENEGLYCIDATE
Submitted by: Richard H. Hunt, Leland J. Chinn,
and William S. Johnson
Checked by: N. J. Leonard and F. P. Hauck, Jr
Published in Org. Synth. 1954, 34, 54
Org. Synth. 1963, Coll. Vol. 4, 459
ETHYL PHENYLCYANOACETATE
35 | P a g e
Submitted by: E. C. Horning and A. F. Finelli
Checked by: William S. Johnson and H. Wynberg
Published in Org. Synth. 1950, 30, 43
Org. Synth. 1963, Coll. Vol. 4, 461
ETHYL (1-
PHENYLETHYLIDENE)CYANOACETATE
Submitted by: S. M. McElvain and David H.
Clemens
Checked by: W. E. Parham, Perry W. Kirklin, Jr,
and Wayland E. Noland
Published in Org. Synth. 1959, 39, 25
Org. Synth. 1963, Coll. Vol. 4, 463
ETHYL N-PHENYLFORMIMIDATE
Submitted by: Royston M. Roberts and Paul J.
Vogt
Checked by: T. L. Cairns and J. J. Drysdale
Published in Org. Synth. 1955, 35, 65
Org. Synth. 1963, Coll. Vol. 4, 464
ETHYL α-(1-PYRROLIDYL)PROPIONATE
Submitted by: Robert Bruce Moffett
Checked by: N. J. Leonard and S. Gelfand
Published in Org. Synth. 1953, 33, 35
Org. Synth. 1963, Coll. Vol. 4, 466
ETHYL PYRUVATE
Submitted by: J. W. Cornforth
Checked by: Charles C. Price, Kenneth N.
Campbell, and John Warnke
Published in Org. Synth. 1951, 31, 59
Org. Synth. 1963, Coll. Vol. 4, 467
1,1'-ETHYNYLENE-bis-CYCLOHEXANOL
Submitted by: G. Forrest Woods and Louis H.
Schwartzman
Checked by: Richard T. Arnold and Stuart W.
Fenton
Published in Org. Synth. 1952, 32, 70
Org. Synth. 1963, Coll. Vol. 4, 471
36 | P a g e
 FERROCENE

Submitted by: G. Wilkinson and G. Wilkinson

Checked by: N. J. Leonard, Kenneth L. Rinehart,
Donald J. Casey, Sung Moon, N. J. Leonard,
Kenneth L. Rinehart, and Peter Woo
Published in Org. Synth. 1956, 36, 31
Org. Synth. 1963, Coll. Vol. 4, 473
9-FLUORENECARBOXYLIC ACID
Submitted by: Henry J. Richter
Checked by: Richard T. Arnold, B. C. W.
Hummel, and W. J. Wolf
Published in Org. Synth. 1953, 33, 37
Org. Synth. 1963, Coll. Vol. 4, 482

5-FORMYL-4-PHENANTHROIC ACID

Submitted by: R. E. Dessy and M. S. Newman

Checked by: J. D. Roberts and D. I. Schuster
Published in Org. Synth. 1958, 38, 32
Org. Synth. 1963, Coll. Vol. 4, 484
FLAVONE

Submitted by: T. S. Wheeler

Checked by: R. L. Shriner and Donald A. Scott
Published in Org. Synth. 1952, 32, 72
Org. Synth. 1963, Coll. Vol. 4, 478

FUMARONITRILE
37 | P a g e
Submitted by: David T. Mowry and John Mann
Butler
Checked by: Charles C. Price and Richard D.
Gilbert
Published in Org. Synth. 1950, 30, 46
Org. Synth. 1963, Coll. Vol. 4, 486

2-FUROIC ACID

Submitted by: R. J. Harrisson and M. Moyle

Checked by: James Cason and W. N. Baxter
FURFURAL DIACETATE Published in Org. Synth. 1956, 36, 36
Org. Synth. 1963, Coll. Vol. 4, 493
Submitted by: R. T. Bertz
Checked by: James Cason, William G. Dauben, W.
B. Fearing, and B. P. Summerer
Published in Org. Synth. 1953, 33, 39
Org. Synth. 1963, Coll. Vol. 4, 489

GLUTARIC ACID AND GLUTARIMIDE

Submitted by: G. Paris, L. Berlinguet, R. Gaudry,

2-FURFURYL MERCAPTAN
Submitted by: Helmer Kofod
Checked by: Richard T. Arnold and Erich Marcus
Published in Org. Synth. 1955, 35, 66
Org. Synth. 1963, Coll. Vol. 4, 491
J. English, Jr, and J. E. Dayan
Checked by: James Cason, Edwin R. Harris,
Arthur C. Cope, and Mark R. Kniter
Published in Org. Synth. 1957, 37, 47
Org. Synth. 1963, Coll. Vol. 4, 496

38 | P a g e

GUANYLTHIOUREA
Submitted by: Frederick Kurzer
Checked by: John C. Sheehan, George Buchi, and
David Knutson
Published in Org. Synth. 1955, 35, 69
Org. Synth. 1963, Coll. Vol. 4, 502
D-GULONIC-γ-LACTONE
Submitted by: J. V. Karabinos
Checked by: R. T. Arnold, Fred Smith, and Bertha
Lewis
Published in Org. Synth. 1956, 36, 38
Org. Synth. 1963, Coll. Vol. 4, 506
HEMIMELLITENE
Submitted by: W. R. Brasen and C. R. Hauser
Checked by: William S. Johnson, Donald W.
Stoutamire, and A. L. Wilds
Published in Org. Synth. 1954, 34, 56
Org. Synth. 1963, Coll. Vol. 4, 508
HENDECANEDIOIC ACID
Submitted by: Lois J. Durham, Donald J. McLeod,
and James Cason
Checked by: N. J. Leonard, D. H. Dybvig, and K.
L. Rinehart, Jr
Published in Org. Synth. 1958, 38, 34
Org. Synth. 1963, Coll. Vol. 4, 510
39 | P a g e
 n-HEPTAMIDE
Submitted by: J. L. Guthrie and Norman Rabjohn
Checked by: William S. Johnson and Duane
Zinkel
Published in Org. Synth. 1957, 37, 50
Org. Synth. 1963, Coll. Vol. 4, 513
3-n-HEPTYL-5-CYANOCYTOSINE
Submitted by: Barbara B. Kehm and Calvert W.
Whitehead
Checked by: M. S. Newman and K. G. Ihrman
Published in Org. Synth. 1957, 37, 52
Org. Synth. 1963, Coll. Vol. 4, 515
HEXAHYDRO-1,3,5-TRIPROPIONYL-s-
TRIAZINE
Submitted by: W. O. Teeters and M. A. Gradsten
Checked by: Arthur C. Cope and Mark R. Kinter
Published in Org. Synth. 1950, 30, 51
Org. Synth. 1963, Coll. Vol. 4, 518
HEXAMETHYLBENZENE
Submitted by: N. M. Cullinane, S. J. Chard, and C.
W. C. Dawkins
Checked by: T. L. Cairns and D. C. England
Published in Org. Synth. 1955, 35, 73
Org. Synth. 1963, Coll. Vol. 4, 520
40 | P a g e
 HEXAMETHYLENE DIISOCYANATE

Submitted by: Mark W. Farlow

Checked by: R. L. Shriner and Robert C. Johnson
Published in Org. Synth. 1951, 31, 62
Org. Synth. 1963, Coll. Vol. 4, 521
6-HYDROXYNICOTINIC ACID
Submitted by: J. H. Boyer and W. Schoen
Checked by: T. L. Cairns and W. J. Linn
Published in Org. Synth. 1956, 36, 44
Org. Synth. 1963, Coll. Vol. 4, 532

n-HEXYL FLUORIDE

Submitted by: Arthur I. Vogel, James Leicester,

and William A. T. Macey
Checked by: T. L. Cairns and C. W. Tullock
Published in Org. Synth. 1956, 36, 40
Org. Synth. 1963, Coll. Vol. 4, 525

3-HYDROXYTETRAHYDROFURAN

Submitted by: Hans Wynberg and A. Bantjes

Checked by: John C. Sheehan and Gregory L.
4-HYDROXY-1-BUTANESULFONIC ACID Boshart
SULTONE Published in Org. Synth. 1958, 38, 37
Org. Synth. 1963, Coll. Vol. 4, 534
Submitted by: A. O. Snoddy
Checked by: T. L. Cairns and W. R. Brasen
Published in Org. Synth. 1957, 37, 55
Org. Synth. 1963, Coll. Vol. 4, 529

41 | P a g e
 IODOCYCLOHEXANE

Submitted by: Herman Stone and Harold Shechter

Checked by: T. L. Cairns and V. A. Engelhardt
Published in Org. Synth. 1951, 31, 66
Org. Synth. 1963, Coll. Vol. 4, 543
INDAZOLE

Submitted by: C. Ainsworth

Checked by: Max Tishler, George Gal, and G. A.
Stein
Published in Org. Synth. 1959, 39, 27
Org. Synth. 1963, Coll. Vol. 4, 536

2-IODOTHIOPHENE

Submitted by: Henry Y. Lew and C. R. Noller

Checked by: Cliff S. Hamilton and Frank A.
Bower
Published in Org. Synth. 1950, 30, 53
Org. Synth. 1963, Coll. Vol. 4, 545

4-IODOVERATROLE

Submitted by: Donald E. Janssen and C. V. Wilson

INDOLE-3-ALDEHYDE Checked by: Max Tishler and George Purdue

Published in Org. Synth. 1956, 36, 46
Submitted by: Philip N. James and H. R. Snyder Org. Synth. 1963, Coll. Vol. 4, 547
Checked by: Virgil Boekelheide and Richard N.
Knowles
Published in Org. Synth. 1959, 39, 30
Org. Synth. 1963, Coll. Vol. 4, 539

ISODEHYDROACETIC ACID AND ETHYL

ISODEHYDROACETATE

42 | P a g e
Submitted by: Newton R. Smith and Richard H.
Wiley
Checked by: R. S. Schreiber and H. H. Fall
Published in Org. Synth. 1952, 32, 76
Org. Synth. 1963, Coll. Vol. 4, 549
ISOPHORONE OXIDE
Submitted by: Richard L. Wasson and Herbert O.
House
Checked by: James Cason and Ralph J. Fessenden
Published in Org. Synth. 1957, 37, 58
Org. Synth. 1963, Coll. Vol. 4, 552
ITACONYL CHLORIDE
Submitted by: Henry Feuer and Stanley M. Pier
Checked by: William S. Johnson and Ernest F.
Silversmith
Published in Org. Synth. 1953, 33, 41
Org. Synth. 1963, Coll. Vol. 4, 554
6-KETOHENDECANEDIOIC ACID
Submitted by: Lois J. Durham, Donald J. McLeod,
and James Cason
Checked by: N. J. Leonard, D. H. Dybvig, and K.
L. Rinehart, Jr
Published in Org. Synth. 1958, 38, 38
Org. Synth. 1963, Coll. Vol. 4, 555
β-KETOISOÖCTALDEHYDE DIMETHYL
ACETAL
Submitted by: Charles C. Price and Joseph A.
Pappalardo
Checked by: R. S. Schreiber, Wm. Bradley Reid,
Jr, and R. W. Jackson
Published in Org. Synth. 1952, 32, 79
Org. Synth. 1963, Coll. Vol. 4, 558
LAURONE
Submitted by: J. C. Sauer
Checked by: William S. Johnson and H. C. Dehm
Published in Org. Synth. 1951, 31, 68
Org. Synth. 1963, Coll. Vol. 4, 560
43 | P a g e
 2-MERCAPTOBENZIMIDAZOLE

Submitted by: J. A. VanAllan and B. D. Deacon

Checked by: Cliff S. Hamilton and Yao-Hua Wu
Published in Org. Synth. 1950, 30, 56
Org. Synth. 1963, Coll. Vol. 4, 569

LAURYLMETHYLAMINE

Submitted by: C. V. Wilson and J. F. Stenberg

Checked by: N. J. Leonard and C. W.
Schimelpfenig
Published in Org. Synth. 1956, 36, 48
Org. Synth. 1963, Coll. Vol. 4, 564

METHANESULFONYL CHLORIDE

Submitted by: Peter J. Hearst and C. R. Noller

Checked by: R. S. Schreiber, B. D. Aspergren, and
R. V. Heinzelmann
Published in Org. Synth. 1950, 30, 58
2-MERCAPTO-4-AMINO-5- Org. Synth. 1963, Coll. Vol. 4, 571
CARBETHOXYPYRIMIDINE AND 2-
MERCAPTO-4-HYDROXY-5-
CYANOPYRIMIDINE

Submitted by: T. L. V. Ulbricht, Takuo Okuda,

and Charles C. Price
Checked by: B. C. McKusick and Stephen
Proskow
Published in Org. Synth. 1959, 39, 34
Org. Synth. 1963, Coll. Vol. 4, 566
o-METHOXYPHENYLACETONE
Submitted by: R. V. Heinzelman
Checked by: M. Tishler and H. L. Slates
Published in Org. Synth. 1955, 35, 74
Org. Synth. 1963, Coll. Vol. 4, 573

44 | P a g e
 o-METHYLBENZYL ALCOHOL

Submitted by: W. R. Brasen and C. R. Hauser

Checked by: William S. Johnson, Donald W.
Stoutamire, and A. L. Wilds
Published in Org. Synth. 1954, 34, 58
Org. Synth. 1963, Coll. Vol. 4, 582

p-METHOXYPHENYLACETONITRILE

Submitted by: Kurt Rorig, J. Derland Johnston,

Robert W. Hamilton, and Thomas J. Telinski
Checked by: William S. Johnson, Stanley Seltzer,
and Peter Yates
Published in Org. Synth. 1956, 36, 50
Org. Synth. 1963, Coll. Vol. 4, 576

2-METHYLBENZYLDIMETHYLAMINE

Submitted by: W. R. Brasen and C. R. Hauser

METHYL p-ACETYLBENZOATE Checked by: William S. Johnson, Mary E. Mills,
and A. L. Wilds
Submitted by: William S. Emerson and George F. Published in Org. Synth. 1954, 34, 61
Deebel Org. Synth. 1963, Coll. Vol. 4, 585
Checked by: Arthur C. Cope and Warren N.
Baxter
Published in Org. Synth. 1952, 32, 81
Org. Synth. 1963, Coll. Vol. 4, 579

45 | P a g e
 O-METHYLCAPROLACTIM

Submitted by: Richard E. Benson and Theodore L.

Cairns
Checked by: Charles C. Price, Kenneth N.
Campbell, and Richard Mcbride
Published in Org. Synth. 1951, 31, 72
Org. Synth. 1963, Coll. Vol. 4, 588

METHYL
CYCLOPENTANECARBOXYLATE

Submitted by: D. W. Goheen and W. R. Vaughan

Checked by: N. J. Leonard, M. J. Konz, W. H.
Pittman, and K. L. Rinehart, Jr
Published in Org. Synth. 1959, 39, 37
3-METHYLCOUMARONE Org. Synth. 1963, Coll. Vol. 4, 594

Submitted by: Werner R. Boehme

Checked by: James Cason and Kenneth L.
Rinehart
Published in Org. Synth. 1953, 33, 43
Org. Synth. 1963, Coll. Vol. 4, 590

METHYL CYCLOPROPYL KETONE

46 | P a g e
Submitted by: George W. Cannon, Ray C. Ellis,
and Joseph R. Leal
Checked by: R. S. Schreiber, Wm. Bradley Reid,
Jr, and R. D. Birkenmeyer
Published in Org. Synth. 1951, 31, 74
Org. Synth. 1963, Coll. Vol. 4, 597
Submitted by: Don M. Balcom and C. R. Noller
Checked by: Homer Adkins and Walter W. Gilbert
Published in Org. Synth. 1950, 30, 59
Org. Synth. 1963, Coll. Vol. 4, 603

N-METHYL-1,2-DIPHENYLETHYLAMINE
AND HYDROCHLORIDE

Submitted by: Robert Bruce Moffett

Checked by: N. J. Leonard and L. A. Miller
Published in Org. Synth. 1954, 34, 64
Org. Synth. 1963, Coll. Vol. 4, 605

2-METHYL-2,5-DECANEDIOL

Submitted by: J. Colonge and R. Marey

Checked by: V. Boekelheide and H. Kaempfen
Published in Org. Synth. 1958, 38, 41
Org. Synth. 1963, Coll. Vol. 4, 601

N-METHYL-2,3-
DIMETHOXYBENZYLAMINE

47 | P a g e

trans-2-METHYL-2-DODECENOIC ACID
Submitted by: C. Freeman Allen and Max J. Kalm
Checked by: William S. Johnson and H. W.
Whitlock, Jr
Published in Org. Synth. 1958, 38, 43
Org. Synth. 1963, Coll. Vol. 4, 608
METHYLENECYCLOHEXANE AND N,N-
DIMETHYLHYDROXYLAMINE
HYDROCHLORIDE
Submitted by: Arthur C. Cope and Engelbert
Ciganek
Checked by: William E. Parham and Robert
Koncos
Published in Org. Synth. 1959, 39, 40
Org. Synth. 1963, Coll. Vol. 4, 612
2-METHYLENEDODECANOIC ACID
Submitted by: C. Freeman Allen and Max J. Kalm
Checked by: William S. Johnson and Kenneth L.
48 | P a g e
Williamson
Published in Org. Synth. 1958, 38, 47
Org. Synth. 1963, Coll. Vol. 4, 616 9-METHYLFLUORENE

Submitted by: Kurt L. Schoen and E. I. Becker

Checked by: William S. Johnson and V. B.
Haarstad
Published in Org. Synth. 1959, 39, 43
Org. Synth. 1963, Coll. Vol. 4, 623

5-METHYLFURFURYLDIMETHYLAMINE

Submitted by: Ernest L. Eliel and Milton T. Fisk

1-METHYL-3-ETHYLOXINDOLE Checked by: James Cason, Mary S. Nakata, and
William G. Dauben
Submitted by: M. W. Rutenberg and E. C. Horning Published in Org. Synth. 1955, 35, 78
Org. Synth. 1963, Coll. Vol. 4, 626
Checked by: William S. Johnson and C. A.
Erickson
Published in Org. Synth. 1950, 30, 62
Org. Synth. 1963, Coll. Vol. 4, 620

3-METHYL-2-FUROIC ACID AND 3-

METHYLFURAN

Submitted by: D. M. Burness

Checked by: James Cason and Robert B.
Hutchison
Published in Org. Synth. 1959, 39, 46
Org. Synth. 1963, Coll. Vol. 4, 628

49 | P a g e
 β-METHYLGLUTARIC ANHYDRIDE
Submitted by: James Cason
Checked by: B. C. McKusick, R. D. Smith, and W.
R. Hatchard
Published in Org. Synth. 1958, 38, 52
Org. Synth. 1963, Coll. Vol. 4, 630
METHYLGLYOXAL-ω-
PHENYLHYDRAZONE
Submitted by: George A. Reynolds and J. A.
VanAllan
Checked by: T. L. Cairns and C. T. Handy
Published in Org. Synth. 1952, 32, 84
Org. Synth. 1963, Coll. Vol. 4, 633
METHYL HYDROGEN
HENDECANEDIOATE
Submitted by: Lois J. Durham, Donald J. McLeod,
and James Cason
Checked by: N. J. Leonard, D. H. Dybvig, and K.
L. Rinehart, Jr
Published in Org. Synth. 1958, 38, 55
Org. Synth. 1963, Coll. Vol. 4, 635
4-METHYL-6-HYDROXYPYRIMIDINE
Submitted by: H. M. Foster and H. R. Snyder
Checked by: R. T. Arnold and P. E. Throckmorton
Published in Org. Synth. 1955, 35, 80
Org. Synth. 1963, Coll. Vol. 4, 638
50 | P a g e
 Published in Org. Synth. 1954, 34, 67
Org. Synth. 1963, Coll. Vol. 4, 645

METHYL 3-METHYL-2-FUROATE

Submitted by: D. M. Burness

1-METHYLISOQUINOLINE Checked by: James Cason and Robert B.
Hutchison
Submitted by: J. Weinstock and V. Boekelheide Published in Org. Synth. 1959, 39, 49
Checked by: N. J. Leonard, Terry W. Milligan, Org. Synth. 1963, Coll. Vol. 4, 649
and William R. Sherman
Published in Org. Synth. 1958, 38, 58
Org. Synth. 1963, Coll. Vol. 4, 641

METHYL γ-METHYL-γ-NITROVALERATE

Submitted by: R. B. Moffett

Checked by: N. J. Leonard and B. L. Ryder
Published in Org. Synth. 1952, 32, 86
Org. Synth. 1963, Coll. Vol. 4, 652

METHYLISOUREA HYDROCHLORIDE

Submitted by: Frederick Kurzer and Alexander

Lawson
Checked by: William S. Johnson and William T.
Tsatsos
3-METHYL-4-NITROPYRIDINE-1-OXIDE
51 | P a g e
Submitted by: E. C. Taylor, Jr and Aldo J. Crovetti

Checked by: Max Tishler and Henry B. Lange

Published in Org. Synth. 1956, 36, 53
Org. Synth. 1963, Coll. Vol. 4, 654

3-METHYLOXINDOLE
Submitted by: Abraham S. Endler and Ernest I.
Becker
Checked by: James Cason and Warren N. Baxter
Published in Org. Synth. 1957, 37, 60
Org. Synth. 1963, Coll. Vol. 4, 657
β-METHYL-β-PHENYL-α,α'-
DICYANOGLUTARIMIDE
Submitted by: S. M. McElvain and David H.
Clemens
Checked by: W. E. Parham, Perry W. Kirklin, Jr,
and Wayland E. Noland
Published in Org. Synth. 1959, 39, 52
Org. Synth. 1963, Coll. Vol. 4, 662

3-METHYL-1,5-PENTANEDIOL
β-METHYL-β-PHENYLGLUTARIC ACID
Submitted by: Raymond I. Longley, Jr and
Submitted by: S. M. McElvain and David H.
William S. Emerson
Clemens
Checked by: T. L. Cairns and John F. Harris, Jr
Checked by: W. E. Parham, Perry W. Kirklin, Jr,
Published in Org. Synth. 1954, 34, 71
and Wayland E. Noland
Org. Synth. 1963, Coll. Vol. 4, 660
Published in Org. Synth. 1959, 39, 54
52 | P a g e
Org. Synth. 1963, Coll. Vol. 4, 664
1-METHYL-3-PHENYLINDANE
Submitted by: Milton J. Rosen
Checked by: R. T. Arnold and William K.
Witsiepe
Published in Org. Synth. 1955, 35, 83
Org. Synth. 1963, Coll. Vol. 4, 665
METHYL 2-THIENYL SULFIDE
Submitted by: J. Cymerman-Craig and J. W. Loder
Checked by: Charles C. Price and E. A. Dudley
Published in Org. Synth. 1955, 35, 85
Org. Synth. 1963, Coll. Vol. 4, 667
METHYL β-THIODIPROPIONATE
Submitted by: Edward A. Fehnel and Marvin
Carmack
Checked by: Arthur C. Cope and James J. Ryan
Published in Org. Synth. 1950, 30, 65
Org. Synth. 1963, Coll. Vol. 4, 669
3-METHYLTHIOPHENE
Submitted by: R. F. Feldkamp and B. F. Tullar
Checked by: Cliff S. Hamilton, Y. H. Wu, and
William J. Raich
Published in Org. Synth. 1954, 34, 73
Org. Synth. 1963, Coll. Vol. 4, 671
METHYL p-TOLYL SULFONE
Submitted by: L. Field and R. D. Clark
53 | P a g e
Checked by: John C. Sheehan and M. Gertrude
Howell
Published in Org. Synth. 1958, 38, 62
Org. Synth. 1963, Coll. Vol. 4, 674
β-METHYL-δ-VALEROLACTONE
Submitted by: Raymond I. Longley, Jr and
William S. Emerson
Checked by: T. L. Cairns and W. W. Gilbert
Published in Org. Synth. 1955, 35, 87
Org. Synth. 1963, Coll. Vol. 4, 677
MONOBENZALPENTAERYTHRITOL
Submitted by: C. H. Issidorides and R. Gulen
Checked by: M. S. Newman and Arlen B. Mekler
Published in Org. Synth. 1958, 38, 65
Org. Synth. 1963, Coll. Vol. 4, 679
MONOBROMOPENTAERYTHRITOL
Submitted by: S. Wawzonek, A. Matar, and C. H.
Issidorides
Checked by: Charles C. Price and G. Venkat Rao
Published in Org. Synth. 1958, 38, 68
Org. Synth. 1963, Coll. Vol. 4, 681
MONOVINYLACETYLENE
Submitted by: G. F. Hennion, Charles C. Price,
and Thomas F. McKeon, Jr
Checked by: Max Tishler and John E. Allegretti
Published in Org. Synth. 1958, 38, 70
Org. Synth. 1963, Coll. Vol. 4, 683
MUCOBROMIC ACID
Submitted by: G. A. Taylor
Checked by: B. C. McKusick, E. L. Martin, and
W. R. Brasen
Org. Synth. 1963, Coll. Vol. 4, 688
1-NAPHTHALDEHYDE
Submitted by: S. J. Angyal, J. R. Tetaz, and J. G.
Wilson
Checked by: R. S. Schreiber and Paul E. Marlatt
Published in Org. Synth. 1950, 30, 67
54 | P a g e
Org. Synth. 1963, Coll. Vol. 4, 690

1,4-NAPHTHOQUINONE

Submitted by: E. A. Braude and J. S. Fawcett

Checked by: Charles C. Price, R. S. Schreiber, R.
D. Birkenmeyer, Paul F. Kirk, and William
Bradley Reid, Jr
Published in Org. Synth. 1953, 33, 50
Org. Synth. 1963, Coll. Vol. 4, 698
NAPHTHALENE-1,5-DISULFONYL
CHLORIDE

Submitted by: P. D. Caesar

Checked by: R. T. Arnold and George P. Scott
Published in Org. Synth. 1952, 32, 88
Org. Synth. 1963, Coll. Vol. 4, 693

α-NAPHTHYL ISOTHIOCYANATE

Submitted by: J. Cymerman-Craig, M. Moyle, and

R. A. White
Checked by: N. J. Leonard and F. H. Owens
Published in Org. Synth. 1956, 36, 56
Org. Synth. 1963, Coll. Vol. 4, 700
1,5-NAPHTHALENEDITHIOL

Submitted by: P. D. Caesar

Checked by: Richard T. Arnold, W. E. Parham,
and R. M. Scribner
Published in Org. Synth. 1953, 33, 47
Org. Synth. 1963, Coll. Vol. 4, 695

NEOPHYL CHLORIDE

Submitted by: W. T. Smith, Jr and J. T. Sellas

Checked by: N. J. Leonard and R. O. Kerr
55 | P a g e
Published in Org. Synth. 1952, 32, 90
Org. Synth. 1963, Coll. Vol. 4, 702
NICOTINAMIDE-1-OXIDE
Submitted by: E. C. Taylor, Jr and Aldo J. Crovetti
Checked by: Charles C. Price and Walter A.
Schroeder
Published in Org. Synth. 1957, 37, 63
Org. Synth. 1963, Coll. Vol. 4, 704
NICOTINONITRILE
Submitted by: Peyton C. Teague and William A.
Short
Checked by: Arthur C. Cope, John C. Sheehan,
and Louis A. Cohen
Published in Org. Synth. 1953, 33, 52
Org. Synth. 1963, Coll. Vol. 4, 706
o-NITROACETOPHENONE
Submitted by: George A. Reynolds and Charles R.
Hauser
Checked by: Cliff S. Hamilton and Yao-Hua Wu
Published in Org. Synth. 1950, 30, 70
Org. Synth. 1963, Coll. Vol. 4, 708
9-NITROANTHRACENE
Submitted by: Charles E. Braun, Clinton D. Cook,
Charles Merritt, Jr, and Joseph E. Rousseau
Checked by: William S. Johnson, George N.
Sausen, and Paul R. Shafer
Published in Org. Synth. 1951, 31, 77
Org. Synth. 1963, Coll. Vol. 4, 711
56 | P a g e
 o- AND p-NITROBENZALDIACETATE

Submitted by: Tamio Nishimura m-NITROBIPHENYL

Checked by: T. L. Cairns and R. E. Foster
Published in Org. Synth. 1956, 36, 58
Org. Synth. 1963, Coll. Vol. 4, 713
Submitted by: C. E. Kaslow and R. M. Summers
Checked by: James Cason and B. H. Walker
Published in Org. Synth. 1953, 33, 56
Org. Synth. 1963, Coll. Vol. 4, 718

m-NITROBENZAZIDE

Submitted by: Jon Munch-Petersen

Checked by: William S. Johnson and W. David
Wood
Published in Org. Synth. 1953, 33, 53
Org. Synth. 1963, Coll. Vol. 4, 715

o-NITROCINNAMALDEHYDE

Submitted by: Robert E. Buckles and M. Peter

Bellis
57 | P a g e
Checked by: Richard T. Arnold and James D.
Groves
Published in Org. Synth. 1953, 33, 60
Org. Synth. 1963, Coll. Vol. 4, 722

1-NITROÖCTANE

Submitted by: N. Kornblum and H. E. Ungnade

Checked by: John C. Sheehan and M. Gertrude
Howell
Published in Org. Synth. 1958, 38, 75
Org. Synth. 1963, Coll. Vol. 4, 724 trans-o-NITRO-α-PHENYLCINNAMIC ACID

Submitted by: DeLos F. DeTar

Checked by: Charles C. Price and J. D. Berman
Published in Org. Synth. 1955, 35, 89
Org. Synth. 1963, Coll. Vol. 4, 730

1-(p-NITROPHENYL)-1,3-BUTADIENE

Submitted by: Gus A. Ropp and Eugene C. Coyner

Checked by: Arthur C. Cope and David J.

Marshall
Published in Org. Synth. 1951, 31, 80
Org. Synth. 1963, Coll. Vol. 4, 727

m-NITROSTYRENE

Submitted by: Richard H. Wiley and Newton R.

Smith
Checked by: Richard T. Arnold, William E.
Parham, and Darwin D. Davis
Published in Org. Synth. 1953, 33, 62
Org. Synth. 1963, Coll. Vol. 4, 731

58 | P a g e
 Checked by: Max Tishler and R. Connell
Published in Org. Synth. 1957, 37, 66
Org. Synth. 1963, Coll. Vol. 4, 739

PARABANIC ACID

Submitted by: Joseph I. Murray

Checked by: M. S. Newman and Tadamichi
6-NITROVERATRALDEHYDE Fukunaga
Published in Org. Synth. 1957, 37, 71
Submitted by: Charles A. Fetscher Org. Synth. 1963, Coll. Vol. 4, 744
Checked by: Richard T. Arnold, W. E. Parham,
and Donald A. Leister
Published in Org. Synth. 1953, 33, 65
Org. Synth. 1963, Coll. Vol. 4, 735

NORBORNYLENE

Submitted by: J. Meinwald and N. J. Hudak

Checked by: J. D. Roberts, C. M. Sharts, and W.
G. Woods
Published in Org. Synth. 1957, 37, 65
Org. Synth. 1963, Coll. Vol. 4, 738 1,4-PENTADIENE

Submitted by: R. E. Benson, B. C. McKusick,

Oliver Grummitt, E. P. Budewitz, and C. C. Chudd

Checked by: N. J. Leonard, A. G. Cook, William

S. Johnson, E. Saito, and Donald J. Reif
Published in Org. Synth. 1958, 38, 78
Org. Synth. 1963, Coll. Vol. 4, 746
OLEOYL CHLORIDE

Submitted by: C. F. H. Allen, J. R. Byers, and W.

J. Humphlett

59 | P a g e
 PENTAERYTHRITYL TETRABROMIDE

Submitted by: Hershel L. Herzog

Checked by: T. L. Cairns and D. W. Woodward
Published in Org. Synth. 1951, 31, 82
Org. Synth. 1963, Coll. Vol. 4, 753

PHENYLACETAMIDE

Submitted by: Wilhelm Wenner

Checked by: William S. Johnson and Robert E.
Ireland
Published in Org. Synth. 1952, 32, 92
Org. Synth. 1963, Coll. Vol. 4, 760

4-PENTYN-1-OL

Submitted by: E. R. H. Jones, Geoffrey Eglinton,

and M. C. Whiting
Checked by: Arthur C. Cope and Ronald M. Pike
Published in Org. Synth. 1953, 33, 68
Org. Synth. 1963, Coll. Vol. 4, 755
PHENYLACETYLENE
Submitted by: Kenneth N. Campbell and Barbara
K. Campbell
Checked by: R. S. Schreiber and H. E. Cupery
Published in Org. Synth. 1950, 30, 72
Org. Synth. 1963, Coll. Vol. 4, 763

PHENANTHRENEQUINONE
γ-PHENYLALLYLSUCCINIC ACID
Submitted by: Ray Wendland and John LaLonde
Submitted by: Christian S. Rondestvedt, Jr
Checked by: William S. Johnson and Sol Shulman
Checked by: Charles C. Price and Wm. J. Belanger
Published in Org. Synth. 1954, 34, 76
Published in Org. Synth. 1951, 31, 85
Org. Synth. 1963, Coll. Vol. 4, 757
Org. Synth. 1963, Coll. Vol. 4, 766

60 | P a g e
 α-PHENYL-α-
CARBETHOXYGLUTARONITRILE

Submitted by: E. C. Horning and A. F. Finelli

Checked by: William S. Johnson and H. Wynberg
Published in Org. Synth. 1950, 30, 80
N-PHENYLBENZAMIDINE Org. Synth. 1963, Coll. Vol. 4, 776

Submitted by: F. C. Cooper and M. W. Partridge

Checked by: T. L. Cairns, R. E. Benson, and V. J.
Webers
Published in Org. Synth. 1956, 36, 64
Org. Synth. 1963, Coll. Vol. 4, 769

α-PHENYLCINNAMIC ACID

Submitted by: Robert E. Buckles and Keith

Bremer
Checked by: T. L. Cairns and J. C. Lorenz
trans-1-PHENYL-1,3-BUTADIENE Published in Org. Synth. 1953, 33, 70
Org. Synth. 1963, Coll. Vol. 4, 777
Submitted by: Oliver Grummitt and Ernest I.
Becker
Checked by: Charles C. Price and T. L. Patton
Published in Org. Synth. 1950, 30, 75
Org. Synth. 1963, Coll. Vol. 4, 771

2-PHENYLCYCLOHEPTANONE

Submitted by: C. David Gutsche and Herbert E.

Johnson
Checked by: N. J. Leonard and F. P. Hauck, Jr
61 | P a g e
Published in Org. Synth. 1955, 35, 91
Org. Synth. 1963, Coll. Vol. 4, 780
PHENYLDICHLOROPHOSPHINE
Submitted by: B. Buchner and L. B. Lockhart, Jr
Checked by: Cliff S. Hamilton and P. J.
Vanderhorst
Published in Org. Synth. 1951, 31, 88
Org. Synth. 1963, Coll. Vol. 4, 784
4-PHENYL-m-DIOXANE
Submitted by: R. L. Shriner and Philip R. Ruby
Checked by: Richard T. Arnold, W. E. Parham,
and John E. Franz
Published in Org. Synth. 1953, 33, 72
Org. Synth. 1963, Coll. Vol. 4, 786
o-PHENYLENE CARBONATE
Submitted by: R. S. Hanslick, W. F. Bruce, and A.
Mascitti
Checked by: Arthur C. Cope, Harris E. Petree, and
Elmer R. Trumbull
Published in Org. Synth. 1953, 33, 74
Org. Synth. 1963, Coll. Vol. 4, 788
α-PHENYLGLUTARIC ANHYDRIDE
Submitted by: E. C. Horning and A. F. Finelli
Checked by: William S. Johnson and H. Wynberg
Published in Org. Synth. 1950, 30, 81
Org. Synth. 1963, Coll. Vol. 4, 790
1-PHENYL-1-PENTEN-4-YN-3-OL
Submitted by: Lars Skattebøl, E. R. H. Jones, and
Mark C. Whiting
Checked by: Melvin S. Newman and Raymond E.
Dessy
62 | P a g e
Published in Org. Synth. 1959, 39, 56
Org. Synth. 1963, Coll. Vol. 4, 792
1-PHENYLPIPERIDINE
Submitted by: A. N. Bourns, H. W. Embleton, and
Mary K. Hansuld
Checked by: R. T. Arnold, William E. Parham,
and Carl Serres
Published in Org. Synth. 1954, 34, 79
Org. Synth. 1963, Coll. Vol. 4, 795
3-PHENYL-1-PROPANOL
Submitted by: R. L. Shriner and Philip R. Ruby
Checked by: Richard T. Arnold, W. E. Parham,
and Hans Wynberg
Published in Org. Synth. 1953, 33, 76
Org. Synth. 1963, Coll. Vol. 4, 798
PHENYLPROPARGYLALDEHYDE
DIETHYL ACETAL
Submitted by: B. W. Howk and J. C. Sauer
Checked by: N. J. Leonard and S. W. Blum
Published in Org. Synth. 1959, 39, 59
Org. Synth. 1963, Coll. Vol. 4, 801
PHENYLSUCCINIC ACID
Submitted by: C. F. H. Allen and H. B. Johnson
Checked by: H. R. Snyder, D. J. Mann, and
Leonard E. Miller
Published in Org. Synth. 1950, 30, 83
Org. Synth. 1963, Coll. Vol. 4, 804
o-PHTHALALDEHYDE
Submitted by: J. C. Bill and D. S. Tarbell
Checked by: Arthur C. Cope and Harris E. Petree
Published in Org. Synth. 1954, 34, 82
Org. Synth. 1963, Coll. Vol. 4, 807
63 | P a g e
 α-PHTHALIMIDO-o-TOLUIC ACID

Submitted by: J. Bornstein, P. E. Drummond, and

S. F. Bedell
Checked by: John C. Sheehan and Y. L. Yeh
Published in Org. Synth. 1958, 38, 81
Org. Synth. 1963, Coll. Vol. 4, 810

PUTRESCINE DIHYDROCHLORIDE

Submitted by: Peter A. S. Smith

Checked by: James Cason and Wm. DeAcetis
Published in Org. Synth. 1956, 36, 69
Org. Synth. 1963, Coll. Vol. 4, 819

PROPIOLALDEHYDE

Submitted by: J. C. Sauer

Checked by: John C. Sheehan and E. R. Gilmont
Published in Org. Synth. 1956, 36, 66
Org. Synth. 1963, Coll. Vol. 4, 813

PSEUDOPELLETIERINE
Submitted by: Arthur C. Cope, Hugh L. Dryden,
Jr, and Charles F. Howell
Checked by: N. J. Leonard, D. F. Morrow, and W.
D. Smart
Published in Org. Synth. 1957, 37, 73
Org. Synth. 1963, Coll. Vol. 4, 816
2,3-PYRAZINEDICARBOXYLIC ACID
Submitted by: Reuben G. Jones and Keith C.
McLaughlin
Checked by: H. R. Snyder and R. E. Heckert
Published in Org. Synth. 1950, 30, 86
Org. Synth. 1963, Coll. Vol. 4, 824

64 | P a g e
 Submitted by: Robert M. Silverstein, Edward E.
Ryskiewicz, and Constance Willard
Checked by: Max Tishler and George Purdue
Published in Org. Synth. 1956, 36, 74
Org. Synth. 1963, Coll. Vol. 4, 831

PYRIDINE-N-OXIDE

Submitted by: Harry S. Mosher, Leslie Turner, and

Allan Carlsmith
Checked by: N. J. Leonard and E. D. Sutoris
Published in Org. Synth. 1953, 33, 79
Org. Synth. 1963, Coll. Vol. 4, 828

Top of Form

2-(1-PYRROLIDYL)PROPANOL

Submitted by: Robert Bruce Moffett

Checked by: N. J. Leonard and S. Gelfand
Published in Org. Synth. 1953, 33, 82
Org. Synth. 1963, Coll. Vol. 4, 834

2-PYRROLEALDEHYDE
65 | P a g e

QUINACETOPHENONE MONOMETHYL
ETHER
Submitted by: G. N. Vyas and N. M. Shah
Checked by: William S. Johnson and R. T. Keller
Published in Org. Synth. 1951, 31, 90
Org. Synth. 1963, Coll. Vol. 4, 836
SEBACIL
Submitted by: A. T. Blomquist and Albert
Goldstein
Checked by: N. J. Leonard and J. C. Little
Published in Org. Synth. 1956, 36, 77
Org. Synth. 1963, Coll. Vol. 4, 838
SEBACOIN
Submitted by: Norman L. Allinger
Checked by: N. J. Leonard, J. C. Little, and F. H.
Owens
Published in Org. Synth. 1956, 36, 79
Org. Synth. 1963, Coll. Vol. 4, 840
SODIUM NITROMALONALDEHYDE
MONOHYDRATE
Submitted by: Paul E. Fanta
Checked by: Cliff S. Hamilton and Philip J.
Vanderhorst
Published in Org. Synth. 1952, 32, 95
Org. Synth. 1963, Coll. Vol. 4, 844
SODIUM β-STYRENESULFONATE AND β-
STYRENESULFONYL CHLORIDE
Submitted by: Christian S. Rondestvedt, Jr and F.
G. Bordwell
Checked by: T. L. Cairns and H. E. Winberg
Published in Org. Synth. 1954, 34, 85
Org. Synth. 1963, Coll. Vol. 4, 846
66 | P a g e

STEAROLIC ACID
Submitted by: N. A. Khan, F. E. Deatherage, and
J. B. Brown
Checked by: Max Tishler, W. J. Paleveda, and E.
F. Schoenewaldt
Published in Org. Synth. 1957, 37, 77
Org. Synth. 1963, Coll. Vol. 4, 851
STEARONE
Submitted by: A. G. Dobson and H. H. Hatt
Checked by: R. L. Shriner and Philip R. Ruby
Published in Org. Synth. 1953, 33, 84
Org. Synth. 1963, Coll. Vol. 4, 854
cis-STILBENE
Submitted by: Robert E. Buckles and Norris G.
Wheeler
Checked by: T. L. Cairns and J. C. Lorenz
Published in Org. Synth. 1953, 33, 88
Org. Synth. 1963, Coll. Vol. 4, 857
trans-STILBENE OXIDE
Submitted by: Donald J. Reif and Herbert O.
House
Checked by: Melvin S. Newman and Donald K.
Phillips
Published in Org. Synth. 1958, 38, 83
Org. Synth. 1963, Coll. Vol. 4, 860
α-SULFOPALMITIC ACID
Submitted by: J. K. Weil, R. G. Bistline, Jr, and A.
J. Stirton
Checked by: James Cason and Gerhard J. Fonken
Published in Org. Synth. 1956, 36, 83
Org. Synth. 1963, Coll. Vol. 4, 862
SYRINGIC ALDEHYDE
Submitted by: C. F. H. Allen and Gerhard W.
Leubner
Checked by: R. S. Schreiber, Wm. Bradley Reid,
67 | P a g e
Jr, and R. W. Jackson
Published in Org. Synth. 1951, 31, 92
Org. Synth. 1963, Coll. Vol. 4, 866

TETRAACETYLETHANE

Submitted by: Robert G. Charles

Checked by: Virgil Boekelheide and Henry
Fleischer
Published in Org. Synth. 1959, 39, 61
Org. Synth. 1963, Coll. Vol. 4, 869

TETRACYANOETHYLENE

Submitted by: R. A. Carboni

Checked by: James Cason and Edwin R. Harris
Published in Org. Synth. 1959, 39, 64
Org. Synth. 1963, Coll. Vol. 4, 877

dl-4,4',6,6'-TETRACHLORODIPHENIC ACID

Submitted by: Edward R. Atkinson, Donald M.

Murphy, and James E. Lufkin
Checked by: R. S. Schreiber, Wm. Bradley Reid,
Jr, and R. D. Birkenmeyer
Published in Org. Synth. 1951, 31, 96
Org. Synth. 1963, Coll. Vol. 4, 872
TETRAETHYLTIN

Submitted by: G. J. M. Van Der Kerk and J. G. A.

Luijten
Checked by: M. S. Newman and L. L. Wood
Published in Org. Synth. 1956, 36, 86
68 | P a g e
Org. Synth. 1963, Coll. Vol. 4, 881

1,2,3,4-TETRAHYDROCARBAZOLE

Submitted by: Crosby U. Rogers and B. B. Corson

Checked by: Charles C. Price, Kenneth N.
Campbell, and Robert P. Kane
Published in Org. Synth. 1950, 30, 90
Org. Synth. 1963, Coll. Vol. 4, 884

cis-Δ4-TETRAHYDROPHTHALIC
ANHYDRIDE

Submitted by: Arthur C. Cope and Elbert C.

Herrick
Checked by: Charles C. Price, Kenneth N.
Campbell, and Robert P. Kane
Published in Org. Synth. 1950, 30, 93
Org. Synth. 1963, Coll. Vol. 4, 890
ar-TETRAHYDRO-α-NAPHTHOL

Submitted by: C. David Gutsche and Hugo H.

Peter
Checked by: John C. Sheehan, George H. Buchi,
and Dwain M. White
Published in Org. Synth. 1957, 37, 80
Org. Synth. 1963, Coll. Vol. 4, 887

TETRAHYDROTHIOPHENE

Submitted by: J. Keith Lawson, William K.

Easley, and William S. Wagner
Checked by: William S. Johnson and W. David
Wood
Published in Org. Synth. 1956, 36, 89
Org. Synth. 1963, Coll. Vol. 4, 892

69 | P a g e
 TETRALIN HYDROPEROXIDE

Submitted by: H. B. Knight and Daniel Swern

Checked by: John C. Sheehan and Curt W. Beck
Published in Org. Synth. 1954, 34, 90
Org. Synth. 1963, Coll. Vol. 4, 895

2,2,6,6-
α-TETRALONE TETRAMETHYLOLCYCLOHEXANOL

Submitted by: Cecil E. Olson, Alfred R. Bader,
and G. Dana Johnson
Checked by: James Cason, Gerhard J. Fonken,
William G. Dauben, James Cason, William G.
Dauben, Bradford H. Walker, and Charles E. Stehr
Published in Org. Synth. 1955, 35, 95
Org. Synth. 1963, Coll. Vol. 4, 898
Submitted by: Harold Wittcoff
Checked by: R. S. Schreiber, Wm. Bradley Reid,
Jr, and John L. White
Published in Org. Synth. 1951, 31, 101
Org. Synth. 1963, Coll. Vol. 4, 907

TETRAPHENYLARSONIUM CHLORIDE
HYDROCHLORIDE
β-TETRALONE
Submitted by: R. L. Shriner and Calvin N. Wolf
Submitted by: M. D. Soffer, M. P. Bellis, Hilda E.
Checked by: Cliff S. Hamilton and Yao-Hua Wu
Gellerson, and Roberta A. Stewart
Published in Org. Synth. 1950, 30, 95
Checked by: N. J. Leonard and R. C. Fox
Org. Synth. 1963, Coll. Vol. 4, 910
Published in Org. Synth. 1952, 32, 97
Org. Synth. 1963, Coll. Vol. 4, 903

70 | P a g e
 TETRAPHENYLETHYLENE

Submitted by: Robert E. Buckles and George M.

Matlack
Checked by: T. L. Cairns and C. J. Albisetti
Published in Org. Synth. 1951, 31, 104
Org. Synth. 1963, Coll. Vol. 4, 914
3-THENOIC ACID
Submitted by: E. Campaigne and William M.
LeSuer
Checked by: Charles C. Price and E. A. Dudley
Published in Org. Synth. 1953, 33, 94
Org. Synth. 1963, Coll. Vol. 4, 919

2-THENALDEHYDE

Submitted by: Arthur W. Weston and R. J.

Michaels, Jr
Checked by: Cliff S. Hamilton and Joe R. Willard
Published in Org. Synth. 1951, 31, 108
Org. Synth. 1963, Coll. Vol. 4, 915
3-THENYL BROMIDE
Submitted by: E. Campaigne and B. F. Tullar
Checked by: Charles C. Price and E. A. Dudley
Published in Org. Synth. 1953, 33, 96
Org. Synth. 1963, Coll. Vol. 4, 921

3-THENALDEHYDE

Submitted by: E. Campaigne, R. C. Bourgeois, and

W. C. McCarthy
Checked by: Charles C. Price and E. A. Dudley THIOBENZOIC ACID
Published in Org. Synth. 1953, 33, 93
Org. Synth. 1963, Coll. Vol. 4, 918 Submitted by: Paul Noble, Jr and D. S. Tarbell
71 | P a g e
Checked by: William S. Johnson and Robert A.
Kloss
Published in Org. Synth. 1952, 32, 101
Org. Synth. 1963, Coll. Vol. 4, 924
THIOBENZOPHENONE
Submitted by: B. F. Gofton and E. A. Braude
Checked by: Charles C. Price and J. Frank
Gillespie
Published in Org. Synth. 1955, 35, 97
Org. Synth. 1963, Coll. Vol. 4, 927
THIOLACETIC ACID
Submitted by: E. K. Ellingboe
Checked by: Arthur C. Cope and Malcolm
Chamberlain
Published in Org. Synth. 1951, 31, 105
Org. Synth. 1963, Coll. Vol. 4, 928
o-TOLUALDEHYDE
Submitted by: H. B. Hass and Myron L. Bender
Checked by: Arthur C. Cope and Malcolm
Chamberlain
Published in Org. Synth. 1950, 30, 99
Org. Synth. 1963, Coll. Vol. 4, 932
p-TOLUENESULFENYL CHLORIDE
Submitted by: Frederick Kurzer and J. Roy Powell
Checked by: Richard S. Schreiber and Fred Kagan
Published in Org. Synth. 1955, 35, 99
Org. Synth. 1963, Coll. Vol. 4, 934
p-TOLUENESULFINYL CHLORIDE
Submitted by: Frederick Kurzer
Checked by: Richard S. Schreiber and Fred Kagan
Published in Org. Synth. 1954, 34, 93
Org. Synth. 1963, Coll. Vol. 4, 937
p-TOLUENESULFONIC ANHYDRIDE
Submitted by: L. Field and J. W. McFarland
Checked by: William S. Johnson, Raymond R.
Hindersinn, and A. G. Fisher
Published in Org. Synth. 1956, 36, 91
Org. Synth. 1963, Coll. Vol. 4, 940
72 | P a g e
 p-
TOLYLSULFONYLMETHYLNITROSAMIDE
Submitted by: Th. J. de Boer and H. J. Backer
Checked by: James Cason, John B. Rogan, and
Wm. G. Dauben
Published in Org. Synth. 1954, 34, 96
Org. Synth. 1963, Coll. Vol. 4, 943
2,4,6-TRIBROMOBENZOIC ACID
Submitted by: Michael M. Robison and Bonnie L.
Robison
Checked by: N. J. Leonard and Kenneth Conrow
Published in Org. Synth. 1956, 36, 94
Org. Synth. 1963, Coll. Vol. 4, 947
TRICHLOROMETHYLPHOSPHONYL
DICHLORIDE
Submitted by: Kenneth C. Kennard and Cliff S.
Hamilton
Checked by: John C. Sheehan and J. L. Yeh
Published in Org. Synth. 1957, 37, 82
Org. Synth. 1963, Coll. Vol. 4, 950
p-TRICYANOVINYL-N,N-
DIMETHYLANILINE
Submitted by: B. C. McKusick and L. R. Melby
Checked by: James Cason and Ralph J. Fessenden
Published in Org. Synth. 1959, 39, 68
Org. Synth. 1963, Coll. Vol. 4, 953
73 | P a g e
 TRIETHYL PHOSPHITE

Submitted by: A. H. Ford-Moore and B. J. Perry

Checked by: William S. Johnson and James
Ackerman
Published in Org. Synth. 1951, 31, 111
Org. Synth. 1963, Coll. Vol. 4, 955
α,α,β-TRIPHENYLPROPIONITRILE

Submitted by: C. R. Hauser and W. R. Dunnavant

Checked by: Virgil Boekelheide and Donald R.
Arnold
Published in Org. Synth. 1959, 39, 73
Org. Synth. 1963, Coll. Vol. 4, 962
2,4,4-TRIMETHYLCYCLOPENTANONE

Submitted by: George D. Ryerson, Richard L.

Wasson, and Herbert O. House
Checked by: James Cason and Ralph J. Fessenden

Org. Synth. 1963, Coll. Vol. 4, 957

TRIPTYCENE

Submitted by: George Wittig

Checked by: John D. Roberts, M. C. Caserio, E. S.
Johnson, and L. Skattebøl
Published in Org. Synth. 1959, 39, 75
Org. Synth. 1963, Coll. Vol. 4, 964

α,β,β-TRIPHENYLPROPIONIC ACID

Submitted by: C. P. Krimmel, L. E. Thielen, E. A.

Brown, and W. J. Heidtke
Checked by: William S. Johnson, A. L. Wilds, and
J. S. Jellinek
Published in Org. Synth. 1953, 33, 98
Org. Synth. 1963, Coll. Vol. 4, 960

74 | P a g e
 Checked by: T. L. Cairns and D. H. Smith
Published in Org. Synth. 1952, 32, 104
Org. Synth. 1963, Coll. Vol. 4, 969

TRITHIOCARBODIGLYCOLIC ACID
VANILLIC ACID
Submitted by: R. E. Strube
Submitted by: Irwin A. Pearl and Irwin A. Pearl
Checked by: John D. Roberts and Stanley L.
Checked by: R. L. Shriner, Calvin N. Wolf, R. L.
Manatt
Shriner, and Robert C. Johnson
Published in Org. Synth. 1959, 39, 77
Published in Org. Synth. 1950, 30, 101
Org. Synth. 1963, Coll. Vol. 4, 967
Org. Synth. 1963, Coll. Vol. 4, 972

VINYL LAURATE AND OTHER VINYL

ESTERS

Submitted by: Daniel Swern and E. F. Jordan, Jr

10-UNDECYNOIC ACID Checked by: William S. Johnson and Leland J.
Chinn
Submitted by: N. A. Khan Published in Org. Synth. 1950, 30, 106
75 | P a g e
Org. Synth. 1963, Coll. Vol. 4, 977

2-VINYLTHIOPHENE

Submitted by: W. S. Emerson and T. M. Patrick, Jr

Checked by: Max Tishler, P. Tishler, and F. W.

Bollinger
Published in Org. Synth. 1958, 38, 86
Org. Synth. 1963, Coll. Vol. 4, 980

o-XYLYLENE DIBROMIDE

Submitted by: Emily F. M. Stephenson

Checked by: William S. Johnson, C. W. Taylor,
and William DeAcetis
Published in Org. Synth. 1954, 34, 100
Org. Synth. 1963, Coll. Vol. 4, 984

76 | P a g e