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PROPERTIES OF MALAYSIAN FIRED CLAY BRICKS AND THEIR

EVALUATION WITH INTERNATIONAL MASONRY SPECIFICATIONS


A CASE STUDY

ZAINAB ARMAN ALI

UNIVERSITI TEKNOLOGI MALAYSIA

PROPERTIES OF MALAYSIAN FIRED CLAY BRICKS AND THEIR


EVALUATION WITH INTERNATIONAL MASONRY SPECIFICATIONS
A CASE STUDY

ZAINAB BINTI ARMAN ALI

A thesis submitted in fulfilment of the


requirements for the award of the Degree of
Master of Engineering (Structure and Materials)

Faculty of Civil Engineering


Universiti Teknologi Malaysia

MAY 2005

iii

This thesis is dedicated to the people very dear to my heart:


my late parents, Arman Ali Hj Mohibullah and Zabedah Hamzah
my husband, Ayob Sharif
and my children
Amlina, Aliza, Alira, Afandi Akmal, Alia Atika and Arfa Adlina

iv

ACKNOWLEDGEMENTS

The author wish to acknowledge the guidance, advice and assistance


given by her supervisor, Associate Professor Dr. Faridah Shafii and to thank her
for her encouragement and friendship, without which this thesis would not be
possible. The author is also greatly thankful to her for the limitless time she spent
in helping through with the writing of the thesis.
The author would like to acknowledge the support awarded by the
Government of Malaysia under the IRPA scheme in funding this research.
Appreciation is also due to Claybricks & Tiles Sdn Berhad for its contribution in
providing the bricks used in this research.
To the staff of concrete laboratory of the Civil Engineering Faculty of
UTM, thanks are due to the technicians, Ros, Amirul and Shahrul for helping
with works in the laboratory and sampling activity at the factory. Special thanks
are conferred to dear friends at the Faculty of Civil Engineering especially Zaiton
Haron who had given the author a lot of encouragement and motivation at the
beginning of the research. The author is also grateful to Dr. Zalina Daud of the
Science Faculty of UTM for her assistance in enlightening the mathematics of
statistics and Encik Yasin for his help in the Chemistry Laboratory.
Last but not least the author would like to thank all members of her family
especially the children who had given a hand on some computations and
computer skills.

ABSTRACT

The research examined and assessed the properties of Malaysian fired clay
bricks to provide information for the development and revision of Malaysian
Standard MS 76:1972. Some laboratory investigations on bricks were conducted in
conjunction with the use of various masonry standards to evaluate the compressive
strength, dimensional tolerances, water absorption, initial rate of suction,
efflorescence, density and soluble salt content. The test methods were mostly based
on MS 76:1972 and BS 3921:1985 and in some cases new testing approaches were
adopted to assess new property requirements not catered in existing masonry
specifications. The analysis on random samples indicated the acceptance of the use
of a normal probability theory even for data with values of coefficient of variation
close to 30%. In the case where the coefficient of variation exceeded 30 % the lognormal probability function applies. The statistical control charts traced data
homogeneity for the population and data lying beyond the 5 % confidence limit,
which were not accounted for in the analysis. The compressive strengths of facing
bricks ranged from about 40 N/mm2 to 50 N/mm2 with lower values for common
bricks, i.e. 30 N/mm2 to 40 N/mm2. These ranges of compressive strengths fall in the
top range specified in Singapore Standard, SS 103:1974. The compressive strengths
specified in ASTM were based on dry curing whilst British Standard, Singapore
Standard and Malaysian Standard were tested in saturated conditions. Curing
methods affect compressive strength with air curing giving higher values. Water
absorption for the bricks under investigation range from 10 % to 12 % and therefore
do not fit in the category of Engineering A or B of MS 76:1972 and BS 3921:1985,
however satisfy the requirements for the categories of SW (severe weathering)
bricks in ASTM. The dimensions satisfy the tolerances given in BS 3921:1985
except for the height. However, the dimensional tolerance fits the T1 category of the
European Standard EN 771-1. The initial rate of suction for the bricks ranged from
1.4 to 2.0 kg/min/m2 indicating high suction property thus implying the necessity of
wetting bricks before laying. Efflorescence does not seem to be a major problem
hence these bricks could be satisfactorily used for facing construction purposes
without resulting in salt deposition on the surfaces. The range of density (1760 to
1800 kg/m3) exhibited by the bricks satisfy the sound insulation requirements
specified in the United Kingdom Building Regulations. In this research a method of
predicting the compressive strength of bricks when laid in the different orientations
was derived. This is a useful means of estimating the compressive strength of brick
in practice where test are only conducted on the bed face. The research also
highlighted a method of estimating the porosity of bricks for values of known water
absorption.

vi

ABSTRAK

Penyelidikan ini mengkaji dan menilai sifat-sifat kejuruteraan bata tanah liat
bakar negara bagi membekalkan maklumat yang diperlukan untuk pembangunan
Standard Malaysia MS 76:1972. Beberapa ujian makmal ke atas bata telah
dijalankan selaras dengan penggunaan beberapa standard masonry untuk
menganalisis kekuatan mampatan, toleransi pendimensian, penyerapan air, kadar
resapan awal, ketumpatan, kesan peroi dan kandungan garam larut. Sebahagian
besar ujian-ujian ini adalah berdasarkan kaedah MS 76:1972 dan BS 3921:1985
manakala pendekatan ujian semasa juga digunakan bagi menganalisis ciri-ciri baru
yang tidak terkandung dalam spesifikasi sedia ada. Analisis sampel yang dipilih
secara rawak menunjukkan penerimaan penggunaan teori kebarangkalian normal
walaupun untuk data di mana nilai pekali perubahan menghampiri 30 %. Bagi kes
dimana nilai pekali perubahan melebihi 30 %, fungsi kebarangkalian log-normal
digunakan. Carta kawalan statistik digunakan untuk mengesan kehomogenan data
dan data melampaui 5 % had keyakinan yang tidak diambil kira di dalam analisis.
Kekuatan mampatan bata permukaan adalah antara 40 hingga 50 N/mm2 manakala
bata biasa mempunyai nilai lebih rendah iaitu 30 hingga 40 N/mm2. Julat kekuatan
mampatan ini tergulung dalam kategori tertinggi Standard Singapura, SS 103: 1974.
Kekuatan mampatan dalam spesifikasi ASTM adalah berdasarkan bata diawet udara.
Berbeza dengan Standard British, Singapura dan Malaysia, di mana bata di uji
dalam keadaan tepu. Pengawetan udara memberikan nilai yang lebih tinggi.
Penyerapan air adalah antara 10 hingga 12 %. Nilai ini tidak menepati keperluan MS
76:1972 dan BS 3921:1985 untuk kategori bata kejuruteraan A dan B. Walau
bagaimanapun ia memenuhi syarat yang ditentukan dalam spesifikasi ASTM bagi
bata jenis SW (terdedah pada kesan cuaca yang teruk). Dimensi bata dapat
memenuhi keperluan toleransi pendimensian bagi standard BS 3921: 1985, kecuali
ketinggiannya. Di bandingkan dengan Standard Eropah EN 771-1 pula, didapati ia
menepati kategori T1. Kadar resapan awal bata ialah dari 1.4 hingga 2.0 kg/min/m2,
menunjukkan ciri resapan yang tinggi, oleh itu bata perlu dibasahkan sebelum
diikat. Bata tidak menghadapi masalah peroi, jadi ia boleh digunakan sebagai bata
permukaan tanpa berlaku pemendapan garam di permukaannya. Julat ketumpatan
bata ialah 1760 hingga 1800 kg/m3, sesuai bagi penggunaan dinding bangunan
dengan nilai rintangan kebisingan memenuhi spesifikasi kanun bangunan di United
Kingdom. Dalam penyelidikan ini kaedah untuk meramalkan kekuatan mampatan
bata apabila disusun dengan orientasi yang berlainan telah dapat dihasilkan. Kaedah
ini berguna bagi menganggarkan kekuatan mampatan bata secara praktikal dimana
ujian mampatan hanya dilakukankan di permukaan atas bata. Kajian ini juga
menerangkan kaedah menganggarkan keliangan bata daripada nilai penyerapan
airnya.

vii

TABLE OF CONTENTS

CHAPTER

TITLE

PAGE

TITLE PAGE

DECLARATION

ii

DEDICATION

iii

ACKNOWLEDGEMENT

iv

ABSTRACT

ABSTRAK

vi

TABLE OF CONTENTS

vii

LIST OF TABLES

xiii

LIST OF FIGURES

xviii

LIST OF SYMBOLS AND ABBREVIATIONS

xxi

LIST OF APPENDICES

xxii

INTRODUCTION

1.1

History and Development of Masonry

1.2

Manufacturing of Clay Bricks

1.3

Construction Requirements for Masonry and

the Needs for Specification

viii

1.4

Masonry Standardisation and International

Development
1.5

Defining the Contents for Standard

Specifications

1.6

Research Problem

1.7

Aim and Objectives of the Research

1.8

Scope of Work

1.9

Layout of Thesis

10

LITERATURE REVIEW

12

2.1

Introduction

12

2.2

Compressive Strength

12

2.2.1

Strengths Variability

12

2.2.2

Brick Strength and Masonry Strength

13

2.2.3

Effects of Brick Type and Geometry

15

2.2.4

Effects of Test Methods and

15

Measurements
2.3

Dimensional Tolerance

17

2.4

Water absorption

19

2.5

Initial Rate of Suction

22

2.6

Soluble Salt Content and Efflorescence

24

Effects
2.7

Density

24

2.8

Brick Specifications in International

26

Standards
2.8.1

Compressive Strengths

26

2.8.2

Water Absorption

28

ix

2.9

2.8.3

Initial Rate of Suction (IRS)

29

2.8.4

Dimensional Tolerance

30

2.8.5

Efflorescence

33

2.8.6

Soluble Salt Content

35

Test Methods and Measurements in

37

International Standards
2.9.1

Methods of Sampling for Tests in

37

International Standards

2.10
3

2.9.2

Compressive Strengths

38

2.9.3

Water Absorption

39

2.9.4

Initial Rate of Suction

41

2.9.5

Dimensional Tolerance

41

2.9.6

Efflorescence

42

Conclusions

LABORATORY TESTS ON PHYSICAL

49
54

PROPERTIES OF BRICKS
3.1

Introduction

54

3.2

Sampling of Bricks

54

3.3

Testing Programme

55

3.4

Dimensional Tolerance

58

3.5

Density

61

3.6

Initial Rate of Suction

63

3.7

Water Absorption (5-hours boiling test)

66

3.8

Compressive Strength

67

3.9

Soluble Salt Content

72

3.10

Efflorescence

79

x
4

STATISTICAL ANALYSIS OF TEST SPECIMENS

81

4.1

Introduction

81

4.2

General Approach for Analysing Sample

81

4.2.1

Description of Data

82

4.2.2

Histograms and Normal Distribution

84

Curve
4.2.3

Log-normal Distribution Curve

86

4.2.4

Derivation of Population Estimates

87

4.2.5

Hypothesis Testing

89

4.2.5.1

89

Analysis of Variance
(ANOVA)

4.2.5.2
4.3

Control Charts

Application of Statistical Methods for

90
93

Samples Under Investigation


4.3.1

Description and Presentation of

96

Sample Data
4.3.2

Test for Data Homogeneity

103

4.3.3

Determination of Sample Variance

105

Using the ANOVA


4.3.4
4.4

Estimates of Population Mean

Conclusions

RESULTS AND DISCUSSIONS

107
107

110

5.1

Introduction

110

5.2

Compressive Strength

110

5.3

Dimensional Tolerance

125

xi
5.3.1

Overall Dimension of 24 Bricks

125

5.3.2

Dimension of Individual Brick for

125

Length, Width and Height

5.4

Water Absorption

135

5.5

Initial Rate of Suction

138

5.6

Density

142

5.7

Efflorescence

146

5.8

Soluble Salt Content

146

APPLICATION OF RESEARCH FINDINGS


6.1

Relationship of Aspect Ratio to Compressive

148
148

Strength
6.2

Relationship of Water Absorption to Porosity

151

and Compressive Strength

CONCLUSIONS AND RECOMMENDATIONS

154

FOR FURTHER WORK


7.1

Conclusions

154

7.2

General Conclusions

154

7.3

Detailed Conclusions

155

7.3.1

Compressive Strength

155

7.3.2

Water Absorption

156

7.3.3

Dimensional Tolerance

157

7.3.4

Initial Rate of Suction

157

7.3.5

Soluble Salt Content

156

7.3.6

Density

158

xii
7.4

Recommendations for Further Work

158

REFERENCES

161

APPENDICES

165

xiii

LIST OF TABLES

TABLE
2.1

TITLE
Compressive strengths of bricks tested in different

PAGE
16

orientations (Hendry, 1997)


2.2

Aspect Ratio Factor (Ka)

17

2.3

Limits of durability indices (Surej et al., 1998)

21

2.4

Characteristic flexural strengths and levels of water

21

absorption (BS 5628 Pt. 1, 1985)


2.5

Typical sound insulation values of masonry walls

25

(Curtin et al., 1995)


2.6

Classification of bricks by compressive strength and

26

water absorption (BS 3921:1985)


2.7

Physical requirements for building bricks (ASTM C

27

62-89a, 1990)
2.8

Characteristic compressive strength in accordance to

27

Australian Standard (AS 1225:1984)


2.9

Dimensional tolerance based on measurement of 24

30

bricks and coordinating and work size in accordance to


British Standard (BS 3921:1985)
2.10

Dimensional tolerance in accordance to Australian

31

Standard (AS 1225 1984)


2.11

Dimensional tolerance of facing bricks in accordance

32

to ASTM C 216-90a (1990)


2.12

Dimensional tolerance for mean value of work size in


accordance to European Standard (prEN 771-1, 2000)

33

xiv
2.13

Dimensional tolerance for range of work size in

33

accordance to European Standard (prEN 771-1)


2.14

Classification of bricks in accordance to dimensional

33

deviation limits in Singapore Standard (SS103: 1974)


2.15

Levels of efflorescence in British Standard (BS

34

3921:1985)
2.16

Levels of efflorescence for the Australian Standard

35

(AS 1225 1984)


2.17

Levels of efflorescence in Singapore Standard

35

(SS103: 1974)
2.18

Maximum salt content for the low category (L) in

36

accordance to British Standard (BS 3921:1985)


2.19

Soluble salt content categories in accordance to

37

European Standard (prEN 771-1)


2.20

Sample size for tests in international standards

38

2.21

Comparison of water absorption from 5-hr boiling and

40

the 24-hr cold immersion tests using whole brick and


brick lumps (Khalaf and DeVenny, 2002)
2.22

Test methods and measurements for compressive

43

strength in international standards


2.23

Test methods and measurements for water absorption

44

in international standards
2.24

Test methods and measurements for initial rate of

45

suction in international standards


2.25

Test methods and measurements for dimensional

46

tolerance in international standards


2.26

Test methods and measurement for efflorescence in

48

international standards
3.1

Testing programme

56

3.2

Overall dimensions of 24 bricks

58

3.3

Individual brick measurement of length, width, and

59

height for all batches.


3.4

Density of bricks for Batch 1

62

xv
3.5

Initial rate of suction in samples for Batch 1

65

3.6

Water absorption of bricks for Batch 1

67

3.7

Compressive strength of common bricks tested on bed

70

face
3.8

Compressive strength of facing bricks tested on bed

71

face
3.9

Compressive strength of facing bricks tested on the

72

stretcher face
3.10

Compressive strength of facing bricks tested on the

72

header face.
3.11

Percentage of sulphate content in samples for all

73

batches
3.12

Standard calibration for calcium

75

3.13

Percentage of calcium in samples for all batches

76

3.14

Standard calibration for sodium and potassium

76

3.15

Percentage of potassium in samples for all batches

77

3.16

Percentage of sodium in samples for all batches

78

3.17

Standard calibration for magnesium

78

3.18

Percentage of magnesium in samples for all batches

79

4.1

Components of variance from ANOVA

90

4.2

Water absorption of specimens in each sample for

98

facing brick
4.3

Frequency distribution of data for facing bricks

99

4.4

Normal and log-normal curve fit for water absorption

100

4.5

Normal and log-normal curve fit for compressive

101

strengths of common bricks


4.6

Comparisons of 33 percentile values from normal and

103

log-normal curve for compressive strength of common


brick
4.7

Probability that x will not be exceeded

103

4.8

Sample means and ranges for water absorption

104

xvi
4.9

Control limits for means and ranges for water

104

absorption
4.10

Samples accounted for in the estimate of population

106

mean for water absorption


4.11

ANOVA and components of variance for water

106

absorption
5.1

Compressive strength of specimens in each sample for

111

facing bricks tested on bed face


5.2

Compressive strength of specimens in each sample for

112

facing bricks tested on stretcher face


5.3

Compressive strength of specimens in each sample for

112

facing bricks tested on header face


5.4

Normal curve fit for compressive strength of facing

113

bricks tested on bed and stretcher face


5.5

Log-normal curve fit for compressive strength of

114

facing brick tested on header face


5.6

ANOVA and variance components for compressive

117

strengths of facing bricks tested on bed, stretcher and


header faces
5.7

Compressive strength of facing brick when tested on

120

bed face as computed from net areas


5.8

Compressive strength of facing and common bricks

122

and standard requirements


5.9

Compressive strength of specimens in each sample for

123

common bricks
5.10

Overall measurement of length, width and height of 24

126

bricks and individual brick dimensional deviations


from work size
5.11

Dimensional deviations of brick from work size and


comparisons with values of dimensional tolerance for
BS 3921:1985 and prEN 771-1

128

xvii
5.12

Individual brick dimensions for length, width and

130

height in all samples


5.13

Mean dimensions of individual length, width and

135

height of brick compared with British Standard (BS


3921:1985)
5.14

Water absorption of specimens in each sample for

135

facing bricks
5.15

Comparison of water absorption with limits specified

137

by British Standard and ASTM


5.16

Relationship between characteristic flexural strengths

138

and levels of water absorption (BS 5628 Pt. 1)


5.17

Computed values for initial rate of suction of

139

specimens for facing bricks based on gross area of


immersion
5.18

Computed values for initial rate of suction of

142

specimens of facing bricks based on net area of


immersion
5.19

Density of specimens in each sample for facing bricks

143

5.20

Density of bricks for walls and walls with plaster finish

145

(Building regulations of the UK)


5.21

Typical sound insulation values of masonry walls

145

(Curtin et al., 1995)


5.22

Percentage of soluble salts in samples from all batches

146

6.1

Relationship between bricks compressive strength,

152

water absorption and porosity (Khalaf, 2002)

xviii

LIST OF FIGURES

FIGURES
2.1

TITLE
Mean compressive strength of walls against brick

PAGE
14

strength for 102mm thick brickwork in various mortars


2.2

Expansion of kiln-fresh bricks due to absorption of

19

moisture from atmosphere


2.3

Relationship of flexural strength of brickwork with

22

water absorption of bricks in plane of failure (a) and (c)


parallel to bed joints and (b) and (d) perpendicular to
bed joints (Morton, 1986)
3.1

Sequence of testing

56

3.2

Overall Measurement of (a) length, (b) width

60

and (c) height for 24 bricks


3.3

Apparatus for the measurement of density

63

3.4

Apparatus for measuring the initial rate of suction

65

3.5

Apparatus for water absorption test

66

3.6

Compressive machine -Tonipact 3000

69

3.7 a

Bricks tested on bed face

69

3.7 b

Bricks tested on stretcher face

69

3.7 c

Bricks tested on header face

70

3.8

A schematic diagram of an atomic absorption

74

spectrometer (Hammer, 1996)


3.9

Calibration curve for detection of calcium

75

3.10

Calibration curve for detection of sodium and

77

potassium
3.11

Calibration curve for detection of magnesium

78

xix
3.12

Efflorescence test

80

4.1

Mean, median and mode in a distribution skewed to the

84

right.
4.2

Areas under normal probability curve

88

4.3

T-distribution curves for various values of n (Chatfield,

89

1978)
4.4

Control charts for sample means and ranges (Neville,

93

1985)
4.5

Process of statistical analysis

95

4.6

Histogram, normal curve and log-normal curve, for

99

water absorption of bricks


4.7

Histogram, normal and log-normal curve for

103

compressive strength of common bricks (c.v.


approaching 30%)
4.8

Control chart for means values of water absorption

105

4.9

Control chart for ranges of water absorption.

105

5.1

Histogram, normal and log-normal curve for

115

compressive strength of facing bricks tested on (a) bed


face (b) stretcher face (c) header face
5.2

Control charts of mean values and ranges for

116

compressive strengths tested on (a) bed face (b)


stretcher face (c) header face
5.3

Relationship between compressive strength and h/t

119

ratio of bricks
5.4

Relationship between the computed compressive

121

strength (based on net loaded area of bed face) to h/t


ratio
5.5

Histogram and normal curve for compressive strength

123

of common bricks
5.6

Control charts of mean values and ranges of samples

125

for compressive strength of common bricks


5.7

Comparison of overall dimensions of (a) length (b)

127

xx
width and (c) height with allowable range of British
and Singapore Standard
5.8

Histogram and normal curve for individual dimensions

133

of length, width and height of bricks


5.9

Control charts for mean values and ranges of samples

134

for (a) length (b) width and (c) height of bricks


5.10

The histogram and the normal curve fit for water

136

absorption of bricks
5.11

Control chart of mean values and ranges of samples

137

for water absorption of bricks


5.12

Histogram and normal curve fit for IRS based on gross

140

area of immersion
5.13

Control charts for means and ranges for IRS based on

140

gross area of immersion


5.14

Histogram and normal curve fit for density of bricks

144

5.15

Control charts for mean values and ranges of samples

144

for density of bricks


6.1

Relationship between compressive strength and h/t

149

ratio of bricks
6.2

Orientations of bricks in a brick laying (a) header face

149

(b) bed face and (c) stretcher face.


6.3

Relationship of water absorption with porosity from

152

Table 6.1
6.4

Relationship of porosity with compressive strength


from Table 6.1

152

xxi

LIST OF SYMBOLS AND ABBREVIATIONS

ANOVA

analysis of variance

Mpa

Megapascals

AS

Australian Standard

ASTM

American Standard of Testing Materials

BS

British Standard

c.v.

Coefficient of variation

df

Degree of Freedom

EN

European standard

MS

Malaysian Standard

MS

Mean of Squares

Sample size

N.H.

Null Hypothesis

NZS

New Zealand Standard

Range

Sample standard deviation

SS

Sum of squares

Std. dev.

Standard deviation

Var

Variance

Coefficient of variation

Mean of sample means

Population mean

Population standard deviation

s2

Sample variance

Sample mean

xxii

LIST OF APPENDICES

APPENDIX

A1.

TITLE

Results of Tests Specimens for Dimensional

PAGE

166

Tolerance of Individual Bricks


A2.

Results of Test Specimens for Density of Bricks

170

A3.

Results of Tests Specimens for Initial Rate

175

of Suction of Bricks
A4.

Results of Tests Specimens for Water Absorption

183

of bricks
A5.

Results of Tests Specimens for Compressive

188

Strength of Bricks
B.

Statistical Tables

200

CHAPTER 1

INTRODUCTION

1.1

History and Development of Masonry


The history of civilisation is synonymous to the history of masonry. Mans

first civilisation, which started about 6000 years ago, was evident by the remains of
the Mesopotamians masonry heritage. During those days masonry buildings were
constructed from any available material at hand. The Mesopotamians used bricks,
made from alluvial deposits of the nearby River Euphrates and Tigris to build their
cities beside these two rivers. Where civilisation existed in the vicinity of mountains
or rocky outcrops, stone was used. The Egyptians pyramids that existed along the
rocky borders of the Nile valley were examples of such stone masonry. In the
Eastern civilisation remains of historical masonry is the reputed Great Wall of
China, which is considered as one of the seven construction wonders in the world.
The materials used in the construction varied from tamped earth between timbers
and adobe i.e. sun-dried bricks to local stones and kiln-fired bricks. The part of the
wall that remains until today is mainly those made of bricks and granite.
The early forms of masonry application in Malaysia dated back about 350
years ago with the construction of the Stadthuys in Malacca, built by the Dutch in
1650. A more modern form of masonry construction was initiated by the British who
colonised the then Malayan Peninsula. Brickwork buildings were at that time built
specially for government offices, quarters and residential. The administrative block,

2
Sultan Abdul Samad building built in 1894 and given a face-lift during the Fourth
Malaysian Plan (1981 1985) is an example of a masonry heritage, which stands as
a remarkable landmark of Kuala Lumpur.
In its early forms masonry structures were built without any structural
calculations. Units of masonry consisting of stones or bricks were either stacked dry
or bonded with any adhesive material to form structures and self weight being used
to stabilise the construction. The Great Wall of China for example, stood at 6.5
meters wide at the base and 5.8 meters at the top, constructed at this massive scale
mainly for stability.
With the advancement of engineering technologies and manufacturing the
development of masonry units and their applications have extended beyond the
conventional approaches and processes leading to a more efficient design and
economy. Situations where considerable lateral forces have to be resisted, the low
tensile strength of bricks could be overcome by using reinforced masonry.
Construction where greater span lengths is desired, post tensioned bricks are used,
making it possible for bricks to be used in large single cell buildings.

1.2

Manufacturing of Clay Bricks


Clay brick is the most extensively used type of masonry units throughout the

world. Its widespread use is mainly due to the availability of clay and shale in most
countries. Its durability and aesthetics appeal also contribute to its extensive
application in both load bearing and non-load bearing structures.
Manufacturing techniques for the production of clay bricks have changed
from the initially hand moulded processes to modern mechanisation. At present
bricks are formed either by the process of extrusion, moulding or dry pressing.
These advance techniques of manufacturing allow greater flexibility in its design;
with a more efficient and varied burning process a wide range of products can be
manufactured. Longer burning processes also tend to produce denser units thus

3
allowing its use for load bearing purposes. Other variations including appearance,
colours, textures, sizes and physical properties could be designed accordingly to the
type of bricks to be produced and its application.

1.3

Construction Requirements for Masonry and the Needs for Specification


Due to the varying manufacturing process and the raw materials, bricks

produced could have a wide range of variability in its appearance and physical
properties making brick a versatile building unit in construction. Bricks are of great
importance for load bearing walls in low and medium rise buildings and for nonload bearing walls as cladding for buildings. It serves several functions including
structure, fire protection, thermal and sound insulation, weather protection and
subdivision of space.
The several functions of bricks and the availability of a variety of bricks that
are able to serve the different construction requirements therefore require an
efficient and consistent guideline in achieving a safe, efficient and economical
design. This is often dictated by specifications and standards.
Load bearing brickworks, besides functioning as subdivision of space should
also have the load carrying capacity, necessary thermal and acoustics insulation as
well as fire and weather protection. Consequently, bricks in load bearing
applications should have adequate strength so that it could safely carry the loads
imposed by the structure and be able to meet the other physical requirements
specified in standards. On the other hand, non-load bearing brickworks are nonstructural, which are designed not to carry load and therefore consideration for
strength is of less importance compared to the requirements needed in load-bearing
masonry.
A damp-proof-course in brick walls at ground floor level prevent moisture
from the ground rising through the bricks and mortar and causing dampness in the
lower parts of the ground floor walls. For this reason bricks used as damp-proof-

4
course must be sufficiently impermeable and this could be ascertain through its
water absorption property.
Facial bricks are mostly produced as quality bricks with high compressive
strength and low water absorption as they can be efficiently applied as structural
bricks with aesthetics quality for use in external walls. These bricks should also
possess other physical requirements essential in good brickwork practices.

1.4

Masonry Standardisation and International Developments


The earliest standard was for weights and measures, which could be traced

back to the ancient civilisation of Babylon and early Egypt (IEEE, 2001). However,
the importance of standardisation was only fully realised until during the industrial
revolution of early nineteenth century.
As for masonry, standards had evolved through research discoveries and the
experience acquired over the years in the use of masonry. Each masonry standard is
different and unique for any country as it incorporates the national requirements. As
such the brick specifications for Australia, America, Britain differs. However, the
basic approach may be similar, to some extent. These standards were developed
more than several decades ago and used the prescriptive approach.
The trend towards globalisation requires harmonisation of standards and this
is evident with the European Standard (EN), which was established to encourage
trade between the European member states and the EN 771 became the new standard
thus setting new specifications of masonry units for Europe.

5
1.5

Defining the Contents for Standard Specifications


The international masonry standards define specifications by consideration

of the parameters described in the foregoing paragraph.


With respect to the mechanical properties of bricks, the most important is
compressive strength, which as well as being direct importance to the strength of a
wall, serves as a general index to the characteristics of the bricks. It is measured by
a standardised test, the results rely to a certain degree on the standard procedures
and conditions for testing prescribed in standards.
Bricks vary in their dimensions due to the variable shrinkage occurring
during and after manufacturing. This dimensional variability should be a minimum
in facing brickwork to ensure even joints for an aesthetically pleasant wall.
Water absorption of brick, which indicates bricks permeability, is dependent
on its porosity. Porous bricks will allow water to penetrate a wall more easily thus
contributing to problems of water seepage in masonry walls. This is an important
factor to be considered in masonry materials especially for tropical regions where
there is abundance of rain. In temperate countries, water absorption property of a
brick is used in standards in defining bricks durability in terms of its resistance to
freezing and thawing.
The initial rate of suction, which is the amount of water sucks by the brick
from mortar during laying, affects the bond between bricks and mortar in a
brickwork and is a required parameter in design of flexural walls. Optimum bond
strength could be achieved by ensuring the initial rate of suction is within the
specified limits in standards.
The other property, which is known to affect the appearance of a wall and
therefore critical in facing bricks is the effects of efflorescence. The whitish salts
deposits that appear on bricks surfaces are called efflorescence. Efflorescence is
caused by the presence of soluble salt in the bricks and water as the carrier, which
transport the salts to bricks surfaces.

6
The content of detrimental soluble salts in bricks also affects the durability of
brickwork. For example, if the amount of water-soluble sulphate exceeds the
allowable, sulphate attack will occur which will cause the disintegration of
brickwork and thus affecting its durability.
The various standards adopt different methods of measurement for
evaluating the properties of bricks. Limits may be specified to provide guidelines in
achieving satisfactory results of the final construction.
The Malaysian standard MS 76:1972 was a mere adoption of BS 3921,
excluding certain properties not relevant to Malaysian requirements, and therefore
limiting to a number of main properties only. With the advent of highly technical
manufacturing techniques and subsequently the presence of new range materials,
materials may have to be tested for additional physical and chemical properties, to
ensure its best performance after laid on construction site.
An improvement of Malaysian Standard is essential to cater with current
technical requirements and ensuring effectiveness of masonry applications. This
entailed investigations on brick properties before any recommendations could be
made on the materials and limits set to achieve satisfactory results in construction.
The research examine the various masonry specifications including
Malaysian Standard in an attempt to establish a better understanding of the various
standards and in deriving recommendations for Malaysian applications relating to
new technical requirements.

1.6

Research Problem
The development of the existing Malaysian standard MS 76:1972

(Specification for bricks and blocks of fired brickearth, clay or shale) were based on
BS 3921:Part 2:1969 (Specification for Bricks and blocks of fired brick-earth, clay
or shale). The British Standard had been revised twice, the latter versions being BS

7
3921:1974 and the existing BS 3921:1985. The revisions incorporate significant
details pertaining to material requirements and construction practices. Some of the
significant changes in existing British Standard BS 3921:1985 (British standard
specification for clay bricks) include bricks classifications, designations for
durability and new requirements on physical properties and revision of testing
methods.
The shift of British standard to European standard and eventual withdrawal
of the British Standard, therefore requires the Malaysian Standard to be revised
accordingly to suit to current market products and requirements for masonry
applications. Subsequently a research is necessary to study the various international
masonry specifications in providing a detailed understanding of the specifications
requirements, before recommendations be made to improve the existing brick
specification for Malaysia. These efforts will also facilitate the development of a
national standard capable of complying with standard global requirements.
In producing a national brick specification, data on local brick performance
are required to guide and support the new set of recommendations proposed for the
new standard.
The Malaysian Standard MS 76:1972 requires some essential amendments to
its specification to cater for present masonry application. For example, the existing
specification does not require any limit of salt content for ordinary quality facing
and common bricks, which are meant for external applications. Limits of soluble salt
content in bricks are essential as a preventive measures for salt deposition and
detrimental chemical reaction, which could damage the appearance of facial
brickwork construction. Investigation on the initial rate of suction property for
Malaysian bricks is crucial as this property, which is at present not included in the
specification, is an important criterion in structural brickwork design and
calculations.
The supplementation of data relating to local bricks performance is essential
to guide and support the new recommendations proposed for the improved
standard mentioned above.

8
1.7

Aim and Objectives of the Research


The aim of the research is to establish a detailed understanding of brick

properties through some laboratories investigations in conjunction with use of


various masonry standards to assess the material performance. The results of these
work supplemented with statistical studies and reviews of past research provides a
useful guidance to brick properties for local production. These work will also
provide data pertaining to current production of bricks which may be considered
significant to any revision or amendment made to the existing Malaysian Standard
for masonry MS 76:1972, currently under revision.
The objectives of the research are:
(i)

To conduct an experimental investigation on compressive strength,


dimensional tolerances, density, initial rate of suction, water
absorption, efflorescence and soluble salt content of facing bricks.

(ii)

To examine the compressive strength of common bricks.

(iii)

To examine the compressive strengths of bricks tested in various


orientations as recommended by Australian/New Zealand and
European standard. Thus establish the relationship between the aspect
ratio (h/t) and compressive strength of bricks.

(iv)

To study the density of bricks and its relation to acoustics properties


of masonry.

(v)

To examine the statistics of locally manufactured bricks and the


respective control charts representing the population of bricks under
study.

(vi)

To establish the relationship of water absorption, porosity and


compressive strength of bricks and to predict compressive strength
from known values of water absorption and porosity.

The studies were conducted through laboratory investigations of local bricks


and literatures establishing the state-of-the art of previous works and references to
international specification of masonry.

1.8

Scope of Work
The research is a case study, which dealt with the investigation of fired clay

facing and common bricks from a local manufacturer. The bricks were tested under
laboratory conditions as specified by the respective standards. The brick properties
examined were confined to studies on compressive strength, dimensional tolerance,
density, initial rate of suction, water absorption, efflorescence and soluble salt
content. Majority of the tests were based on the Malaysian Standard MS 76:Part 2
1972, which is basically an adoption of British Standard, BS 3921:1969. Since then
the British Standard for masonry has been revised several times to accommodate
changes for current needs.
Other standards used in the study were ASTM (American society for testing
and material), Australian/New Zealand standard, Singapore standard and European
standard. These standards formed the major references for comparisons of the
applications and methods of testing and determining the bricks properties
investigated in this programme. They form the major references for discussions in
this thesis.
Studies on bricks density are new to masonry and this was included in this
research in aligning with the new recommendations specified by the European
Standard.
The outcomes of the laboratory investigations were based on a local brick
manufacturer and therefore the results are inconclusive to suggest a representation of
the national population, however provides some guides to the properties of
Malaysian clay bricks.

10

1.9

Layout of Thesis
Chapter II describes the significance of physical and chemical properties of

bricks and its effects upon masonry behaviour. A review was conducted to examine
the various international masonry specifications, the recommended methods of
testing and measurements and comparisons between them. A considerable amount of
attention was given to the studies on masonry specifications by Malaysian Standard,
British Standard, and the Eurocode. Comparisons were also made by referring to
Australian/New Zealand Standard and ASTM. The limitations and advantages of the
various standards were highlighted and these form the basis of knowledge for the
work carried out in this thesis and where possible recommended for future standard
development.
Chapter III describes the laboratory works to identify the physical and
chemical properties of local clay bricks in providing data for Malaysian bricks. The
compressive strength, density, dimensions, water absorption, initial rate of suction,
efflorescence and salt content were investigated mainly using British Standard and
in specific cases other standards were also used. The British Standard is regarded as
the main reference used in this research as it is used widely in practice in Malaysia.
Chapter IV presents the statistical analysis of bricks properties investigated
in Chapter III. The descriptive statistics of data were computed and the graphical
distribution of data shown by histograms and normal curves. The application of
control charts was presented for testing data homogeneity. The analysis of variance,
ANOVA was used to derive the components of variances in samples, which in turn
will be used to calculate the bricks population mean.
Chapter V presents the experimental and statistical results for the bricks
properties investigated in the programme. The results for every parameter were
discussed and compared to previous research works and specification requirements
set by existing international standards.

11
Chapter VI presents a method of predicting compressive strength and
porosity properties of bricks based on the findings of work carried out in this thesis.
Chapter VII presents the conclusions of the works and recommendations for
future studies.

CHAPTER 2

LITERATURE REVIEW

2.1

Introduction
The properties of bricks affect the appearance and the quality of masonry

construction. Therefore, emphasis has been given by codes and standards to specify
the properties of units and component materials, in order to achieve the designated
durability, quality and strength.
This chapter presents works conducted on bricks for specifications
development and standardisations. Evaluation of bricks made on compressive
strengths, absorption properties, initial rate of suction, dimensional deviations,
efflorescence effects, soluble salt content and density i.e. the parameters contributing
to specification development.

2.2

Compressive Strength

2.2.1

Strengths Variability
The compressive strengths of bricks vary considerably with the material used

in manufacturing and the duration and degree of burning. Bricks compressive

13
strengths can be defined into three levels i.e. the high strength engineering bricks
with compressive strength ranging from 55 to 69 N/mm2, the medium strength
bricks range from 27 to 48 N/mm2 and the low strength brick range from
approximately 14 to 25 N/mm2 (Lenczner, 1972). Due to these considerable
variations, strengths of bricks are classified accordingly to its application in
construction. Bricks with compressive strengths of approximately 5 N/mm2 are
sufficient for the construction of low-rise buildings like dwelling houses
(Hendry et al., 1981). For high-rise structures, engineering bricks and those of high
compressive strengths should be used (Hendry, 2001).
The compressive strengths of bricks were associated with materials and
manufacturing features as highlighted by Grimm (1975). Additionally, the
compressive strength can be generally higher for the following cases:

2.2.2

Units made of shale by the stiff mud process

Burned at high temperatures

Cored less than 35% of its gross area with no sharp re-entrant corners

Units with small heights

Brick Strength and Masonry Strength


Compressive strength of a brick is important as an indicator of masonry

strength and as a result, brick strength has become an important requirement in


brickwork design. A considerable amount of past research and studies on masonry
(Hendry, 1990, Lenczner, 1972, Sahlin, 1971,) indicated that stronger bricks
contribute to greater brickwork strength.
Brickwork is strongest in compression and research shows that the
compressive behaviour of brickwork depends on the strength of brick and mortar.
However there is no suggestion of a direct relationship between the individual
component strength and the resultant masonry strength. The complex nature of

14
analysis for masonry (composite material) contributes to the difficulties in
establishing such relationship.
Some existing work based on the analysis of experimental data conducted on
102.5 mm and 215 mm thick walls (Hendry and Malek, 1990) showed that the
compressive strength of walls (f) could be estimated by the following equations:

For wall thickness of 102.5 mm

f = 1.242 f b

0.531

For wall thickness of 215.0 mm

f = 0.334 fb

0.778

fm

fm

0.208

0.234

(2.1)

(2.2)

Where,
fb and fm are the brick and mortar compressive strengths respectively.
Equations 2.1 and 2.2 were represented graphically as shown in Figure 2.1
(Hendry, 1990) and has been used as a basis for estimation in design codes for

Compressive strength of wall


(N/mm2)

masonry, BS 5628 Part 1: 1985: Structural use of unreinforced masonry.

30
25

1:1/4:3 mortar
1:1/2:41/2 mortar
1:1:6 mortar
1:2:9 mortar

20
15
10
5
0
0

20

40

60

80

100

120

Compressive strength of brick (N/mm )

Figure 2.1: Mean compressive strength of walls against brick strength for
102mm thick brickwork in various mortars (Hendry, 1990).
Brickwork strength can also be estimated by other simple relationship with
unit strength. Hendry et al. (1996) proposed that the compressive strength of
brickwork could be approximated to the square root of unit strength and to the third

15
or fourth root of the mortar cube strength. The Brick Development Association of
UK (1974) relates bricks with compressive strength of 35 N/mm2 to wall strength,
with a ratio of 0.3 to 0.35:1.

2.2.3

Effects of Brick Type and Geometry


The type and geometry of bricks whether solid, perforated, or hollow have

an effect on the compressive strength of masonry. Hendry (1990) reported an earlier


findings done by Schellbach (1971) on the compressive strengths of highly
perforated units, and reported that the highest ratio of masonry strength to brick
strength was obtained for bricks with perforation ratio of 38-43 %. Hendry (1990)
highlighted that holes of round shape or slots with round corners have no
distinguished effects on compressive strengths of brickwork, Conversely, a decrease
in compressive strengths of brickwork were observed for bricks with cores of
rectangular slots. Rectangular slots tend to initiate shear failure.

2.2.4

Effects of Test Methods and Measurements


The compressive strengths of brick are measured by loading bricks in

compression. Conventional tests require bricks to be loaded normal to its bed face
and the faces are capped or packed before testing to reduce the effects of roughness,
lack of plane and platen effects. Different materials could be used for packing or
capping. Malaysia/British Standard recommended soft capping using sheets of
plywood between loaded surfaces of bricks specimen. On the other hand, ASTM
specifies the use of hard capping consisting of either a thin layer of molten sulphur
compound or a gypsum plaster compound. Soft packing has the advantage of a
reduction in the time of preparation for testing and it has occasionally been claimed
that soft capping produced a more representative strength than hard capping
(Drysdale et al., 1994). Grimm (1975) highlighted that if a brick specimen is
unrestrained through the insertion of a teflon pad between brick and machine head

16
the compressive strength of the unit is further reduced. This is due to reduction in
effects of the machine platen.
Besides the influence of platen restraint and capping material, the
compressive strengths of bricks are also affected by the orientation of the specimen
during testing. Bricks tested on its bed, edge and end would give different
compressive strengths due to the different heights of the specimen. The platen effect
on the brick will be reduced with increase in height subsequently decrease its
compressive strength. Table 2.1 shows the work reported by Hendry (1997) on the
compressive strengths of bricks when tested in different orientations. Maximum
strength was achieved when tested on bed whilst minimum strength was obtained
when tested on end. Considerations for this shape factor are given its importance in
the European Standard prEN 771-1, which requires bricks compressive strength to
be declared with the intended orientation for testing.
Table 2.1:

Compressive strengths of bricks tested in different


orientations (Hendry, 1997)

Brick type

Tested
On bed

On edge

On end

14 hole

74.3

26.2

10.4

10 hole

70.2

29.5

21.7

3 hole

82.0

53.2

40.2

5 slots

64.1

51.8

13.8

The influence on the shape factors was considered in the Australian Standard
AS/NZS 4456.4:1997, Masonry units and segmental pavers- Methods of tests. In
this standard, the compressive strength of brick is multiplied with a factor called the
aspect ratio factor, Ka which depends on the height to thickness ratio, to provide the
unconfined compressive strength. The unconfined compressive strength is given by
equation 2.3.

C = Ka

1000 P
A

Where,
C = unconfined strengths in megapascals.

(2.3)

17
P = total load at which the specimen fails in Kn.
A = net area in mm2
Ka = aspect ratio factor (Table 2.2)
Table 2.2:

Aspect Ratio Factor (Ka)

Height to thickness ratio

0.4

1.0

5.0 or more

Aspect Ratio Factor (Ka)

0.5

0.7

1.0

The curing of bricks specimen before testing also affects the compressive
strength of brick. Wet bricks tend to show lower strengths than dry ones. Grimm
(1975) reported that dry brick can be 15% stronger than wet ones.

2.3

Dimensional Tolerance
Fired clay bricks vary in size due to the varying property of natural clay and

variations in the manufacturing drying and firing conditions. The total variations,
which may take place due to variable shrinkage properties of clay during and after
manufacturing can account to approximately 5 to 15 % of original dimensions. Due
to the presence of this wide range of variability, dimensional tolerances are specified
in standards to achieve the desired dimensional consistency. This is important in
brickwork because it has been proven from research and observations that
dimensional variation would affect brickwork aesthetically as well as structurally
Bricks dimension should not vary more than the tolerance specified in
standards. Limits for dimensional tolerance is specified in facing brickwork to
ensure that sizes of bricks do not differ too much as to affect the appearance of a
wall. This is especially important for very short length walls and piers. Besides this,
research has also shown that careful control of dimensions would markedly increase
the speed of brick laying (Haller, 1964).

18
Previous research on masonry has shown that units with low dimensional
variation will produce a wall of higher compressive strengths. The use of bricks with
well-controlled dimensions is also essential for high strength brickworks since
brickwork with non-uniform joint thickness would be subjected to bending moments
and stress concentration. According to Grimm (1975), the compressive strength of
relatively short brick masonry prisms, built from conventional materials which were
concentrically loaded and tested in accordance to ASTM E477 (7) may be predicted
from the following equation:
f m' = 1.42 f b'108 ( f c2 + 9.45 106 )(1 + ) 1

(2.4)

Where,
f m' = compressive strength of brickwork masonry prism
fb' = compressive strength of brick

= prism slenderness ratio


= material size factor
= workmanship factor and this factor depend upon the verticality of the
wall, dimensional variation and quality of mortar joints. For good
workmanship,

= 0.
It is evident from equation 2.4 that the dimensional variation constitutes the
workmanship factor, affects the compressive strength of brickwork.
Quality control measures during manufacturing are important to ensure that
bricks dimensions are within limits specified in standards. One of the causes for
variation lies partly with the mould and wearing of dies. Moisture movement within
the brick can also contribute to size variations after manufacturing. Clay bricks tend
to expand as they pick up moisture after being unloaded from the kilns. The
magnitude of this movement varies accordingly to types of bricks and brick firing
temperatures. About half of the expansion occurs within a few days after
manufacturing and the remainder gradually stabilised after a few months (Fig.2.2).

19
Therefore, generally bricks are only taken to the site two weeks after coming out
from the kilns.

Expansion

Maximum Expansion

0 1

Figure 2.2:

Days

100

Expansion of kiln-fresh bricks due to absorption of


moisture from atmosphere. (Hendry et al., 1997)

2.4

Water Absorption
Water absorption of a brick is defined as the weight of water in a brick

expressed as a percentage of the bricks dry weight. It varies roughly from 4.5 to 21
% and the variation is mainly due to the variable raw material and the manufacturing
process.
The extrusion process in the manufacturing produces denser brick in
comparisons to the moulded bricks and denser bricks in turn would exhibit less
absorption. This was proven through experiments (Sahlin, 1971), which showed that
extruded bricks contain small percentage of voids and therefore are less absorbent to
water.
The effects of bricks absorption property due to variable raw material used in
its manufacturing was shown by Surej et al. (1998) who reported the work carried
out by Kung (1987) on the effects of raw material to water absorption. The report
showed that within the normal brick firing temperature range, the water absorption

20
and the porosity of the burnt bricks increases with increasing calcium carbonate or
limestone content in the raw materials.
Water absorption of bricks is usually measured by the 5-hours boiling and
24-hours cold immersion test. The 24-hours cold immersion test allows water to be
absorbed into pores, which are easily filled under cold condition while the 5 hours
boiling test gives fully saturated condition where all pores are filled up with water.
The ratio of 24 hours cold immersion to maximum absorption in vacuum or
boiling (C/B ratio) gives the saturation coefficient, which is used to indicate bricks
durability. The saturation coefficient, which is actually a measure of the relative
open pore space present in brick is crucial during freeze-thaw action to
accommodate the volume change in water as it freezes. The saturation coefficient
ranges from about 0.4 to 0.95, the lower value of around 0.4 indicates high
durability and higher values of around 0.95, low durability (F. M. Khalaf and A. S.
De Venny, 2002).
Other durability indices have also been developed based on relationship of
porosity and water absorption. Table 2.3 shows the durability indices developed by
Surej et al. (1998). Theses durability indices, which are a function of porosity and
water absorption of bricks is shown in equation 2.5 and 2.6. DIAP(C) and DIAP(S)
refers to durability index based on absorption properties derived from the cold
immersion absorption property and the suction property respectively.

DIAP(C ) =

450.70
C1

+ 387.98 0.87
(2.94 + B )
B

(2.5)

DIAP( S ) =

450.70
S4

+ 329.81 0.97

(2.94 + B )
B

(2.6)

Where,
B is the absorption due to 5-hr. boiling.
C1 is the absorption due to 1-hr.immersion absorption.
S4 is the 4-hr. capillary suction achieved through similar test as in the initial
rate of suction.

21

Table 2.3:

Limits of durability indices (Surej et al., 1998)


Limiting Values

Index

Durable

Non-durable

DIAP(C)

>90

<75

DIAP(S)

>85

<70

Studies on the effects of water absorption to structural performance of fired


clay masonry shows that water absorption of masonry units has a relation with
flexural behaviour of masonry. Research carried out by the British Ceramic
Research Association on test wallettes to study the relationship of flexural strength
of brickwork and water absorption of bricks has derived the relationship between
flexural strength and water absorption (Figure 2.3). The curved line indicated in
brown is the 95 % confidence limit and this was approximated to the stepped line,
which relates to three levels of water absorption i.e. less than 7%, 7% to 12% and
beyond12% to the respective values of characteristic flexural strengths. These limits
of water absorption associated with the flexural strength of brickwork are used in BS
5628: Part 1 for design of laterally loaded walls (Table 2.4).
Table 2.4:

Characteristic flexural strengths and levels of


water absorption (BS 5628 Pt. 1, 1985)
Characteristic flexural strength, fkx N/mm2

Mortar designation
Clay bricks having a water
absorption less than 7%
Between 7 % and 12 %
Over 12 %

Plane of failure parallel


to bed joints
(i)
(ii) and
(iv)
(iii)

Plane of failure perpendicular


to bed joints
(i)
(ii) and
(iv)
(iii)

0.7

0.5

0.4

2.0

1.5

1.2

0.5

0.4

0.35

1.5

1.1

1.0

0.4

0.3

0.25

1.1

0.9

0.8

22

Flexural strength N/mm

Flexural strength N/mm2

BS Mortar
Designation (i) 1 : : 3

1.5
1
0.5
0
0

10

20

4
3
2
1
0
0

30

10

20

30

Water absorption %

Water absorption %

(a)

(b)

Flexural strength N/mm

Flexural strength N/mm

BS Mortar
Designation (iii) 1 : 1 : 6

1.5
1
0.5
0
0

10

20

Water absorption %

30

4
3
2
1
0
0

10

30

Water absorption %

(c)
Figure 2.3

20

(d)

Relationship of flexural strength of brickwork with water


absorption of bricks in plane of failure (a) and (c) parallel to bed
joints and (b) and (d) perpendicular to bed joints (Morton, 1986)

2.5

Initial Rate of Suction


The initial rate of suction (IRS) denotes the amount of water sucked by the

brick upon contact with mortar during laying. The IRS, resulting from the presence
of capillary mechanism of the small pores in the bricks, is an important property in a
masonry construction since it affects the bond strength between the brick and mortar
thus affecting water tightness and durability of masonry.

23
Bricks with IRS less than 0.25 kg/m2.min can be considered as low suction
bricks whilst bricks with IRS more than 1.5 kg/m2.min can be regarded as high
suction bricks (Drysdale et al., 1994). Tests have indicated that IRS values between
0.25 to 1.5 kg/m2.min generally produce good bond strength when used with the
appropriate mortar designations. High suction bricks absorb water from the mortar
rapidly thus impairing bond properties. This water is needed for the proper hydration
of cement where the mortar contacts the brick. On the other hand, low suction bricks
do not absorb much water and hence the surplus water will float on to the surface of
mortar to result in poor initial and final bonding strength. However, recent tests to
evaluate the bond strength and water penetration of masonry built with low IRS
brick, demonstrated that flexural bond strength of very low IRS brick (less than 0.25
kg/m2.min) can equal or exceed those of higher IRA brick with proper selection of
mortar materials and type (BIA, 2001).
The initial rate of suction (IRS) is determined by the amount of water
absorbed through the bed face when immersed in 3mm depth of water for a period of
1 minute. The British Standard recognises the IRS as a crucial requirement for
highly stressed masonry and a test method to determine IRS is given in the appendix
of BS 3921:1985. However, no limit for IRS has been specified. On the other hand,
ASTM, gives guidance on limits for IRS. It recommends that bricks with IRS
greater than 30g/min per 30 in2 (equivalent to about 1.5 kg/ m2.min) should be
wetted prior to laying.
Wetting of bricks before laying are more vital for construction in hot weather
especially for highly absorptive bricks. However, the wetting of bricks has its
shortcoming. The bricks will have variable degree of wetness giving rise to variable
compatibility with mortar (Drysdale et al., 1994).

24
2.6

Soluble Salts Content and Efflorescence Effects


All clay bricks contain soluble salts originating from raw clay deposits. In a

brickwork, salts may also originate from mortar or drawn up from the ground.
Efflorescence, which is the white deposition of salts on bricks surfaces, occurs due
to the presence of these salts carried by water to the brick surfaces.
Salts leading to efflorescence are mostly sulphates of sodium, potassium,
magnesium and calcium salts. Efflorescence usually occurs in new constructions and
takes place when water-carrying salts evaporates leaving the salts depositions on
masonry surfaces. The dissolved salts in crystalline form lead to visible white stains
on surfaces but are normally harmless. However, in extreme cases, crystallisation
may take place within the brick causing internal stresses and leading to spalling and
cracking (Hendry et al., 1997).
Sulphate action occurs when water carries sulphate from bricks into mortar,
containing tricalcium aluminate, one of the constituents of Portland cement and
hydraulic lime. This reaction causes mortar to expand, causing cracking or spalling
of mortar joints and occasionally spalling of facing bricks. Hendry (1981) suggested
a limit for sodium sulphate content in bricks, which should not exceed 3% by weight
of a brick in order to avoid spalling and disruption of bricks surface.

2.7

Density
Raw materials and manufacturing process affects bricks density, which could

vary between 1300 kg/m3 to 2200 kg/m3. The density of bricks influences the weight
of walls and the variation in weight have implications on structural, acoustical and
thermal design of the wall. Incorrect assumptions on wall weight can result in
inaccurate dead loads and seismic loads, reduced factor of safety in shear walls and
overestimate of acoustical transmission loss (Grimm, 1996)

25
For acoustical design the sound resistance of a solid masonry wall is related
principally to its weight; the heavier the wall the less is the noise transmitted through
it. Typical sound insulation values for a 102.5 mm and 215 mm thick wall is shown
in Table 2.5. Loudness of 45 dB 50 dB is considered as moderate loudness
suitable for average home and general office (Drysdale et al., 1994).
Table 2.5:

Typical sound insulation values of masonry walls


(Curtin et al., 1995)

Material and construction

Thickness
(mm)

Weight
(kg/m2)

Approximate sound
reduction index
(dB)

Brick wall plastered both


sides with a minimum of
12.5 mm thick plaster

215

415

49.5

102.5

220

46

Brick wall plastered both


sides with a minimum of
12.5 mm thick plaster

In most existing standards for clay bricks density was not included as
requirements for standardisations. However, in the recent European Standard prEN
771-1: Specifications for clay masonry units, requirements for density should be
declared by the manufacturer for acoustic purposes. The specified tolerances for
density of test samples are graded as D1 and D2 with difference of 10% and 5%
respectively from the manufacturers declared values. The declared values may also
be intended for the calculation of load assumptions and thermal insulation.
One of the main functions of a wall is to provide some degree of thermal
insulation between the exterior and interior environments. Thermal considerations
for buildings include the comfort of users and the energy requirements of heating
and air conditioning equipment. Brickwork has relatively low resistance to thermal
effects, which means that brick is a good conductor of heat. Thermal resistance of
wall increases with the decrease in the density of the materials; hence, a walls
thermal resistance is increased by using bricks made of less dense or aerated
materials.

26
However, brick as a high mass building material has the inherent energy
saving features of thermal storage, which means that they are slow to heat up and
slow to cool down. This thermal inertia or thermal storage of brickwork is affected
considerably by its mass, which depended on the density of brick and therefore its
importance in the design load for both heating and cooling.

2.8

Bricks Specifications in International Standards


This section deals with the comparisons of bricks specifications for existing

standards, namely, British Standard (BS), American Standard (ASTM), Australian /


New Zealand Standard (AS/NZS), European Standard (EN) and Singapore Standard
(SS). Malaysian Standard (MS), which is adopted from the earlier version of the
British Standard, was also reviewed. The comparisons is aimed at developing a
better understanding on the way each parameter is being treated for standardisations
in accordance to a particular countrys requirements.

2.8.1

Compressive Strengths
The British Standard (BS 3921:1985) categorised compressive strengths into

classes of Engineering A and B (Table 2.6). These classifications of bricks are


commonly used for construction with aesthetics and strength requirements. All other
bricks and the damp proof-course bricks should have strengths not less than 5
N/mm2, however, the damp-proof course is divided into 2 in accordance to water
absorption.

27
Table 2.6:

Classification of bricks by compressive strength and water


absorption (BS 3921:1985)

Class

Average compressive
strength (N/mm2)

Water absorption (5-hr.


boiling) % by weight

Engineering A
Engineering B
Damp-proof course 1
Damp-proof course 2
All others

70
50
5
5
5

4.5
7.0
4.5
7.0
No limits

In the American Standards (ASTM), compressive strengths are classified in


accordance to the different grades of weathering and exposure conditions as
indicated in Table 2.7. The grades of weathering can be either negligible (NW),
moderate (MW) or severe (SW) depending on the map zoning as given in ASTM.
Table 2.7:

Physical requirements for building bricks (ASTM C 6289a, 1990)

Minimum compressive
strengths brick flat wise
lb/in2 (N/mm2)
Average of Individual
5 bricks

Maximum water
absorption (5-hr.
boiling), %
Average
Individual
of 5 bricks

Maximum saturation
coefficient
Average
of 5 bricks

Individual

Grade SW

3000(20.7)

2500(17.2)

17.0

20.0

0.78

0.80

Grade MW

2500(17.2)

2200(15.2)

22.0

25.0

0.88

0.90

Grade NW

1500(10.3)

1250(8.6)

No limit

No limit

No Limit

No limit

Designation

Similar requirements of compressive strengths are given for Facing (ASTM


C 216 90a) and Hollow Bricks(ASTM C 652 89a) in the category of Grade SW
and MW. However, there is no category for Grade NW in both Facing and Hollow
Bricks.
In the Australian Standard (AS 1225 1984) the characteristics compressive
strength is specified, against values for the ratio of manufacturing height to
manufacturing width (Table 2.8).

28
Table 2.8:

Characteristic compressive strength in accordance to


Australian Standard (AS 1225:1984)

Ratio of manufacturing height to


manufacturing width

Characteristics compressive
strength, MPa

0.7
2

7.0
5.0

In Singapore Standard (SS 103:1974) compressive strengths are classified as


First, Second and Third Grade with minimum compressive strength of 35 N/mm2, 20
N/mm2 and 5.2 N/ mm2 respectively.
It can be seen from the comparisons that the British Standard specified
stringent limits than the ASTM. A minimum compressive strength of 70 and 50
N/mm2 respectively for Engineering A and B was specified in the British Standard.
Whereas, in ASTM the minimum compressive strength specified for structural
facing bricks were 20.7 and 17.2 N/mm2 for Grade SW and MW bricks respectively.
On the other hand, the minimum specification for building bricks in ASTM for
structural or non structural use is higher, i.e. a minimum value of 10.3 N/mm2. The
BS specifies a value of 5 N/mm2. Likewise, a stringent water absorption limit of
minimum 4.5% was found in BS compared to a minimum of 17% in ASTM.

2.8.2

Water Absorption
The BS 3921:1985 defines the limits of water absorption in order to

categorise engineering bricks and bricks for damp-proof course (Table 2.6). The
standard specifies a low water absorption ( 4.5 %) to classify Engineering A bricks
and bricks for damp-proof course 1; higher water absorption ( 7.0 %) to classify
Engineering B bricks and bricks for damp-proof course 2. There is no limit of water
absorption for all other types of bricks.
Similarly, ASTM relates compressive strengths to water absorption but with
an additional parameter, the saturation coefficient (Table 2.7). However, the water

29
absorption limits in ASTM were less stringent than the BS. The limits given for the
designation of SW and MW are equal for all three types of bricks: Building, Facing
and Hollow. The maximum water absorption limits are given for the average of five
bricks and for individual bricks. For SW bricks the maximum water absorption
specified are 17 % while the MW bricks are 22 %. No water absorption limits are
required for the grade NW bricks.
On the contrarily, the Australian Standard (AS 1225 1984) which was set
up as a basic standard specifies the properties common to most bricks and put no
limit to the water absorption properties as well as the initial rate of suction.
However, it was mentioned in the standard that if the need arises such requirements
should be provided by the purchasers.
Singapore standard (SS 103:1974) specifies some general requirements for
water absorption. The water absorption is limited to 25 % for common bricks, and
no requirement is set for facing bricks. This is probably due to the reason that
brickwork being widely used as infill walls there, which do not require structural or
facing bricks and therefore the water absorption is not critical.
On similar trend with the Australian Standard, water absorption was not
considered as a basic requirement for product description and designation in
European Standard prEN 771-1. Requirements for water absorption will depend on
its relevance in construction and in this case, the limits are to be declared by the
manufacturers.

2.8.3

Initial Rate of Suction (IRS)


British Standard BS 3921:1985 does not specify any limit for IRS. However,

a test method for determining this value is included in Appendix H of the standard.

30
ASTM specified that bricks to be tested for IRS, if the value exceeded
1.5 kg/ m2.min in which case for applications, bricks are to be wetted. The European
Standard prEN 771-1 does not specify any limits for IRS but these values will have
to be declared by manufacturers when relevant to the uses for which the unit is put
on the market. The mean IRS of the sample tested should fall within the range of the
declared values.
The Australian Standard does not specify any requirements for IRS, however
a test method to determine IRS is provided in AS/NZS 4456. Singapore Standard
SS 103:1974 and Malaysian Standard MS 76:1972 specifies no requirement at all on
IRS since both standards were developed using BS 3921:1969 as reference whereby
the initial rate of suction was not accounted for.

2.8.4

Dimensional Tolerance
Sizes and tolerance specified by the British Standard BS 3921:1985 are

meant only for the 225 mm 112.5 mm 75 mm format bricks. Requirements for
other bricks format are given in separate standards such as BS 4729(special shapes).
In BS 3921:1985, dimensional tolerance is measured by the deviations in the
overall length, width and height based on 24 bricks (Table 2.9). In addition,
individual brick dimension should not exceed the coordinating size for length, width
and height. Coordinating size is the work size including the allowance for mortar
joints and tolerances and work size is the manufactured size. The overall
measurement is based on the expectation that individual brick dimension should not
differ from the work size by more than 6.4 mm for length whilst 4.0 mm for both
width and height.

31
Table 2.9:

Dimensional tolerance based on measurement of 24 bricks


and coordinating and work size in accordance to British
Standard (BS 3921:1985)

Coordinating
size
mm
225
112.5
75

Work size

Overall measurement of 24 bricks

mm
215
102.5
65

Maximum (mm)
5235
2505
1605

Minimum (mm)
5085
2415
1515

Dimensional variations are used in the Australian Standard (AS 125 1984)
to classify the categories of bricks. The categories are as follows:
ST0 bricks not required to be precise in dimensions
ST2 bricks manufactured to finer tolerances for special applications.
ST3 bricks where regularity in size is necessary
Limits in dimensional tolerance (Table 2.10) for each of these categories are
based on the variations of length, width and height of 20 bricks for the respective
dimensions. In addition, the length shall not be less than 1.5 times the width or not
exceeding 390 mm. The height shall not be greater than 70 percent of the length.
Table 2.10:

Dimensional tolerance in accordance to Australian


Standard (AS 1225 1984)
Dimensional tolerance of 20 bricks

Size Category

ST0
ST2
ST3

Length

Width

Height

90 mm
40 mm
60 mm

50 mm
25 mm
40 mm

50mm
25 mm
40 mm

General criteria for dimensions and proportions


(a) Length not less than 1.5 times width nor more than 390mm
(b) Height shall not be greater than 70 percent of length.

Tolerance on dimensions specified by ASTM is based on a sample of 10


bricks and each brick should not lie outside the tolerance limits given in the
respective standards for Facing, Hollow and Building bricks. Table 2.11 shows the
tolerance limits for facing bricks. Unlike the British Standard, variations in

32
dimensions are not given in terms of length, width and height but are specified with
respect to some intervals of dimensions. Dimensional variations for facing and
hollow bricks are classified into categories defined by usage, exposure and
architectural requirements corresponding to Type FBX and FBS. In addition, the
facing and hollow bricks are also required to satisfy the tolerances on distortion and
out of square.
Table 2.11:

Dimensional tolerance of facing bricks in


accordance to ASTM C 216-90a (1990)

Specified dimensions,
(mm)

76 and under
76 to 102, incl.
102 to 152, incl.
152 to 203, incl.
203 to 305, incl.
305 to 406, incl.

Maximum permissible variation from


specified dimension, plus or minus (mm)
Type FBX

Type FBS

1.6
2.4
3.2
4.0
5.6
7.1

2.4
3.2
4.7
6.4
7.9
9.5

Note:
FBX: Brick for general use in exposed exterior and interior walls where a
high degree of mechanical perfection, narrow colour range and minimum
permissible variation in size are required.
FBS: Brick for general use in exposed exterior and interior masonry walls
where wider colour ranges and greater variation in sizes are permitted than
are specified for type FBX.
In European Standard prEN 771-1, the dimensional tolerances are specified
under three categories i.e. T1, T2 and T0 and the respective tolerances for each
category are to be computed using the formula, which depends on the work size
dimensions (Table 2.12). The mean values for all dimensions i.e. the length, width
and height in a sample of 10 bricks should not exceed the declared values by the
respective tolerance in the category. In addition, for works, which require acoustical
property, dimensional tolerance in terms of the range values from a measurement of
10 bricks in a sample should be within the categories given in Table 2.13.

33
Table 2.12:

Dimensional tolerance for mean value of work size in


accordance to European Standard (prEN 771-1, 2000)

Category

Tolerance

T1

0.40 (work size dimension) mm or 3mm whichever is greater

T2

0.25 (work size dimension) mm or 2mm whichever is greater

T0

A deviation in mm declared by the manufacturer

Table 2.13:

Dimensional tolerance for range of work size in


accordance to European Standard (prEN 771-1)

Category

Maximum range

R1

0.6 (work size dimension) mm

R2

0.3 (work size dimension) mm

R0

A range in mm declared by the manufacturer

In Singapore Standard (SS 103: 1974) the dimensional tolerance are


categorised as First, Second and Third Grade in accordance to the dimensional
deviations of the overall measurements of length, width and height of 24 bricks
respectively (Table 2.14).
Table 2.14: Classification of bricks in accordance to dimensional deviation
limits in Singapore Standard (SS 103: 1974)
Overall measurements of 24 bricks (mm)
First Grade

Second Grade

Third Grade

Width

5085 to 5235
2415 to 2505

5280 to 5472
2445 to 2580

Height

1530 to 1620

1704 to 1800

Bricks satisfying all other


requirements but having
dimensions and compressive
strength outside First Grade and
Second Grade.

Length

34
2.8.5

Efflorescence
In the British Standard, the levels of efflorescence of bricks are categorised

either as slight, moderate and heavy (Table 2.15). Bricks showing efflorescence in
the heavy category is considered as not complying with the standard. An evaluation
for efflorescence is based on the visual examination of 10 specimens in a sample,
tested in accordance to Appendix C of BS 3921:1985. Slight efflorescence refers to
bricks with up to 10 % of its surface area contaminated with salts and more than 10
% but not exceeding 50 % are categorised as moderate whilst heavy category refers
to bricks with more than 50 % of its surface area affected. In addition, the heavy
category of efflorescence is accompanied by powdering and flaking of the surface.
Table 2.15:

Levels of efflorescence in British Standard (BS3921: 1985)

Nil

No perceptible deposit of salt

Slight

Up to 10% of the area of the face covered with a deposit of salt, but
unaccompanied by powdering or flaking of the surface.

Moderate

More than 10% but not more than 50% of the area of the face covered
with a deposit of salts but unaccompanied by powdering or flaking of
the surface.

Heavy

More than 50% of the area of the face covered with a deposit of salts
and/or powdering or flaking of the surface.

In ASTM requirements for efflorescence is meant only for facing and hollow
bricks. The test method and rating based on 5 pairs of bricks are given in ASTM C
67 90a. The bricks are rated as effloresced if perceptible differences are noted and
otherwise. The standard requires bricks of rating not effloresced.
In the Australian Standard (AS 1225 1984) the level of efflorescence for
brickwork constructed for appearance should not exceed the limits defined by the
slight category (Table 2.16). The classification is based on the worst case of
efflorescence category occurring in the 5 pairs of bricks tested.

35

Table 2.16:

Levels of efflorescence for the Australian Standard


(AS 1225 1984)

Nil
Slight

Moderate

No observable efflorescence
Not more than 10% of the total external above-water surface
covered by a deposit of salts.
More than 10% of one external above-water surface but not
more than 50% of the total external above-water surface
covered by a deposit of salts.

Heavy

A deposit of salts covering more than 50% of the total


external above-water surface.

Severe

Any efflorescence that is accompanied by powdering or


flaking of the surface of the specimen.

The Singapore standard specifies level of efflorescence similar to the British


standard, however with the addition of another category designated, Serious. This
level refers to cases where a heavy deposit of salts, accompanied by powdering
and/or flaking of the surface and tending to increase with repeated wetting of the
specimen. Facing bricks and common bricks should not exceed the conditions stated
for slight and the moderate efflorescence (Table 2.17).
Table 2.17:

Levels of efflorescence in Singapore Standard


(SS 103:1974)

Nil

No perceptible deposit of salt

Slight

Not more than 10% of the area of the face covered with a
thin deposit of salt.

Moderate

A heavier deposit than slight and covering up to 50% of


the face, but unaccompanied by powdering or flaking of
the surface.

Heavy

A heavy deposit of salts covering 50% or more of the area


of the face but unaccompanied by powdering or flaking of
the surface.

Serious

A heavy deposit of salts accompanied by powdering and/or


flaking of the surface and tending to increase with repeated
wettings of the specimen.

36
2.8.6

Soluble Salt Content


In the British Standard (BS 3921:1985) bricks are classified as Low (L) and

Normal (N) indicated by the salt content. The normal category (N) assumes no limit
on soluble salt content while the low category (L) should have salt content not
exceeding the values given in Table 2.18.
Table 2.18:

Maximum salt content for the low category (L)


in accordance to British Standard (BS 3921:1985)

Soluble salts

Maximum content %

Sulphate
Calcium
Magnesium
Potassium
Sodium

0.5
0.3
0.03
0.03
0.03

The Singapore Standard (SS 103:1974) specifies a total salt content of 1%


and 2% for Facing and Common bricks respectively. In addition, the Standard also
specifies the content of sulphuric anhydride (SO3), which should not exceed 0.3%
by mass for all the three grades of bricks classifications.
The Australian standard (AS 1225 - 1984) and the ASTM do not include any
requirements for soluble salt content. However, a test to determine the resistance of
bricks to salt attack is given in the Australian Standard, AS/NZS 4456.10:1997. In
this test, specimens are subjected to cycles of soaking in salt solution, oven drying
and cooling. The specimens are then weighed to determine the total mass lost and
this is used to define the salt attack resistance categories i.e. exposure, general
purpose and protected.
The recent European Standard prEN 771-1 designate soluble salt content in
bricks in terms of category of application i.e. S0, S1 and S2 as shown in Table 2.19.
S0 is suitable for completely dry applications, S1 is for normal exposure condition
and S2 is meant for masonry structures subjected to prolonged saturation. There is
no requirement for salt limits in the S0 category of application. An example of such

37
application is in rendered walls where protection from water and moisture
penetration is provided by the layer of plaster applied on bricks surfaces.
Table 2.19:

Soluble salt content categories in accordance to


European Standard (prEN 771-1)

Category

Total % by mass not greater than


Na+ + K+

Mg 2+

S0

No requirement

No requirement

S1

0.17

0.08

S2

0.06

0.03

There is no limit given by the pr EN 771-1 on the sulphate content and it was
noted in the standard that consideration on this may be dealt with in national design
codes. There is no requirement for calcium and potassium and sodium is given in
combined form.

2.9 Tests Methods and Measurements in International Standards


2.9.1

Methods of Sampling for Tests in International Standards


Bricks to be tested are to be selected at random from a lot. A lot consists of

the whole population of bricks to be tested. The bricks selected from the lot would
constitute the samples, which are representative of the bricks population. Methods of
sampling and sample size i.e. the number of bricks in a sample could vary from one
standard to another. American Standard specifies the lot size for samples (for the
compressive strength and absorption determinations) as 250,000 brick. For larger
lots 5 bricks are to be selected from each 500,000 brick. The British Standard
limited the lot size as not greater than 15,000 bricks. The lot size was not specified
exactly in the Australian Standard (AS/NZS 4456.1:1997). It states that:
For testing a lot, the sample shall comprise masonry units selected
as representative from an identifiable lot and the test results shall
apply to that lot.

38
The sample size required for the various tests differs according to the
standard requirements as illustrated in Table 2.20.
Table 2.20:

Sample size for tests in international standards


Number of bricks required for tests in standards
BS 3921

ASTM

Tests

AS/NZS

SS 103

PrEN 771-1

4456

Compressive strength

10

10

10

10

Cumulative dimensions

24

20

24

Individual dimensions

24

10

20

24

10

Water absorption

10

10

10

10

10

10

Efflorescence

10

10

10

10

Salts content

10

10

10

10

Initial rate of suction

Density

The British Standard adopts a larger number of sample size for dimensional
tests whilst the number of bricks were kept to 10 for testing other parameters. The
Singapore Standard and Malaysian Standard were derivations from British Standard,
therefore similarity in the number of bricks used in the respective tests. The ASTM
and Australian/New Zealand Standard are based on metrics, therefore sampling was
based on 5 and 10 units respectively. The European Standard is more consistent in
that all tests are restricted to 10 bricks.

2.9.2

Compressive Strengths
The Compression tests used for determining the brick compressive strength

are carried out differently for various standards (Table 2.22). For example, the
packing materials used are different for test conducted in accordance to BS and
ASTM. Whilst the BS used plywood, the ASTM favours the use of hard capping
made of gypsum and sulphur. Conversely, the European Standard requires bricks
surfaces to be grounded to parallel tolerance before testing.

39
The rate of loading applied to the bricks differ in each standard, and could
vary throughout each test, except for AS/NZS, which adopt a constant loading
method.
The calculation of compressive strength also differs among the standards. BS
3921, ASTM C67 and SS 103 based their calculation on gross area. On the other
hand, AS/NZS 4456 compute the compressive strength based on net area, which
gives a higher value of compressive strength compared to calculation using net area.
In general, the ASTM implement an entirely different test approach
including the number of specimens, curing condition and capping material in
comparison to others.

2.9.3

Water Absorption
Table 2.23 shows the comparisons of the test and measurement methods used

in determining the water absorption of bricks in the various standards. British and
Singapore Standard only adopted the 5-hours boiling test, whereas ASTM specified
both the 5-hours boiling and the immersion tests. These two tests are required for the
determination of the saturation coefficient, which is the ratio of absorption by 24-hr
immersion in cold water to that of the 5-hr boling.
The Malaysian Standard MS 76:1972 allows two alternative methods to
measure water absorption i.e. the 5-hours and the vacuum method, which is similar
to the earlier version of the British standard. However, in BS 3921:1985 only the 5hours boiling test is specified since research has shown that there is no simple
relationship between these two methods and results of the two tests could be
different.
The European standard prEn 771-1 specifies the 24-hr water immersion test
to determine water absorption. Water absorption measured by the 24 hr immersion

40
would apparently show a lower value of water absorption in comparison with the 5hr. boiling test.
A new method of test for water absorption was introduced recently (Khalaf
and DeVenny, 2002). In this test, 20 mm-brick lumps instead of full brick units were
used. Table 2.21 shows the comparison of results between whole brick and the 20mm brick lump for the 24-hr cold immersion and the 5-hr. boiling tests. The results
showed that the5-hrs boiling test underestimates the absorption of bricks. In
addition, results for the 5-hr boiling test were almost equivalent to the 24-hr cold
immersion for the brick lump and in this respect; the saturation coefficient could not
be measured. However, it should be noted that the test for cold immersion was
carried out after bricks were vacuum. The advantage of this new test is that it could
be conveniently carried out without the necessity of big tanks for boiling of whole
bricks and thus saving on the fuel consumption.

Table 2.21: Comparison of water absorption from 5-hr boiling and the
24-hr cold immersion tests using whole brick and brick lumps
(Khalaf and DeVenny, 2002)

Brick type
Class B
Engineering
Clay 10-hole
Clay 3 slot
and 8 hole
Clay frogged
common
Granite

Water
absorption of
brick units BS
3921 (5-hr boil)
(%)
6.0

Water
absorption of
brick units (24hr cold) (%)

Water
absorption of
brick lumps (5hr boil) (%)

Water
absorption of
brick lumps
(24-hr cold) (%)

5.2

6.3

6.2

6.2

4.6

7.4

7.2

5.8

5.3

7.4

7.4

12.9

10.3

14.1

11.5

2.63

2.55

2.63

2.55

Besides implementing the different types of test for the measurement of


water absorption there are also some differences observed in the number of bricks
used and preparation of specimens before testing. ASTM requires five half-brick
while AS/NZS and BS specify the use of 10 whole bricks. Another difference is in
the duration for attaining constant mass when drying bricks in the oven. BS 3921

41
assumes 48 hours of heating in the oven to achieve constant mass whereas the
AS/NZS and ASTM monitor the weight loss during drying and constant mass is
assumed if subsequent drying indicate that the change in mass is not greater than
0.1 % of the previous weight for the AS/NZS and 0.2 % for ASTM.

2.9.4

Initial Rate of Suction


Table 2.24 shows the comparisons of test and measurement methods for the

initial rate of suction as required by the various standards. The tests principles are
similar in all standards, whereby bricks capillary suction is measured by immersing
bricks in about 3 mm depth of water for a duration of 1 minute. The ASTM and the
Australian Standard specify some means to set up the apparatus in maintaining water
level to the required height of immersion.
In the Australian / New Zealand Standard (AS/NZS 4456:1997) IRS are
given in terms of Anet and Agross as shown in Table 2.24. The ASTM specified that
the IRS measured for cored bricks should be modified with a factor depending on
the net area of immersion, which will result in a higher value of IRS compared with
calculation based on gross area. The BS on the other hand based its IRS calculation
on the gross area of immersion.

2.9.5

Dimensional Tolerance
Methods of testing to determine dimensional tolerances vary between the

standards (Table 2.25). British, Australian/New Zealand, Malaysian and Singapore


standard specify dimensional tolerance measured from the cumulative dimensions of
specified numbers of bricks, whereas, ASTM and European standard specify an
individual brick dimensional tolerance. Other variations include the numbers of
bricks required for the cumulative dimensions and the methods of measuring the
tolerance.

42
ASTM based their tolerance on a sample of 10 bricks and each brick should
not depart from the specified size by more than the tolerance given in the standard.
While, the British and Singapore standard establish the tolerance limits based on two
approaches namely (i) individual dimension (ii) the overall measurement for 24
bricks. While AS/NZS, tolerance limit is based on overall measurement of 20 bricks.
The European standard specifies an entirely different dimensional tolerance
limit based on the mean and range values for a sample of 10 bricks according to the
different categories. The mean deviation refers to basic requirement and constitute a
minimum description of a unit whilst the range is only required when relevant to the
needs of application. In addition, European standard also specified some geometry
requirements for bricks to be used in elements subjected to acoustics requirements.

2.9.6

Efflorescence
The test for efflorescence in existing standards involved cycles of wetting

and drying of bricks in laboratory after which they are examined for the salts
depositions on the surface. The procedures for quantifying efflorescence differ
between the standards (Table 2.26). British standard and Australian/New Zealand
standard categorise efflorescence into levels in accordance to the degree of
contaminants. In contrast, the ASTM quantify efflorescence in bricks either simply
effloresced or not effloresced. The new amendments made to BS 3921 in 1995
ignored the effects of efflorescence. Similarly, European Standard prEN 771-1 does
not specify any requirement for efflorescence in bricks.

Table 2.22:
Test
Standards

Test methods and measurements for compressive strength in international standards


Sample
size

BS 3921
Appendix. D

10
(Whole
brick)

ASTM C6790a

5
(Half
brick)

AS/NZ
4456:1997

PrEN 771 1

10
(Whole
bricks)
10
(Whole
bricks)

Preparation of
specimen

Speed of testing

Capping material

Immerse brick in
water for 24 hrs or
saturate by boiling

Convenient rate not


exceeding 35
N/(mm2.min) until half of
expected max. load after
that reduces to 15
N/(mm2.min) until failure.

Soft capping: three-ply


4mm thick plywood

Maximum load
smaller bed of the overall dimension

Dry specimen in
the oven for not
less than 24 hrs.

Convenient rate until


about half of expected
maximum load after that
uniform rate.

Hard capping:
Gypsum
Sulphur

Maximum load
Average of gross area of upper
and lower bearing surfaces

Moisture content
as sampled

Constant rate within a


range equivalent to a
stress of 150 kPa/s (9
N/mm2.min) to 700 kPa/s
(42 N//mm2.min)

Soft capping:
4 -6 mm plywood
12mm fibreboard

Not available

No capping needed.
Surfaces ground to a
parallel tolerance

Bricks tested dry

Compressive strength
calculations

1000 P
A
where, K a = aspect ratio factor

Unconfined C = K a
A = net area

Not available

43

Table 2.23:
Test
Standards

BS 3921
Appendix. E
/SS 103

ASTM C6790a

AS/NZ
4456.14:
1997

prEN 771 - 1

Test methods and measurements for water absorption in international standards

Sample
size

10
(Whole
brick)

5
(Half
brick)

10
(Whole
bricks)

10
(Whole
bricks)

Type of
test

5-hour
boiling
test

Determination of dry mass


Drying in oven (110 8C) for at
least 48 h. Cooling bricks left
unstacked in a ventilated room for
4 h, with 2 h of continuous air
using an electric fan. Dry mass is
determined when bricks are cool.

i) 5-hour
boiling
and
ii) 24-hour
immersion
test.

Drying in oven (110 to 115C


for not less than 24 h and until two
successive weighing at intervals of
2 hrs. show an increment of loss
not greater than 0.2% of previous
weight. Cooling in a room
temperature maintained at 24
8C, relative humidity 30 70%.
Record the average dry mass of all
specimens as Wd.

i) 5-hour
boiling
and
ii) 24-hour
immersion
test.

Drying in oven (110 8C) until


consecutive weighing at intervals
of 4 hrs show a change in mass of
not greater than 0.1 %. Record the
lowest average weight for all
specimens at room temperature as
the dry mass m1.

24-hour
immersion
test.

Not available

Test procedures
5-hr.boiling Bricks are boiled in a tank of
water for 5 hrs. Then are cooled naturally in the
water for not less than 16 hours nor more than
19hrs.Then take the weight (wet mass).

Immersion test submerge cool bricks in clean


water at 15.5-30C, for 24 h. Then remove
specimens wipe dry and weigh. Record the
average weight of all specimens as Wsc.
5-hr.boiling bricks are boiled in a tank of
water for 5 hrs. Then cool naturally to 15.530C. After that remove specimens wipe dry and
weigh. Record the average weight of all
specimens as Wsb.
Immersion test submerge cool bricks in clean
water at ambient temperature, for 24 h. Then
remove specimen wipe dry and record the
average mass of all specimens as m2.
5-hr boiling bricks are boiled in a tank of
water for 5 hrs. Then cool naturally to 15.530C. Then take this saturated weight and record
the average mass of all specimens as m3.
Not available

Calculation of water absorption

(wet mass-dry mass)


%
dry mass
Average of 10 specimens to the
nearest 0.1%.
100

Absorption by immersion:
=(Wsc-Wd)/ Wd
Absorption by boiling:
=(Wsb-Wd)/ Wd
(Saturation coeff. = absorption by
immersion / absorption by boiling)
Absorption by immersion:
Wi (%) = 100(m2-m1)/ m1
Absorption by boiling:
Wb (%) = 100(m3-m1)/ m1
Saturation coefficient = Wi / Wb
Not available

44

Table 2.24:
Test
Standards

BS 3921
Appendix. H

ASTM C6790a

Test methods and measurements for initial rate of suction in international standards

Sample
size

Not
specified

5
(Whole
brick)

AS/NZS
4456.17:
1997

10
(Whole
brick)

prEN 771 - 1

10
(Whole
bricks)

Preparation of specimen

The bricks are dried in the oven


as in absorption test. The weight
of the dry brick is recorded as
m1 in gm.

Test procedures

The dry brick is immersed in water at a depth


of 3 1mm for 1 min. Record this weight m2 in
gm.

i) Oven drying as in absorption


test or
ii) Ambient air drying

The dry brick is immersed in water at a depth


of 3 1mm for 1 min. Record this weight as
m2 in gm.

The weight of the dry brick is


recorded as m1 in gm.

Some means of maintaining water level at a


depth of immersion of 3 1mm is provided in
the standard.

Bricks are dried in the oven as in


absorption test. The weight of the
dry brick is recorded as m1 in gm.

The dry brick is immersed in water at a depth


of 3 1mm for 60 1 sec. Record this weight
m2 in gm.
A set up of the apparatus suggesting a way of
maintaining immersion at depth of 3 1mm is
provided in the standard.

Initial rate of suction calculations


1000(m2 m1 )
in kg/m 2 . min .
A
where A= gross area of the immersed face
IRS =

of the brick in mm 2
IRS = m1 m2 in gm.
IRS is measured in gm/min/30 in2.
For cored bricks the measurement of
IRS i.e. m1 m2 has to be multiplied
with a factor of

IRS gross =

30
.
net area

1000(m2 m1 )
Agross

1000(m2 m1 )
Anet
2
IRS (kg/m .min) for each brick and mean of
the 10 specimens.
IRSnet =

Not available

45

Table 2.25:

Test methods and measurements for dimensional tolerance in international standards


Measurement of dimensional tolerance

Test
Standards

Individual brick dimension

Cumulative (overall dimension)


1.

BS 3921
Appendix. A

ASTM C6790a

1. Each brick from the 24 bricks for the


cumulative measurements must not
exceed the coordinating size as given
in Table 2.9.
1.

Each brick from the 10 bricks in a


sample should not vary from the
specified allowable dimensional
tolerance as given in Table 2.8

2.

Tolerance on distortion and out


of square is also specified for
facing bricks.

No cumulative dimension specified

1.
AS/NZS
4456.17:
1997

Cumulative dimensions of 24 bricks must not exceed the


specified range for length width and height as indicated in
Table 2.9. The cumulative measuremen is based on the
assumption that each brick should not differ from the work size
by more than 6.4mm for
length, 4mm for width and height.

1.

Each brick from the 20 bricks should


comply with the general criteria as
given in Table 2.7.

Cumulative dimensions of 20 bricks must not exceed the


specified range for length width and height for the three
categories (Table 2.10). These categories identify bricks
tolerance requirements:
ST0 bricks no required to be precise in dimensions
ST2 bricks manufactured to finer tolerance for special
application
ST3 bricks where regularity in size is necessary.

46

Table 2.25 (cont.):


Test
Standards
PrEn 771-1

Test methods and measurements for dimensional tolerance in international standards


Measurement of dimensional tolerance
Individual brick dimension

1.

Cumulative (overall dimension)

Mean dimensions for the test sample should not be greater than
declared means for categories T1, T2 and T0
Where,
T1: 0.40 (work size dimensions ) mm or 3 mm whichever is greater
T2: 0.25 (work size dimensions ) mm or 2 mm whichever is greater
T0: a deviation in mm declared by the manufacturer.
No cumulative dimension specified
2.

The declared range should be within the range determined


within the test sample for the categories R1, R2 and R0
Where,
R1: 0.60 (work size dimensions ) mm
R2: 0.30 (work size dimensions ) mm
R0: a range in mm declared by the manufacturer.

47

Table 2.26:
Test
Standards
BS 3921
Appendix. C
*

ASTM C6790a

AS/NZS
4456.6:
1997
prEn 771-1

Test methods and measurements for efflorescence in international standards

Specimen
Numbers

10
(Whole brick)

5 pairs
(Whole brick)

5 pairs
(Whole brick)

Test procedures

Measurements of efflorescence

One face of the brick is subjected to 2 cycles of wetting and


drying for the specified time. Then examined for
efflorescence by comparing this face with the other faces
that is not subjected to the wetting and drying cycles.

Levels for efflorescence as shown in Table 2.7. Bricks are


categorised according to the worst occurrence. Bricks with
Heavy efflorescence are considered as not complying with
the standard.

One specimen from each pair is allowed to stand on ends


partially immersed in water for 7 days. The other pair is
kept in a room with specified humidity and temperature.
Then dry both sets in oven for 24 hrs. After that compare
and examine both sets for efflorescence.

Efflorescence is recognised as either effloresced or not


effloresced

One specimen from each pair is allowed to stand on ends


partially immersed in water for 7 days then air dry for 2
days. After that compare and assessed with respect to a
matching brick.

Levels for efflorescence as shown in Table 2.13. Bricks are


categorised according to the worst occurrence. Bricks
exposed to view should not exceed slight.

No requirements

*Note: Efflorescence test has been removed from BS 3921 (AMD 8946/December 1995)

48

49
2.10

Conclusions
A considerable amount of past research and studies on masonry indicated the

relationship between masonry strength and unit strength. An example of such


relationship developed by Hendry (Equation 2.1 and 2.2) and is used in the code for
masonry design (BS 5628:1985). The compressive strength is therefore one of the
most important bricks properties for design requirements, and dealt by
specifications.
The compressive strengths of bricks can vary from 5 N/mm2 to over 100
N/mm2, depending upon materials and types of manufacturing and to some extent
are affected by the methods of testing in evaluating the compressive strength.
Malaysia Standard / British Standard identifies its clay bricks as Engineering A and
B (compressive strength ranging from more than 70 N/mm2 to not less than 50
N/mm2) for structural purposes and as All others for strengths above 5 N/mm2. On
the other hand, ASTM classifies bricks into three categories i.e. building, facing and
hollow, with a minimum compressive strength of 20.7 N/mm2 and 17.2 N/mm2 to be
used in regions of severe (SW) and moderate weathering (MW) respectively. Grade
NW bricks with minimum compressive strength of 10.3 N/mm2 is meant for
applications in regions with negligible weathering. Singapore Standard defines
bricks as First, Second and Third Grade in accordance to the levels of compressive
strengths, with a minimum value of 5.2 N/mm2 for general purpose construction.
The methods of testing compressive strength are known to affect the
computed values obtained in standards. The usage of soft capping specified by the
British and Australian/New Zealand Standard is believed to reduce platen restraints.
Platen restraint induces artificial strengthening thereby enhancing the compressive
strength. Hard capping is used in ASTM and European Standard prEN 771-1 uses no
capping material, however requires the surfaces to be ground parallel and free of
irregularities.
The British, ASTM, Malaysian and Singapore standards based the evaluation
of compressive strength upon bricks tested on bed faces with the exception of
Australian/New Zealand, which accommodate the compressive strength for tests in

50
other orientations, producing a different height to thickness ratio (h/t) depending on
the bricks orientation in the tests. The aspect ratio, h/t, has a considerable effect on
the compressive strength, the higher the ratio the least is the compressive strength.
Subsequently, bricks tested on the bed face (lowest h/t ratio) display the largest
compressive strength. The development of European specification for masonry units,
prEN 771-1 introduces similar test methods to Australian/New Zealand Standard,
but the strength limits are to the discretion of the manufacturers declared values. The
EN and Australian approach of defining the unit strength in various orientations
provide a comprehensive information on the unit and this is useful for structural
design purposes.
Amongst others the compressive strength of units are affected by the curing
methods. Previous research; tend to indicate higher strength for dry bricks as high as
15 % greater than cured bricks. Evaluation of compressive strengths by ASTM and
European Standard was based on dry bricks in contrast to British, Malaysian, and
Singapore standards, which cured the bricks by saturating them in cold immersion or
by boiling. On the contrarily, Australian/New Zealand Standard carried out the
compressive strength on bricks as received i.e. the bricks having a moisture content
as sampled. However, if the bricks moisture content exceeds 25 %, air-drying is
required.
Most masonry standards dictate the requirements of water absorption for
bricks with structural applications and cases where resistance to water and moisture
penetration are critical. For example, in British Standard BS 3921: 1985 low water
absorption limits is specified for Engineering A and B and damp-proof course 1 and
2 bricks with water absorption of 4.5 % and 7.0 % respectively. Bricks for other
applications than those already mentioned are not restricted to any water absorption
limits. Similarly, masonry specification in ASTM C 62-89a, ASTM C 652-89a and
ASTM C 216-90a specified limits for water absorption of bricks with high levels of
compressive strengths where applications are specifically for severe and moderate
weathering regions. For negligible weathering regions bricks are not required to
conform to any limits of water absorption.

51
The Australian Standard, AS 1225-1984, is a general standard for all
masonry materials and does not specify limits for water absorption however has
included test methods for determining these values. The European Standard for
masonry units (pr EN 771-1), specifies water absorption requirements for bricks to
be used in external applications and the value is as declared by the manufacturers.
Recent research indicated the existence of some relationship between water
absorption to bricks porosity and compressive strength. The research revealed that
bricks with the least water absorption and small porosity produce higher
compressive strengths and this relationship could be used as an early indicator for
compressive strength. Other studies carried out on the relationship of water
absorption and bricks porosity had established durability indices, which provide
guideline for resistance of masonry against the freeze and thaw actions. These
indexes provide limits that can be used to identify durable and non-durable bricks.
The two types of test methods used for measuring water absorption i.e. the 5hours boiling and 24-hours cold immersions are known to give different
measurements. The 5 hours boiling test provides results for saturated conditions,
while the 24 hours cold immersion gives partial saturation. The prEN 771-1 requires
water absorption of bricks to be determined by the 24 hours cold immersion test,
hence producing a lower value of water absorption measurement.
The IRS is the rate at which a brick sucks water from mortar during laying
and therefore affects the bond strength between units and mortar. The suction
properties are crucial to the design of walls subjected to lateral load particularly in
highly stressed masonry structures. The IRS does not form an integral part of the
specifications for both the Australian/New Zealand and British Standards. However,
testing method to determine IRS is provided by the standards. On similar grounds
the European standard pr EN 771-1, requires IRS to be specified for relevant cases
of applications and the value of IRS to be declared by the manufacturer. In contrast,
ASTM requires the IRS values for bricks to be known and recommends that bricks
to be wetted before laying if the IRS is higher than 30 g/min per 30 in2 (1.5
kg/min/m2). The practice of wetting bricks before laying ensures proper bond
development between mortar and the highly absorptive bricks. In highly stressed

52
structures a good bond between mortar and bricks is essential to prevent the
occurrence of cracks in mortar joints and thus enhancing the water-tightness
property of facing brickwork.
The dimensions and tolerances of bricks are used to describe and designate
masonry units in standards. Dimensional variations are expected due to the
shrinkages in the natural clay deposits, which take place during drying and burning
processes. The standards specified dimensional tolerances to restrict these variations
in satisfying the required construction criteria. For facing bricks, dimensional
control is more stringent for wall appearance and lesser for other applications. Most
standards specify dimensional tolerances according to the types of masonry
construction.
There are two approaches of measuring dimensional tolerances in standards,
namely the individual and cumulative dimension of a set of bricks. In the recent
European Standard dimensional tolerance are specified in terms of the mean and the
range from a sample of 10 bricks and this should be within the range defined in the
specified categories. The dimensional tolerance determined from cumulative
dimensions of a set of bricks as given by Australian Standard AS 1225:1984,
Malaysian Standard MS 76 Part 2:1972 and British Standard BS 3921:1985 helps to
offset the individual brick dimensional variation, which maybe useful in determining
variation within and between batches of bricks delivered on site.
Efflorescence, that appear on the surfaces of bricks after construction, is
usually not harmful to a masonry structure but unsightly in facing brickwork. These
white stains indicate the presence of soluble salts in bricks. The test method for
efflorescence in all standards involves simple laboratory works and measurements
and evaluations of efflorescence are based on visual inspection. The test seems not
related to the field exposure that a brick is exposed to in a masonry structure.
Furthermore, with the introduction of limits for soluble salt content in all bricks, the
efflorescence requirement was considered as unnecessary and had been omitted by
the British Standard and the new European standard. However, this test is being used
by manufacturers to indicate the soluble salt content in bricks and its liability to
efflorescence.

53
Recent global development in standardisation works particularly in Europe
has brought about some significant changes to masonry standards. The British
Standard, upon which the existing Malaysian standard is based on, will soon be
replaced by the harmonised European Standard prEN 771-1 specifications for
masonry units. The new standard introduces some modifications to the BS 3921,
which include new test methods and requirements criteria, prompted by research
discovery and new technological development in masonry. A study on the
performance of local bricks is therefore timely to provide comprehensive
information on bricks considered relevant to the current construction industry and
market and design requirements pertaining to modern construction.

CHAPTER 3

LABORATORY TESTS ON PHYSICAL


PROPERTIES OF BRICKS

3.1

Introduction
This chapter examines the physical properties of the bricks. Laboratory

investigations were performed on samples of bricks at the Structural Laboratory of


the Faculty of Civil Engineering, Universiti Teknologi Malaysia. Tests were
conducted to examine dimensional tolerance, density, initial rate of suction, water
absorption, compressive strength, soluble salt content and efflorescence.

3.2

Sampling of Bricks
Sampling is a process involving the collection of bricks at random to make

up a sample to represent the population of bricks used in this research. The number
of specimens in a sample i.e. the size of sample (n) is the number of bricks required
for any tests. Sampling was carried out at a brick factory, which is considered a
major producer of brick in the country. The factory has a monthly production
capacity of 10,000,000 units of bricks and it is also a major exporter of bricks to
counties in Asia like Japan and Singapore.

55
Two categories of bricks comprising of the facing brick and the common
brick were sampled at random from the factory output. Facing bricks are quality
bricks with attractive external appearance and common bricks are meant for general
building works that do not require external look. Random selection means that every
brick must have a probability of being selected. However, this was found to be quite
impossible at times when bricks were in big piles making it difficult to reach and
acquired. Four factory visits were made and for each visit a batch of approximately
100 pieces of facing bricks and 40 pieces common bricks were selected. A batch is a
collection of bricks acquired at every visit.

3.3

Testing Programme
The testing programme (Table 3.1) shows the extent of the work detailing the

total number of batches used for the laboratory investigations including the number
of samples in every batch for the various tests. The test procedures and the sample
size (n), i.e. number of bricks required in every sample for testing of dimensional
tolerance of 24 bricks, Initial rate of suction (IRS), absorption, compressive strength,
soluble salt content and efflorescence were generally in accordance to BS 3921:
British Standard Specifications for Clay bricks (1985), with the exception of the
density test which were done with reference to the AS/NZS 4456.8:1997.
The tests were performed in sequence as shown in Figure 3.1, such that it
will optimise the quantity of sample used in the investigation. For example, each test
will commence with dimensional measurements, and the same 10 bricks be tested
for density, IRS, absorption and compression. The fragments from the compressive
strength will then be used for testing of soluble salt content. The efflorescence test
was conducted separately on another 10 bricks from each batch of samples.
The series of tests shown in Figure 3.1 were performed for the facing bricks,
which are referred to as structural bricks. The common bricks were only tested for
their compressive strengths. Structural bricks entailed design calculation which
requires the compressive strengths of units to be known, for this reason, it is

56
essential to examine the strengths characteristics and other physical properties.
Hence, the properties of facing bricks need to be investigated in this case. On the
other hand, common bricks, which are meant for general building works do not
require specification on the properties except for its compressive strength. Thus,
they are only tested for this particular property. Compressive strength test was
carried out on common bricks to examine the variation of strengths in order to
categorise the brick into their strengths classification. Efflorescence, which tends to
affect external appearance may be considered insignificant for common bricks as
they are usually used for infill walls with plastered surfaces. The water absorption
property may also not be considered essential in this case since the plaster may help
in resisting water penetration into a wall to a certain degree.

24 bricks
Dimension

10 bricks

10 bricks
Density

Initial rate of suction

Absorption

Compressive strength

Soluble salt content

Figure 3.1:

Sequence of testing

Efflorescence

Table 3.1:

Testing programme

100 facing
bricks
40 common
bricks
2 13/6/2001 100 facing
bricks
40 common
bricks
3 25/7/2001 100 facing
bricks
40 common
bricks
4 19/9/2001 100 facing
bricks
40 common
bricks
Total samples for all batches
1

26/4/2001

Number of
bricks
sampled in a
batch

Date of
sampling

Batch

Number of samples per batch for the various tests


Dimensional tolerance
Overall
Individual
dimension
dimensions
(n = 24)
(n = 6)
2
8

Density

Initial rate
of suction

Water
Absorption

Compressive
strength

Soluble salt
content

Efflorescence

(n = 10)

(n = 10)

(n = 10)

(n = 10)

(n = 10)

(n = 10)

12

16

16

16

14

56

27

27

27

3
8
3
8
3
8
3
30

12

57

58
3.4

Dimensional Tolerance
Dimensional tolerances were measured from the respective length, width and

height of overall dimension of 24 bricks and individual brick dimension. Tests were
conducted on 24 bricks to examine the dimensional tolerance in accordance to BS
3921. The 24 bricks were selected at random from a batch of 100 bricks. For the
measurement of overall lengths, the bricks were placed in two rows, each of 12
numbers, on a flat surface in the laboratory. Measurements were made using an
inextensible steel tape. The measurements for the two rows were added to give the
overall dimension of length for 24 bricks. Measurements of width and height were
taken for 24 bricks in a row. A long steel channel, aligned against the row of bricks
ensured that bricks were arranged in a straight line (Figure 3.2). For individual
dimensions the vernier calliper were used in which a measurement to two decimal
places was recorded. The results for the overall dimension of length, width and
height are shown in Table 3.2. Table 3.3 shows the individual dimension for length
width and height in the samples. The complete tabulation of results for the
individual dimensions in each specimen is shown in Appendix A1.
Table 3.2: Overall dimensions of 24 bricks
Batch
1

Batch
2

Batch
3

Batch
4

Sample
1
2
3
4
5
6
7
8
9
10
11
12
13
14

Length
(mm)
5240
5254
5216
5263
5241
5243
5175
5218
5185
5178
5203
5211
5210
5213

Width
(mm)
2415
2410
2408
2426
2421
2419
2405
2412
2413
2397
2416
2400
2409
2414

Height
(mm)
1638
1646
1648
1651
1650
1653
1628
1640
1625
1634
1638
1643
1643
1644

59
Table 3.3:

Individual brick measurement of length, width,


and height for all batches
Sample

Length (mm)

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56

218.43
218.43
216.58
218.03
216.57
217.68
217.68
219.08
216.64
215.53
216.13
216.35
218.01
217.67
217.68
218.82
216.78
218.97
216.66
217.74
219.05
217.49
216.29
217.97
215.74
214.62
215.09
214.67
215.43
216.26
214.71
215.71
215.19
215.45
215.13
215.10
216.06
214.98
214.77
215.18
216.42
216.23
215.63
215.09
215.09
215.69
215.72
216.18
216.92
214.57
216.83
217.00
215.83
215.36
216.14
216.28
216.42
1.912

Batch 1

Batch 2

Batch 3

Batch 4

Mean x
Std. dev. s

Width (mm)

Height (mm)

100.20
99.79
99.00
99.63
98.96
99.81
99.97
99.91
99.93
99.31
99.33
98.85
100.41
100.27
99.83
100.73
99.77
100.89
99.76
100.22
100.22
101.03
99.81
99.97
99.73
99.53
99.81
99.90
99.67
100.45
99.38
100.27
99.39
99.99
99.03
98.70
99.82
99.22
99.59
100.17
100.23
99.78
99.63
98.89
98.73
99.43
99.13
99.15
100.23
99.01
100.03
99.73
99.96
99.48
100.27
99.80
99.73
1.116

67.08
67.23
67.45
67.19
66.37
67.16
67.91
68.01
68.18
67.83
68.06
67.67
68.18
67.25
67.67
68.81
67.60
68.95
68.18
68.10
68.08
68.57
67.86
67.89
67.80
66.93
67.09
67.08
67.43
67.67
67.37
67.54
67.35
67.23
66.93
67.05
67.04
66.83
66.96
67.08
67.70
67.53
67.41
67.13
67.28
67.43
66.58
67.58
67.35
67.03
67.53
67.01
68.28
67.19
67.43
67.46
67.48
0.888

60

(a)

(b)

(c)

Figure 3.2:

Overall Measurement of (a) length, (b) width


and (c) height for 24 bricks

61
3.5

Density
The bricks density was measured in accordance to AS/NZS 4456.8, since BS

3921 does not provide for such testing specification. However, this is a new
requirements in the European Standard for which bricks are to be tested. Ten bricks
were selected from the 24 bricks used for dimensional testing. Each brick was
labelled with numbers for example 51, 27, 4899 (Table 3.4) using permanent
waterproof ink for identifications. The weight of each brick was taken to represent
the ambient mass i.e. the mass at the time of measurement, mo. The bricks were then
immersed in water for 2 hours, then removed from the water and allowed to drain
for not more than 1 min. Any excess water on the surface were then removed by
wiping with a cloth. The brick was then weighed and the mass recorded i.e. m1.
After that, the brick was placed in an apparatus to measure its submerged mass, m2.
These procedures were repeated for all 10 bricks.
The device used to measure submerged mass of bricks throughout the testing
programme is shown in Figure 3.3. This device was an existing unit used previously
for measuring the density of concrete cubes in the laboratory. It consists of a water
bath and an attached steel cage to hold the specimens under investigations. The steel
cage is connected to a digital weight indicator. Upon lowering the cage and
specimen, the readings of submerged mass will be indicated by the digital indicator.
Based on Archimedes principle the submerged mass were used to evaluate the
volume.
Volume was calculated using submerged mass as stated in equation 3.1.

V (mm ) = ( m1 m2 ) 1000
3

(3.1)

Where,
m1 = mass of wet brick in gram.
m2 = submerged mass of brick in gram.
The volume is then used to calculate the ambient density Da using equation 3.2.
Density ( Da ) =

mo
1000000 in kg/m3
V

(3.2)

62
Where,

mo = ambient mass in gram.


An example of the test results for density determined for bricks of Batch 1 is
shown in Table 3.4. A complete tabulation of results for tests carried out throughout
the research is given in Appendix A2.

Sample 3

Sample 2

Sample 1

Table 3.4:

Density of bricks for Batch 1

Brick
Identification

Ambient
mass
( m0 ) gm.

Mass after
2 hours
soaking
( m1 ) gm.

Immersed
mass
( m2 ) gm.

51
27
48
67
32
6
19
22
50
9

2395
2440
2400
2435
2390
2395
2335
2410
2475
2365

2630
2590
2620
2650
2630
2600
2470
2610
2690
2600

1270
1270
1270
1300
1280
1260
1220
1260
1310
1250

1360000
1320000
1350000
1350000
1350000
1340000
1250000
1350000
1380000
1350000

36
44
43
64
38
45
62
30
70
66

2435
2455
2325
2460
2400
2450
2455
2355
2440
2430

2690
2640
2570
2670
2600
2680
2670
2560
2620
2630

1300
1280
1240
1300
1270
1300
1300
1250
1290
1280

1390000
1360000
1330000
1370000
1330000
1380000
1370000
1310000
1330000
1350000

85
92
41
96
87
43
91
42
81
99

2315
2305
2390
2510
2420
2385
2270
2420
2465
2405

2520
2530
2680
2770
2650
2680
2490
2640
2690
2650

1230
1230
1250
1350
1300
1290
1200
1290
1330
1310

1290000
1300000
1430000
1420000
1350000
1390000
1290000
1350000
1360000
1340000

Volume (V)
V=(m1m2)*1000
mm3

Density (Da)
(mo/V)*1,000,000
kg/m3
1761.03
1848.48
1777.78
1803.70
1770.37
1787.31
1868.00
1785.19
1793.48
1751.85
Mean x = 1794.719
Std. dev. s = 37.030
1751.80
1805.15
1748.12
1795.62
1804.51
1775.36
1791.97
1797.71
1834.59
1800.00
Mean x = 1790.483
Std. dev. s = 25.923
1794.57
1773.08
1671.33
1767.61
1792.59
1715.83
1759.69
1792.59
1812.50
1794.78
Mean x = 1767.456
Std. dev. s = 43.169

63

Figure 3.3: Apparatus for the measurement of density

3.6

Initial Rate of Suction


The bricks used for density tests were retested for the initial rate of suction.

Initially the bricks were dried in a ventilated oven for two and a half days at a
temperature of 110 C. In accordance to BS 3921 constant mass is assured if bricks
are subjected to heating at 110 C for not less than 48 hours. The bricks were
removed from the oven and cool to room temperature for a period of approximately
4 hours. Cooling was assisted by passing air over the bricks using an electric fan for
a period of 2 hours. Upon cooling, the bricks were weighed and the dry mass md
recorded.
In the tests a large shallow rectangular pan of size 600mm 600mm giving,
an area of 0.36m2 was used. Two 10mm steel bar were placed at the bottom of the
pan at approximately 100 mm apart, to form a platform for the bricks to rest during
measurement process (Figure 3.4). The steel bar was firstly immersed with water to
a depth of about 3mm. The pre-weighed dry brick was placed on the bar whilst the
water level is closely observed with a measuring gauge to ensure that depth of the
immersion for the brick was maintained at 3 1mm throughout the duration of
immersion, 1 minute. After 1 minute, the brick was removed from the water and
excess water wiped off with a damp cloth. The brick was reweighed and the mass

64
mw recorded. These procedures were repeated for 10 bricks. Some typical results for
Batch 1 are shown in Table 3.5 and others can be found in Appendix A3. The initial
rate of suction due to gross area of immersion (IRSgross), in kg/m2.min is calculated
using equation 3.3a.
IRS gross =

1000(mw md )
Agross

(3.3a)

Where,
md

is the mass of the dry brick in gram.

mw

is the mass of the wet brick in gram.

Agross is the gross area of the immersed face of the brick in mm2.
The IRS for net area of immersion (IRSnet) was determined as shown in
equation 3.3b.
IRS net =

1000(mw md )
Anet

(3.3b)

Where,
Anet is the net area of immersion i.e. gross area less the area of perforations.
Precautions were taken so that the limits of immersion remained at 3 1mm
as required by BS 3921. The size of pan used in this testing programme was 0.36m2
in area and this did not cause a significant drop in water level after a subsequent test
was conducted at the immersion limits recommended by BS 3921. The minimum
size of the tank recommended by AS/NZS 4456 is 0.25m2.
The role of the pan size here is not considered very significant, for as long as
the tests were conducted in accordance to the depth of immersion and the duration of
absorption (1 min.). The larger the pan, the smaller the drop in water level and the
less frequent to top up the level to 3 1mm limit. The BS 3921 does not specify the
size of the pan. ASTM C67 specifies that pan should be at least 0.19 m2.
Additionally, the Brick Institute of America through its Technical Note 39,
recommended a pan size of 0.19m2 and observations on bricks with IRS
40g/min./30in.2, equivalent to 2.05 kg/min.m.2, only caused a water level drop of
less than 0.25mm. In this regards, this is hardly measurable.

65

Figure 3.4:

Apparatus for measuring the initial rate of suction

Sample 3

Sample 2

Sample 1

Brick
identifica

Table 3.5:

16
2
11
4
9
17
19
3
7
8
1
12
10
18
6
15
5
20
14
13
35
69
63
37
68
40
29
41
71
39

Dry
mass,
md
(gm)
2445
2390
2415
2370
2435
2430
2440
2435
2415
2410
2380
2420
2485
2430
2410
2465
2460
2410
2370
2370
2410
2420
2435
2400
2430
2410
2410
2415
2440
2440

Wet
mass
mw
(gm)
2485
2420
2450
2400
2485
2465
2490
2455
2450
2435
2410
2455
2515
2450
2445
2500
2490
2435
2400
2410
2440
2455
2490
2425
2470
2445
2445
2450
2485
2475

Initial rate of suction in samples for Batch 1

Length
(mm)

221.15
216.50
218.30
216.05
221.45
220.05
220.10
217.55
217.10
216.60
216.55
217.95
218.60
216.30
217.00
216.30
217.50
217.50
217.75
217.50
217.30
217.35
216.95
216.40
208.50
217.00
217.25
217.10
218.10
216.95

Width
(mm)

100.75
98.80
99.70
98.30
102.25
100.75
100.10
98.80
100.00
99.80
99.55
99.75
99.65
97.95
99.80
99.15
99.65
99.15
99.65
99.90
99.20
99.70
99.25
99.25
101.20
99.25
99.65
99.60
100.05
99.35

Immersed
area,
Agross
(mm2)
22280.86
21390.20
21764.51
21237.72
22643.26
22170.04
22032.01
21493.94
21710.00
21616.68
21557.55
21740.51
21783.49
21186.59
21656.60
21446.15
21673.88
21565.13
21698.79
21728.25
21556.16
21669.80
21532.29
21477.70
21100.20
21537.25
21648.96
21623.16
21820.91
21553.98

IRSgross
(kg/m2.min)
1000

(m w md )
A

1.795
1.403
1.608
1.413
2.208
1.579
2.269
0.930
1.612
1.157
1.392
1.610
1.377
0.944
1.616
1.632
1.384
1.159
1.383
1.841
1.39
1.62
2.55
1.16
1.90
1.63
1.62
1.62
2.06
1.62

Immersed
area, Anet
(mm2)

IRSnet
(kg/m2.min)

18905.86
18015.20
18389.51
17862.72
19268.26
18795.04
18657.01
18118.94
18335.00
18241.68

2.116

18182.55

1.650

18365.51

1.906

18408.49

1.630

17811.59

1.123

18281.60

1.914

18071.15

1.937

18298.88

1.639

18190.13

1.374

18323.79

1.637

18353.25

2.179

18181.16

1.650

18294.80

1.913

18157.29

3.029

18102.70

1.381

17725.20

2.257

18162.25

1.927

18273.96

1.915

18248.16

1.918

18445.91

2.440

18178.98

1.925

1000

( mw md )
A

1.665
1.903
1.679
2.595
1.862
2.680
1.104
1.909
1.370

66
3.7

Water Absorption (5-hours boiling test)


The same 10 bricks used for initial rate of suction tests were used for water

absorption test. The dry mass md , were as recorded earlier in the initial rate of
suction test.
A large urn was used to accommodate two sets of samples comprising of 20
bricks (Figure 3.5). The bricks arranged in two tiers with spaces in between bricks
and tiers, were boiled for 5 hours and then allowed to cool naturally in the water for
about 18 hours. A minimum of 16 hours and a maximum of 19 hours of cooling
period were recommended by BS 3921. Each brick was weighed and the saturated
mass ms , recorded. Water absorption W, in percentage was calculated using the
following equation 3.4.
W % = 100

(ms md )
md

(3.4)

Where,

md is the dry mass


ms is the saturated mass
The experimental results for Batch.1 were shown in Table 3.6. Detailed
results for other bricks can be found in the Appendix A4.

Figure 3.5:

Apparatus for water absorption test

67

Brick
identification

Dry mass
md (gm)

Saturated mass
ms (gm)

7
5
1
13
8
14
4
20
19
10

2415
2460
2380
2370
2410
2370
2370
2410
2440
2485

2670
2710
2640
2670
2640
2645
2625
2665
2775
2745

Sample 2

2
9
11
3
15
17
12
18
6
16

2390
2435
2415
2435
2465
2430
2420
2430
2410
2445

2590
2760
2665
2650
2700
2720
2675
2625
2690
2740

39
69
35
41
37
29
40
68
63
71

2440
2420
2410
2415
2400
2410
2410
2430
2435
2440

2695
2685
2680
2695
2655
2685
2670
2745
2735
2710

Sample 1

3.8

Water absorption of bricks for Batch 1

Sample 3

Table 3.6:

W (Water
absorption)%
( m md )
100 s
md
10.559
10.163
10.924
12.658
9.544
11.603
10.759
10.581
13.730
10.463
Mean x = 11.098
Std. dev. s =1.248
8.37
13.35
10.35
8.83
9.53
11.93
10.54
8.02
11.62
12.07
Mean x =10.461
Std. dev. s =1.772
10.45
10.95
11.20
11.59
10.63
11.41
10.79
12.96
12.32
11.07
Mean x =11.337
Std. dev. s =0.248

Compressive Strength
The bricks were tested for their compressive strength by imposing the bricks

to compression load until failure. The compressive machine used in the laboratory
was the Tonipact, with a capacity of 3000 kN. The machine was calibrated at the
early stage of the duration of the study.

68
In this work a study on the effects of compressive strengths of facing bricks
if tested in different orientations i.e. on its bed, stretcher and header face (Figure 3.7)
were conducted. Common bricks were only tested on their bed face.
Compressive strength tests were carried out on the same bricks after the
absorption test. Thus, the bricks were assumed to be fully saturated resulting from
the 5-hour boiling. To reduce friction caused by irregularities of the surface of the
bricks to be loaded, the bricks, placed in the machine were packed between two
pieces of plywood sheets, cut about 10mm bigger all round than the dimensions of
the brick. A fresh piece of plywood was used for every test.
In the test procedure, British Standard specifies that the rate of loading can
be gradually increased at a convenient rate not exceeding 35 N/mm2 until half of the
anticipated maximum load. Thereafter, the rate could be smoothly reduced to 15
N/mm2 and this rate to be maintained until failure. Although a higher rate of loading
could be used before half of the expected failure load, a constant rate of 15 N/mm2
were applied throughout the test in this work. A higher rate of loading was allowed
merely to reduce the time of testing and it is explained in the BS that higher rate of
loading at this stage has no influence on the ultimate strength. Therefore, a constant
rate of loading of 15 N/mm2 used throughout the test was justifiable. At failure the
brick collapsed and the machine stopped automatically. The maximum load was
recorded and the strength calculated by dividing the maximum load with the area of
the face subjected to loading i.e. bed face (length width), stretcher face (length
height) or the header face (width height). These areas used in the calculation were
based on the smaller of the two opposite faces.
Some typical results of compressive strengths of common bricks and facing
bricks for Batch. 1 are shown in Table 3.7 and 3.8 respectively. Example of results
for bricks tested on the stretcher face and header face are shown in Table 3.9 and
3.10 respectively. The complete results for compressive strengths are shown in
Appendix A5

69

Figure 3.6:

Compressive machine -Tonipact 3000

Figure 3.7 a: Bricks tested on bed face

Figure 3.7 b: Bricks tested on stretcher face

70

Figure 3.7 c: Bricks tested on header face


Table 3.7:

Compressive strength of common bricks for Batch 1 tested on bed


face

Sample 2

Sample 1

Length Width
(mm) (mm)

Area 1
(mm2)

Length Width
(mm) (mm)

Area 2
(mm2)

216.10
215.90
217.50
218.55
217.85
217.25
217.95
219.20
218.80
219.00

99.25
97.45
100.05
99.15
98.95
100.80
99.65
101.25
100.85
100.65

21447.93
21039.46
21760.88
21669.23
21556.26
21898.80
21718.72
22194.00
22065.98
22042.35

216.20
215.50
217.45
219.05
217.70
217.25
217.70
219.25
219.45
219.50

99.50
97.45
100.25
99.95
101.45
101.20
100.25
100.40
101.20
101.50

21511.90
21000.48
21799.36
21894.05
22085.67
21985.70
21824.43
22012.70
22208.34
22279.25

214.75
214.25
215.50
214.55
214.9
216.55
216.00
216.25
216.20
215.70

100.00
100.75
100.80
100.25
100.75
100.75
100.25
100.50
100.75
100.40

21475.00
21585.69
21722.40
21508.63
21651.17
21817.41
21654.00
21733.12
21782.15
21656.28

215.70
213.85
215.55
215.50
215.10
216.25
216.45
216.15
216.25
215.50

99.75
100.00
100.75
99.45
100.70
100.95
101.00
100.15
101.45
99.90

21516.07
21385
21716.663
21431.475
21660.57
21830.438
21861.45
21647.423
21938.563
21528.45

Smaller Maximum Compressive


area
load Kn. Strength
(mm2)
N/mm2
21447.93
825.30
38.48
21000.48
829.30
39.49
21760.88
631.30
29.01
21669.23
866.30
39.98
21556.26
671.30
31.14
21898.80
791.30
36.13
21718.72
546.30
25.15
22012.70
866.30
39.35
22065.98
613.30
27.79
22042.35
750.30
34.04
Mean x = 34.06
Std. dev. s = 5.47
21475.00
850.0
39.58
21385
813.0
38.02
21716.66
783.0
36.05
21431.48
582.0
27.16
21651.18
855.0
39.49
21817.41
730.0
33.46
21654
543.0
25.08
21647.42
786.0
36.31
21782.15
745.0
34.20
21528.45
695.0
32.29
Mean x = 34.16
Std. dev. s = 4.90

71

Sample 3

Table 3.7 (cont.)


216.20
215.90
216.50
217.75
217.85
217.35
218.20
218.75
218.80
219.00

99.05
97.00
100.25
99.25
98.35
100.20
99.15
101.05
100.85
100.65

21414.61
20942.30
21704.13
21611.69
21425.55
21778.47
21634.53
22104.69
22065.98
22042.35

216.20
215.50
217.45
219.05
217.70
217.25
217.70
219.25
219.45
219.50

99.35
97.45
100.30
99.95
101.25
101.20
100.25
100.40
101.20
101.50

21479.47
21000.48
21810.24
21894.05
22042.13
21985.70
21824.43
22012.70
22208.34
22279.25

21414.61
20942.30
21704.13
21611.69
21425.55
21778.47
21634.53
22012.70
22065.98
22042.35

830.00
38.76
790.00
37.72
636.00
29.30
840.00
38.87
567.00
26.46
794.00
36.46
543.00
25.10
833.00
37.84
614.00
27.83
749.00
33.98
Mean x = 33.23
Std. dev. s = 5.49

Table 3. 8: Compressive strength of facing bricks for Batch. 1 tested on the


bed face

Sample 2

Sample 1

Length Width Area 1


(mm) (mm) (mm2)

Length Width Area 2


(mm) (mm) (mm2)

216.10 98.50 21285.85 216.20 98.50 21295.70


212.85 100.00 21285.00 217.85 99.90 21763.22
217.75 99.35 21633.46 217.90 99.65 21713.74
218.95 99.95 21884.05 218.75 99.65 21798.44
219.50 100.55 22070.73 219.40 100.75 22104.55
217.25 99.40 21594.65 217.10 99.85 21677.44
219.50 100.25 22004.88 220.10 100.20 22054.02
217.20 99.80 21676.56 217.45 99.65 21668.89
215.20 97.60 21003.52 215.55 98.20 21167.01
216.60 98.70 21378.42 216.30 98.65 21338.00

217.05
219.25
217.30
219.90
217.50
217.55
216.95
217.50
217.00
217.00

100.50
101.00
99.50
101.45
99.85
99.10
99.25
99.55
100.00
99.40

21813.53
22144.25
21621.35
22308.86
21717.38
21559.21
21532.29
21652.13
21700.00
21569.80

218.15
219.50
217.35
220.50
217.05
217.70
217.00
217.10
217.20
216.45

100.75
101.10
99.45
101.35
100.05
99.00
99.15
99.50
99.85
99.25

21978.61
22191.45
21615.46
22347.68
21715.85
21552.30
21515.55
21601.45
21687.42
21482.66

Smaller Maximum Compressive


area load Kn. Strength
N/mm2
(mm2)
21285.85 894.10
42.00
21285.00 988.80
46.46
21633.46 944.90
43.68
21798.44 1036.90
47.57
22070.73 840.90
38.10
21594.65 820.90
38.01
22004.88 776.90
35.31
21668.89 913.90
42.18
21003.52 694.90
33.08
21338.00 844.90
39.60
Mean x = 40.60
Std. dev. s = 4.66
21813.53 1064.30
48.79
22144.25 957.30
43.23
21615.46 964.30
44.61
22308.86 977.00
43.79
21715.85 1091.90
50.28
21552.30 1106.00
51.32
21515.55 1113.00
51.73
21601.45 1187.00
54.95
21687.42 965.00
44.50
21482.66 1159.90
53.99
Mean x = 48.72
Std. dev. s = 4.40

72

Table 3. 9:

Compressive strength of facing bricks tested on the stretcher face

Sample 1

Length Width
(mm) (mm)
218.00
217.00
217.55
217.25
217.10
217.95
216.85
218.00
216.50
217.70

Table 3.10:

Area 1 Length Width


(mm2) (mm) (mm)

67.50 14715.00
67.30 14604.10
64.50 14031.98
67.75 14718.69
68.35 14838.79
66.90 14580.86
67.30 14594.01
67.10 14627.80
67.90 14700.35
67.75 14749.18

Sample 2

3.9

67.45
66.75
64.50
68.00
68.00
67.00
68.00
66.00
68.00
67.75

Compressive strength of facing bricks tested on the header face

Length Width Area 1


(mm) (mm) (mm2)
101.10
99.65
100.85
100.10
100.00
98.55
100.15
100.10
96.45
98.60

214.90
216.50
217.30
217.00
217.15
217.50
216.85
217.65
216.50
217.00

Smaller Maximum Compressive


load
Strength
area
(Kn.)
N/mm2
(mm2)
14495.01 14495.01
570.00
39.32
14451.38 14451.38
569.00
39.37
14015.85 14015.85
488.00
34.82
14756.00 14718.69
573.00
38.93
14766.20 14766.20
581.00
39.35
14572.50 14572.50
540.00
37.06
14745.80 14594.01
538.00
36.86
14364.90 14364.90
529.00
36.83
14722.00 14700.35
544.00
37.01
14701.75 14701.75
490.00
33.33
Area 2
(mm2)

68.95
68.05
67.25
67.85
68.75
67.95
67.30
68.20
67.70
67.95

6970.85
6781.18
6782.16
6791.79
6875.00
6696.47
6740.10
6826.82
6529.67
6699.87

Length Width Area 2


(mm) (mm) (mm2)
101.55
99.91
100.65
100.15
99.95
97.25
100.25
99.85
98.55
99.00

68.42
68.00
67.00
67.77
68.30
67.55
67.85
68.25
68.05
68.30

6948.05
6793.88
6743.55
6787.17
6826.59
6569.24
6801.96
6814.76
6706.33
6761.70

Smaller Maximum Compressive


load
Strength
area
N/mm2
(mm2) (Kn.)
6948.05
18.50
2.66
6781.18
27.00
3.98
6743.55
23.60
3.50
6787.17
26.70
3.93
6826.59
15.60
2.29
6569.24
29.70
4.52
6740.10
24.30
3.61
6814.76
20.80
3.05
6529.67
27.90
4.27
6699.87
28.40
4.24

Soluble Salt Content


Fragments of 10 bricks from the compressive strength test were randomly

selected to represent the exterior and interior of the bricks to make up the sample for
tests on soluble salts content. The sample was prepared by the crushing method as
given in BS : 3921 1985. About 25 gm. of ground brick passing sieve size 150 m.
were then collected as the sample and dried in the oven at 110 C.

73

The chemical test to determine the soluble salt content was carried out in the
laboratory of the Science Faculty of the Universiti Teknologi Malaysia. The soluble
salt comprises of water-soluble salts of calcium, magnesium, sodium and potassium
and acid-soluble sulphate. The acid-soluble sulphate was extracted in accordance to
the methods found in BS 3921 Appendix B.3.1 and the water-soluble salts,
Appendix B.4.1.
Sulphate was determined by the gravimetric method as described in BS
3921, Appendix B.3.2.2. In this traditional analytical process sulphate was
precipitated, filtered, and finally burned in a crucible. The mass of the acid soluble
sulphate M in gram was determined using equation 3.5 (BS 3921:1985). Results
showing the percentage of sulphates present in the various samples are shown in
Table 3.11.
M = 0.4115 ( m1 m0 )

(3.5)

Where,

m0 is the mass of the crucible in gm.


m1 is the mass of the crucible and burnt precipitate and paper in gm.
Table 3.11: Percentage of sulphate content in the samples from all batches

Sample

Batch 1

Batch
2

Batch
3

Batch
4

1
2
1
2
3
1
2
3
4
1
2
3

Mass of
precipitate
in gm.
( m1 m0 )

Mass of
sample,

0.0049
0.0045
0.0056
0.0031
0.0045
0.0010
0.0043
0.0020
0.0010
0.0011
0.0009
0.0009

2.6889
2.5288
2.4917
2.0387
2.0255
2.0315
2.0224
2.0224
2.0465
2.0819
2.0371
2.0072

Mass of sulphate
M = 0.4115 ( m1 m0 )

0.00202
0.00185
0.0023
0.00128
0.00185
0.00041
0.00177
0.00082
0.00041
0.00045
0.00037
0.00037

Percentage of
sulphate in
sample
M
100%
W
0.07
0.07
0.09
0.06
0.09
0.02
0.09
0.04
0.02
0.02
0.02
0.02

74

Calcium, magnesium, sodium and potassium were determined by the


instrumental method. The instrument used was the atomic absorption spectroscopy
(AAS) called GBC Avanta PGF 3000 Spectrometer. The AAS, which measures the
presence of metals in liquid samples works on the principal of atomising a sample
and quantitatively determining the concentration of atoms in the gas phase by
measuring the intensity of light absorbed. The schematic presentation of the process
is shown in Figure 3.8.

Flame

Light
source

Photomultiplier
Sample

Monochromator
Atomizer-burner

Figure 3.8:

A schematic diagram of an atomic absorption


spectrometer (Hammer, 1996)

Before testing the samples in the AAS, calibration curves for the salts of
calcium, magnesium, sodium and potassium were determined. This was carried out
by running standard solution, with known concentrations of the respective salts, on
the AAS and observing the absorbance readings from AAS (Table 3.12, 3.14 and
3.17). The salts concentrations (x) were plotted against the absorbance (y) to produce
calibration curves for each salt and the relationship between absorbance and
concentration were determined as shown by the equations in Figures 3.9, 3.10 and
3.11 for calcium, sodium and potassium and magnesium respectively.
Salts of calcium, sodium, potassium and magnesium were extracted from the
samples as given in Appendix B of BS 3921:1985. The filtrate from the samples was
run in the AAS which gave the readings of absorbance for each salts. Using the
equations from the calibration curves and with readings of the absorbance from

75

AAS, the concentration of the salts in the samples could be determined. Tables 3.13,
3.15, 3.16 and 3.18 show the corresponding percentage of calcium, potassium,
sodium and magnesium in the samples.
Table 3.12:
Sample
label

Standard calibration data for calcium

Concentration
Mean
mg/l
Absorbance
from AAS

Blank

Replicates

0.002

0.002

0.002

0.002

Standard 1

0.202

0.203

0.201

0.202

Standard 2

10

0.41

0.409

0.413

0.41

Standard 3

15

0.618

0.615

0.619

0.62

Standard 4

20

0.814

0.811

0.81

0.82

Standard 5

25

1.023

1.023

1.023

1.023

Absorbance

1,2
1
0,8
0,6

y = 0,0409x - 0,0004
R2 = 0,9999

0,4
0,2
0
0

10

15

20

25

30

Concentration,mg/l

Figure 3.9: Calibration curve for detection of calcium

76

Batch 4

Batch 3

Batch 2

Batch 1

Table 3. 13: Percentage of calcium in samples for all batches


Absorbance
Sample from AAS,
y

Concentration, x
y + 0.0004
x=
0.0409
mg/l

Volume
of solution, v
mL

Percentage of
Weight
calcium in sample
of sample, w
xv
100
gm.
w 106

0.543

13.286

100.0

10.1117

0.013

0.580

14.185

100.0

10.3982

0.014

0.122

3.013

100.0

10.1036

0.003

0.238

5.854

100.0

10.0147

0.006

0.647

15.813

100.0

10.0549

0.016

0.414

10.147

100.0

10.0096

0.010

0.281

6.904

100.0

10.0337

0.007

0.450

11.023

100.0

10.0844

0.011

0.284

6.977

100.0

10.0238

0.007

0.311

7.636

100.0

10.0161

0.008

0.390

9.562

100.0

10.0294

0.009

0.420

10.293

100.0

10.0366

0.010

Table 3.14:
Sample
Label

Standard calibration for sodium and potassium


Sodium

Potassium

Concentration
Mean
Concentration
Mean
mg/l
Absorbance
mg/l
Absorbance
from AAS
from AAS
0.004

Blank

0.002

Standard 1

0.222

0.172

Standard 2

0.44

0.338

Standard 3

0.681

0.514

Standard 4

0.887

0.682

Standard 5

1.099

10

0.865

77

Absorbance

1,2

y = 0,2201x + 0,0055
2
R = 0,9993

y = 0,0865x - 0,0048
R2 = 0,9998

0,8
0,6
0,4
0,2
0
0

10

12

Concentration Mg/l

Sodium

Potassium

Figure 3.10: Calibration curve for detection of sodium and potassium

Batch 4

Batch 3

Batch 2

Batch 1

Table 3. 15: Percentage of potassium in samples for all batches


Absorbance
Sample from AAS,
y

Concentration, x
y + 0.0048
x=
0.0865
mg/l

Volume
of solution, v
mL

Percentage of
Weight potassium in sample
of sample, w
xv
100
gm.
w 106

0.282

13.286

100.0

10.1117

0.003

0.276

14.185

100.0

10.3982

0.003

0.549

3.013

100.0

10.1036

0.006

0.743

5.854

100.0

10.0147

0.009

0.623

15.813

100.0

10.0549

0.007

0.297

10.147

100.0

10.0096

0.003

0.511

6.904

100.0

10.0337

0.006

0.399

11.023

100.0

10.0844

0.005

0.290

6.977

100.0

10.0238

0.003

0.352

7.636

100.0

10.0161

0.004

0.356

9.562

100.0

10.0294

0.004

0.367

10.293

100.0

10.0366

0.004

78

Absorbance
Sample from AAS,
y

Concentration, x
y 0.0055
x=
0.2201
mg/l

Volume
of solution, v
mL

Weight
of sample, w
gm.

Percentage of
sodium in sample
xv
100
w 106

0.587

2.642

100.0

10.1117

0.003

0.427

1.915

100.0

10.3982

0.002

0.791

3.569

100.0

10.1036

0.004

0.546

2.456

100.0

10.0147

0.002

0.564

2.537

100.0

10.0549

0.003

0.316

1.411

100.0

10.0096

0.001

0.574

2.583

100.0

10.0337

0.003

0.355

1.588

100.0

10.0844

0.002

0.332

1.483

100.0

10.0238

0.001

0.538

2.419

100.0

10.0161

0.002

0.498

2.238

100.0

10.0294

0.002

0.374

1.674

100.0

10.0366

0.002

Table 3.17: Standard calibration for magnesium


Sample
label

Concentration
mg/l

Mean
Absorbance from
AAS
0.001

Blank
Standard 1

0.176

Standard 2

0.349

Standard 3

0.514

Standard 4

0.701

Standard 5

0.887

Absorbance

Batch 4

Batch 3

Batch 2

Batch 1

Table 3. 16: Percentage of sodium in samples for all batches

0,8
0,6
y = 0,1774x - 0,0068

0,4

R = 0,9993

0,2
0
0

Concentration mg/l

Figure 3.11: Calibration curve for detection of magnesium

79

Concentration, x
Absorbance
y + 0.0068
Sample from AAS, x =
0.1774
y
mg/l

Volume
of solution, v
mL

Weight
of sample, w
gm.

Percentage of
magnesium in
sample
xv
100
w 106

0.476

2.722

100.0

10.1117

0.003

0.29

1.673

100.0

10.3982

0.002

0.428

2.451

100.0

10.1036

0.002

0.57

3.251

100.0

10.0147

0.003

1.069

6.064

100.0

10.0549

0.006

0.694

3.950

100.0

10.0096

0.004

0.588

3.353

100.0

10.0337

0.003

0.747

4.249

100.0

10.0844

0.004

0.573

3.268

100.0

10.0238

0.003

0.477

2.727

100.0

10.0161

0.003

0.513

2.930

100.0

10.0294

0.003

0.832

4.728

100.0

10.0366

0.005

3.10

Efflorescence

Batch 3

Batch 2

Batch 4

Batch 1

Table 3. 18: Percentage of magnesium in samples for all batches

Ten bricks were required for the efflorescence test. Each brick was covered
with plastic sheet around the three sides, leaving one side exposed to the atmosphere
(Figure 3.12). A wide mouth bottle filled with distilled water was then inverted on
top of this exposed surface for a duration of 48 hours. The bottle should always
contain water and toped up whenever necessary. After 48 hours, the bottle was
removed and the exposed surface left to dry for 9 days in the laboratory conditions.
A warm place in the laboratory with natural air circulating was selected for this
purpose. This procedure was repeated but for the second time a drying period of 16
days was allowed. After these cycles of wetting and drying the exposed surface of
each specimen was examined for efflorescence. Efflorescence was rated in
accordance to the bricks that showed maximum effects.

80

Figure 3.12:

Efflorescence test

CHAPTER 4

STATISTICAL ANALYSIS OF TEST SPECIMENS

4.1

Introduction
This chapter presents the theoretical approaches to statistical calculations and

methods of sample analyses in deriving estimates of population representation.

4.2

General Approach for Analysing Samples


In principle, the processing of sample data involves several steps. The first

step is usually to describe data characteristics by showing its averages and


dispersion. Data could be represented graphically by the histograms and frequency
curve. Besides showing data distribution, the histogram and frequency curve
provides selection on the probability functions to be used as a mathematical model
in deducing the estimate of population mean from samples.
In a typical statistical analysis, before any estimates could be accepted,
results from samples have to be tested and this is referred to as hypothetical testing.
Quality control charts developed from normally distributed data could be regarded
as a form of hypothetical testing (BS 2846:Part 1:1991- Guide to statistical
interpretation of data). In this graphical form, a quick assessment could be made to
detect the homogeneity of data.

82
The analysis of variance (ANOVA) is another form of statistic hypothetical
testing. In an ANOVA, the F-test is carried out to test the null hypothesis (N.H.) of
no significance difference between variances in samples. From the ANOVA the
components of variance could be analysed and the best estimate of population
variance derived.

4.2.1

Description of Data
A group of observations or data is usually described by computing its

descriptive statistics comprising of its averages which include the mean, median and
mode and its dispersion, consisting of the standard deviation, variance and the range.
The sample mean shows the average value of data in a sample, given by
Equation 4.1 (Bland, 1985)
Sample Mean x =

n
i =1 i

(4.1)

For a set of n values x1 , x2 ,...xn


Where,
x= the measurements or observations
n= the numbers of observations.
The median and the mode are also averages that described the sample. The
median in a set of data is the central observation, the values being ranked in order of
size. In other words, half of the data will have a value less than the median, and the
other half of the data will have a value greater than the median.
Mode is a value that occurs with the greatest frequency. A comparison of the
mean and median and mode can reveal information about skewness of the
distribution curve as illustrated in Figure 4.1.

83
The spread of the data or the dispersion can be measured by the standard
deviation, range, variance and the coefficient of variation (c.v.). These
measurements show the variation of each data from their mean. Variance and
standard deviation is computed using equation 4.2 and 4.3 respectively (Bland,
1985). The standard deviation for a sample is a square root of the variance and is
more often used to describe data. The standard deviation has an advantage over the
variance since it has the same unit as the variable tested. The c.v. given in equation
4.4 is a measurement of relative dispersion since it is given on a percentage basis.
Range (equation 4.5), is the difference between the highest and the lowest data. It is
a quick way of analysing data variation. However, its use is limited to small sample
only since it is obtained from two extreme values without giving consideration on
other data in the range.
The range and standard deviation are related so that for any given value of
observations n, an estimate of the standard deviation, sestimate can be made from the
mean value of sample range R (equation 4.6).
n
2
(x x )

Sample variance, s 2 = i =1
n 1

Sample standard deviation, s =

Coefficient of variation, c.v. =

n
2
( xi x )
i =1

n 1

s
100 %
x

(4.2)

(4.3)

(4.4)

Range, R = max xi min xi

(4.5)

sestimate = R d (BS 2846: Part 1, 1991)

(4.6)

Where,
d is a coefficient based on the number of observations n, given in Appendix
B Table B3.

84

Frequency

Mode

Value of observation

Median
Mean

Figure 4.1:

Mean, median and mode in a distribution


skewed to the right

4.2.2 Histograms and Normal Distribution Curve


Histograms are statistical graphs showing frequency of data where horizontal
axis and vertical axis represent the class interval (i) and the frequency respectively.
In a histogram, if the number of data were increases, the number of classes will
increase and subsequently the class widths decreases. As a result the histogram
approaches a smooth curve, thus called the frequency distribution curve.
Past observations revealed that most physical measurements could be
approximated to a normal distribution curve (Chatfield, 1979, Paradine and Rivettes,
1960); the approximation improves as number of variables increased. In virtue of the
central limit theorem, we can assume that data would eventually approach a normal
distribution for greater number of data. The normal distribution function also known
as normal probability density functions is given by equation 4.7 (Grimm, 1988).

f ( x) = (2 ) 1 2 exp ( x x ) / 2s

(4.7)

85
Where,

f ( x) = normal probability density function for a sample. This refers to the


height of an ordinate at a distance x x from the mean.
s = standard deviation of sample.
Equation 4.7 is transformed to the standard normal distribution function by
putting z = ( x x ) s as shown by equation 4.8 (Grimm, 1988).
f ( z ) = ( 2 )

1 2

exp ( z 2 2 )

(4.8)

Where,
f ( z ) is the normal probability density function for a sample in terms of z.
The computed frequency illustrated in the form of a histogram is given by equation
4.9 (Grimm, 1988).
y = ni f ( z ) s

(4.9)

Where,
n= number of samples
i= number of units in a class interval
s= standard deviation of sample
The integration of equation 4.8 between any values of z produces the normal
probability function, i.e. the area under the curve between the stated values of z. The
area under the probability curve divided into hundred equal parts gives the percentile
values and a 33-percentile value divides the curve into three parts. Grimm (1988),
highlighted that values falling in the upper 33 percentile could be grouped as those
of high values. The lower 33 percentile are regarded as low values whilst normal
values are those lying in the middle third of the distribution.

4.2.3

Log-normal Distribution Curve


If distribution of data is skewed, where the mean, mode and median are not

coincident as in normal distribution then log normal distribution could be used. The
log-normal distribution is essentially the same as the normal, but with ln (x)

86
substituted for x. The log-normal has probability distribution function given by
equation 4.10. Grimm (1988) suggested that log-normal distribution is useful for
data with c.v. ( ) exceeding 30%.

f ( x) = (2 ) 0.5 ( x) 1 exp ( ln x ) / 2 2

(4.10)

0.5
= ln x (1 + 2 )

(4.11)

=s x

(4.12)

= ln (1 + 2 )

0.5

(4.13)

Where,
z = ( ln x ) 1

(4.14)

f ( z ) = (2 ) 0.5 1 exp ( z 2 2 ) z

(4.15)

y = ni f ( z )

(4.16)

Where,
y = the histogram ordinate at any value of x in the histogram,
n = number of data in the histogram,
i = x interval in the histogram,

= c.v. in decimal.
An application of this statistical analysis will be demonstrated in section 4.3
for samples used in this research.

4.2.4 Derivation of Population Estimates


Assuming that data is normally distributed, therefore the functions of the
normal distribution curve could be used to derive estimates for the population.
For a normal distribution curve the integration of equation 4.8 of the normal
curve between specified limits is a probability function, which represents the area

87
under the normal curve. The full range of this probability function could be found in
statistical table. However, limits, which are of importance to this work is shown here
in Figure 4.2. From Figure 4.2 it can be seen that approximately 70 % of sample
data will lie within the area covered by a point on each side of the mean value,
denoted by one unit of standard deviation i.e.1 . About 95 % will lie within the
area bounded by 1.96 on each side of the mean and 99 % at 3.09 from each side
of the mean. The distribution at 95 % probability is important in a production. It
provides a 95 % confidence that not more than 1 in 40 results would be below the
required specification limits. Therefore, a 95 % confidence of the population mean
can be estimated from sampling distribution using equation 4.17 (Bland, 1985).

= x 1.96 s

(4.17)

Where,

= population mean
x = sample mean
s = sample standard deviation
n = sample size

x= -3.09 x= -1.96
z=-3.09 z=-1.96

13.60 %

34 13%

13.60 %

2.14%

34 13%

f(x), f(z)

x = -1

x= 0

x=1

z=-1

z=0

z=1

Figure 4.2:

2.14%

x=1.96 x= 3.09
z=3.09
z=1.96

x
z

Areas under normal probability curve

In virtue of the central limit theorem, the estimate is good on normally


distributed data with large samples size, i.e. n greater than 30 (Bland, 1985 and
Triola, 1989). If n is smaller than 30 the distribution of sample data will follow, the t

88
distribution and value of 1.96 from equation 4.7 will be replaced by tc (the
percentage point of the t distribution which can be obtained from Appendix B Table
B2). Thus, the population estimate of the mean ( ) for a small sample is given by
equation 4.18 (Bland, 1985).

= x tc

s
n

(4.18)

The t-distribution, formulated by W.S. Gosset in 1908 has similar properties


to the normal distribution except that it has more spread about the mean as shown in
Figure 4.3. Another important feature of the t-distribution is that it has different
curves for different sample sizes. The t distribution depends on a parameter called
degrees of freedom (df) given by n-1, where n denotes the samples size.

x (Mean)
N orm al distribution
t distributio n w ith n= 20
t distribution w ith n=10

Figure 4.3:

T-distribution curves for various values of n


(Chatfield, 1978)

The sample size in this research is smaller than 30, therefore, the tdistribution was used in conjunction with equation 4.18 to arrive at the mean value
of the population. Example of these will be illustrated in section 4.3.4.

89
4.2.5

Hypothesis Testing

4.2.5.1 Analysis of Variance (ANOVA)


The analysis of variance (ANOVA) is a statistical tool developed from
normal distribution theory and is used for testing the significance difference of
several means. The ANOVA in testing a hypothesis that there is no difference in the
means between samples is called a single factor ANOVA.
A single factor ANOVA is accomplished by analysing the variance and by
partitioning the total variance into two, the component due to true random error i.e.
within samples ( MS within ) and the component due to differences between means of
several samples ( MSbetween ). These two components are compared by means of an Ftest as shown in equation 4.19.
Fcalc = MSbetween MS within

(4.19)

If Fcalc is smaller than the value of the Fcrit given in statistical table of the Fdistribution (Appendix B Table B1), then the N.H. is accepted. This implies that
there is no significant difference between the means of the several samples and
within samples and therefore, the best estimate for the variance is the total variance
from within and between samples. On the other hand if Fcalc is larger than Fcrit , then
the differences between the variance is considered significant. Therefore, the null
hypothesis of no differences between means is rejected and the alternative
hypothesis that the means are significantly different is accepted. Table 4.1 shows the
components of variance for the case when the N.H. is accepted or rejected.

90
Table 4.1: Components of variance from ANOVA
Source of Sum of
Variation Squares
(1)

Degrees of
Freedom

SS
(2)

df
(3)

Mean square When the N.H. When the N.H. is


MS
is accepted the rejected the mean
mean square is square (MS) is an
(2)(3)
an estimate of
estimate of
(4)
(5)
(6)
SSbetween df

Between SS
between
samples

No. of samples 1

Within
samples

Total specimens
SS within df
in samples No. of
samples

Total

SS within

SSbetween Total specimens


+ SS within in samples 1

Total SS
Total df

2 + c r2
c= sample size

Best estimate of

Referring to Table 4.1 of the ANOVA, when the N.H. is rejected, the mean
square (MS) is an estimate of 2 + c r2 . With c known i.e. size of sample and the
value of 2 + c r2 can be obtained from col. (4) of Table 4.1, r2 the variance
between samples can be computed. This gives the new estimate of population
variance from the ANOVA as 2 + r2 (Loveday). In this study, the ANOVA was
particularly used to derive the best estimate for the variance between and within
samples in estimating the population means.
4.2.5.2 Control Charts
Control charts are graphical techniques used mainly to assess quality of a
production in an industry since it gives a rapid indication of the population quality
and enables appropriate action to be undertaken when necessary. A process is said to
be in control if there is no significant changes in the means and standard deviation.
Thus two control charts are required, one for monitoring the mean and the other one
for monitoring the variations. Examples of control charts for means and ranges are
as shown in Figures 4.4 and 4.5 respectively.
The three basic components of a control charts (Figure 4.4) are:
(i)

A centre line, which represents the mean, for the respective mean or
range chart of samples.

91
(ii)

Statistical control limits, i.e. the upper and lower action and warning
lines. These define the constraints for variations and if exceeded
shows that the process is out of control or data is not homogeneous.

(iii)

Performance data plotted over time of production.

Two pairs of control limits are used. The first pair represents warning or
inner limits. These are set so that there is a 2.5 % probability (1 in 40) of a sample
mean having a value below the lower limit and a 2.5 % probability of its having a
value above the upper limit. The action or outer limits are set so that there is a
probability of 0.1 % (1 in 1000) of the mean falling above the upper limit and a
probability of 0.1 % of its falling below the lower limit. A process is said to be in
statistical control if only 1 out of 40 samples is found outside the warning lines and
1 out of 1000 samples outside the action lines.
Control charts could also be used to test homogeneity of data in samples (BS
2846: Part 1:1991- Guide to statistical interpretation of data). In terms of
homogeneity the occurrence of a single point outside 1 in 1000 control lines or of
more than one or two outside the 1 in 40 control lines is considered to be evidence
that data are not homogeneous.
The upper and lower warning and action lines for means are given by
equation 4.20 and 4.21.
Warning lines = x 1.96 x

(4.20)

Action lines = x 3.09 x

(4.21)

Where,
x = mean of sample means

x = standard deviation of mean


x =

s
n

(4.22)

Where s is the estimate of the population standard deviation and n the sample size.
The value s is given in equation 4.6.
s = Rd

(4.23)

92

Hence, the warning limits for the mean (MWL)= x


Putting

1.96Rd
n

(4.24)

1.96d
'
= A0.025
, the warning limit for the mean become
n

'
R
MWL = x A0.025

(4.25)

Similarly the action limits for the mean (MAL) are


MAL = x
Putting

3.09Rd
n

(4.26)

3.09d
'
= A0.001
, the action limits for the mean become
n

'
R
MAL = x A0.001

(4.27)

In the range chart, warning (RWL) and action (RAL) lines are given by
equation 4.28, 4.29, 4.30 and 4.31 respectively (BS 2846: Part 1:1991).
'
The upper RWL = D0.025
R

(4.28)

'
R
The lower RWL = D0.975

(4.29)

'
R
The upper RAL = D0.001

(4.30)

'
R
The lower RAL = D0.999

(4.31)

The control limit factors A' for mean and D ' for range can be obtained from
Appendix B, Table B4.

93

130

Upper action line


Upper warning line

Sample mean

125

Mean
120
Lower warning line
115
110

Lower action line


1

10
20
15
Sample Number

25

20

Upper action line


Upper warning line

Sample range

15

10

Mean

5
0

Lower warning line


Lower action line
1

Figure 4.4:

20
10
15
Sample Number

25

Control charts for sample means and ranges


(Neville, 1985)

4.3

Application of Statistical Methods for Samples Under Investigation


The statistical principles explained in section 4.2 were used throughout the

work for processing sample data. The statistical computations in this work were
facilitated by the computer software, Microsoft Excel 2000.

94
An example of the application of these analyses is shown here with the
results of water absorption test. The statistical process as shown in Figure 4.5 is
described below:
i)

First, the average and dispersion of data from samples in all batches
were determined through the computations of the descriptive
statistics consisting of the mean, median, mode, standard deviation,
range, and c.v. (Table 4.2).

ii)

The distribution of data was shown graphically by plotting the


histogram. Assuming data to be normally distributed a normal curve
fit was computed (Table 4.4) and the normal curve superimposed on
the histogram as shown in Figure 4.6. Using the normal probability
function the 33-percentile values were determined to identify the
distribution of data for good, medium and low values corresponding
to the upper, middle and lower 33-percentile values.

iii)

Control charts of samples means and ranges were plotted to check the
homogeneity of data. The data were examined for outliers i.e. data
not complying with control charts criteria for homogeneity and would
be regarded as not representing the population in the study and thus
ignored in the analysis of estimates.

iv)

The F-test from ANOVA was performed to test the null hypothesis
that there was no significant difference between the variances in the
samples. From the ANOVA the components of variance were used to
derive estimate of population variance.

v)

Lastly, estimates of population mean for small sample i.e. n< 30 at 95


% confidence were deduced using equation 4.18. Since the size of
samples i.e. number of specimens in a sample were less than 30 for
all the tests considered in this research therefore, equation 4.18 were
used throughout in this study.

95

Data

Descriptive statistics

Mean
Median
Mode
Standard deviation
Range
Coefficient. of variation

Histogram and
frequency curve
Assuming data to be
normally distributed

To test data
homogeneity

Control charts
Non-homogeneous
Homogeneous
Examine data
for outliers

Deriving estimates from


normal probability function

ANOVA /F-test

To test
significance of
difference in the
variance of
samples

No significance
difference in
the variance

Significant

Components
of variance

Deducing population
estimates

Figure 4.5:

Process of statistical analysis

96
4.3.1

Description and Presentation of Sample Data


Water absorption in every specimen of bricks from samples in Batches 1, 2,

3 and 4 were determined and the descriptive statistics consisting of the mean,
median, mode, standard deviation, variance, range, and c.v. for all data were
computed and tabulated (Table 4.2).
The graphical presentation of data is shown by plotting the histogram and the
normal curve fit. To plot the histogram, data were grouped into 10 classes. In
accordance to BS 2849 (Guide to statistical interpretation of data), groupings could
consist of between 10 and 20 classes. Having decided on the number of classes, the
class intervals (i) were determined. From Table 4.2, the maximum value was 14.376
and the minimum was 7.655. The range (R) is the difference between the maximum
and the minimum. If there were 10 class intervals, there were about R/10 or 0.7 units
per class interval, i.e. i = 0.7. The frequency of data occurrence against these
selected class intervals could then be determined. Data frequency distribution is
given in Table 4.3 and its histogram plotted as shown in Figure 4.6. It could be
observed from the histogram that a few range of high values were located
approximately towards the centre of the distribution and smaller values tailing on
both sides from the centre, a typical feature of a normally distributed data.
Therefore, in virtue of the central limit theorem, with greater number of data it could
be assumed that the contour of the histogram would eventually approach a normal
curve.
Since data were assumed to be normally distributed a curve normalised to fit
in the distribution were constructed. In the construction of the normal curve, the
ordinates were computed at every midpoint of the intervals in the histogram using
equation 4.9. These ordinates as shown in column 5 of Table 4.4 were used to plot
the normal curve, which is superimposed on the histogram (Figure 4.6). From the
normal curve, it was seen that the values of the mean, median and mode did not
coincide meaning that it was skewed. In cases like this, Grimm (1988) suggested
that normal curve function could still be used for the probability analysis if the c.v.
of data in the samples does not exceed 30%.

97
Coefficient of variation was found to be 11.4 % which is less than 30 % and
therefore, in accordance to Grimm do not require a log-normal function for its
probability analysis. However, a log-normal curve was plotted to verify this theory
by Grimm. The ordinates for the log-normal curve were derived using equations
4.11 through equations 4.16.These ordinates as shown in column 8 of Table 4.4 were
used to plot the log-normal curve (Figure 4.6). It was found that it almost overlap
with the normal curve. Hence, this proved Grimms theory that a log-normal curve is
only useful for data with c.v. of more than 30%.
To enhance the application of this theory further, some verifications
regarding this application for a case of higher c.v. was felt necessary. Therefore,
results for compressive strength of common bricks having a c.v. of 25.4 %, was
computed for its log-normal curve. Table 4.5 shows the computed normal and lognormal frequency at the midpoint of each interval in the histogram and with these
data, the normal and log-normal curves were drawn on the histogram (Figure 4.7). It
was found that there was a greater shift between these two curves. In order to check
the reliability of results, if probability is based on normal curve for such cases, the
33 percentile values for both the normal and log-normal curve were computed. The
33 percentile values for the normal curve were computed with the aid of the
Microsoft Excel statistical programme. As for the log-normal curve, since,
z = (ln x ) 1
Therefore, x = exp( z + )

(4.32)

The upper 33 percentile was at z = 0.4317 and lower 33 percentile was at


z = -0.4317 (From Table 4.7). Using equation 4.11 and 4.13 to calculate values of

and , x could then be determined from equation 4.32 for both the upper and
lower 33 percentile values. These values were compared against the values from the
normal curve and tabulated in Table 4.6. It was found that the differences were
relatively small, approximately 2.5%. Therefore, this verified Grimms theory that
the normal distribution probability function could be used for data with c.v. less than
30 %.

98
Table 4.2: Water absorption of specimens in each sample for facing bricks
Sample
Batch
1

Water Absorption in specimens (%)

10.56 10.16 10.92


1
8.37
13.35 10.35
2
10.45 10.95 11.20
3
11.58 12.59 10.71
4
11.83 12.93 12.22
5
10.82 13.12 12.37
6
12.03 11.45 10.85
Batch 7
2
12.36 10.36 10.12
8
11.89 12.70 11.20
9
12.01 10.37 11.63
10
13.14 11.45 12.67
11
11.89 11.30 12.05
12
9.86
8.95 11.01
13
12.37 11.16 12.21
14
11.87 11.63 10.50
Batch 15
3
7.66
10.31 11.33
16
8.84
9.18
9.27
17
10.37 10.24 11.05
18
11.15 10.82 12.09
19
8.57
13.61 11.63
20
12.61
8.64 12.14
21
10.32
9.64 11.44
22
9.31
13.14 11.98
Batch 23
4
12.29 10.95 13.03
24
12.71
8.94
9.56
25
11.70
7.93
9.34
26
12.54 12.17 12.00
27
Descriptive Statistics
Mean, x
= 11.23%
Median
= 11.35 %
Mode
= 12.25 %
Variance
= 1.649
Standard deviation, s = 1.284 %
Maximum
= 14.377
Minimum
= 7.655
Range, R
= 6.72 %
Coefficient of variation, c.v. = 11.43 %

12.66
8.83
11.59
10.80
13.79
12.43
11.60
12.37
9.65
10.03
12.10
12.70
11.40
10.55
10.30
12.03
8.80
10.29
9.35
12.40
11.74
11.08
10.36
12.61
11.69
10.06
7.92

9.54
9.53
10.63
11.57
11.13
10.87
11.74
11.56
11.56
11.70
11.03
10.49
11.77
12.12
11.08
9.67
10.13
11.51
9.86
11.04
9.67
10.62
12.74
13.48
12.36
11.65
12.67

11.60
11.93
11.41
12.03
10.40
11.49
12.33
10.65
11.94
12.79
12.25
10.52
10.21
12.83
11.79
11.36
9.59
11.91
10.11
11.47
12.09
13.99
12.94
12.44
13.39
12.09
12.40

10.76
10.54
10.79
10.83
12.40
10.04
12.21
11.99
11.12
10.29
12.15
10.38
11.55
11.12
9.15
11.55
9.25
11.41
10.24
8.47
12.03
13.33
9.31
12.75
10.69
8.58
11.33

10.58
8.02
12.96
11.25
11.18
11.93
12.98
11.53
12.75
9.40
11.14
12.74
11.95
10.66
10.84
10.30
9.12
11.41
10.45
11.64
8.61
11.10
12.74
14.38
11.76
9.23
8.83

13.73
11.62
12.32
13.37
12.44
11.26
12.95
12.25
13.15
12.15
11.76
10.43
12.25
11.31
11.71
10.84
9.49
9.46
12.17
9.97
11.78
9.86
13.52
12.11
12.67
11.05
11.46

10.46
12.07
11.07
10.58
10.91
11.20
11.93
10.45
12.02
13.55
11.52
11.29
10.78
11.01
10.00
9.84
10.37
10.57
11.41
11.69
8.25
10.03
11.34
11.91
11.13
13.02
11.76

99
Table 4.3:

Frequency distribution of data for facing bricks


Class interval

Frequency

7.555-8.255
8.255-8.955
8.955-9.655
9.655-10.355
10.355-11.055
11.055-11.755
11.755-12.455
12.455-13.155
13.155-13.855
13.855-14.555

6
15
19
24
48
59
58
28
10
3

70

Frequency

60

Log- normal
curve

50
40

Normal
curve

30

x = 11.23%
Median = 11.3%
Mode = 12.25%
s = 1.28
c.v. = 11.4%

Low<10.68 %
Normal=10.68- 11.85 %
High >11.85 %

20
10

13.855-14.555

13.155-13.855

12.455-13.155

11.755-12.455

11.055-11.755

10.355-11.055

9.655-10.355

8.955-9.655

8.255-8.955

7.555-8.255

Water absorption in percentage

Figure 4.6:

Histogram, normal curve and log-normal curve, for water


absorption of bricks

Table 4.4:

Normal and log-normal curve fit for water absorption

Normal curve
Interval
midpoint

Observed
frequency

Number of
standard
deviations, z

(x - x) s
(1)
7.905
8.605
9.305
10.005
10.705
11.405
12.105
12.805
13.505
14.205

(2)
6
15
19
24
48
59
58
28
10
3

(3)
-2.589
-2.043
-1.498
-0.953
-0.408
0.137
0.682
1.228
1.773
2.318

f ( z)

( 2 )

-1 2

exp - ( z 2 2 )

(4)
0.014
0.049
0.130
0.253
0.367
0.395
0.316
0.188
0.083
0.027

Log-normal curve
Computed frequency
ordinate, y
ni f ( z ) s
(Normal curve in Fig.
4.6 shown in red.)
(5)
2.059
7.278
19.112
37.282
54.029
58.167
46.520
27.639
12.199
4.000

Number of standard
deviations, z
( ln x - ) -1

f ( z)

( 2 )

-1

exp - ( z 2 2 ) - z -

(6)
-3.023
-2.279
-1.593
-0.956
-0.363
0.193
0.715
1.208
1.675
2.119

-0.5

(7)
0.005
0.030
0.106
0.221
0.306
0.301
0.224
0.132
0.064
0.026

Computed frequency
ordinate, y
ni f(z)
(Log-normal curve in Fig.
4.6 shown as broken line.)
(8)
0.866
5.728
19.995
41.849
57.851
56.933
42.312
24.889
12.035
4.934

100

Table 4.5:

Normal and log-normal curve fit for compressive strengths of common bricks
Normal curve

Interval
midpoint

Observed
frequency

Number of
standard
deviations, z

(x - x) s
(1)
20.35
24.35
28.35
32.35
36.35
40.35
44.35
48.35
52.35
56.35

(2)
14
11
11
14
18
24
10
13
4
1

(3)
-1.695
-1.253
-0.812
-0.371
0.070
0.512
0.953
1.394
1.836
2.277

f ( z) =

( 2 )

-0.5

exp - ( z 2 2 )

(4)

Log-normal curve
Computed
frequency
ordinate, y
ni f ( z ) s
(5)

0.095
0.182
0.287
0.372
0.398
0.349
0.253
0.151
0.074
0.029

5.025
9.630
15.191
19.721
21.071
18.530
13.412
7.990
3.918
1.581

Number of
standard
deviations, z
( ln x - ) -1
(6)
-2.126
-1.408
-0.799
-0.271
0.196
0.614
0.992
1.338
1.656
1.951

f ( z) =

( 2 )

-0.5

-1

exp - ( z 2 2 ) - z -
(7)

Computed
frequency
ordinate, y
y = ni f ( z )
(8)

0.0082
0.0243
0.0409
0.0476
0.0431
0.0328
0.0220
0.0135
0.0077
0.00423

3.9287
11.6834
19.6463
22.8401
20.6849
15.73416
10.5646
6.4784
3.7163
2.0291

101

102
30

Log-normal
curve

Frequency

25

Normal
curve

20
15
10
5

54.35-58.35

50.35-54.35

46.35-50.35

42.35-46.35

38.35-42.35

34.35-38.35

30.35-34.35

26.35-30.35

22.35-26.35

18.35-22.35

Compressive Strength N/mm2

Figure 4.7: Histogram, normal curve and log-normal curve for compressive
strength of common bricks (c.v. approaching 30%)
Table 4.6:

Comparisons of 33 percentile values from normal and log-normal


curve for compressive strength of common brick

Percentile
33

Normal curve
31.86735

Log-normal curve
31.07525

67

39.53042

38.55586

Table 4.7:

Probability that x will not be exceeded (adapted


From Grimm, 1988)

Probability, %
1
5
10
20
25
30
33.3
40
Mode
50 (median)
Mean
60
66.7
70
80
90
95
99
99.5
99.9

z
-2.3267
-1.645
-1.28
-0.842
-0.674
-0.524
-0.4317
-0.253

0
2
0.253
0.4317
0.524
0.842
1.28
1.645
2.3267
2.575
3.10

103
4.3.2

Test for Data Homogeneity


The control chart was used for testing data homogeneity. The first step in the

construction of the control chart was to divide the observations into a convenient
subgroup on a time basis. The 27 samples constitute the subgroups. The means and
ranges of each sample were then determined (Table 4.8).
The means and ranges for every sample were plotted for the respective mean
and range chart (Figure 4.8 and 4.9).The upper and lower warning limits (MWL)
and action limits (MAL) for the mean chart were determined using equations 4.25
and 4.27, respectively. With respect to the range chart, the upper and lower warning
limit (RWL), were computed from equations 4.28 and 4.29 respectively. While, the
upper and lower action limits (RAL) were determined from equation 4.30 and 4.31,
respectively. These values for control limits were shown in Table 4.9.
From the control chart for sample means in Figure 4.8 it could be seen that
there were 2 points each located outside the upper and the lower action lines. These
two points from sample 17 and 24 were considered as outliers and were assumed to
contribute to the non-homogeneity of data. Therefore, to be reasonably confident
that estimates derived from samples were representative of the population these two
data points were disregarded in the analysis of the population mean. On the other
hand, the range chart in Figure 4.9 was found to be in compliance with the
requirements of homogeneity criteria of a control chart since all the data points are
within the inner control limits (RWL). This may indicate that the production had
achieved a reasonably good control over the variance.

104

Table 4.8: Sample means and ranges for water absorption


Sample no.
1
2

10.461

5.322

11.337

2.512

11.531

2.796

11.923

3.396

11.552

3.074

12.007

2.131

11.367

2.246

11.797

3.496

10

11.393

4.145

11

11.921

2.117

12

11.379

2.362

13

10.973

3.297

14

11.534

2.279

15

10.887

2.718

16

10.489

4.374

17

9.404

1.572

18

10.822

2.452

19

10.765

2.816

20

11.048

5.137

21

10.756

4.358

22

11.141

4.355

23

11.738

4.210

24

12.592

3.430

25

11.489

4.454

26

10.464

5.088

27

11.309

4.751

Grand Mean, x
Mean Range, R

Table 4.9:

11.229
3.788

Control limits for means and ranges for water absorption

Grand mean, x = 11.229


Mean range, R = 3.788
For means
Warning lines
Action lines
x 0.202 R
=11.994, 10.464

Mean
Range
11.098
4.186

x 0.317 R
=12.430, 10.028

Lower
action line
R 0.35
= 1.326

For ranges
Lower
Upper
warning line
warning line
R 0.54
R 1.55
=2.046
=5.872

Upper
action line
R 1.94
=7.349

Water Absrption (%)


Mean

105

13,00
12,50
12,00
11,50
11,00
10,50
10,00
9,50
9,00

Upper action line


Upper warning line
Mean
Lower warning line
Lower action line
0

10

15

20

25

30

Sample Numbers

Water Absorption (%)


Range

Figure 4.8:

Control chart for mean values of water absorption

8.00
7.00

Upper action line

6.00

Upper warning line

5.00
4.00

Mean

3.00

Lower warning line

2.00

Lower action line

1.00
0.00
0

10

15

20

25

30

Sample Numbers

Figure 4.9:

4.3.3

Control chart for ranges of water absorption

Determination of Sample Variance Using the ANOVA


A single factor ANOVA at 95 % confidence was carried out on the

remaining 25 samples (Table 4.10), after ignoring the two samples i.e. sample no
17 and 24, which were found to contribute to the non-homogeneity of data. Table
4.11 shows the results from ANOVA a single factor analysis carried out using a
statistical programme by Microsoft Excel 2000. From ANOVA it was found
that Fcalc was smaller than Fcrit which indicates that the differences between the
means in the samples from the different batches were not significant and therefore

106
the N.H. is accepted. From here the best estimate for the variance derived was 1.53
as shown in column 4 of Table 4.11
Table 4.10:

Samples accounted for in the estimate of population


mean for water absorption

Sample
Batch
1

1
2
3
4
5
6
Batch 7
2
8
9
10
11
12
13
14
Batch
15
3
16
18
19
20
21
22
Batch
23
4
25
26
27
Mean = 11.247

Table 4.11:
Source of
Variation

Water Absorption in specimens (%)


10.56
8.37
10.45
11.58
11.83
10.82
12.03
12.36
11.89
12.01
13.14
11.89
9.86
12.37
11.87
7.66
10.37
11.15
8.57
12.61
10.32
9.31
12.71
11.70
12.54

10.16
13.35
10.95
12.59
12.93
13.12
11.45
10.36
12.70
10.37
11.45
11.30
8.95
11.16
11.63
10.31
10.24
10.82
13.61
8.64
9.64
13.14
8.94
7.93
12.17

10.92
10.35
11.20
10.71
12.22
12.37
10.85
10.12
11.20
11.63
12.67
12.05
11.01
12.21
10.50
11.33
11.05
12.09
11.63
12.14
11.44
11.98
9.56
9.34
12.00

12.66
8.83
11.59
10.80
13.79
12.43
11.60
12.37
9.65
10.03
12.10
12.70
11.40
10.55
10.30
12.03
10.29
9.35
12.40
11.74
11.08
10.36
11.69
10.06
7.92

9.54
9.53
10.63
11.57
11.13
10.87
11.74
11.56
11.56
11.70
11.03
10.49
11.77
12.12
11.08
9.67
11.51
9.86
11.04
9.67
10.62
12.74
12.36
11.65
12.67

11.60
11.93
11.41
12.03
10.40
11.49
12.33
10.65
11.94
12.79
12.25
10.52
10.21
12.83
11.79
11.36
11.91
10.11
11.47
12.09
13.99
12.94
13.39
12.09
12.40

10.76
10.54
10.79
10.83
12.40
10.04
12.21
11.99
11.12
10.29
12.15
10.38
11.55
11.12
9.15
11.55
11.41
10.24
8.47
12.03
13.33
9.31
10.69
8.58
11.33

10.58
8.02
12.96
11.25
11.18
11.93
12.98
11.53
12.75
9.40
11.14
12.74
11.95
10.66
10.84
10.30
11.41
10.45
11.64
8.61
11.10
12.74
11.76
9.23
8.83

13.73
11.62
12.32
13.37
12.44
11.26
12.95
12.25
13.15
12.15
11.76
10.43
12.25
11.31
11.71
10.84
9.46
12.17
9.97
11.78
9.86
13.52
12.67
11.05
11.46

10.46
12.07
11.07
10.58
10.91
11.20
11.93
10.45
12.02
13.55
11.52
11.29
10.78
11.01
10.00
9.84
10.57
11.41
11.69
8.25
10.03
11.34
11.13
13.02
11.76

ANOVA and components of variance for water absorption

Sum of Degrees Mean When the N.H. When the N.H.


Fcalc.
Fcrit.
square
of
square is accepted the is rejected the MS
From
between
(SS) freedom (MS) mean square is mean square is
F-Table
MS
within
(df)
an estimate of an estimate of
(5)
(6)
(1)
(2)
(3)
(4)
(7)
(8)
2
2
2
c

r
24
2.1453
Between rows 51.487
2
2
329.94
225 1.4664
Within rows
1.463
1.566
Best estimate of
2
381.43
249
1.53
Total

107
4.3.4

Estimates of Population Mean


The estimates for the population mean , were determined using equation

4.18. This estimate was based on the remaining 25 samples (Table 4.10) after
ignoring data from sample 17 and 24, which were considered as not representative
of the population.

= x tc

s
n

Where,
x = mean for sample = 11.247 (Table 4.10)
tc = 2.262 (From Appendix B, Table B2)
s =sample standard deviation = 1.53 ( s 2 = 1.53 derived from ANOVA)
n = sample size = 10
= 11.247 2.262

1.53
= 10.36 to 12.13
10

The mean for water absorption in percentage was11.247 0.885 i.e. ranging
from 10.36 % to 12.13 %. Therefore, water absorption for the population falls in the
range of 10 % - 12 %.

4.4 Conclusions
In norm with the central limit theorem it is widely acknowledged that most
physical measurements could be assumed normally distributed. On this basis
therefore, the normal probability function has been used throughout this work for
processing sample data. The validity of the normally distributed assumption is
verified as shown by the results of the histogram plot for the various tests. A typical
example taken for the water absorption tests showed that most data were
concentrated about the mean and it could be assumed that the histogram would
approach a normal curve as the size of data increases. Similarly, the other results

108
comprising of the dimensional tolerance, IRS, density and compressive strength also
displayed comparable characteristics of a normally distributed data.
The population mean derived from normal probability curve is good if size
of sample is large i.e. a sample having more than 30 data. In this work, however,
there were less than 30 bricks in a sample. Hence, the sample was considered small.
Under this condition the percentage points from the t-distribution curve was used to
derive the population estimates.
Control charts are graphical techniques used mainly to assess quality of a
production. It consists of performance data plotted against the control limits, i.e. the
upper and lower action and warning lines. These control limits define the constraints
for variations and if exceeded shows that the process is out of control or data is not
homogeneous. For this research samples, which did not satisfy the homogeneity
criteria, set by these control limits were considered as not representative of the
population and were not accounted for in the derivation of population estimates.
In a normal curve, data are symmetrically distributed about the mean, i.e. the
mean, median and mode are all coincident on the curve. The histogram plotted for
data in this work reveals some skewness in the data distribution for which the mean,
median and mode were not coincident. For this case, the coefficient of variation
(c.v.) is used to indicate the reliability of the assumption of a normal curve. Grimm
suggested that the log-normal probability function would be found helpful for data
having c.v.s exceeding 30 %. In the log-normal distribution the natural logarithm is
normally distributed. With respect to this, the c.v.s determined for dimensional
tolerance, density, IRS, water absorption and compressive strengths, for facing
bricks loaded on its bed and stretcher face and common bricks were all below 30 %
and therefore did not need the log-normal probability function. However, to further
justify the appropriateness of the normal probability function application in the
analyses, the 33-percentile values for the compressive strength of common bricks
with a c.v. of 25.4 % were computed for both the normal and log-normal curves.
Results showed comparatively small differences between the two values verifying
that the normal probability function could be used for data with c.v. less than 30 %.

109
In this research samples were taken from the factory in different batches at
intervals of approximately two months. Therefore to ascertain that the differences of
the means in the different batches were not significant a single factor ANOVA was
computed. From the ANOVA the components of variance between the several
samples in the different batches were determined. The variance was then used in
arriving at the population mean.

CHAPTER 5

RESULTS AND DISCUSSIONS

5.1

Introduction
This chapter presents results for the compressive strength, dimensional

tolerance, water absorption, initial rate of suction, density, efflorescence effects and
soluble salt content of bricks. The results were analysed and interpreted through the
process as described in Chapter IV. Comparisons and correlations of the results with
specified limits of other standards were also carried out for the purpose of
evaluation.
Results from efflorescence test and soluble salt content were deduced from
observations based on small samples and hence found not required to be analysed by
the statistical approach as described in Chapter IV.

5.2

Compressive Strength
The compressive strength of facing brick was determined with respect to the

different orientations of testing i.e. on its bed face, stretcher face and header face.
The common bricks were only tested on their bed face. The loaded area used in the
calculation of compressive strength in all cases was the gross area. However,

111
compressive strength for results tests conducted on the bed face was also compared
with results based on calculations using net loaded area. The net loaded area is the
gross area less the area of perforations.
Table 5.1, 5.2 and 5.3 show the compressive strengths of specimens in the
samples for all batches of facing bricks when tested on their bed, stretcher and
header face respectively.
Table 5.1:

Compressive strength of specimens in each sample for facing


bricks tested on bed face

Sample
Batch
1

42.0 46.5 43.7


1
48.8 43.2 44.6
2
35.6 41.8 44.7
3
36.5 41.1 48.4
Batch
4
2
56.3 41.0 57.7
5
39.9 39.0 45.8
6
61.8 59.1 54.8
7
45.5 51.1 50.3
Batch
8
3
53.5 42.1 53.8
9
48.2 52.2 52.4
10
45.4 43.2 42.6
11
51.8 35.2 47.8
Batch
12
4
64.1 48.9 40.9
13
39.4 41.5 50.1
14
Descriptive Statistics
Mean, x = 46.07 N/mm2
Median = 45.01 N/mm2
Mode = NA
Standard deviation, s = 8.55 N/mm2
Maximum = 72.5 N/mm2
Minimum = 27.1 N/mm2
Range, R = 45.4 N/mm2
Coefficient of variation, c.v. = 18.5 %

Compressive strength N/mm2


47.6
43.8
35.8
38.5
41.8
48.6
72.5
49.9
48.5
40.6
53.5
40.0
57.8
41.6

38.1
50.3
31.0
30.6
34.1
40.4
60.0
28.8
47.7
55.5
38.4
41.9
51.2
39.8

38.0
51.3
45.5
29.4
46.5
43.3
59.5
55.4
50.4
53.5
40.4
45.3
38.5
41.2

35.3
51.7
40.6
27.1
52.0
38.7
63.6
56.6
50.7
50.2
41.2
42.4
39.2
56.6

42.2
55.0
35.5
38.3
59.0
48.8
66.1
53.1
54.5
47.0
48.8
59.0
42.7
48.6

33.1
44.5
42.9
35.6
40.0
54.6
46.8
68.4
60.7
49.9
44.3
34.0
39.5
43.5

39.6
54.0
36.2
29.7
42.1
57.6
44.4
53.2
47.7
48.7
43.6
36.1
36.8
40.6

112
Table 5.2:

Compressive strength of specimens in each sample for facing


bricks tested on stretcher face
Compressive strength of specimens N/mm2

Sample
Batch
1

39.3
39.4
34.8
1
33.8
26.8
33.5
2
35.3
37.7
43.5
Batch
3
2
34.4
35.7
33.2
4
40.9
49.5
44.6
Batch
5
3
37.9
28.3
33.7
6
22.2
31.3
45.5
Batch
7
4
28.9
23.8
26.5
8
Descriptive Statistics
Mean, x = 34.74 N/mm2
Median = 34.49 N/mm2
Mode = 35.27 N/mm2
Standard deviation, s = 6.45 N/mm2
Maximum = 55.0 N/mm2
Minimum =22.2 N/mm2
Range, R = 32.8 N/mm2
Coefficient of variation, c.v. = 18.6%

38.9
32.6
34.0
40.2
45.3
38.0
37.8
25.6

39.4
28.9
34.4
34.5
38.9
34.0
25.9
25.3

37.1
38.0
29.7
35.3
44.8
47.8
30.0
27.9

36.9
31.4
22.5
37.7
44.0
37.5
32.7
29.7

36.8
27.9
34.4
43.5
35.6
37.9
30.1
30.9

37.0
30.9
35.0
34.0
55.0
35.1
27.8
30.9

33.4
27.0
35.4
27.5
43.0
36.9
24.0
34.4

Table 5.3: Compressive strength of specimens in each sample for


facing bricks tested on header face.
Sample

Compressive strength N/mm2

Batch
9.5 9.3 9.0
1
1
2.7 4.0 3.5
2
5.0 4.3 4.6
Batch
3
2
5.4 5.4 5.1
4
10.6 5.6 4.3
Batch
5
3
4.5 5.6 3.9
6
5.5 2.4 3.2
Batch
7
4
8.4 8.9 5.5
8
Descriptive Statistics
Mean, x = 5.51 N/mm2
Median = 5.07 N/mm2
Mode = 5.03 N/mm2
Standard deviation, s = 2.15 N/mm2
Maximum = 11.4 N/mm2
Minimum = 0.8 N/mm2
Range R =10.06 N/mm2
Coefficient of variation, c.v. =39.0 %

9.2
3.9
2.2
6.2
7.2
4.7
3.7
6.0

8.0
2.3
4.6
4.1
5.5
4.2
5.6
7.3

8.4
4.5
6.9
5.0
11.4
5.0
3.2
6.4

7.9
3.6
4.7
4.3
7.6
4.7
4.3
6.1

9.2
3.1
4.7
4.6
6.7
3.2
5.6
6.9

8.8
4.3
5.4
5.1
6.1
3.0
0.8
4.8

9.1
4.2
2.5
4.6
7.6
6.9
3.0
5.8

The descriptive statistics consisting of the mean, median, mode, standard


deviation, range and coefficient of variation were shown in Table 5.1, 5.2 and 5.3.
The mean compressive strength was 46.1, 34.7 and 5.51 N/mm2 when tested on bed,
stretcher and header face respectively. With a mean strength of 46 N/mm2 when
tested on the bed face, the bricks from this research easily surpass the top range of

113
the specified limits for ASTM, AS and the SS with exception of the Engineering
category of the BS (Table 5.8).
Data distribution was presented by the histograms as shown in Figure 5.1.
The histogram could be seen to represent a normally distributed data and in virtue of
the central limit theorem the histogram would eventually form a normal curve with
increasing number of data. Hence, assuming data to be normally distributed the
normal curve fit (Table 5.4) was computed for the compressive strengths tested on
the bed and stretcher face (having c.v.s of 18.5 % and 18.6 % respectively). With
respect to the bricks tested on the header face the c.v. was 39.0 % which was greater
than 30 %. Therefore, the compressive strengths tested on the header face were fitted
with a log-normal curve (Table 5.5). The normal and log-normal curves were plotted
superimposed on the histograms as shown in Figure 5.1.
Table 5.4:

Normal curve fit for compressive strength of facing bricks tested


on bed and stretcher face

Testing
orientations

Interval
midpoint
x

Observed
frequency

Number of
standard
deviations, z

(x - x) s

Bed face

Stretcher
face

29.269
33.807
38.345
42.883
47.421
51.959
56.497
61.035
65.573
70.111
74.649
23.642
26.925
30.208
33.491
36.774
40.057
43.340
46.623
49.906
53.189
56.472

6
9
24
31
23
23
12
7
3
1
1
4
11
11
18
18
7
6
3
1
0
1

-1.966
-1.435
-0.904
-0.373
0.1576
0.6886
1.2195
1.7505
2.2814
2.8124
3.3433
-1.727
-1.217
-0.707
-0.198
0.312
0.822
1.331
1.841
2.351
2.861
3.370

f ( z) =

( 2 )

-1 2

exp - ( z 2 2 )

0.0577
0.1424
0.265
0.3721
0.394
0.3147
0.1896
0.0862
0.0296
0.0076
0.0015
0.0898
0.1902
0.3106
0.3912
0.3799
0.2846
0.1644
0.0732
0.0252
0.0067
0.0014

Computed
frequency
ordinate, y
nif ( z ) s
4.2918
10.587
19.701
27.655
29.285
23.392
14.096
6.4072
2.197
0.5683
0.1109
3.6622
7.7552
12.6652
15.9513
15.4933
11.6054
6.7041
2.9866
1.0261
0.2719
0.0556

114
Table 5.5:

Log-normal curve fit for compressive strength of facing


brick tested on header face

Interval
midpoint
x

1.034
2.101
3.168
4.235
5.302
6.369
7.436
8.503
9.570
10.637
11.704

Observed
frequency

Number of
standard
deviations, z
( ln x - ) -1

1
4
9
22
17
9
6
5
5
1
1

-4.253
-2.370
-1.280
-0.509
0.088
0.575
0.986
1.342
1.656
1.937
2.190

f ( z) =

( 2 )

-0.5

-1

exp - ( z 2 2 ) - z -
0.000
0.030
0.147
0.220
0.199
0.141
0.088
0.051
0.028
0.015
0.008

Computed
frequency
ordinate, y
ni f(z)
0.010
2.594
12.587
18.759
16.988
12.035
7.478
4.321
2.398
1.303
0.701

From the normal and log-normal probability functions the 33-percentile


values for all the three cases of loadings were determined and are shown in Figures
5.1 (a), (b) and (c). The high and low values were meant for the upper and lower 33percentile while the medium values were for the middle third distribution. The upper
33-percentile for bricks tested on the bed face i.e. about one-third of the distribution
had compressive strengths exceeding 50 N/mm2 i.e. the minimum requirements for
Engineering B bricks of the BS.
The mean compressive strength representative of the population of bricks in
the study was computed after examining the homogeneity of data using the control
charts for means and ranges of samples (Figure 5.2). Data not complying with the
homogeneity criteria as explained in Chapter IV were not taken into account when
determining the population mean. In this case the control charts showed that data
from samples 4 and 7 of the bed face compressive strengths, 5 and 8 of the stretcher
face and 1, 2, 5 and 7 of the header face were lying outside the upper and lower
action lines and thus data from these samples were ignored for the computation of
population mean.

115

35

Frequency

x = 46.1 N / mm 2
s = 8.55 N / mm 2
c.v. = 18.55%
median = 45.0 N / mm 2
mod e = NA

Normal
curve

30
25
20
15

Low < 42.0 N/mm2


Medium 42.0 50.0 N/mm2
High > 50.0N/mm2

10
5
72.380-76.918

67.842-72.380

63.304-67.842

58.766-63.304

54.228-58.766

49.690-54.228

45.152-49.690

40.614-45.152

36.076-40.614

31.538-36.076

27.000-31.538

Compressive Strength, N/mm2

(a) Bed face

Frequency

20

x = 34.7 N / mm 2
s = 6.45 N / mm 2
c.v. = 18.56 %
median = 34.5 N / mm 2
mod e = 35.3 N / mm 2

Normal
curve

15
10

Low < 33.0 N/mm2


Medium 33.0 37.0 N/mm2
High > 37.0N/mm2

54 83-58.113

51.547-54.83

48.264-51.547

44.981-48.264

41.698-44.981

38.415-41.698

35.132-38.415

31.849-35.132

28.566-31.849

25.283-28.566

22.00-25.283

Compressive strength, N/mm

(b) Stretcher face


25
20

Frequency

x = 5.5 N / mm 2
s = 2.15 N / mm 2
c.v. = 39.0 %
median = 5.1 N / mm 2
mod e = 5.0 N / mm 2

Log-normal
curve

15
10

Low < 4.0 N/mm2


Medium 4.0 6.0 N/mm2
High > 6.0N/mm2

11.17-12.237

10.103-11.17

9.036-10.103

7.969-9.036

6.902-7.969

5.835-6.902

4.768-5.835

3.701-4.768

2.634-3.701

1.567-2.634

0.500-1.567

Compressive strength, N/mm2

(c) Header face


Figure 5.1:

Histogram, normal and log-normal curve for compressive


strength of facing bricks tested on (a) bed face (b)
stretcher face (c) header face

50

UAL
UWL

40

LWL
LAL

30
5

10

15

50
45
UAL
UWL

40
35

LWL
LAL

30
25
20
0

UAL
UWL

x
LWL
LAL

10

15

Comressive strengths
Range

Compressive strength
Range

50
40
30
20
10
0
5

UAL
UWL

LWL

LAL

2
0

10

40
UAL

30

UWL

20

10

LWL
LAL

0
0

Sample

UAL Upper action line

10

LAL Lower action line

10

UAL
UWL

6
4

LWL
LAL

0
0

10

Sample

(b) Stretcher face


UWL Upper warning line

Sample

Sample

(a) Bed face

Figure 5.2:

Sample

Sample

10

Compressive strength
Range

Compressive strength
Mean

60

Compressive strength
Mean

Compressive strength
Mean

70

(c) Header face


LWL Lower warning line

Control charts of mean values and ranges for compressive strength tested on (a) bed face
116

(b) stretcher face (c) header face

117
The ANOVA for compressive strengths tested on the different orientations
were carried out on the remaining samples. From the ANOVA, shown in Table 5.7
Fcal. for all cases were found greater than Fcrit and therefore, the N.H. was rejected
indicating that there was significant difference in the variances of the various
samples. The ANOVA from Table 5.7 also gave the components of variance, which
were used to determine the population mean. Detail explanation of the procedures
for the determination of variance from ANOVA and derivation of population mean
is shown in Chapter IV. The estimate of variances for the different orientations of
loading were 54.40, 28.32 and 10.757 tested on bed, stretcher and header face
respectively.

Table 5.6:

ANOVA and variance components for compressive strengths of


facing bricks tested on bed, stretcher and header faces

Testing
orientations

When the
Degree
When the N.H.
N.H. is
Sum of
Mean
of
Source of
is accepted the rejected the
Squares freedo Square
mean square is mean square
Variation
(SS)
m
an estimate of is an estimate
(df)
of
(2)
(3)
(4)
(5)
(6)
(1)
Between
2 + c r2
1672.023
11
152.002
2
samples
Within
4704.06
108
43.556
2
2
samples
Bed face
Best estimate of
53.58
Total 6376.082 119
2
Between
2 + c r2
398.699
5
79.740
2
samples
Within
Stretcher
1220.659
54
22.605
2
2
samples
face
Best estimate of
59
27.447
Total 1619.358
2
Between
2 + c r2
29.687
3
9.896
2
samples
Within
36
1.282
2
2
Header face samples 46.151
Best estimate of
75.839
39
1.945
Total
2

Fcalc.

Fcrit.

(7)

(8)

3.489 1.878

3.528 2.386

7.719 2.866

The corresponding mean compressive strengths for the population tested on


bed, stretcher and header face were in the range of 40 to 51 N/mm2, 30 to 38 N/mm2
and 4.1 to 6.2 N/mm2.

118
Comparisons with other standards shows that the population mean, like the
sample mean supersedes the top range compressive strengths of ASTM, AS and SS.
However, the population did not fit in the category of Engineering A and B of the
BS which requires a minimum compressive strength of 70 N/mm2 and 50 N/mm2
respectively.
Results from the tests clearly demonstrated that a considerable amount of
compressive strength reduction occurred with increased slenderness ratio for the
bricks orientations. Samples results show that a maximum strength of 46 N/mm2
was achieved when brick was tested on its bed face. When tested on the header face
the compressive strength was less than 20 % of that on bed face. Similarly, the
compressive strength when tested on the stretcher face reduced to 34.74 N/mm2, i.e.
a reduction by about 20 % in comparison to bed face.
These results, showing the relative compressive strength reduction
corresponding to the different orientations of testing were approximately in
agreement with the study reported by Hendry (1997). Hendry showed that, bricks
tested on the stretcher and header faces produced compressive strength of about 80
% and 20 % respectively of the strength when tested on the bed face (Table 2.1).
The reduction in compressive strength was due to the effects of platen
restraint, which imposed a degree of confinement to the specimens, the greater the
height of specimen during testing the lesser was the platen effects. In the Australian
Standard the effect of platen restraint are being considered by multiplying the
compressive strength with a factor depending on the height to thickness ratio
(Table 2.2) and it diminishes at height to thickness ratio of 5 and above.
A relationship between compressive strength and height to thickness ratio
was developed in this study. The mean values ( x ) for the three orientations of
testing i.e. on bed (46.1 N/mm2), stretcher (34.7 N/mm2) and header faces (5.5
N/mm2) were plotted against the height to thickness ratio as shown by the graph in
Figure 5.3. The value of the height to thickness ratio (h/t) was based on the mean
measurements of both dimensions for samples used in the study. The graph for the

119
compressive strength versus h/t ratio was plotted and joined with a best fit line
described by equation 5.1 with a regression coefficient of R2 = 0.998
f = 16.353 x + 58.168

(5.1)

Where,
f = compressive strengths in N/mm2
x = ratio of height to thickness (h/t).
Where,
h = the height in relation to the orientation of tests
t = the smallest dimension of the loaded face.
This relationship was derived specifically for standard format bricks with 5
rectangular slots. The equation can also provide estimation on the compressive
strength of bricks for the same standard format made from the same material or
comprised of the same amount of perforations. In this respect, the perforations are
rectangular with an average area of 3375 mm2 i.e. about 16 % of the total gross area.
The results could also be used to estimate the compressive strength of the same brick
format with circular holes as generally used in other manufacturing, however the
prediction is expected to be conservative in view that shearing will occur at higher

Compressive strength, f
N/mm2

levels at failure.

50
40

Bed face
h/t = 0.7

30

f = -16.353x + 58.168
R2 = 0.998

Stretcher face
h/t =1.5

20
10

Header face
h/t =3.2

0.5

1.5

2.5

3.5

Height to thickness ratio, h/t

Figure 5.3:

Relationship between compressive strength and h/t ratio


of bricks

120
The calculation for compressive strength specified in standards could either
be based on the net or gross area of loaded face. Australian Standard uses the net
area i.e. gross area less the area of perforations while ASTM specifies that the
compressive strength to be calculated using gross area. BS specified the area used in
the calculation as the overall dimension.
Compressive strengths of bricks tested on bed face determined using net area
i.e. the mean area of bed face less the area of the 5 rectangular slots is shown in
Table 5.7. The mean compressive strength was 54.4 N/mm2, which indicates an
increase of about 20 % compared to values obtained using the gross area. The
population mean was in the range of 50 to 60 N/mm2. Thus, taking into account the
net area resulted in a higher value, which qualifies the bricks as Engineering B of the
BS.
Table 5.7:

Compressive strengths of facing brick tested on bed face as


computed from net areas

Sample
Batch
1

Compressive strength based on net area, N/mm2

49.9 55.2 51.8


1
57.7 51.0 52.9
2
41.8 49.9 53.3
3
43.4 48.5 57.6
Batch 4
2
66.9 48.2 68.1
5
46.9 45.9 54.0
6
73.3 70.0 64.8
7
53.8 60.5 59.6
Batch 8
3
63.7 49.9 63.6
9
57.2 62.1 62.1
10
53.8 51.2 50.5
11
61.4 41.3 57.0
Batch 12
4
76.1 58.0 48.4
13
20.0 49.5 60.3
14
Descriptive Statistics
Mean, x = 54.4 N/mm2
Median = 53.5 N/mm2
Mode = NA
Standard deviation, s = 10.62 N/mm2
Maximum = 86.5 N/mm2
Minimum = 20.0 N/mm2
Range, R = 66.5 N/mm2
Coefficient of variation, c.v. = 19.5 %

56.3
51.6
42.1
45.4
49.2
57.5
86.5
59.1
57.2
48.1
63.6
47.3
68.9
49.2

45.0
59.5
36.6
36.1
40.2
47.6
71.2
34.2
56.7
65.9
45.4
49.6
60.6
47.1

45.1
60.9
54.3
35.0
55.2
51.1
70.5
65.8
59.7
63.5
48.1
53.8
45.5
48.8

41.7
61.4
48.0
32.1
61.6
45.5
75.7
67.2
60.2
59.4
48.8
50.2
46.1
67.6

50.0
65.1
41.8
45.1
69.9
57.8
78.6
63.1
64.7
55.8
58.1
70.0
50.6
58.0

39.4
52.7
50.7
42.1
47.2
65.2
55.5
81.5
72.1
59.2
52.8
40.0
46.7
51.6

47.0
64.1
42.9
35.2
49.6
68.3
52.5
63.1
56.3
57.7
51.6
42.4
43.7
48.0

121
A relationship between compressive strength with h/t ratio considering net
loaded area for the bed face orientation is shown in Figure 5.4. The relationship
shows an increase of about 13 % in the compressive strength compared to the results
obtained by considering gross area of the bed face. Thus, the relationship of
compressive strength to h/t ratios given by equation 5.1 for perforated bricks is

Compressive strength, f
N/mm 2

considered as conservative.

60
50

Bed face
h/t = 0.7

40
30

f = -19.187x + 66.07
2

R = 0.9913

Stretcher face
h/t = 1.5

20
10

Header face
h/t = 3.2

0.5

1.5

2.5

3.5

Height to thickness ratio, h/t

Figure 5.4:

Relationship between the computed compressive strength


(based on net loaded area of bed face) to h/t ratio

It should be noted that in this study compressive strength tests were carried
out after the test for water absorption. In this case, the bricks were in a saturated
condition and research has shown that wet bricks tend to show lower strengths than
dry ones. Grimm, (1975), reported that dry brick can be 15% stronger than wet ones.
Some compressive tests done on dry bricks in this study also showed that the dry
bricks had strengths of about 15 to 20 % higher than the wet bricks.
The tests conducted on wet bricks based on gross area yield lower
compressive strengths as the effects of curing and gross loaded area contribute to
both physical and theoretical determination of strength. Consequently, the evaluation
of compressive strength of bricks studied in this research implies conservative
results compared to values stated in ASTM.

Compressive strength of facing and common bricks and standard requirements

(Upper
33percentile)

(Middle
33percentile)

(Lower
33percentile)

46.00

>50.0

42.0 50.0

<42.0

Bed face
h. 67
=
0.7
t 98

40.0 51.0

Stretcher face
h 98
=
1.5
t 67
Header face
h 216
=
3.2
t
67
Bed face

30.0 38.0

34.7

>37.0

33.0 37.0

<33.0

4.12 6.20

5.5

>6.0

4.0 6.0

<4.0

30.0 40.0

35.7

>40.0

32.0 40.0

<32.0

70

50

Others

Not
less
than
20.7

Not
less
than
17.2

Not
less
than
10.3

0.7

Not
less
than
7.0

Not
less
than
5.0

SS (Mean of 10
bricks)

Third grade

Sample
x

Engineering
NW

Low

AS
(Characteristic
strength)
Ratio of
manufacturing
height to
width

Second grade

Common
bricks

Normal

MW

Population
Facing
brick

High

Mean

Testing
orientations

ASTM (Mean of
5 bricks)

First grade

BS (Mean of 10
bricks)

Compressive strength from research results

SW

Table 5.8:

Not
less
than
35.0

Not
less
than
20.0

Not
less
than
5.2

122

123
Results for compressive strength of common bricks are shown in Table 5.9.
In this study common bricks were referred to bricks for general building works with
no aesthetic application
Table 5.9:

Compressive strength of specimens in each sample for common


bricks
Compressive strength determined from net area, N/mm2

Sample

38.5 39.5 29.0


1
39.6 38.0 36.1
2
38.8 37.7 29.3
3
28.5 25.9 22.5
4
Batch
21.0 27.2 39.1
5
2
20.6 26.2 19.0
6
29.6 37.9 26.8
7
Batch
41.6 42.8 36.4
8
3
34.1 38.4 36.7
9
51.4 58.0 51.7
10
Batch
38.4 44.1 44.4
11
4
48.6 34.6 44.5
12
Descriptive Statistics
Mean, x = 35.71 N/mm2
Median = 36.42 N/mm2
Mode = 40.86 N/mm2
Standard deviation, s = 9.06 N/mm2
Maximum = 58.0 N/mm2
Minimum = 18.4 N/mm2
Range, R = 39.6 N/mm2
Coefficient of variation, c.v. = 25.4 %
Batch
1

40.0
27.2
38.9
25.2
39.0
25.3
30.8
38.4
35.7
49.2
38.1
25.8

31.1
39.5
26.5
22.7
33.7
23.1
28.6
41.4
40.5
50.4
49.1
41.9

30

Frequency

25

Normal curve

20

36.1
33.5
36.5
24.7
32.9
24.6
33.6
48.6
47.3
49.1
45.2
50.1

25.2
25.1
25.1
21.3
35.4
20.7
31.7
49.8
49.0
47.0
48.9
45.0

39.4
36.3
37.8
24.4
31.7
36.2
21.2
39.6
36.9
46.7
39.6
43.7

27.8
34.2
27.8
20.1
39.2
18.4
20.2
43.6
45.5
47.2
48.2
41.6

34.0
32.3
34.0
22.2
40.2
21.7
46.0
40.9
40.9
34.2
33.1
34.2

x = 35.7 N / mm 2
s = 9.06 N / mm 2
c.v. = 25.38%
median = 36.4 N / mm 2
mod e = 40.9 N / mm 2

15
Low < 31.87 N/mm2
Medium 31.87 39.50 N/mm2
High > 39.50 N/mm2

10
5
18.35-22.35
22.35-26.35
26.35-30.35
30.35-34.35
34.35-38.35
38.35-42.35
42.35-46.35
46.35-50.35
50.35-54.35
54.35-58.35

Compressive strength N/mm2

Figure 5. 5: Histogram and normal curve for compressive strength of


common bricks

124
The histogram and the normal curve fit is shown in Figure 5.5. The sample
mean was 36 N/mm2, which lie within the ranges specified for structural bricks of
ASTM for the category of SW bricks and just exceed the minimal requirement
specified of First Grade brick in Singapore Standard. However, from the normal
curve function the middle 33-percentile comprises of strengths in the range of 31.9
to 39.5 N/mm2 exceeding values for the top range of the structural bricks of ASTM
(Table 5.7).
The quality control charts (Figure 5.6) shows that 5 out of 12 samples lie
outside the upper and lower action lines thus indicating considerable scatter of
compressive strengths. This is in contrast with the results observed for facing bricks.
The wide scatter of data for common bricks shows lacking of production control.
However, it must be borne in mind that some of the common bricks were rejected
products of facing brick, therefore the properties might not be consistent with actual
common bricks production.
The population mean was derived after ignoring these 5 data points. The
variance from the ANOVA was 48.55 from which the standard deviation of the
population is estimated as 6.968 N/mm2. The population mean range computed
using this standard deviation was 30.38 to 40.34 N/mm2 and this value exceeds the
requirements for SW bricks of ASTM. and Second grade bricks of the Singapore
Standard.
The compressive strength ranged from 30 to 40 N/mm2, therefore the
common bricks in this study suffice the requirements for structural bricks under the
classification of SW bricks of the ASTM. The common bricks investigated in this
study could be used as load-bearing applications although not suitable for facing
brickwork due to lacking of other physical and dimensional properties. Previous
research on common bricks of the same manufacturers product showed water
absorption exceeding 10%.

Compressive strength
Mean

125

50,0
40,0

UAL
UWL

30,0

LWL
LAL

20,0
0

10

12

14

Compressive strength
Range

Sample

40,0
UAL

30,0

UWL

20,0

10,0

LWL
LAL

0,0
0

10

12

14

Sample

Figure 5.6:

Control charts of mean values and ranges of samples for


compressive strength of common bricks

5.3

Dimensional Tolerance

5.3.1

Overall Dimensions of 24 Bricks


Table 5.10 shows the results of overall dimension of length, width and height

of 24 bricks and the deviations of these dimensions from the work sizes for the
individual brick. These deviations were derived from the results of the overall
dimensions as shown in Table 5.10 columns (4), (6) and (8). The work sizes were as
given in the BS for length, width and height i.e. 215 mm, 102.5 mm and 65 mm
respectively. The mean value of overall length was 5218 mm, which is within the
limits of BS i.e. 5085 mm to 5235 mm. The mean value of overall width of
2412 mm was slightly out of range compared to the BS limits of 2415 mm to 2505
mm. The height had a mean value of 1642 mm, exceeding the limit of BS by 37 mm.

126
Table 5.10:

Overall measurement of length, width and height of 24 bricks

(1)
Batch
1

Sample

and individual brick dimensional deviations from work size


Overall
Length
of 24
bricks

(2)
(3)
1
5240
2
5254
3
5216
Batch 4
5263
2
5
5241
6
5243
7
5175
Batch 8
5218
3
9
5185
10
5178
11
5203
12
5211
Batch
13
5210
4
14
5213
Descriptive statistics
Mean, x
5218
5215
Median
#N/A
Mode
Standard
27.55
deviation, s
5263
Maximum
5175
Minimum
88
Range, R
0.53%
c.v.
Max.
British
Standard
5235

Deviations of
Individual
length of brick
from work
size
[(3) 24]- 215
(4)
3.33
3.92
2.33
4.29
3.38
3.46
0.63
2.42
1.04
0.75
1.79
2.13
2.08
2.21

Overall
width of
24
bricks

Deviations of
individual width
of brick from
work size

Overall
height
of 24
bricks

(5)
2415
2410
2408
2426
2421
2419
2405
2412
2413
2397
2416
2400
2409
2414

[(5) 24]- 102.5


(6)
-1.88
-2.08
-2.17
-1.42
-1.63
-1.71
-2.29
-2.00
-1.96
-2.63
-1.83
-2.50
-2.13
-1.92

(7)
1638
1646
1648
1651
1650
1653
1628
1640
1625
1634
1638
1643
1643
1644

2.41

2412
2413
#N/A

Min.
5085

7.86
2426
2397
29
0.33%
Max.
2505

-2.01

Min.
2415

Deviations
of individual
height of
brick from
work size
[(7) 24]- 65
(8)
3.25
3.58
3.67
3.79
3.75
3.88
2.83
3.33
2.71
3.08
3.25
3.46
3.46
3.50
3.40

1642
1643
1638
8.35
1653
1625
28
0.51%
Max.
1605

Min.
1515

Note: Work sizes as in BS 3921:1985 Length = 215 mm, width = 102.5 mm,
height = 65 mm
A plot of sample overall dimensions against specified limits of BS and SS is
shown in Figure 5.7. The SS provides three grades of dimensional tolerance i.e. first,
second and third grade, depending on the degree of dimensional accuracy required,
however bricks under the category of the third grade are not limited to any
dimensional tolerance.
Figure 5.7 clearly demonstrates that the bricks in this research had lengths
and widths marginally in agreement with the BS and SS first grade bricks but the
height was oversize. The length belongs to the higher range of the BS as evident by

127
5 samples lying outside the upper range [Figure 5.7 (a)], while the width were in the
lower range of the BS with 5 samples lying below the lower range of the width
measurement [Figure 5.7 (b)]. On the other hand, all samples for the height exceeds
the maximum limit of the British Standard.

Overall Length (mm)

5500
5400

SS Second Grade

5300
5200

BS and SS First Grade

5100
5000
0

10

15

20

Sample

(a)

Overall Width (mm)

2600
2550

SS Second Grade

2500
BS and SS First Grade

2450
2400
2350
0

10

15

20

Sample

(b)
1810
SS Second Grade

Overall Height (mm)

1760
1710
1660
1610

SS First Grade

BS

1560
1510
1460
0

10
Sample

15

20

(c)

Figure 5.7: Comparison of overall dimensions of (a) length (b) width and
(c) height with allowable range of British and Singapore Standard.

128
The dimensional tolerance of the bricks investigated in this research was also
evaluated against values of tolerances provided in the European Standard
prEN 771-1 and the derived tolerance limit for individual brick based on the
cumulative measurement of 24 bricks. Table 5.11 shows the comparisons of
dimensional tolerances for individual brick from results of this research (col. 2) with
values derived from specified tolerance for 24 bricks of BS 3921 (col.5) and the
tolerance categories of T1 and T2 in prEN 771-1 (col. 3 and 4). In the prEN 771-1
the mean dimensions of 10 bricks in a sample should not differ from the declared
value of either categories T1 and T2, which correspond to the following:
T1: 0.4 (work size dimension) mm or 3 mm whichever is greater.
T2: 0.25 (work size dimension) mm or 2 mm whichever is greater.

The dimensional deviations for individual brick derived from BS 3921


(col.5), was calculated based on the limits given for the overall dimensions of 24
bricks. For example, the overall length of 24 bricks should not exceed 5235 mm and
not less than 5085 mm, which equal to a tolerance of 6.25 mm or 3 .125 mm for
the length of individual brick.
Table 5.11:

Dimensional deviations of brick from work size and comparisons


with values of dimensional tolerance for BS 3921:1985 and prEN

Dimensions

Test results of mean


dimensional deviations
from work size derived
from measurement of
24 bricks (mm)
(From Table 5.10)

(1)

(2)

(3)

(4)

BS 3921
Individual brick
deviations from
work size
derived from
tolerances of 24
bricks
(5)

Length

+ 2.41

0.4 215 = 5.9

0.25 215 = 3.7

3.125

Width

- 2.01

0.4 102.5 = 4.0

0.25 102.5 = 2.5

1.875

Height

771-1

+ 3.4

0.4 65 = 3.2

0.25 65 = 2.0

1.875

prEN 771-1
Dimensional tolerance for BS work
size.
T1
(mm)

T2
(mm)

129

Therefore, from the comparisons of individual bricks dimensional tolerance


of prEN 771-1 and BS 3921 it could be observed that the dimensional tolerance for
individual bricks derived from BS tolerance for 24 bricks is more stringent than the
prEN 771-1 for both the T1 and T2 categories. Research results showed that the
mean deviations of the dimensions of bricks from the work size (Table 5.11, col. 2)
for length i.e. +2.41 mm was within the derived deviation of the BS ( 3 mm)
however the width and height had a deviation of 2.01 mm and +3.4 mm which
exceeded the deviations i.e. 1.875 for both width and height. Nevertheless, it
should be borne in mind that the strict dimensional deviations provided in the British
Standard was derived from the cumulative dimensions of 24 bricks. Moreover, these
deviations are restricted to bricks of the standard format specified in BS 3921.
Table 5.11 shows that the bricks investigated fulfil the requirements for category T1
of the dimensional tolerance specified in the prEN 771-1. The bricks however could
not satisfy the tolerance limit for category T2 due to the height exceeding the range
specified for the T2 category.

5.3.2

Dimension of Individual Brick for Length, Width and Height


Table 5.12 shows sample data with the mean, ranges, standard deviations,

and coefficient of variation for length, width and height of individual brick. The
mean for length, width and height were 216 mm (s =1.91 mm), 100 mm (s =1.12
mm) and 67 mm (s =1.91 mm) respectively and the normal values which is in the
middle third of the 33-percentile values were 216 to 218 mm for length, 98 to100
mm for width and 67 to 68 mm for height (Figure 5.8).

Table 5.12:

Individual brick dimensions for length, width and height in all samples
Length

Batch
1

Batch
2

Sample

Mean

Range

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24

x
218.4
218.4
216.6
218.0
216.6
217.7
217.7
219.1
216.6
215.5
216.1
216.4
218.0
217.7
217.7
218.8
216.8
219.0
216.7
217.7
219.1
217.5
216.3
218.0

R
1.6
2.6
6.2
2.7
1.5
2.8
2.8
3.2
4.1
10.5
3.9
5.8
6.5
3.7
6.2
4.5
1.7
2.6
4.0
3.7
4.7
7.0
4.9
11.0

Standard
deviation
s
0.57
0.94
2.12
1.00
0.61
0.99
1.13
1.36
1.62
3.63
1.57
2.29
2.72
1.67
2.16
1.77
0.73
0.94
1.76
1.43
1.85
2.60
1.91
4.14

Width
c.v.
%
0.26
0.43
0.98
0.46
0.28
0.45
0.52
0.62
0.75
1.68
0.72
1.06
1.25
0.77
0.99
0.81
0.34
0.43
0.81
0.66
0.84
1.20
0.88
1.90

Mean
100.2
99.8
99.0
99.6
99.0
99.8
100.0
99.9
99.9
99.3
99.3
98.9
100.4
100.3
99.8
100.7
99.8
100.9
99.8
100.2
101.0
99.8
99.4
100.0

Range
R
2.4
1.9
2.2
1.1
2.5
1.8
1.9
2.3
4.4
4.1
2.4
4.8
4.3
2.8
3.7
3.9
2.2
1.2
2.3
2.6
4.4
5.9
3.3
4.2

Standard
deviation
s
0.81
0.78
0.94
0.37
0.95
0.80
0.66
0.81
1.64
1.43
0.95
1.82
1.57
1.16
1.39
1.52
0.88
0.44
0.86
0.85
1.65
2.07
1.43
1.60

Height
c.v.
%
0.81
0.78
0.95
0.37
0.96
0.80
0.66
0.81
1.64
1.44
0.95
1.84
1.56
1.15
1.39
1.51
0.88
0.44
0.86
0.85
1.63
2.07
1.44
1.60

Mean
x
67.1
67.2
67.5
67.2
66.4
67.2
67.9
68.0
68.2
67.8
68.1
67.7
68.2
67.3
67.7
68.8
67.6
68.2
68.2
68.1
68.1
68.6
67.9
67.9

Range
R
1.2
1.6
2.6
5.5
1.1
1.1
1.0
2.0
4.3
3.4
2.5
2.5
2.0
1.9
1.7
4.3
1.6
1.9
2.2
1.6
3.1
3.4
2.0
2.7

Standard
deviation
s
0.41
0.68
0.91
2.05
0.39
0.44
0.42
0.82
1.45
1.19
0.83
0.83
0.65
0.86
0.73
1.42
0.62
0.81
0.75
0.61
1.09
1.21
0.69
0.95

c.v.
%
0.62
1.02
1.35
3.04
0.59
0.65
0.62
1.21
2.13
1.75
1.22
1.22
0.95
1.28
1.08
2.06
0.91
1.18
1.11
0.89
1.60
1.77
1.02
1.39

130

Table 5.12 (cont.):

Brick dimensions for length, width and height in all samples.

Length
Sample

Batch
3

25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40

Mean
x
215.7
214.6
215.1
214.7
215.4
216.3
214.7
215.7
215.2
215.5
215.1
215.1
216.1
215.0
214.8
215.2

Range,
R
2.1
2.5
2.2
3.3
2.3
2.3
3.9
2.2
3.1
2.8
1.8
2.2
2.3
1.5
1.4
2.2

Standard
deviation
s
0.98
0.98
0.89
1.19
0.80
0.82
1.33
0.79
1.26
1.21
0.72
0.75
0.80
0.51
0.57
0.94

Width
c.v. %
0.46
0.46
0.42
0.55
0.37
0.38
0.62
0.37
0.59
0.56
0.34
0.35
0.37
0.24
0.26
0.44

Mean
x
99.7
99.5
99.8
99.9
99.7
100.5
99.4
100.3
99.4
100.0
99.0
98.7
99.8
99.2
99.6
100.2

Range
R
2.3
1.7
3.2
1.7
2.2
1.8
3.3
2.1
2.3
0.9
3.0
1.3
3.0
1.4
1.4
1.4

Standard
deviation
s
0.89
0.71
1.22
0.73
0.79
0.60
1.13
0.74
0.97
0.32
1.13
0.43
1.08
0.54
0.61
0.49

Height
c.v. %

Mean

Range

0.89
0.71
1.22
0.73
0.79
0.60
1.14
0.74
0.97
0.32
1.15
0.43
1.08
0.54
0.62
0.49

x
67.2
66.9
67.1
67.1
67.4
67.7
67.4
67.5
67.4
67.2
67.0
67.1
67.0
66.8
67.0
67.1

R
1.1
1.0
2.0
1.0
0.6
0.8
2.6
1.5
2.9
1.6
0.4
1.8
1.1
1.0
0.6
1.3

Standard
deviation
s
0.37
0.40
0.67
0.34
0.25
0.34
1.03
0.53
0.94
0.57
0.11
0.58
0.38
0.38
0.20
0.44

c.v. %
0.55
0.60
1.00
0.51
0.38
0.51
1.52
0.79
1.40
0.85
0.17
0.86
0.57
0.57
0.30
0.65

131

Table 5.12 (cont.):

Sample

Mean
x

Batch
4

41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56

216.4
216.2
215.6
215.1
215.1
215.7
215.7
216.2
216.9
214.6
216.8
217.0
215.8
215.4
216.1
216.3

Length
Ranges Standard
deviation
R
s
1.6
0.54
3.4
1.24
2.7
1.02
3.5
1.46
3.5
1.27
3.3
1.12
3.8
1.30
4.9
1.81
5.7
2.63
3.2
1.18
6.2
2.04
6.9
2.37
4.1
1.56
1.6
0.59
2.1
0.72
1.5
0.58

Brick dimensions for length, width and height in all samples.


c.v.
%

Mean
x

0.25
0.57
0.48
0.68
0.59
0.52
0.60
0.84
1.21
0.55
0.94
1.09
0.72
0.27
0.33
0.27

100.2
99.8
99.6
98.9
98.7
99.4
99.1
99.2
100.2
99.0
100.0
99.7
100.0
99.5
100.3
99.8

Width
Ranges Standard
deviation
R
s
1.8
0.65
2.8
1.03
3.0
1.24
4.3
1.64
3.3
1.15
3.2
1.18
2.5
1.02
3.2
1.32
4.4
1.93
1.7
0.62
3.2
1.10
2.2
0.79
1.1
0.40
3.1
1.00
1.2
0.40
1.4
0.55

c.v.
%

Mean
x

0.65
1.03
1.24
1.66
1.17
1.19
1.03
1.33
1.93
0.62
1.10
0.79
0.40
1.00
0.40
0.56

67.7
67.5
67.4
67.1
67.3
67.4
66.6
67.6
67.4
67.0
67.5
67.0
68.3
67.2
67.4
67.5

Height
Ranges Standard
deviation
R
s
1.4
0.51
1.4
0.49
1.2
0.40
1.9
0.74
1.7
0.66
1.6
0.62
2.8
1.06
2.9
1.12
1.6
0.71
2.2
0.71
1.9
0.74
3.3
1.06
2.1
0.82
1.1
0.37
1.7
0.61
0.6
0.27

c.v.
%
0.75
0.72
0.60
1.10
0.97
0.93
1.59
1.66
1.05
1.06
1.10
1.59
1.21
0.55
0.90
0.40

132

133
90
80

Frequency

x = 216.4 mm
s = 1.91mm
c.v. = 0.88 %
Median= 216.2 mm
Mode= 215.0 mm

Normal Curve

70
60
50
40
30

Low <216 mm
Normal 216218 mm
High >218 mm

20
10

221.34-222.50

220.18-221.34

219.02-220.18

217.86-219.02

216.70-217.86

215.55-216.70

214.39-215.55

213.23-214.39

212.07-213.23

210.91-212.07

209.75-210.91

x = 99.7 mm
s = 1.12 mm
c.v. = 1.12 %
Median= 99.8 mm
Mode= 100 mm

Normal curve

102.90-103.56

Individual width (mm)

102.24-102.90

101.58-102.24

100.92-101.58

100.26-100.92

99.6-100.26

98.94-99.60

98.28-98.94

97.62-98.28

Low < 98 mm
Normal 98 100 mm
High > 100 mm
96.96-97.62

100
90
80
70
60
50
40
30
20
10
0

96.30-96.96

Frequency

Individual length (mm)

120

Frequency

100

x = 67.5 mm
s = 0.89 mm
c.v. = 1.32 %
Median= 67.4 mm
Mode= 67.0 mm

Normal curve

80
60
40

Low < 67 mm
Normal 67 68 mm
High > 68 mm

20
70.55-71.26

69.85-70.55

69.14-69.85

68.44-69.14

67.73-68.44

67.03-67.73

66.32-67.03

65.62-66.32

64.91-65.62

64.21-64.91

63.50-64.21

Individual height (mm)

Figure 5.8: Histogram and normal curve for individual dimensions


of length, width and height of bricks
Control charts for the dimensions shows that all data points for the width
were lying within the upper and lower action line and showing less scatter about the
mean (Figure 5.9). All samples were then considered to represent the population
estimates for the width. For length and height, sample data lying outside the upper
and lower warning and action lines were ignored for the derivation of the population
mean.

134
12.0

219.0

9.0

Length (mm)
Range

Length (mm)
Mean

220.0
218.0
217.0
216.0
215.0

6.0
3.0

214.0

0.0
0

10

20

30
40
Sample

50

60

10

20

30

40

50

60

40

50

60

Sample

101,5
101,0
100,5
100,0
99,5
99,0
98,5
98,0

Width (mm)
Range

Width (mm)
Mean

(a)

10

20

30

40

50

7,0
6,0
5,0
4,0
3,0
2,0
1,0
0,0

60

10

20

Sample

30

Sample

69,5
69,0
68,5
68,0
67,5
67,0
66,5
66,0

Height (mm)
Range

Height (mm)
Mean

(b)

10

20

30

40

50

60

6,0
5,0
4,0
3,0
2,0
1,0
0,0
0

10

Sample

20

30

40

50

60

Sample

(c)

Figure 5.9:

Control charts for mean values and ranges of samples for (a)
length (b) width and (c) height of bricks

The components of variances for samples from the different batches were
computed from the ANOVA. A single factor ANOVA was carried out on the
remaining samples after ignoring those outliers from the control charts. The
variances computed from the ANOVA were 1.98, 1.25 and 0.49 for length, width
and height respectively. Table 5.13 shows the comparisons of mean dimension from
results of this research with specified values of BS 3921. It could be seen that the
population mean dimensions of length i.e. 215 to 218 mm, width 99 to 101 mm and
height 67 to 68 mm were within the allowable dimensions of the BS (i.e. less than
the coordinating size for the respective length, width and height). Moreover,
individual measurements also showed that none of the bricks in the sample had

135
dimensions exceeding the specified coordinating size (Appendix A1, Table A1-1,
A1-2, A1-3)
Table 5.13:

Mean dimensions of individual length, width and height of


bricks compared with British Standard (BS 3921:1985)

Mean dimensions (mm)

Population
estimates
@ 95 %
confidence
(mm)

Work size
(mm)

Coordinating
size (mm)

British standard
Specification

High
(upper 33percentile)
>218

Normal
(middle 33percentile)
216 218

Low
(lower 33percentile)
< 216

215 218

215

225

Width

>100

98 100

< 98

99 101

102.5

112.5

Height

>68

67 68

< 67

67 68

65

75

Length

5.4

Water Absorption
Table 5.14 shows specimens results for water absorption for all samples.

The descriptive statistics computed shows that the mean water absorption in
percentage was 11.23 with a standard deviation of 1.284 and c.v. of 11.43 %.
Table 5.14:

Water absorption of specimens in each sample for facing bricks

Sample
Batch
1

Batch
2

1
2
3
4
5
6
7
8
9
10
11

Water absorption of bricks (%)


10.6
8.4
10.5
11.6
11.8
10.8
12.0
12.4
11.9
12.0
13.1

10.2
13.4
11.0
12.6
12.9
13.1
11.5
10.4
12.7
10.4
11.5

10.9
10.4
11.2
10.7
12.2
12.4
10.9
10.1
11.2
11.6
12.7

12.7
8.8
11.6
10.8
13.8
12.4
11.6
12.4
9.7
10.0
12.1

9.5
9.5
10.6
11.6
11.1
10.9
11.7
11.6
11.6
11.7
11.0

11.6
11.9
11.4
12.0
10.4
11.5
12.3
10.7
11.9
12.8
12.3

10.8
10.5
10.8
10.8
12.4
10.0
12.2
12.0
11.1
10.3
12.2

10.6
8.0
13.0
11.3
11.2
11.9
13.0
11.5
12.8
9.4
11.1

13.7
11.6
12.3
13.4
12.4
11.3
13.0
12.3
13.2
12.2
11.8

10.5
12.1
11.1
10.6
10.9
11.2
11.9
10.5
12.0
13.6
11.5

136
Table 5.14 (cont.)
12
11.9
11.3
12.1
13
9.9
9.0
11.0
14
12.4
11.2
12.2
15
11.9
11.6
10.5
16
7.7
10.3
11.3
Batch
3
17
8.8
9.2
9.3
18
10.4
10.2
11.1
19
11.2
10.8
12.1
20
8.6
13.6
11.6
21
12.6
8.6
12.1
22
10.3
9.6
11.4
23
9.3
13.1
12.0
Batch
4
24
12.3
11.0
13.0
25
12.7
8.9
9.6
26
11.7
7.9
9.3
27
12.5
12.2
12.0
Descriptive Statistics
Mean, x = 11.2 %
Median = 11.4 %
Mode = 12.3 %
Standard deviation, s = 1.28 %
Maximum = 14.4 %
Minimum = 7.7 %
Range, R = 6.7 %
Coefficient of variation, c.v. = 11.44 %

12.7
11.4
10.6
10.3
12.0
8.8
10.3
9.4
12.4
11.7
11.1
10.4
12.6
11.7
10.1
7.9

10.5
11.8
12.1
11.1
9.7
10.1
11.5
9.9
11.0
9.7
10.6
12.7
13.5
12.4
11.7
12.7

10.5
10.2
12.8
11.8
11.4
9.6
11.9
10.1
11.5
12.1
14.0
12.9
12.4
13.4
12.1
12.4

10.4
11.6
11.1
9.2
11.6
9.3
11.4
10.2
8.5
12.0
13.3
9.3
12.8
10.7
8.6
11.3

12.7
12.0
10.7
10.8
10.3
9.1
11.4
10.5
11.6
8.6
11.1
12.7
14.4
11.8
9.2
8.8

10.4
12.3
11.3
11.7
10.8
9.5
9.5
12.2
10.0
11.8
9.9
13.5
12.1
12.7
11.1
11.5

11.3
10.8
11.0
10.0
9.8
10.4
10.6
11.4
11.7
8.3
10.0
11.3
11.9
11.1
13.0
11.8

The histogram with the normal curve superimposed to represent the data

70
60
50
40
30
20
10
0

x = 11.2 %
s = 1.28 %
c.v. = 11.43 %
Median = 11.4 %
Mode = 12.3 %

Normal
curve

13.85-14.55

13.15-13.85

12.45-13.15

11.75-12.45

11.05-11.75

10.35-11.05

8.95-9.65

9.65-10.35

8.25-8.95

Low < 11%


Normal 11 12%
High > 12%
7.55-8.25

Frequency

distribution is shown in Figure 5.10.

Absorption in percentage

Figure 5.10:

The histogram and the normal curve fit for water


absorption of bricks

The 33-percentile values were computed from the normal curve. The middle
third of the distribution, which refers to the normal values of water absorption was
11 to 12 %. The control charts as shown in Figure 5.11 shows that sample 17 and

137
24 were lying outside the upper and lower action line. Therefore, these two samples
were ignored in the determination of the population mean. The variance derived
from ANOVA was 1.53 with the standard deviation of 1.24 %. The population

13,0
12,0
11,0
10,0
9,0
0

10

20

30

Water Absorption
(%)
Range

Water Absrption
(%)
Mean

mean for water absorption at 95 % confidence falls in the range of 10 to 12 %.

8,0
6,0
4,0
2,0
0,0
0

10

Sample

20

30

Sample

Figure 5.11: Control chart of mean values and ranges of samples for
water absorption of bricks
In most standards water absorption is often specified against compressive
strength to designate bricks classification. In conjunction with this classification the
bricks population under investigation have a mean compressive strengths of 40 to
over 50 N/mm2 with water absorption of 10 to12 %, appears to supersede the top
range of SW bricks meant for structural application in ASTM.
Table 5.15:

Comparison of water absorption with limits specified by British


Standard and ASTM
Water absorption %

Research results
at 95%
confidence

British Standard (BS 3921)


Engineering A

Engineering B

10 12 %

4.5 %

7.0 %

ASTM C 62 89a
Grade
SW

Grade
MW

Grade
NW

Maximum
17 %

Maximum
22 %

No limit

Comparison of the values for water absorption tests with limits specified in
BS and ASTM (Table 5.15) shows that water absorption of bricks for the
population in this study did not lie in the range of the Engineering A and B of the
BS. However, it can be seen that this range was within the requirements in ASTM
for bricks of the SW and MW category.

138
The British standard specifies bricks of high strength and low water
absorption for their Engineering bricks, which are meant for structural masonry.
Corresponding characteristic flexural strength to three levels of water absorption is
provided in BS 5628: Part 1 i.e. less than 7 %; between 7 % and 12 % and over 12
% to be used in designs (Table 5.16). In this respect, the water absorption
characterised by the bricks in this investigation relates to second level of water
absorption i.e. between 7 and 12 % to yield an estimated characteristic flexural
strength of 0.35 to 1.5 depending upon the mortar designation and plane of failure.

Table 5.16:

Relationship between characteristic flexural strengths and levels


of water absorption (BS 5628 Pt. 1)
Characteristic flexural strength , fkx N/mm2

Mortar designation

Plane of failure parallel to


bed joints

Plane of failure
perpendicular to bed joints

(i)

(i)

(ii) and (iii)

(iv)

(ii) and (iii)

(iv)

Water absorption less than


7%
Between 7 % and 12 %

0.7

0.5

0.4

2.0

1.5

1.2

0.5

0.4

0.35

1.5

1.1

1.0

Over 12 %

0.4

0.3

0.25

1.1

0.9

0.8

A relationship between water absorption and porosity was developed for


bricks investigated in this research. The relation was a projection from results
obtained by Khalaf (2002) and is shown in Chapter VI.

5.5

Initial Rate of Suction


The initial rate of suction for bricks in this investigation was computed based

on gross and net area of immersion. In the BS, IRS is determined based on gross
area of immersion without considering the reduced area due to perforations for cored
bricks. However, in the ASTM and AS/NZS the IRS for cored bricks is calculated
based on the net area of immersion i.e. the gross area less the area of perforations

139
Table 5.17 shows the results of IRS in the specimens for all samples. The
sample mean based on gross area of immersion was 1.6 kg/m2.min. with a standard
deviation of 0.49 kg/m2.min. and a c.v. of 29.6 %.
Table 5.17:

Computed values for initial rate of suction of specimens


for facing bricks based on gross area of immersion

Sample

IRS kg/(m2.min.)

1
1.8
1.4
1.6
1.4
2
1.4
1.6
1.4
0.9
3
1.4
1.6
2.6
1.2
4
1.6
1.7
1.6
1.9
5
1.7
1.8
2.0
1.4
6
1.8
1.6
1.8
1.4
7
2.0
2.0
2.0
2.0
Batch
2
8
2.0
2.3
2.4
2.0
9
1.9
1.3
2.0
1.7
10
1.6
1.1
1.8
2.6
11
2.0
1.9
1.9
2.1
12
1.4
2.0
1.2
2.0
13
1.7
1.9
1.5
1.6
14
2.0
1.6
2.1
1.8
15
1.4
1.5
2.5
1.2
16
0.1
1.0
1.8
1.1
17
2.0
1.2
1.5
1.4
18
1.1
1.5
1.1
1.0
19
1.9
1.9
1.7
1.6
20
2.1
0.6
1.1
2.0
21
1.7
0.9
2.0
2.1
22
1.9
2.1
1.6
2.1
23
1.8
2.1
1.8
1.8
Batch
4
24
2.5
3.1
1.5
1.6
25
2.3
0.8
2.2
2.5
26
1.2
0.2
0.6
2.2
27
1.1
2.3
0.9
0.2
Descriptive Statistics
Mean, x = 1.6 kg/(m2.min.)
Median = 1.7 kg/(m2.min.)
Mode = 2.3 kg/(m2.min.)
Standard deviation, s = 0.49 kg/(m2.min.)
Maximum = 3.1 kg/(m2.min.)
Minimum =0.1 kg/(m2.min.)
Range, R = 3.0 kg/(m2.min.)
Coefficient of variation, c.v. = 29.6 %
Batch
1

2.2
1.6
1.9
2.2
1.7
2.0
1.7
1.3
1.6
1.7
2.2
2.1
2.1
1.3
2.0
1.2
1.4
1.8
1.9
1.8
0.9
1.5
0.8
2.3
2.2
0.8
0.9

1.6
1.6
1.6
1.6
2.0
2.9
2.2
1.5
1.6
1.8
0.8
1.4
1.9
1.9
1.9
1.5
1.4
1.0
1.8
1.6
2.1
1.3
1.6
2.1
1.5
2.3
1.9

2.3
1.4
1.6
1.8
2.1
1.6
1.9
1.7
1.4
1.5
1.7
2.0
1.7
1.6
1.1
1.4
1.1
1.9
1.2
2.0
0.8
0.4
2.5
2.4
2.3
2.5
1.3

0.9
1.2
1.6
1.8
1.7
1.7
1.7
1.4
1.1
1.5
1.7
1.6
1.2
1.9
1.5
1.5
1.4
1.7
1.6
0.7
1.8
1.5
0.7
2.5
1.8
0.9
1.0

1.6
1.4
2.1
1.7
2.1
1.5
1.8
1.9
2.0
1.9
1.7
1.5
1.4
1.6
2.0
1.0
1.0
1.2
1.5
1.2
1.5
0.6
2.3
0.8
0.7
2.4
1.1

1.2
1.8
1.6
1.7
2.3
1.5
1.8
2.3
1.9
1.9
1.1
2.3
2.4
2.5
1.6
1.8
0.7
1.7
1.1
1.9
1.7
2.7
1.5
1.1
2.3
0.9
2.2

The c.v. for IRS in the samples was almost 30.0 % and therefore the lognormal probability curve was used to represent the data distribution. Figure 5.12
shows the histogram with the log-normal curve superimposed. The 33-percentile

140
values in the sample data were computed from the log-normal probability curve and
data in the middle third i.e. 1.0 to1.30 kg/m2.min. indicated normal values for IRS.

x = 1.6 kg / m 2 .min
s = 0.49 kg / m 2 .min
c.v. = 30.0 %
median = 1.7 kg / m 2 .min
mod e = 2.3 kg / m 2 .min

Log-normal
curve

2.633 - 2.910

2.356 - 2.633

2.079 - 2.356

1.802 - 2.079

1.525- 1.802

1.248 - 1.525

0.971 - 1.248

0.694 - 0.971

Low < 1.0 kg/m2.min


Normal =1.0 1.30 kg/m2.min
High > 1.30 kg/m2.min
0.14 - 0.417

80
70
60
50
40
30
20
10
0

0.417 - 0.694

frequency

These values were within the limits of IRS denoted to produce good bond.

Initial rate of suction kg/(m2.min)

Figure 5.12: Histogram and normal curve fit for IRS based on

IRS kg/(m .min)


Range

2.50
2.00

IRS kg/(m2.min)
Mean

gross area of immersion

1.50
1.00
0

10

15

20

25

30

Sample

Figure 5.13:

3.00
2.00
1.00
0.00
0

10

15

20

25

30

Sample

Control charts for means and ranges for IRS based on


gross area of immersion

The control charts of means and ranges (Figure 5.13) shows that some
samples were lying outside the control limits i.e. the upper and lower warning and
action lines. Therefore, these samples i.e. samples 4, 7, 16, 17, 22, 24, 26 and 27
were taken as not representative of the population and were ignored in the
determination of the population mean. The estimate of variance derived from
ANOVA for all data after ignoring the samples described above was 0.178. The
corresponding standard deviation was 0.422 kg/m2.min.and the population mean
ranging from 1.4 to 2.0 kg/m2.min i.e. at 95 % confidence (5 % reject).

141
ASTM specifies that bricks with IRS greater than 1.5 kg/m2.min should be
well wetted before laying and recommended that the wetting be carried out 3 to 24
hours before use. On the other hand there is no provision of IRS limits in the BS
3921:1985. However, a test method for determining IRS is included in the British
standard as this parameter is important for highly stressed masonry structures. In
prEN 771-1 the IRS values are only required in application where the work warrant
its use and in this respect the value should be declared by the manufacturer.
Although the normal values of IRS in the middle third distribution, ranged
from 1.0 to 1.3 kg/m2.min is within the recommended limit of the ASTM the upper
range of the 95 % confidence limits were higher than 1.5 kg/m2.min. Hence,
consideration for wetting of the bricks should be emphasised especially in
application where bond strength is critical.
Wetting bricks before laying is more critical in hot weather construction
since suction rate of bricks is influenced by the temperature of the bricks and the
surrounding temperature (Davidson, 1982). Warmer units will absorb more water
from the mortar and in addition, the water from mortar is evaporated at a faster rate.
For this reason, in hot weather construction, bricks with high suction rates (over 1.5
kg/m2.min) should be well wetted before laying. On this basis, the IRS should be
regarded as an important property of brick for this country, which experience hot
weather throughout the year.
Table 5.18 shows the results for IRS based on net area of immersion. The
mean IRS was 1.9 kg/m2.min, which showed a considerable increase of about 20 %
from the IRS determined by gross area of immersion. The ASTM considers this
factor and specified that the IRS should be calculated based on the net area of
immersion for perforated bricks while the AS/NZS 4456:1997 specifies both values
of IRS due to net and gross area of immersion.

142
Table 5.18:

Computed values for initial rate of suction of specimens of


facing bricks based on net area of immersion
IRS kg/(m2.min.)

Sample
1
2.11 1.65
2
1.64 1.90
3
1.64 1.90
4
1.90 1.96
5
1.95 2.08
Batch
6
2.14 1.83
1
7
2.40 2.33
8
2.37 2.65
9
2.23 1.48
10
1.92 1.31
11
2.35 2.19
12
1.67 2.34
13
2.02 2.28
14
2.38 1.93
15
1.59 1.71
Batch
3
16
0.17 1.21
17
2.37 1.44
18
1.32 1.73
19
2.19 2.17
20
2.45 0.68
21
2.02 1.06
22
2.25 2.44
23
2.08 2.46
Batch
4
24
2.97 3.59
25
2.66 0.94
26
1.45 0.22
27
1.24 2.66
Mean x = 1.933 kg/(m2.min.)

5.6

1.89
1.62
3.01
1.93
2.38
2.06
2.33
2.82
2.35
2.11
2.27
1.39
1.71
2.43
2.94
2.07
1.80
1.34
2.03
1.28
2.29
1.90
2.07
1.81
2.57
0.71
1.04

1.66
1.11
1.37
2.18
1.62
1.65
2.30
2.41
1.97
3.07
2.42
2.39
1.88
2.09
1.40
1.27
1.65
1.17
1.91
2.29
2.49
2.53
2.11
1.92
2.92
2.60
0.28

2.60
1.90
2.23
2.62
1.99
2.35
1.98
1.49
1.85
1.98
2.60
2.42
2.44
1.55
2.38
1.35
1.69
2.17
2.22
2.09
1.11
1.78
0.96
2.71
2.55
0.99
1.04

1.86
1.92
1.91
1.88
2.38
3.43
2.53
1.71
1.88
2.06
0.89
1.59
2.19
2.22
2.21
1.70
1.70
1.23
2.13
1.89
2.50
1.49
1.86
2.52
1.70
2.71
2.19

2.67
1.63
1.90
2.13
2.48
1.89
2.29
1.96
1.70
1.78
2.01
2.34
1.99
1.87
1.24
1.60
1.27
2.28
1.44
2.32
0.89
0.45
3.00
2.78
2.68
2.93
1.52

1.10
1.37
1.91
2.08
2.05
2.00
2.00
1.62
1.31
1.80
2.04
1.86
1.40
2.25
1.75
1.75
1.70
1.98
1.93
0.79
2.16
1.73
0.85
2.92
2.07
1.06
1.20

1.90
1.63
2.43
1.97
2.50
1.74
2.12
2.24
2.30
2.22
2.02
1.73
1.67
1.87
2.35
1.17
1.16
1.39
1.76
1.35
1.80
0.68
2.73
0.98
0.82
2.77
1.30

1.36
2.17
1.91
1.99
2.74
1.74
2.12
2.71
2.26
2.18
1.26
2.73
2.81
2.94
1.89
2.11
0.83
2.02
1.29
2.19
1.98
3.19
1.78
1.28
2.66
1.04
2.59

Density
Table 5.19 shows the results for the density test in the specimens for all

samples. The mean density from sample data was 1781.51 kg/m3 with a standard
deviation of 35.858 kg/m3 and a c.v. of 2.013 %.

143

Table 5.19:

Density of specimens in each sample for facing bricks

Sample
1
1761.03 1848.48 1777.78
2
1751.80 1805.15 1748.12
3
1794.57 1773.08 1671.33
4
1776.60 1782.95 1731.06
5
1785.27 1784.96 1757.64
6
1781.69 1754.29 1800.75
7
1705.15 1794.96 1771.74
Batch
2
8
1847.73 1754.55 1770.21
9
1782.48 1778.10 1786.86
10 1773.91 1823.13 1784.44
11 1797.81 1761.59 1778.99
12 1802.17 1789.05 1822.39
13 1783.94 1770.29 1784.67
14 1856.72 1836.30 1805.15
Batch 15 1796.27 1842.97 1764.93
3
16 1851.16 1763.16 1763.70
17 1766.92 1891.27 1775.56
18 1834.38 1797.66 1767.65
19 1733.82 1762.69 1817.69
20 1784.44 1685.00 1696.40
21 1768.15 1705.93 1742.96
22 1829.46 1770.45 1743.61
Batch 23 1821.54 1778.63 1738.35
4
24 1783.58 1766.21 1789.84
25 1767.45 1742.24 1748.89
26 1756.83 1879.38 1795.56
27 1836.83 1806.39 1805.15
Descriptive Statistics
Mean, x = 1781.51 kg/m3
Median = 1781.158 kg/m3
Mode = 1805.147 kg/m3
Standard deviation, s = 35.858 kg/m3
Maximum = 1902.273 kg/m3
Minimum =1671.329 kg/m3
Range, R = 230.944 kg/m3
Coefficient of variation, c.v. =2.013%
Batch
1

Density kg/m3
1803.70
1795.62
1767.61
1794.57
1783.46
1794.78
1795.62
1773.53
1748.57
1794.16
1810.29
1802.21
1814.07
1842.22
1792.42
1799.25
1809.85
1760.00
1800.76
1810.24
1736.09
1725.19
1719.05
1728.56
1830.37
1805.85
1842.22

1770.37
1804.51
1792.59
1775.74
1780.85
1752.67
1778.52
1760.31
1789.78
1771.18
1805.88
1795.59
1820.90
1756.83
1813.85
1749.62
1751.82
1773.33
1754.74
1793.02
1716.18
1760.00
1765.12
1792.77
1803.45
1741.94
1726.54

1787.31
1775.36
1715.83
1734.85
1792.03
1756.12
1738.89
1769.23
1783.94
1775.36
1793.38
1836.09
1828.15
1766.91
1833.86
1817.56
1806.15
1759.84
1692.09
1739.85
1798.50
1761.48
1754.81
1773.95
1792.74
1795.26
1716.82

1868.00
1791.97
1759.69
1781.48
1755.47
1780.14
1750.35
1757.86
1749.29
1831.58
1820.44
1774.64
1807.41
1813.33
1771.64
1784.09
1762.12
1840.94
1800.00
1770.00
1754.55
1739.10
1758.02
1720.93
1810.54
1761.12
1797.33

1785.19
1797.71
1792.59
1746.48
1754.74
1780.14
1815.56
1775.00
1756.12
1755.71
1783.45
1834.81
1836.09
1786.86
1902.27
1791.85
1788.64
1773.48
1725.18
1793.28
1737.31
1791.73
1782.71
1763.33
1780.34
1768.64
1825.95

1793.48
1834.59
1812.50
1802.33
1721.01
1779.70
1747.33
1759.85
1789.05
1774.64
1819.12
1800.73
1843.28
1822.06
1747.76
1787.97
1761.65
1817.32
1739.42
1755.56
1790.15
1747.37
1738.35
1788.46
1811.22
1759.74
1802.17

1751.85
1800.00
1794.78
1765.38
1740.58
1785.21
1781.29
1772.22
1778.99
1814.81
1830.08
1824.26
1827.61
1781.02
1878.74
1716.79
1856.25
1775.38
1695.71
1751.11
1739.10
1747.73
1766.92
1768.82
1795.16
1806.25
1781.02

Figure 5.14 shows the histogram to represent data distribution. Assuming


that the data is normally distributed, the normal curve fit is analysed and the curve
superimposed on the histogram. From the normal curve the 33-percentile computed
from sample data shows the middle third distribution, which consists of the normal
values for density ranging from 1766 to 1795 kg/m3.

144
From Control charts for means and ranges of density (Figure 5.15), the
samples lying outside the upper and lower warning and action lines were ignored to
determine the population mean. A single factor ANOVA was carried out on the
remaining sample data to determine the components of variance in the samples
among the different batches. The variance determined from the ANOVA was 1114.0
with standard deviation of 33.38 kg/m3. The population mean neglecting the samples
outside the zones mentioned above, and with 95 % confidence limits was 1757
to1804 kg/m3. This value was higher than the average value of density i.e.1610
kg/m3 (Table 5.20) required for sound insulation purposes of the Building

80
70
60
50
40
30
20
10
0
1901.0-1924.1

1877.9-1901.0

1854.8-1877.9

1831.7-1854.8

1808.6-1831.7

1785.5-1808.6

1762.4-1785.5

1739.3-1762.4

1716.2-1739.3

1693.1-1716.2

x = 1781.51kg / m3
s = 35.86kg / m3
median = 1781.16kg / m3
mod e = 1805.15kg / m3
c.v. = 2.013%

1670.0-1693.1

Frequency

Regulations of the United Kingdom.

Low < 1767 kg/m3


Normal 1767 1795 kg/m3
High > 1795 kg/m3

De nsity kg/m 3

Figure 5.14: Histogram and normal curve fit for density of

1820

Density kg/m
Range

Density kg/m
Mean

bricks

1800
1780
1760
1740
0

10

15

20

25

Sample

Figure 5.15:

30

200
150
100
50
0
0

10

20

30

Sample

Control charts for mean values and ranges of samples for


density of bricks

145
Table 5.20:

Density of bricks for sound insulation in walls and walls


with plaster finish for (Building regulations of the UK)
Wall

Plaster finish

Average
density of
brick to be
used
(kg/m3)

Material
and
dimensions
(mm)

Thickness
(mm)

Specified
weight at least
(kg/m2) includes
finish

Number
of sides

Type

Solid wall
Brick size
mm
65 x 102.5 x
215

215

375

Lightweight

1610

Gypsum

1610

Cavity wall

255

Lightweight

1970

Gypsum

1970

415

Density of brick has been given more emphasis recently in masonry


standards. The prEN 771-1 included density as a requirement especially to identify
the acoustic property of a brick. A brick wall with thickness 102.5 mm could give a
sound reduction index of 46 dB (Curtin, et. al). Table 5.21 shows the typical sound
insulation values of masonry walls with respect to its thickness and weight.
Loudness of 40 to 50 dB is considered as faint to moderate loudness suitable for an
average home and general to private office (Drysdale, et.al).
Table 5.21: Typical sound insulation values of masonry walls
(Curtin, et. al)
Thickness
(mm)

Weight
(kg/m2)

Approximate sound
reduction index
(dB)

Brick wall plastered both


sides with a minimum of
12.5 mm thick plaster

215

415

49.5

Brick wall plastered both


sides with a minimum of
12.5 mm thick plaster

102.5

220

46

Material and construction

146
5.7

Efflorescence
The results in the test for efflorescence were based on the 4 samples

(1 sample in each batch). Every brick in a sample of 10 bricks were examined for
efflorescence after the test. Based on visual examination of the exposed surfaces for
all the samples in the 4 batches no deposits of salts or any other effects of
efflorescence such as powdering or flaking could be detected.

5.8

Soluble Salt Content


Bricks were tested for the presence of acid soluble sulphates and water-

soluble salts of calcium, magnesium, potassium and sodium. Table 5.22 shows the
content of soluble salt in the samples from the various batches and the maximum
limit of salt content provided by BS 3921:1985 for the category of low salt.
Table 5.22:
Sample
Batch
1
Batch
2
Batch
3

Batch
4

Percentage of soluble salts in samples from all batches


Calcium

Sodium

Potassium

Magnesium

Sulphate

0.013

0.003

0.003

0.003

0.014

0.07

0.002

0.003

0.002

0.07

0.003

0.004

0.006

0.002

0.09

0.006

0.002

0.009

0.003

0.06

0.016

0.003

0.007

0.006

0.09

0.010

0.001

0.003

0.004

0.02

0.007

0.003

0.006

0.003

0.09

0.011

0.002

0.005

0.004

0.04

0.007

0.001

0.003

0.003

0.02

10

0.008

0.002

0.004

0.003

0.02

11

0.009

0.002

0.004

0.003

0.02

12

0.010

0.002

0.004

0.005

0.02

Mean, x %

0.010

0.002

0.005

0.003

0.05

Sample standard
deviation, s

0.004

0.0006

0.002

0.001

0.03

c.v. %

40.0

30.0

40.0

33.3

60.0

BS 3921:1985

0.3 %

0.03 %

0.03 %

0.03 %

0.50 %

147
The results indicated that the percentage of salts i.e. calcium, sodium,
magnesium, potassium and sulphate in the bricks were very small in comparisons
with the limits for the category of Low salt content as defined in BS 3921:1985.
The c.v. in the test for sulphate was considerably high which was about
60 %. The reason for this was most probably due to the test method used. Sulphate
was determined by the gravimetric method, which is confined to relatively high
sulphate content. The method was also considered as rather complicated and this
may contributed to the significant variability in the results (Brachtel, 2003).
The results of salt content compared with the European Standard prEN 771-1
also showed that the bricks investigated had very low salt content. The combined
content of sodium and potassium in the bricks from this research was 0.007 %,
which is very much below the maximum limits provided in prEN 771-1 for category
S1 (0.17 %) and S2 (0.06 %). Similarly, with a mean percentage of 0.003,
magnesium was also below the specified maximum limit i.e. 0.08 and 0.03 for
category S1 and S2 respectively. Thus the bricks fit into the category of application
of S1 and S2 as defined in the European Standard; S1 is for normal exposure and S2
is suitable for prolonged saturation applications.

CHAPTER 6

APPLICATIONS OF RESEARCH FINDINGS

6.1

Relationship of Aspect Ratio to Compressive Strength


In masonry construction bricks are normally laid on the bed face, which yield

the greatest compressive strength compared to if laid in the stretcher or header faces.
A relationship between the compressive strengths of units and their aspect ratio (h/t),
was proposed through the research findings described in the earlier chapters. The
compressive strengths are related to h/t as described by the following relationship:
f = 16.35 x + 58.17

(6.1)

Where,
f = compressive strengths of a brick (N/mm2)
x =aspect ratio (height to thickness ratio, h/t).
The above relationship was obtained by the best-fit line with a regression
coefficient of R2 = 0.998 (Figure 6.1)

Compressive strength, f
N/mm2

149
50
40
f = -16.353x + 58.168

30

R2 = 0.998

20
10
0

0.5

1.5

2.5

3.5

Height to thickness ratio, h/t

Figure 6.1:

Relationship between compressive strength


and h/t ratio of bricks.

Equation 6.1 can be used to estimate compressive strength of a brick for


various h/t ratio greater than 0.7 but less than 3.2. The dimensions h and t are
defined accordingly to the orientation of bricks in a brick laying (Figure 6.2), where
h = height of the brick normal to the loading axis,
t = smaller dimension of the loaded surface area.

h
(a)

h
(b)

W= direction of loading on wall

t
h
(c)

Figure 6.2:

Orientation of bricks in a brick laying (a) header face


(b) bed face (c) stretcher face

150
The estimated strength provides useful information to manufacturers as well
as designers in assessing the compressive strength of a brick when loaded in the
various orientations without conducting any tests, as yet giving an important data for
use in preliminary design or strength assessment. The proposed relationship is also
convenient to users where facilities for testing are not available at hand. The
applicability of the proposed estimated relationship is only valid under the following
conditions:

The bricks are fired clay bricks.

Percentage of perforations is about 20 %

The aspect ratio h/t must lie between 0.7 to 3.2

It should be noted that the estimated compressive strengths for bricks loaded
on the bed face as derived in equation 6.1 is based on gross loaded area whereby
perforated areas were ignored. This tends to yield a smaller compressive strength
than if computed using net area. Hence, the prediction given by this formula for
perforated bricks tested on bed face is conservative.
Conventionally the compressive strength test provides the strength of bricks
when loaded on bed face. The relationship between the compressive strength of
bricks when loaded on the bed face and in other test orientations are considered
important for design and preliminary assessment purposes.
An attempt is made to establish this relationship, based on the research
findings described in previous chapters and illustrated below. The compressive
strength of bricks when loaded on the bed face is used as a standard measure as it is
the only available data in any compressive test.
Assuming fb, fs and fh are the corresponding compressive strength of bricks
in the bed, stretcher and header faces. Substituting the values of fb and fs as 46.1 and
34.7 N/mm2 for compressive strengths of bricks in this research, therefore a ratio of
fs : fb can be established as shown in equation 6.2.

151
f s 34.7
=
= 0.75
f b 46.1

(6.2)

or,
f s = 0.75 fb

(6.3)

Similarly, the compressive strength due to loading on the header face (fh=
5.5 N/mm2) can be derived in terms of fb as shown in equation 6.4.
fh
5.5
=
= 0.12
fb 46.1
fh = 0.12 fb

(6.4)
(6.5)

For fired clay bricks the ratio of compressive strength for bricks tested on the
f
stretcher face to bed face, s = 0.75 . The ratio of compressive strength for bricks
fb
f
tested on the header face to the bed face, h = 0.12 .
fb
This is a convenient method of projecting the test results to other orientations
in the absence of laboratory facilities, and also acts as a guide to some preliminary
design work. It is to be noted, however, that the relationship of equation 6.3 and 6.5,
are valid provided that the conditions stated earlier are satisfied.

6.2

Relationship of Water Absorption to Porosity and Compressive Strength


Recent investigation on brick porosity and water absorption (Khalaf, 2002)

has indicated that there is a relationship between water absorption, porosity and
compressive strength. Table 6.1 shows the results of bricks compressive strength,
water absorption and porosity obtained by Khalaf.

152
Table 6.1:

Relationship between bricks compressive strength, water


absorption and porosity (Khalaf, 2002)
Full-brick
compressive
strength
(N/mm2)
92
81
68
39
-

Brick Type
Class B engineering
Clay 10 hole
Clay 3 slot and 8 hole
Clay frogged common
Granite

Water absorption of
brick units BS 3921
(5-hr boil)
(%)
6.0
6.2
5.8
12.9
2.63

Porosity of brick
lumps by
vacuum (%)
14.85
16.75
17.39
25.04
6.15

Using the results from Table 6.1 the graphs as shown in Figure 6.3 and 6.4
were plotted to show the relationship of water absorption to porosity and

Water absorption,%
( 5-hr boiling)

compressive strength of bricks respectively.

14
12
10
8
6
4

y = 0.74x - 6.05
R2 = 0.9348

14

16

18

20

22

24

26

Porosity (%)

Figure 6.3:

Relationship of water absorption with porosity

Full-brick compressive
strength, f (N/mm2)

from Table 6.1

100
80
60
40
20
0

f = -4.97x + 161.96
R2 = 0.9497

14

16

18

20

22

24

26

Porosity (%)

Figure 6.4:

Relationship of porosity with compressive strength


from Table 6.1

The relationship of water absorption with porosity (Figure 6.3) was used to
determine the porosity of the bricks in this investigation as shown in equation 6.6

153
y = 0.74 x 6.05

(6.6)

Where,
y = water absorption (%)
x = porosity (%)
Substituting y = 11.2% i.e. the mean water absorption for the bricks in this
investigation, in equation 6.6, the porosity, x = 23 %
The relationship of porosity with compressive strength is shown in Figure
6.4. Knowing the porosity the compressive strength could be derived from the
relationship as described by equation 6.7
f = 4.97 x + 161.96

(6.7)

Where,
f = compressive strength (N/mm2)
x = porosity ( %)
Substituting the porosity, x = 23 % in equation 6.7, the compressive strength
computed was 47.65 N/mm2, which was close to the value of the mean compressive
strength in this research i.e. 46.1 N/mm2. Thus it could be assumed that the bricks in
this investigation had a porosity of about 23 %. However it is to be noted that the
porosity derived in this equation was based on results of 20 mm bricks lumps.

CHAPTER 7

CONCLUSIONS AND RECOMMENDATIONS


FOR FURTHER WORK

7.1

Conclusions
The conclusions are divided into two sections i.e. the general conclusions

and the detailed conclusions. The general conclusions dealt with properties found in
the present Malaysian standards (MS 76 Part 2:1972) i.e. compressive strengths,
water absorption, dimensional tolerance and soluble salt content. The detailed
conclusions consist of other aspects of the properties evaluation arising from
comparisons conducted with other international standards and the varying test
methods and measurements used by these standards. The section also contains new
properties consisting of initial rate of suction and density useful for the development
of masonry standards.

7.2

General Conclusions
The mean compressive strength of facing bricks falls in the range of

40 N/mm2 to 50 N/mm2 and common bricks 30 N/mm2 to 40 N/mm2. The bricks fall
within the higher range of compressive strengths specified in Malaysian Standard
MS 76:1972 and therefore regarded as load bearing units.

155
The mean water absorption of the bricks investigated was 10 % to 12 %,
which lied outside the specified limits for Engineering A ( 4.5 %) and Engineering
B ( 7 %) of the Malaysian/British Standard.
The results on the overall dimensions of 24 bricks showed that both the
length and the width fall within the permissible tolerance of the Malaysian
Standard/British Standard. However, the height exceeded the Malaysian Standard/
British Standard tolerance limit considerably by about 37 mm. Therefore, the
category of dimensional deviations in existing Malaysian standard, which was based
on the BS overall measurement of 24 bricks need to be modified accordingly.
The content of calcium, magnesium, potassium, sodium and sulphate in the
bricks was very negligible and thus they fall under the durability designation of
Low (L) of soluble salt content as per BS 3921:1985. In accordance to European
Standard, the bricks could be applied even for the worst condition of construction
application i.e. S2, which is meant for masonry structures subjected to prolonged
wet situation.

7.3

Detailed Conclusions

7.3.1

Compressive strengths
The range of mean compressive strength obtained in the bricks surpass the

minimum value i.e. 20.7 N/mm2 specified for compressive strength of facing brick
in ASTM C216-90a to be used in SW (severe weathering) regions. Under Singapore
Standard SS 103:1974, the bricks could be categorised as the First Grade bricks.
Considerable reduction of compressive strength was observed when bricks
were tested in the different orientations. When tested on the stretcher face the
compressive strength was approximately 60 % to 90 % of the compressive strength
tested on bed face. On the header face the compressive strength was further reduced

156
to about 10 % to 15 % of the strength tested on bed face. Hence, compressive
strength should be indicated with the brick orientation for testing.
Compressive strength of bricks is affected by curing conditions before
testing. Dry bricks show higher compressive strengths than wet bricks. The
compressive strength of bricks evaluated in the tests was based on saturated
condition, therefore, providing conservative values by about 15 to 20 %.
Additionally, the compressive strength was computed based on gross area, further
reducing the compressive strength by approximately 20 %.

7.3.2

Water Absorption
Although the bricks researched could not satisfy the requirements for the

water absorption in the Malaysian Standard (MS 76:1972), the values were well
within the requirements provided in ASTM for Grade SW and MW bricks with
water absorption limits of 17 % and 22 % respectively.
Malaysian bricks tend to have high water absorption, typically greater than
10 %, and this can be explained by the limestone content in the soil. This is not a
characteristic of British soil, therefore water absorption in British bricks are usually
lower.
The water absorption of the bricks investigated corresponds to the second
level of the characteristic flexural strength of BS 5628: Part 1, denoted by strengths
of 0.35 to 1.5 N/mm2, which depend on the mortar designation and the plane of
failure. These values are required in the design of masonry structures.
The relation of water absorption to porosity showed that the porosity of the
bricks in this investigation was about 23 %. Compressive strength of bricks could be
related to their porosity and this relationship would be useful for a preliminary
estimation of compressive strength.

157

7.3.3

Dimensional Tolerance
Comparison of results with the recent European Standard shows that the

bricks investigated satisfy the category of T1 of prEN 771-1.

7.3.4

Initial Rate of Suction


The bricks in this investigation had a mean initial rate of suction of 1.4 to 2.0
2

kg/m .min, which fall under the high range of IRS. Ideally, the value of IRS should
be between 0.25 to 1.5 kg/min.m2 for the development of appropriate bond strength
between the bricks and the mortar interface. ASTM recommends that bricks with
IRS exceeding 1.5 kg/min.m2 should be wetted before laying. The bricks indicted
high values of IRS hence requiring pre-wetted surface before laying in order to
optimise bonding upon laying on to mortar. This is considered more critical in hot
weather construction since hot bricks will absorb more water and the water in mortar
will be depreciated at a faster rate with high temperature.
The range of IRS values of 1.4 to 2.0 kg/m2.min demonstrated by the bricks
in this investigation was determined using gross area i.e. without reducing the area
of immersion by the area of perforations. The IRS calculated using net area of
immersion shows an IRS value higher than about 18 % if based on gross area. The
BS 3921:1985 computed the IRS based on gross area while the ASTM and AS/NZS
use the net area. It is therefore significant that IRS values be clearly indicated for
both cases of calculation to avoid confusion. Therefore, specification for IRS values
should be denoted as IRSgross or IRSnet depending on the surface area of immersion.

158
7.3.5

Soluble Salt Content


The soluble salt content for all the minerals under investigations i.e. calcium,

sodium, potassium, magnesium and sulphate were all below the maximum limits
specified in the British Standard. This justifies the reason why salt does not appear
on the brick surfaces in the efflorescence test. The effects of sulphate have been
given a considerable attention in existing standards, however this is not the case for
EN 771-1. The European standard considered the sulphate action a complex matter
to be dealt with in the national design codes. Sodium and potassium has been
analysed as a combined effect in the EN, with maximum values of 0.17 %
depending on the application category. In this case the research results of 0.007 %
does not exceed the recommended percentage of the EN. The percentage of sulphate
present in the bricks was 0.05 %. This value is much below the maximum of 0.5 %
allowed for in the BS 3921.

7.3.6

Density
The density of the bricks in this investigation is within the range of 1757
3

kg/m to 1804 kg/m3. Previous works imply that the bricks in this range use in a
102.5 mm thick wall could give a sound insulation of 40 to 50 dB (Curtin et al.,
1995) which is considered as faint to moderate loudness suitable for an average
home and general to private office (Drysdale et al., 1994). The density of the bricks,
also suffice the requirements for sound insulation specified in the building
regulations in the United Kingdom.

7.4

Recommendations for Further Work


The bricks properties reported herein was based on a production from a

single manufacturer of clay bricks. Future studies should include other


manufacturers of clay bricks in order to achieve results representative of the entire

159
population of bricks in the country. The results representing the whole population
would characterise local production and therefore useful in the development of
national standards. Recommendations for future research should include the
following:
(i)

Sampling should be obtained from a larger number of manufacturers

across the country for a more representative estimate of the properties and to
include various types of bricks in local production.
(ii)

In order to get a more comprehensive relationship of the compressive

strengths with the bricks aspect ratio (h/t), bricks samples should comprise
other formats and configurations to include a wider range of bricks types.
In this research, bricks were generally tested in accordance to the British
standard procedure. However, procedures from other standards were also looked
into and regarded as more reliable and accurate. Some recommendations to be
considered in the testing methods for future studies include:
(i)

Investigation on the density of bricks should be determined for both

the dry and ambient condition.


(ii)

Evaluation of water absorption by the 5-hr boiling test involving the

use of small brick lumps as specimen instead of the normal whole brick may
be considered. This new method would certainly be more economical
because less fuel would be needed in boiling the small specimen. Moreover,
the handling of experiments would be more convenient with small specimens
especially in testing that implicate a large amount of samples as experienced
in this research. Further, it was claimed that this new method could produce
results that are more accurate.
(iii)

In the preparation of specimens for the tests of water absorption and

IRS, BS 3921 procedure for attaining constant mass when drying bricks in
the oven is by heating the bricks for at least 48 hrs. The ASTM and
Australian standard monitor the change of mass at specified intervals. Bricks,

160
which are recently manufactured, normally have very small moisture content.
Thus, they may not need too long a duration for example the 48 hours
assumed to attain constant mass. Therefore, by monitoring the weight loss
may reduce the time of heating and consequently economise on the use of
energy. For this matter, it is recommended that the AS/NZS 4456 or the
ASTM C 67 be adopted in the laboratory procedure for attaining constant
mass of bricks.
(iv)

In the test for IRS, standard method should incorporate ways of

ensuring a consistent 3 mm immersion during the test. This could be helpful


in attaining more precise results.

REFERENCES

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ACI 530.1-92/ASCE 6-92/TMS 602-92, Reference manual.
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America, ASTM C 216-90a.
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Brick (Hollow Masonry Units Made from Clay or Shale). United States of
America, ASTM C 652-89a.
American Society for Testing Materials (1990), Standard Specification for Building
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ASTM C 67-90a.
Beall, Christine (1993). Masonry design and detailing. Third Edition. New York.
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Bland, J. A. (1985). Statistics for construction students. London: Construction
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Brachtel, G. Water-soluble and acid-soluble sulphate content of heavy products.
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British Standards Institution (1985). British Standard Code of Practice for use of
Masonry, Part 1. Structural Use of unreinforced masonry. London, BS 5628
British Standards Institution (1985). British Standard Code of Practice for use of
Masonry, Part 2. Structural Use of reinforced and Prestressed masonry.
London, BS 5628
British Standards Institution (1985). British Standard Specification for Clay
Bricks. London, BS 3921
British Standards Institution (1991). Guide to Statistical Interpretation of Data.
London, BS 2846: Part 1
British Standards Institution (2000). Specification for masonry units (draft
candidate harmonised standard). London, Draft: pr EN 771-1
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Curtin, W.G., Shaw, G., Beck J. K. and Bray W.A. (1995). Structural Masonry
Designers Manual. Second Edition. London: Blackwell Science Ltd.
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and Evaluation (ASTM) Vol. 10, No.3, pp81 82.
Drysdale, R.G., Hamid, A.A. and Baker, L.R. (1994). Masonry Structures
Behaviour and Design. Prentice Hall.
Experimental Building Station (Department of Construction) (1976). Bond
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Grimm, C.T. (1975). Strength and related properties of brick masonry. Journal of
The Structural Division. Technical Publications ASCE.
Grimm, C. T. (1988). Statistical Primer for Brick Masonry. Masonry: Materials,
Design, Construction, and Maintenance, pp. 169-192.
Grimm, C. T. (1996). Clay Brick Masonry Weight Variation. Journal of
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Hammer, M. J. and Hammer M. J. Jr. (1996). Water & Wastewater Treatment.
Singapore: Prentice Hall.
Hendry, A.W. (2001). Masonry walls: materials and constrution. Construction and
building Materials, 15. 323-330. Elsevier.
Hendry, A.W., Sinha, B.P., Davies S.R. (1981). An introduction to load bearing
brickwork design. U.K.: Ellis Horwood Limited.
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Absorption of Fired Clay Bricks. Journal of Material in Civil Engineering.
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and scientist. New York: Harper & Row Publishers.
Lenczner, D. (1972). Elements of Load-bearing Brickwork. Oxford, New York,
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Morton, J. (1986). The design of laterally loaded walls. TGV Publications.
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APPENDICES

A1

RESULTS OF TESTS SPECIMENS


FOR DIMENSIONAL TOLERANCE OF
INDIVIDUAL BRICKS

167
Table A1-1:

Batch
1

Batch
2

Batch
3

Batch
4

Sample
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56

Individual measurement for length


Length
218.00
218.45
217.05
218.60
216.20
219.10
217.40
220.60
215.75
214.50
217.10
213.55
217.20
217.70
219.45
221.30
217.00
218.35
217.80
217.25
220.00
218.25
214.95
218.25
217.00
215.00
214.75
215.00
215.60
215.00
215.30
215.20
215.75
216.90
215.25
215.00
215.50
215.15
215.40
216.10
216.60
215.50
214.75
216.20
213.75
216.50
216.50
218.50
215.55
215.95
214.25
220.95
215.95
215.45
216.25
216.95

218.60
220.20
219.45
219.55
217.20
217.90
216.90
217.40
218.00
220.45
214.50
217.25
220.65
216.10
217.80
217.25
215.75
217.70
218.30
217.00
220.70
218.50
214.95
209.75
214.90
214.70
215.50
215.60
214.65
216.25
214.00
215.00
216.30
214.15
215.55
215.00
216.55
215.00
214.25
214.35
216.60
216.85
214.85
213.55
215.10
217.25
215.00
217.75
214.60
212.75
216.60
216.00
216.75
215.45
215.25
215.50

217.55
217.70
216.90
216.90
217.45
217.45
216.60
219.85
217.85
214.25
217.20
219.35
219.00
216.30
220.55
218.00
215.95
220.25
214.35
217.25
216.00
214.15
214.35
220.30
215.10
213.40
214.25
212.70
216.90
217.00
215.00
215.65
213.30
214.70
216.00
213.85
217.30
215.25
215.00
214.45
215.70
218.00
216.20
214.75
214.05
215.75
215.75
216.00
215.15
215.10
215.75
216.60
216.70
216.00
216.40
216.00

218.50
218.35
213.30
217.90
215.95
218.30
218.75
218.30
216.50
218.40
216.10
218.30
215.30
219.80
217.00
219.25
217.35
218.50
217.95
217.30
217.70
221.15
219.25
220.75
217.00
213.50
215.85
214.70
215.35
215.75
216.80
215.25
215.45
216.95
215.45
215.75
216.00
215.00
214.65
215.25
216.35
214.65
215.00
216.10
215.70
214.00
217.75
213.65
215.65
214.10
220.40
216.00
212.75
214.40
215.55
216.25

218.85
218.30
215.15
218.20
216.35
217.00
217.00
220.35
217.85
215.60
217.85
214.75
221.20
216.50
214.40
216.80
217.20
219.50
217.00
220.65
220.55
214.80
216.50
220.00
215.20
215.25
216.20
216.00
214.85
217.25
214.25
217.15
214.00
215.35
214.25
216.00
216.00
214.00
214.00
214.40
217.25
215.45
215.6
213.25
217.25
215.40
214.00
216.40
220.30
214.00
216.8
214.10
216.00
215.00
216.10
216.00

219.10
217.60
217.65
217.00
216.25
216.30
219.40
217.95
213.90
210.00
214.00
214.90
214.70
219.60
216.85
220.30
217.40
219.50
214.55
217.00
219.35
218.10
217.75
218.75
215.25
215.85
214.00
214.00
215.25
216.30
212.90
216.00
216.35
214.65
214.25
215.00
215.00
215.45
215.30
216.50
216.00
216.95
217.40
216.70
214.70
215.25
215.30
214.75
220.25
215.50
217.25
218.35
216.85
215.85
217.30
216.95

168
Table A1-2:

Batch
1

Batch
2

Batch
3

Batch
4

Sample
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56

Individual measurement for width


Width
100.75
99.85
99.2
99.8
99.3
100.1
99.35
101.1
98.20
98.30
100.05
97.60
99.65
101.75
100.95
102.65
100.65
101.10
100.50
100.00
102.00
101.00
98.75
98.75
100.75
100.10
99.90
100.00
99.20
99.55
97.60
99.85
99.65
100.35
100.00
99.25
100.25
99.50
100.50
100.35
101.10
100.10
98.95
99.25
98.35
100.25
99.75
100.00
99.55
99.20
98.80
100.75
99.85
99.70
100.75
99.70

100.2
101
99.85
100.1
98
100.7
100
99.55
102.50
101.80
98.35
100.00
102.15
99.00
100.50
99.55
98.65
100.85
100.90
99.00
102.30
100.50
98.00
98.80
98.50
98.85
100.55
100.75
99.25
100.55
99.15
99.50
100.45
100.25
98.80
99.00
100.50
99.65
99.25
100.25
100.00
100.55
98.00
97.50
98.30
100.30
99.75
100.25
99.20
98.75
99.95
99.30
100.25
101.00
99.55
100.00

100.3
99.3
99.35
99.8
100.5
99.35
99.9
99.7
100.75
97.70
100.35
101.15
101.35
99.65
101.35
98.80
99.85
101.30
98.65
99.95
98.40
98.45
98.00
99.25
99.40
98.80
99.30
99.25
100.90
100.20
100.00
100.45
98.50
99.75
100.30
98.55
101.30
99.25
99.15
99.75
99.80
100.30
100.95
97.00
97.45
99.70
99.25
98.50
98.45
99.65
99.25
99.65
99.25
99.50
100.25
100.50

98.8
100.4
97.7
99.65
98.25
100.75
99.9
98.85
100.00
99.80
99.75
100.00
100.00
101.25
99.60
101.10
100.85
100.75
100.00
100.25
100.00
102.70
101.25
99.55
100.60
99.10
100.75
99.55
100.25
100.30
100.85
99.75
100.50
100.10
98.25
98.75
98.30
99.65
99.15
99.55
99.30
97.75
98.70
100.20
99.30
97.15
100.25
97.50
98.85
98.00
102.00
99.60
100.15
99.70
100.30
99.10

101.2
99.1
98
99.05
99.4
99
99.45
100.6
100.00
99.25
99.50
98.00
101.45
99.15
97.65
100.10
98.95
100.10
99.25
101.60
102.75
96.80
99.50
102.95
99.10
99.80
100.75
100.75
98.75
101.35
99.90
101.55
98.25
99.50
99.50
98.65
99.45
99.00
99.25
100.15
100.60
100.25
100.45
98.15
100.75
99.25
98.00
100.65
102.50
99.60
99.95
98.60
99.90
97.95
100.50
100.25

100.1
99.1
99.9
99.4
98.3
99
101.2
99.65
98.15
99.00
98.00
96.35
97.85
100.80
98.95
102.20
99.65
101.25
99.25
100.50
100.75
99.40
100.95
100.50
100.05
100.50
97.60
99.10
99.65
100.75
98.80
100.50
99.00
100.00
97.30
98.00
99.10
98.25
100.25
100.95
100.60
99.70
100.75
101.25
98.20
99.90
97.75
98.00
102.85
98.85
100.20
100.50
100.35
99.00
100.25
99.25

169

Table A1-3:

Batch
1

Batch
2

Batch
3

Batch
4

Sample
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56

Individual measurement for height.


Height
67.10
66.75
69.05
69.40
66.20
67.50
67.50
67.50
67.85
67.20
68.10
67.35
67.20
67.95
68.50
68.70
67.00
68.95
69.25
68.75
68.65
69.90
66.75
68.25
67.65
67.15
67.00
67.00
67.15
67.55
66.75
67.25
67.65
67.80
67.20
66.75
67.00
66.60
66.75
67.75
67.30
67.70
67.45
67.60
66.80
67.80
67.80
69.25
66.70
68.25
66.30
68.55
67.75
67.00
67.25
67.25

67.10
67.80
67.20
67.00
66.40
66.75
67.30
67.30
67.65
68.50
67.00
67.65
68.05
66.20
67.75
66.75
68.55
67.25
67.05
67.90
69.10
69.25
68.25
66.10
67.20
67.25
67.20
67.25
67.20
67.95
66.00
67.25
67.50
67.00
67.00
66.25
67.35
67.45
67.00
67.00
68.00
67.55
67.15
66.35
67.50
67.80
65.95
68.25
66.90
66.10
67.00
67.35
68.95
67.35
67.00
67.25

67.75
67.80
67.40
63.95
65.90
67.45
68.20
69.30
71.00
68.00
68.30
69.10
68.25
66.35
68.45
71.00
67.55
68.80
68.00
68.75
66.00
67.95
68.75
67.75
67.00
66.65
66.85
66.50
67.75
68.00
68.30
67.75
66.00
67.75
67.00
68.00
67.60
66.55
66.75
66.50
67.55
68.00
67.50
66.50
66.85
67.90
67.65
67.75
67.00
67.10
67.90
65.25
69.25
67.70
67.75
67.20

66.60
67.90
66.75
66.10
66.60
67.65
68.25
67.75
67.80
69.20
67.50
67.40
68.35
67.95
66.85
69.25
67.50
67.50
68.75
67.75
68.15
68.55
67.75
68.00
67.50
66.25
67.50
67.00
67.45
67.95
67.90
67.00
67.25
67.35
67.00
67.00
66.75
67.15
66.95
67.25
68.35
66.60
66.80
68.25
67.20
66.35
65.00
66.35
67.00
66.85
68.20
66.75
68.80
67.25
67.25
67.80

66.70
66.30
66.50
69.25
66.10
67.00
68.30
68.75
68.00
68.25
69.45
67.90
68.00
66.95
67.60
69.15
66.95
67.85
68.00
68.25
68.55
66.50
68.15
68.75
67.15
67.00
68.00
67.50
67.70
67.25
68.55
68.50
66.85
66.25
66.85
67.25
67.00
66.75
67.00
66.75
68.00
67.50
68.00
66.70
68.50
67.75
66.30
67.50
68.25
66.70
67.60
67.10
67.20
66.60
66.85
67.75

67.25
66.85
67.80
67.45
67.00
66.60
67.90
67.45
66.75
65.80
68.00
66.60
69.20
68.10
66.85
68.00
68.05
69.10
68.00
67.20
68.05
69.25
67.50
68.50
66.60
67.25
66.00
67.25
67.30
67.30
66.70
67.50
68.85
67.20
67.00
67.05
66.55
66.50
67.30
67.25
67.00
67.80
67.55
67.35
66.85
67.00
66.75
66.35
68.25
67.20
68.15
67.05
67.75
67.25
68.50
67.50

A2

RESULTS OF TEST SPECIMENS


FOR DENSITY OF BRICKS

171

Sample 7

Sample 6

Sample 5

Sample 4

Sample 3

Sample 2

Sample 1

Brick
identification
51
27
48
67
32
6
19
22
50
9
36
44
43
64
38
45
62
30
70
66
85
92
41
96
87
43
91
42
81
99
82
88
95
84
98
86
100
97
90
89
2
52
3
1
9
14
6
50
10
7
46
49
55
4
56
57
12
48
54
5
26
69
33
30
35
29
31
59
37
22

Weight (mo)
as received
(gm)
2295
2450
2475
2351
2545
2410
2435
2415
2477
2545
2435
2455
2325
2460
2400
2450
2455
2355
2440
2430
2315
2305
2390
2510
2420
2385
2270
2420
2465
2405
2505
2300
2285
2315
2415
2290
2405
2480
2325
2295
2303
2374
2531
2372
2511
2473
2405
2404
2375
2402
2530
2456
2395
2405
2296
2441
2510
2510
2367
2535
2319
2495
2445
2460
2401
2504
2503
2451
2289
2476

Weight after
2 hrs soaking (m1)
(gm.)
2630
2590
2620
2650
2630
2600
2470
2610
2690
2600
2690
2640
2570
2670
2600
2680
2670
2560
2620
2630
2520
2530
2680
2770
2650
2680
2490
2640
2690
2650
2760
2510
2540
2530
2650
2540
2640
2740
2530
2560
2510
2600
2790
2630
2740
2690
2630
2610
2600
2660
2750
2710
2600
2630
2520
2700
2740
2740
2620
2760
2560
2720
2700
2710
2630
2780
2770
2660
2520
2710

Immersed
weight (m2)
(gm)
1270
1270
1270
1300
1280
1260
1220
1260
1310
1250
1300
1280
1240
1300
1270
1300
1300
1250
1290
1280
1230
1230
1250
1350
1300
1290
1200
1290
1330
1310
1350
1220
1220
1240
1290
1220
1290
1320
1240
1260
1220
1270
1350
1300
1330
1310
1260
1240
1220
1280
1330
1310
1270
1290
1210
1310
1330
1330
1290
1340
1200
1330
1320
1340
1280
1340
1340
1310
1210
1320

Volume (V)
V=(m1-m2)*1000
mm3
1360000
1320000
1350000
1350000
1350000
1340000
1250000
1350000
1380000
1350000
1390000
1360000
1330000
1370000
1330000
1380000
1370000
1310000
1330000
1350000
1290000
1300000
1430000
1420000
1350000
1390000
1290000
1350000
1360000
1340000
1410000
1290000
1320000
1290000
1360000
1320000
1350000
1420000
1290000
1300000
1290000
1330000
1440000
1330000
1410000
1380000
1370000
1370000
1380000
1380000
1420000
1400000
1330000
1340000
1310000
1390000
1410000
1410000
1330000
1420000
1360000
1390000
1380000
1370000
1350000
1440000
1430000
1350000
1310000
1390000

Density (Da)
mo/V*1,000,000
kg/m3
1687.50
1856.06
1833.33
1741.48
1885.19
1798.51
1948.00
1788.89
1794.93
1885.19
1751.80
1805.15
1748.12
1795.62
1804.51
1775.36
1791.97
1797.71
1834.59
1800.00
1794.57
1773.08
1671.33
1767.61
1792.59
1715.83
1759.69
1792.59
1812.50
1794.78
1776.60
1782.95
1731.06
1794.57
1775.74
1734.85
1781.48
1746.48
1802.33
1765.38
1785.27
1784.96
1757.64
1783.46
1780.85
1792.03
1755.47
1754.74
1721.01
1740.58
1781.69
1754.29
1800.75
1794.78
1752.67
1756.12
1780.14
1780.14
1779.70
1785.21
1705.15
1794.96
1771.74
1795.62
1778.52
1738.89
1750.35
1815.56
1747.33
1781.29

Sample 14

Sample 13

Sample 12

Sample 11

Sample 10

Sample 9

Sample 8

172
66
28
34
21
67
32
58
45
68
94
16
10
14
20
21
11
24
18
7
23
15
22
19
17
13
9
8
5
12
3
83
82
79
86
72
88
77
91
94
89
92
84
81
93
90
75
80
95
96
76
50
68
73
53
64
49
52
54
55
61
74
56
57
60
71
51
65
66
58
59

2439
2509
2496
2412
2306
2530
2461
2343
2411
2233
2442
2436
2448
2448
2452
2444
2449
2441
2451
2455
2448
2443
2409
2458
2446
2450
2436
2458
2449
2450
2463
2431
2455
2462
2456
2439
2494
2479
2474
2434
2487
2451
2442
2451
2442
2442
2449
2477
2467
2481
2444
2443
2445
2449
2440
2468
2440
2442
2470
2449
2488
2479
2455
2487
2442
2456
2448
2448
2478
2440

2610
2780
2740
2630
2540
2780
2700
2570
2660
2450
2660
2650
2650
2700
2670
2650
2700
2660
2660
2670
2660
2630
2600
2660
2670
2670
2600
2700
2680
2650
2660
2660
2680
2650
2640
2630
2670
2700
2650
2600
2690
2650
2620
2640
2640
2610
2670
2650
2660
2640
2680
2690
2680
2660
2640
2680
2660
2640
2660
2630
2700
2710
2680
2670
2700
2710
2630
2690
2710
2670

1290
1350
1330
1270
1230
1350
1300
1250
1290
1190
1290
1280
1280
1300
1300
1280
1300
1270
1290
1290
1280
1290
1250
1290
1289
1290
1270
1300
1300
1300
1290
1280
1300
1290
1280
1270
1300
1310
1290
1270
1310
1280
1280
1280
1280
1280
1290
1300
1290
1280
1310
1310
1310
1310
1300
1330
1310
1310
1320
1290
1360
1360
1320
1320
1310
1320
1280
1320
1350
1300

1320000
1430000
1410000
1360000
1310000
1430000
1400000
1320000
1370000
1260000
1370000
1370000
1370000
1400000
1370000
1370000
1400000
1390000
1370000
1380000
1380000
1340000
1350000
1370000
1381000
1380000
1330000
1400000
1380000
1350000
1370000
1380000
1380000
1360000
1360000
1360000
1370000
1390000
1360000
1330000
1380000
1370000
1340000
1360000
1360000
1330000
1380000
1350000
1370000
1360000
1370000
1380000
1370000
1350000
1340000
1350000
1350000
1330000
1340000
1340000
1340000
1350000
1360000
1350000
1390000
1390000
1350000
1370000
1360000
1370000

1847.73
1754.55
1770.21
1773.53
1760.31
1769.23
1757.86
1775.00
1759.85
1772.22
1782.48
1778.10
1786.86
1748.57
1789.78
1783.94
1749.29
1756.12
1789.05
1778.99
1773.91
1823.13
1784.44
1794.16
1771.18
1775.36
1831.58
1755.71
1774.64
1814.81
1797.81
1761.59
1778.99
1810.29
1805.88
1793.38
1820.44
1783.45
1819.12
1830.08
1802.17
1789.05
1822.39
1802.21
1795.59
1836.09
1774.64
1834.81
1800.73
1824.26
1783.94
1770.29
1784.67
1814.07
1820.90
1828.15
1807.41
1836.09
1843.28
1827.61
1856.72
1836.30
1805.15
1842.22
1756.83
1766.91
1813.33
1786.86
1822.06
1781.02

Sample 21

Sample 20

Sample 19

Sample 18

Sample 17

Sample 16

Sample 15

173
14
19
1
24
18
17
13
15
20
16
22
11
6
5
4
3
9
2
7
8
31
47
44
35
36
45
39
40
29
32
46
37
40b
26
41
30
38
27
25
28
54
56
53
50
68
67
52
57
58
61
64
62
70
55
65
59
63
66
69
71
74
84
82
76
85
96
94
91
79
78

2407
2359
2365
2366
2358
2329
2374
2511
2342
2386
2388
2345
2381
2393
2327
2381
2355
2419
2378
2352
2350
2383
2397
2389
2400
2348
2326
2361
2343
2376
2348
2301
2404
2376
2394
2235
2338
2341
2308
2308
2358
2362
2363
2359
2404
2352
2322
2398
2383
2374
2409
2359
2358
2299
2313
2314
2301
2403
2370
2364
2387
2303
2353
2309
2334
2392
2316
2328
2363
2313

2620
2520
2610
2580
2540
2470
2600
2640
2600
2510
2550
2590
2600
2600
2580
2590
2560
2650
2600
2640
2600
2510
2660
2570
2620
2550
2580
2580
2590
2520
2520
2510
2630
2630
2640
2470
2490
2570
2490
2540
2590
2570
2520
2530
2630
2640
2510
2650
2620
2670
2620
2670
2660
2450
2500
2530
2520
2590
2590
2590
2620
2550
2600
2560
2560
2590
2550
2580
2580
2560

1280
1240
1270
1260
1240
1200
1260
1320
1260
1240
1260
1260
1250
1270
1250
1280
1240
1300
1270
1270
1270
1250
1310
1250
1250
1250
1260
1260
1260
1240
1240
1230
1270
1280
1290
1200
1220
1250
1220
1240
1230
1230
1220
1220
1260
1250
1220
1260
1250
1270
1270
1270
1270
1180
1210
1200
1220
1250
1240
1240
1270
1200
1250
1230
1200
1260
1230
1240
1260
1230

1340000
1280000
1340000
1320000
1300000
1270000
1340000
1320000
1340000
1270000
1290000
1330000
1350000
1330000
1330000
1310000
1320000
1350000
1330000
1370000
1330000
1260000
1350000
1320000
1370000
1300000
1320000
1320000
1330000
1280000
1280000
1280000
1360000
1350000
1350000
1270000
1270000
1320000
1270000
1300000
1360000
1340000
1300000
1310000
1370000
1390000
1290000
1390000
1370000
1400000
1350000
1400000
1390000
1270000
1290000
1330000
1300000
1340000
1350000
1350000
1350000
1350000
1350000
1330000
1360000
1330000
1320000
1340000
1320000
1330000

1796.27
1842.97
1764.93
1792.42
1813.85
1833.86
1771.64
1902.27
1747.76
1878.74
1851.16
1763.16
1763.70
1799.25
1749.62
1817.56
1784.09
1791.85
1787.97
1716.79
1766.92
1891.27
1775.56
1809.85
1751.82
1806.15
1762.12
1788.64
1761.65
1856.25
1834.38
1797.66
1767.65
1760.00
1773.33
1759.84
1840.94
1773.48
1817.32
1775.38
1733.82
1762.69
1817.69
1800.76
1754.74
1692.09
1800.00
1725.18
1739.42
1695.71
1784.44
1685.00
1696.40
1810.24
1793.02
1739.85
1770.00
1793.28
1755.56
1751.11
1768.15
1705.93
1742.96
1736.09
1716.18
1798.50
1754.55
1737.31
1790.15
1739.10

Sample 27

Sample 26

Sample 24

Sample 23

Sample 22

174
90
73
93
89
77
80
88
79
81
86
61
60
58
57
56
54
53
52
51
50
40
41
42
43
44
45
46
47
39
20
21
22
23
24
25
26
27
28
29
10
11
12
13
14
15
16
17
18
19

2360
2337
2319
2329
2288
2378
2313
2383
2324
2307
2368
2330
2312
2319
2277
2369
2303
2371
2312
2297
2349
2380
2395
2379
2400
2348
2316
2361
2368
2427
2419
2378
2309
2333
2317
2311
2389
2385
2359
2432
2511
2378
2319
2293
2317
2401
2370
2325
2369

2510
2550
2560
2590
2500
2620
2560
2580
2560
2540
2510
2530
2550
2590
2500
2610
2540
2570
2550
2530
2520
2530
2530
2580
2500
2600
2530
2580
2590
2640
2650
2620
2450
2510
2490
2530
2570
2580
2590
2640
2660
2610
2430
2510
2470
2540
2590
2560
2597

1220
1230
1230
1240
1200
1270
1230
1250
1230
1220
1210
1220
1220
1240
1210
1260
1230
1240
1220
1230
1220
1210
1230
1210
1250
1230
1220
1230
1230
1260
1290
1230
1190
1210
1200
1220
1240
1250
1240
1270
1290
1230
1180
1210
1200
1190
1240
1240
1220

1290000
1320000
1330000
1350000
1300000
1350000
1330000
1330000
1330000
1320000
1300000
1310000
1330000
1350000
1290000
1350000
1310000
1330000
1330000
1300000
1300000
1320000
1300000
1370000
1250000
1370000
1310000
1350000
1360000
1380000
1360000
1390000
1260000
1300000
1290000
1310000
1330000
1330000
1350000
1370000
1370000
1380000
1250000
1300000
1270000
1350000
1350000
1320000
1377000

1829.46
1770.45
1743.61
1725.19
1760.00
1761.48
1739.10
1791.73
1747.37
1747.73
1821.54
1778.63
1738.35
1717.78
1765.12
1754.81
1758.02
1782.71
1738.35
1766.92
1806.92
1803.03
1842.31
1736.50
1920.00
1713.87
1767.94
1748.89
1741.18
1758.70
1778.68
1710.79
1832.54
1794.62
1796.12
1764.12
1796.24
1793.23
1747.41
1775.18
1832.85
1723.19
1855.20
1763.85
1824.41
1778.52
1755.56
1761.36
1720.41

A3

RESULTS OF TESTS SPECIMENS FOR


INITIAL RATE OF SUCTION OF BRICKS

176
Sample 1
Brick
identifica
tion

Dry
mass
(md) gm

Wet
mass
(mw) gm

length
(mm)

16

2445

2485

221.15

100.75

22280.86

18905.86

1.795

2.116

2390

2420

216.50

98.80

21390.20

18015.20

1.403

1.665

11

2415

2450

218.30

99.70

21764.51

18389.51

1.608

1.903

2370

2400

216.05

98.30

21237.72

17862.72

1.413

1.679

Width Immersed Immersed


IRSgross
IRSnet
(mm)
area
area
1000(mw md)/Agross 1000(m2 m1)/Anet
2
2
2
(mm )
(mm )
kg/m .min
kg/m2.min
b
Agross
Anet

2435

2485

221.45

102.25

22643.26

19268.26

2.208

2.595

17

2430

2465

220.05

100.75

22170.04

18795.04

1.579

1.862

19

2440

2490

220.10

100.10

22032.01

18657.01

2.269

2.680

2435

2455

217.55

98.80

21493.94

18118.94

0.930

1.104

2415

2450

217.10

100.00

21710.00

18335.00

1.612

1.909

2410

2435

216.60

99.80

21616.68

18241.68

1.157

1.370

Sample 2
1

2380

2410

216.55

99.55

21557.55

18182.55

1.392

1.650

12

2420

2455

217.95

99.75

21740.51

18365.51

1.610

1.906

10

2485

2515

218.60

99.65

21783.49

18408.49

1.377

1.630

18

2430

2450

216.30

97.95

21186.59

17811.59

0.944

1.123
1.914

2410

2445

217.00

99.80

21656.60

18281.60

1.616

15

2465

2500

216.30

99.15

21446.15

18071.15

1.632

1.937

2460

2490

217.50

99.65

21673.88

18298.88

1.384

1.639

20

2410

2435

217.50

99.15

21565.13

18190.13

1.159

1.374

14

2370

2400

217.75

99.65

21698.79

18323.79

1.383

1.637

13

2370

2410

217.50

99.90

21728.25

18353.25

1.841

2.179

Sample 3
35

2410

2440

217.30

99.20

21556.16

18181.16

1.39

1.650

69

2420

2455

217.35

99.70

21669.80

18294.80

1.62

1.913

63

2435

2490

216.95

99.25

21532.29

18157.29

2.55

3.029

37

2400

2425

216.40

99.25

21477.70

18102.70

1.16

1.381

68

2430

2470

208.50

101.20

21100.20

17725.20

1.90

2.257

40

2410

2445

217.00

99.25

21537.25

18162.25

1.63

1.927

29

2410

2445

217.25

99.65

21648.96

18273.96

1.62

1.915

41

2415

2450

217.10

99.60

21623.16

18248.16

1.62

1.918

71

2440

2485

218.10

100.05

21820.91

18445.91

2.06

2.440

39

2440

2475

216.95

99.35

21553.98

18178.98

1.62

1.925

42

2420

2455

217.10

100.10

21731.71

18356.71

1.61

1.907

82

2505

2542

219.50

101.50

22279.25

18904.25

1.66

1.957

98

2403

2439

218.50

100.35

21926.48

18551.48

1.64

1.941

92

2299

2338

214.10

98.40

21067.44

17692.44

1.85

2.204

89

2288

2336

215.75

99.85

21542.64

18167.64

2.23

2.642

81

2447

2482

218.50

100.5

21959.25

18584.25

1.59

1.883

85

2306

2344

214.80

97.65

20975.22

17600.22

1.81

2.159

41

2364

2403

218.15

101.25

22087.69

18712.69

1.77

2.084

88

2292

2327

214.05

98.00

20976.90

17601.90

1.67

1.988

100

2399

2436

217.50

100.60

21880.50

18505.50

1.69

1.999

Sample 4

177
Sample 5
Brick
identifica
tion

Dry
mass
(md) gm

Wet
mass
(mw) gm

length
(mm)

99

2400

2436

218.00

100.00

21800.00

18425.00

1.65

1.954

91

2265

2302

214.10

97.95

20971.10

17596.10

1.76

2.103

97

2472

2516

218.20

99.70

21754.54

18379.54

2.02

2.394

90

2318

2347

214.15

98.30

21050.95

17675.95

1.38

1.641

84

2306

2340

214.75

93.90

20165.03

16790.03

1.69

2.025

95

2280

2323

214.50

99.05

21246.23

17871.23

2.02

2.406

86

2281

2326

215.50

99.00

21334.50

17959.50

2.11

2.506

87

2414

2452

216.95

100.50

21803.48

18428.48

1.74

2.062

96

2500

2548

220.75

102.30

22582.73

19207.73

2.13

2.499

43

2378

2430

218.60

102.20

22340.92

18965.92

2.33

2.742

Width Immersed Immersed


IRSnet
IRSgross
(mm)
area
area
1000(mw md)/Agross 1000(m2 m1)/Anet
(mm2)
kg/m2.min
kg/m2.min
(mm2)
b
Agross
Anet

Sample 6
20

2444

2484

218.50

100.65

21992.03

18617.03

1.82

2.149

19

2450

2484

219.25

100.02

21929.39

18554.39

1.55

1.832

76

2439

2477

217.10

100.00

21710.00

18335.00

1.75

2.073

15

2410

2440

217.20

98.90

21481.08

18106.08

1.40

1.657

17

2434

2478

218.25

101.00

22043.25

18668.25

2.00

2.357

51

2295

2338

215.70

68.5

14775.45

11400.45

2.91

3.772

61

2540

2575

217.70

100.45

21867.97

18492.97

1.60

1.893

11

2391

2428

217.45

100.05

21755.87

18380.87

1.70

2.013

16

2425

2457

217.30

99.85

21697.41

18322.41

1.47

1.746

78

2415

2447

217.55

99.70

21689.74

18314.74

1.48

1.747

74

2407

2451

216.85

99.50

21576.58

18201.58

2.04

2.417

79

2449

2493

219.75

101.25

22249.69

18874.69

1.98

2.331

80

2466

2510

219.55

101.20

22218.46

18843.46

1.98

2.335

62

2447

2490

218.30

100.80

22004.64

18629.64

1.95

2.308

75

2375

2411

217.00

98.95

21472.15

18097.15

1.68

1.989

73

2264

2310

214.90

99.5

21382.55

18007.55

2.15

2.554

72

2300

2341

214.50

98.50

21128.25

17753.25

1.94

2.309

77

2401

2438

217.00

100.25

21754.25

18379.25

1.70

2.013

71

2295

2334

217.05

99.80

21661.59

18286.59

1.80

2.133

60

2446

2485

217.45

99.60

21658.02

18283.02

1.80

2.133

Sample 7

Sample 8
49

2464

2508

217.60

100.60

21890.56

18515.56

2.01

2.376

2483

2533

219.70

101.20

22233.64

18858.64

2.25

2.651

10

2304

2357

219.40

100.95

22148.43

18773.43

2.39

2.823

46

2489

2535

220.60

102.10

22523.26

19148.26

2.04

2.402

2435

2462

216.40

98.80

21380.32

18005.32

1.26

1.500

56

2328

2359

216.10

98.9

21372.29

17997.29

1.45

1.722

52

2370

2406

217.15

99.75

21660.71

18285.71

1.66

1.969

2304

2333

215.65

97.50

21025.88

17650.88

1.38

1.643

14

2456

2498

218.75

101.05

22104.69

18729.69

1.90

2.242

2502

2554

220.75

102.40

22604.80

19229.80

2.30

2.704

178
Sample 9
Width Immersed Immersed
IRSnet
IRSgross
(mm)
area
area
1000(mw md)/Agross 1000(m2 m1)/Anet
(mm2)
kg/m2.min
kg/m2.min
(mm2)
b
Agross
Anet

Dry
mass
(md) gm

Wet
mass
(mw) gm

length
(mm)

2420

2461

217.30

99.75

21675.68

18300.68

1.89

2.240

2430

2457

216.75

99.40

21544.95

18169.95

1.25

1.486

50

2358

2401

218.00

99.00

21582.00

18207.00

1.99

2.362

2497

2534

218.95

100.95

22103.00

18728.00

1.67

1.976

Brick
identifica
tion

2372

2406

217.30

99.65

21653.95

18278.95

1.57

1.860

57

2483

2518

217.75

100.95

21981.86

18606.86

1.59

1.881

55

2412

2443

215.25

100.00

21525.00

18150.00

1.44

1.708

54

2412

2436

216.30

100.00

21630.00

18255.00

1.11

1.315

48

2506

2550

221.00

101.85

22508.85

19133.85

1.95

2.300

12

2493

2536

220.75

101.35

22373.01

18998.01

1.92

2.263

Sample 10
58

2446

2482

217.60

101.75

22140.80

18765.80

1.63

1.918

94

2240

2263

210.00

98.25

20632.50

17257.50

1.11

1.333

35

2398

2437

217.75

100.00

21775.00

18400.00

1.79

2.120

29

2503

2562

220.75

102.50

22626.88

19251.88

2.61

3.065

33

2445

2482

219.25

100.50

22034.63

18659.63

1.68

1.983

34

2495

2534

219.75

101.50

22304.63

18929.63

1.75

2.060

21

2411

2444

219.90

99.25

21825.08

18450.08

1.51

1.789

69

2496

2530

219.50

101.20

22213.40

18838.40

1.53

1.805

26

2318

2359

217.95

99.70

21729.62

18354.62

1.89

2.234

37

2289

2328

214.25

98.35

21071.49

17696.49

1.85

2.204

30

2458

2502

218.35

101.00

22053.35

18678.35

2.00

2.356

68

2412

2452

218.30

98.65

21535.30

18160.30

1.86

2.203

32

2543

2587

221.25

103.05

22799.81

19424.81

1.93

2.265

31

2502

2549

220.50

103.95

22920.98

19545.98

2.05

2.405

28

2509

2559

220.80

102.55

22643.04

19268.04

2.21

2.595

66

2439

2455

214.75

98.85

21228.04

17853.04

0.75

0.896

67

2306

2342

214.40

98.20

21054.08

17679.08

1.71

2.036

22

2477

2515

220.75

99.60

21986.70

18611.70

1.73

2.042

45

2333

2369

214.65

97.75

20982.04

17607.04

1.72

2.045

59

2451

2474

216.00

99.65

21524.40

18149.40

1.07

1.267

Sample 11

Sample 12
22

2443

2473

213.50

99.00

21136.50

17761.50

1.42

1.689

18

2443

2486

215.50

100.55

21668.53

18293.53

1.98

2.351

17

2459

2484

214.95

98.80

21237.06

17862.06

1.18

1.400

12

2449

2493

216.00

100.50

21708.00

18333.00

2.03

2.400

24

2449

2494

217.25

101.00

21942.25

18567.25

2.05

2.424

2449

2478

214.30

100.00

21430.00

18055.00

1.35

1.606

10

2436

2479

215.25

100.75

21686.44

18311.44

1.98

2.348

2452

2486

215.00

100.00

21500.00

18125.00

1.58

1.876

19

2409

2440

213.25

99.25

21165.06

17790.06

1.46

1.743

20

2449

2500

217.00

101.50

22025.50

18650.50

2.32

2.735

179
Sample 13
Width Immersed Immersed
IRSnet
IRSgross
(mm)
area
area
1000(mw md)/Agross 1000(m2 m1)/Anet
(mm2)
kg/m2.min
kg/m2.min
(mm2)
b
Agross
Anet

Dry
mass
(md) gm

Wet
mass
(mw) gm

length
(mm)

15

2448

2485

215.40

100.00

21540.00

18165.00

1.72

23

2456

2498

216.00

100.45

21697.20

18322.20

1.94

2.292

2452

2483

215.00

99.50

21392.50

18017.50

1.45

1.721

14

2448

2482

215.10

99.25

21348.68

17973.68

1.59

1.892

13

2447

2492

215.70

100.75

21731.78

18356.78

2.07

2.451

16

2442

2482

215.00

100.25

21553.75

18178.75

1.86

2.200

21

2452

2488

215.00

99.35

21360.25

17985.25

1.69

2.002

2436

2461

214.35

97.95

20995.58

17620.58

1.19

1.419

11

2444

2474

214.75

98.50

21152.88

17777.88

1.42

1.687

2458

2510

216.25

100.75

21787.19

18412.19

2.39

2.824

38

2467

2511

217.25

100.25

21779.31

18404.31

2.02

2.391

37

2444

2479

215.00

99.50

21392.50

18017.50

1.64

1.943

32

2466

2511

216.75

100.60

21805.05

18430.05

2.06

2.442

41

2437

2475

214.90

99.50

21382.55

18007.55

1.78

2.110

27

2454

2482

214.65

99.25

21304.01

17929.01

1.31

1.562

47

2452

2493

216.25

100.75

21787.19

18412.19

1.88

2.227

45

2455

2489

215.25

99.65

21449.66

18074.66

1.59

1.881

34

2465

2507

217.10

101.25

21981.38

18606.38

1.91

2.257

26

2454

2488

214.80

99.65

21404.82

18029.82

1.59

1.886

28

2468

2522

215.75

100.40

21661.30

18286.30

2.49

2.953

36

2463

2492

214.80

99.75

21426.30

18051.30

1.35

1.607

42

2524

2555

214.65

99.65

21389.87

18014.87

1.45

1.721

48

2478

2533

217.30

101.55

22066.82

18691.82

2.49

2.942

43

2428

2453

215.35

98.00

21104.30

17729.30

1.18

1.410

25

2469

2513

216.00

100.75

21762.00

18387.00

2.02

2.393

44

2493

2534

217.00

100.75

21862.75

18487.75

1.88

2.218

31

2448

2470

212.65

98.55

20956.66

17581.66

1.05

1.251

39

2480

2512

215.90

99.50

21482.05

18107.05

1.49

1.767

29

2458

2501

215.50

100.00

21550.00

18175.00

2.00

2.366

40

2458

2492

215.00

98.80

21242.00

17867.00

1.60

1.903
0.168

Brick
identifica
tion

2.037

Sample 14

Sample 15

Sample 16
94

2476

2479

215.50

98.55

21237.53

17862.53

0.14

60

2488

2510

215.25

99.40

21395.85

18020.85

1.03

1.221

79

2456

2494

216.00

100.00

21600.00

18225.00

1.76

2.085

76

2482

2505

215.75

99.00

21359.25

17984.25

1.08

1.279

75

2443

2467

214.50

97.60

20935.20

17560.20

1.15

1.367

86

2463

2494

214.30

100.00

21430.00

18055.00

1.45

1.717

96

2467

2496

216.00

98.55

21286.80

17911.80

1.36

1.619

58

2479

2511

216.00

99.70

21535.20

18160.20

1.49

1.762

65

2450

2471

215.50

98.25

21172.88

17797.88

0.99

1.180

71

2444

2483

216.35

100.50

21743.18

18368.18

1.79

2.123

180
Sample 17
Width Immersed Immersed
IRSnet
IRSgross
(mm)
area
area
1000(mw md)/Agross 1000(m2 m1)/Anet
(mm2)
kg/m2.min
kg/m2.min
(mm2)
b
Agross
Anet

Dry
mass
(md) gm

Wet
mass
(mw) gm

length
(mm)

51

2457

2501

216.25

100.95

21830.44

18455.44

2.02

88

2439

2465

215.50

99.00

21334.50

17959.50

1.22

1.448

83

2462

2495

215.45

100.50

21652.73

18277.73

1.52

1.805

53

2450

2480

214.50

99.80

21407.10

18032.10

1.40

1.664

57

2457

2488

215.30

100.25

21583.83

18208.83

1.44

1.702

92

2488

2519

214.95

100.00

21495.00

18120.00

1.44

1.711

56

2480

2503

215.00

99.10

21306.50

17931.50

1.08

1.283

72

2458

2489

214.55

100.25

21508.64

18133.64

1.44

1.710

55

2472

2493

214.25

99.25

21264.31

17889.31

0.99

1.174

74

2489

2504

214.55

98.90

21219.00

17844.00

0.71

0.841

Brick
identifica
tion

2.384

Sample 18
49

2468

2492

214.10

100.25

21463.53

18088.53

1.12

1.327

91

2480

2512

216.85

100.45

21782.58

18407.58

1.47

1.738

89

2433

2457

213.70

98.45

21038.77

17663.77

1.14

1.359

61

2450

2471

216.00

98.30

21232.80

17857.80

0.99

1.176

80

2451

2491

216.00

100.50

21708.00

18333.00

1.84

2.182

95

2477

2499

215.25

98.00

21094.50

17719.50

1.04

1.242

82

2432

2474

216.40

100.25

21694.10

18319.10

1.94

2.293

77

2494

2530

215.80

99.50

21472.10

18097.10

1.68

1.989

54

2443

2468

213.95

99.15

21213.14

17838.14

1.18

1.401

84

2453

2490

215.00

100.25

21553.75

18178.75

1.72

2.035

93

2452

2492

215.35

99.75

21481.16

18106.16

1.86

2.209

66

2449

2489

215.50

100.55

21668.53

18293.53

1.85

2.187

59

2437

2474

215.20

99.70

21455.44

18080.44

1.72

2.046

73

2446

2481

215.50

100.25

21603.88

18228.88

1.62

1.920

68

2443

2484

216.20

100.45

21717.29

18342.29

1.89

2.235

50

2445

2484

215.25

100.00

21525.00

18150.00

1.81

2.149

64

2442

2468

214.15

99.00

21200.85

17825.85

1.23

1.459

90

2441

2476

214.50

99.50

21342.75

17967.75

1.64

1.948

52

2440

2472

214.65

99.90

21443.54

18068.54

1.49

1.771

81

2442

2465

213.75

97.90

20926.13

17551.13

1.10

1.310

Sample 19

Sample 20
11

2340

2385

216.00

100.00

21600.00

18225.00

2.08

2.469

32

2345

2357

214.60

97.25

20869.85

17494.85

0.57

0.686

18

2359

2382

215.00

98.75

21231.25

17856.25

1.08

1.288

31

2351

2393

216.25

99.75

21570.94

18195.94

1.95

2.308

2363

2401

216.10

99.35

21469.54

18094.54

1.77

2.100

2396

2431

217.25

100.60

21855.35

18480.35

1.60

1.894

2380

2422

212.80

100.25

21333.20

17958.20

1.97

2.339

38

2338

2352

214.00

97.55

20875.70

17500.70

0.67

0.800

17

2328

2352

214.00

97.55

20875.70

17500.70

1.15

1.371

29

2344

2384

215.85

99.65

21509.45

18134.45

1.86

2.206

181
Sample 21
Width Immersed Immersed
IRSnet
IRSgross
(mm)
area
area
1000(mw md)/Agross 1000(m2 m1)/Anet
(mm2)
kg/m2.min
kg/m2.min
(mm2)
b
Agross
Anet

Dry
mass
(md) gm

Wet
mass
(mw) gm

length
(mm)

13

2355

2392

216.25

100.00

21625.00

18250.00

1.71

25

2307

2326

214.00

98.50

21079.00

17704.00

0.90

1.073

39

2326

2368

215.55

100.10

21576.56

18201.56

1.95

2.307

44

2374

2421

217.85

102.00

22220.70

18845.70

2.12

2.494

22

2358

2378

215.00

98.80

21242.00

17867.00

0.94

1.119

26

2377

2423

216.80

100.00

21680.00

18305.00

2.12

2.513

19

2358

2374

215.00

98.00

21070.00

17695.00

0.76

0.904

41

2371

2411

217.50

100.30

21815.25

18440.25

1.83

2.169

30

2236

2269

215.25

100.15

21557.29

18182.29

1.53

1.815

36

2400

2437

218.50

100.75

22013.88

18638.88

1.68

1.985

Brick
identifica
tion

2.027

Sample 22
40

2347

2388

215.55

99.45

21436.45

18061.45

1.91

2.270

2358

2403

216.80

100.25

21734.20

18359.20

2.07

2.451

37

2300

2334

214.75

98.25

21099.19

17724.19

1.61

1.918

20

2334

2381

217.00

101.00

21917.00

18542.00

2.14

2.535

40

2400

2433

217.75

100.50

21883.88

18508.88

1.51

1.783

35

2383

2410

216.25

98.50

21300.63

17925.63

1.27

1.506

47

2363

2371

214.25

97.35

20857.24

17482.24

0.38

0.458

45

2336

2367

215.25

98.00

21094.50

17719.50

1.47

1.749

16

2361

2373

214.45

97.00

20801.65

17426.65

0.58

0.689

2328

2387

216.25

100.50

21733.13

18358.13

2.71

3.214

24

2334

2372

216.26

99.50

21517.87

18142.87

1.77

2.094

2357

2403

216.90

101.60

22037.04

18662.04

2.09

2.465

27

2341

2379

216.00

99.95

21589.20

18214.20

1.76

2.086

2352

2391

216.85

100.50

21793.43

18418.43

1.79

2.117

15

2482

2499

213.75

98.00

20947.50

17572.50

0.81

0.967

2325

2359

216.00

99.95

21589.20

18214.20

1.57

1.867

14

2366

2422

217.00

101.50

22025.50

18650.50

2.54

3.003

46

2344

2359

214.00

97.25

20811.50

17436.50

0.72

0.860

Sample 23

2354

2404

216.00

99.75

21546.00

18171.00

2.32

2.752

28

2304

2336

216.00

98.00

21168.00

17793.00

1.51

1.798

Sample 24
61

2373

2430

220.70

102.50

22621.75

19246.75

2.52

2.962

62

2359

2428

220.65

102.60

22638.69

19263.69

3.05

3.582

96

2393

2426

216.15

99.15

21431.27

18056.27

1.54

1.828

79

2384

2419

215.75

99.75

21521.06

18146.06

1.63

1.929

76

2310

2360

216.15

100.55

21733.88

18358.88

2.30

2.723

73

2338

2384

216.25

99.25

21462.81

18087.81

2.14

2.543

86

2308

2359

217.25

99.40

21594.65

18219.65

2.36

2.799

70

2356

2412

220.75

102.45

22615.84

19240.84

2.48

2.910

71

2351

2369

216.55

99.90

21633.35

18258.35

0.83

0.986

55

2298

2321

213.90

98.75

21122.63

17747.63

1.09

1.296

182
Sample 25
Width Immersed Immersed
IRSnet
IRSgross
(mm)
area
area
1000(mw md)/Agross 1000(m2 m1)/Anet
(mm2)
kg/m2.min
kg/m2.min
(mm2)
b
Agross
Anet

Dry
mass
(md) gm

Wet
mass
(mw) gm

length
(mm)

78

2313

2362

216.30

100.25

21684.08

18309.08

2.26

53

2363

2380

215.00

98.75

21231.25

17856.25

0.80

0.952

80

2379

2427

217.25

101.25

21996.56

18621.56

2.18

2.578

89

2330

2384

217.05

100.50

21813.53

18438.53

2.48

2.929

88

2313

2360

216.25

100.50

21733.13

18358.13

2.16

2.560

77

2288

2319

215.50

99.50

21442.25

18067.25

1.45

1.716

94

2316

2365

215.90

99.75

21536.03

18161.03

2.28

2.698

85

2332

2370

217.30

99.35

21588.76

18213.76

1.76

2.086

74

2377

2392

217.00

99.50

21591.50

18216.50

0.69

0.823

82

2353

2402

216.85

100.25

21739.21

18364.21

2.25

2.668

52

2321

2347

215.25

98.25

21148.31

17773.31

1.23

1.463

50

2342

2346

214.55

98.75

21186.81

17811.81

0.19

0.225

64

2398

2411

216.50

99.15

21465.98

18090.98

0.61

0.719

84

2299

2347

217.75

100.00

21775.00

18400.00

2.20

2.609

56

2357

2375

215.75

99.75

21521.06

18146.06

0.84

0.992

93

2318

2368

216.90

100.10

21711.69

18336.69

2.30

2.727

67

2351

2407

220.50

102.00

22491.00

19116.00

2.49

2.929

90

2361

2380

215.75

97.85

21111.14

17736.14

0.90

1.071

91

2329

2380

215.85

100.30

21649.76

18274.76

2.36

2.791

59

2302

2321

216.90

99.65

21614.09

18239.09

0.88

1.042

57

2393

2416

217.50

100.45

21847.88

18472.88

1.05

1.245

81

2323

2372

216.30

100.25

21684.08

18309.08

2.26

2.676

69

2365

2384

216.00

99.25

21438.00

18063.00

0.89

1.052

66

2387

2392

215.65

99.10

21370.92

17995.92

0.23

0.278

68

2399

2418

216.25

99.40

21495.25

18120.25

0.88

1.049

79

2363

2403

216.60

99.25

21497.55

18122.55

1.86

2.207

65

2312

2339

214.00

98.00

20972.00

17597.00

1.29

1.534

58

2377

2399

217.00

99.90

21678.30

18303.30

1.01

1.202

54

2346

2370

216.95

100.00

21695.00

18320.00

1.11

1.310

63

2301

2348

215.00

99.35

21360.25

17985.25

2.20

2.613

Brick
identifica
tion

2.676

Sample 26

Sample 27

A4

RESULTS OF TESTS SPECIMENS FOR


WATER ABSORPTION OF BRICKS

184

Sample 1
Brick

Dry mass

identification

W1(gm)

2415

2670

2460

Saturated A (Water
mass
absorption)%
W2 (gm) A= 100( W2W1)/W1

Sample 2
Brick

Dry mass

Saturated
mass

A (Water
absorption)%
A= 100( W2W1)/W1

identification

W1(gm)

10.559

2390

2590

8.37

2710

10.163

2435

2760

13.35

W2 (gm)

2380

2640

10.924

11

2415

2665

10.35

13

2370

2670

12.658

2435

2650

8.83

2410

2640

9.544

15

2465

2700

9.53

14

2370

2645

11.603

17

2430

2720

11.93
10.54

2370

2625

10.759

12

2420

2675

20

2410

2665

10.581

18

2430

2625

8.02

19

2440

2775

13.730

2410

2690

11.62

10

2485

2745

10.463

2445

2740

12.07

39

2440

2695

10.45

82

2505

2795

11.58

69

2420

2685

10.95

95

2280

2567

12.59

35

2410

2680

11.20

85

2306

2553

10.71

41

2415

2695

11.59

84

2306

2555

10.80

37

2400

2655

10.63

92

2299

2565

11.57

29

2410

2685

11.41

98

2403

2692

12.03

40

2410

2670

10.79

81

2447

2712

10.83

68

2430

2745

12.96

100

2399

2669

11.25

63

2435

2735

12.32

89

2288

2594

13.37

71

2440

2710

11.07

2420

2676

10.58

99

2400

2684

11.83

19

2450

2715

10.82

86

2281

2576

12.93

71

2295

2596

13.12

97

2472

2774

12.22

79

2449

2752

12.37

43

2378

2706

13.79

72

2300

2586

12.43

91

2265

2517

11.13

61

2540

2816

10.87

90

2318

2559

10.40

60

2446

2727

11.49

96

2500

2810

12.40

15

2410

2652

10.04

87

2414

2684

11.18

62

2448

2740

11.93

41

2364

2658

12.44

78

2415

2687

11.26

88

2292

2542

10.91

2376

2642

11.20

11

2386

2673

12.03

2483

2790

12.36

77

2401

2676

11.45

55

2412

2662

10.36

16

2425

2688

10.85

2430

2676

10.12

76

2439

2722

11.60

10

2304

2589

12.37

20

2444

2731

11.74

14

2456

2740

11.56

17

2434

2734

12.33

56

2328

2576

10.65

74

2407

2701

12.21

12

2493

2792

11.99

80

2466

2786

12.98

48

2506

2795

11.53

73

2263

2556

12.95

2497

2803

12.25

51

2296

2570

11.93

54

2412

2664

10.45

Sample 3

Sample 5

Sample 7

16
Sample 4

42
Sample 6

75
Sample 8

185
Sample 9
Brick

Dry mass

Sample 10
Brick

Dry mass

identification

W1(gm)
W2 (gm)

A (Water
absorption)%
A= 100( W2W1)/W1

identification

W1(gm)

49

2464

2757

11.89

22

2464

46

2489

2760

12.01

2805

12.70

58

2489

2747

10.37

2304

2562

11.20

37

2304

2572

11.63

2435

2670

9.65

66

2422

2665

10.03

52

2370

2644

11.56

67

2307

2577

11.70

2420

2709

11.94

26

2322

2619

12.79

57

2483

2759

11.12

59

2450

2702

10.29

2502

2821

12.75

45

2382

2606

9.40

50

2358

2668

13.15

28

2518

2824

12.15

2372

2657

12.02

2384

2707

13.55

29

2503

2832

13.14

2447

2738

11.89

21

2411

2687

11.45

2452

2729

11.30

31

2502

2819

12.67

12

2449

2744

12.05

34

2495

2797

12.10

20

2449

2760

12.70

94

2240

2487

11.03

2449

2706

10.49

30

2458

2759

12.25

2452

2710

10.52

33

2445

2742

12.15

19

2409

2659

10.38

69

2496

2774

11.14

24

2449

2761

12.74

35

2398

2680

11.76

11

2444

2699

10.43

32

2543

2836

11.52

2436

2711

11.29

22

2443

2684

9.86

34

2465

2770

12.37

2436

2654

8.95

41

2437

2709

11.16

21

2452

2722

11.01

32

2466

2767

12.21

15

2448

2727

11.40

27

2454

2713

10.55

23

2456

2745

11.77

38

2467

2766

12.12

17

2459

2710

10.21

48

2478

2796

12.83

16

2442

2724

11.55

45

2455

2728

11.12

18

2443

2735

11.95

40

2458

2720

10.66

2458

2759

12.25

29

2458

2736

11.31

14

2448

2712

10.78

2444

2713

11.01

47

2452

2743

11.87

75

2482

2672

7.66

44

2493

2783

11.63

86

2463

2717

10.31

42

2524

2789

10.50

91

2480

2761

11.33

43

2428

2678

10.30

71

2444

2738

12.03

36

2463

2736

11.08

65

2450

2687

9.67

25

2469

2760

11.79

79

2456

2735

11.36

31

2448

2672

9.15

80

2451

2734

11.55

26

2454

2720

10.84

96

2467

2721

10.30

28

2468

2757

11.71

83

2462

2729

10.84

39

2480

2728

10.00

58

2479

2723

9.84

Saturated A (Water
mass
absorption)%
W2 (gm) A= 100( W2W1)/W1

Sample 11

Sample 13

Sample 15

68
Sample 12
13

10
Sample 14

37
Sample 16

Saturated
mass

186
Sample 17
Brick

Dry mass

Sample 18
Brick

Dry mass

identification

W1(gm)
W2 (gm)

A (Water
absorption)%
A= 100( W2W1)/W1

identification

W1(gm)

74

2489

2709

8.84

88

2439

61

2450

2692

10.37

2675

9.18

93

2452

2703

76

10.24

2482

2712

9.27

84

2453

2724

11.05

60

2488

2707

8.80

92

2488

2744

10.29

49

2468

2718

10.13

66

2449

2731

11.51

55

2472

2709

9.59

68

2443

2734

11.91

95

2477

2706

9.25

73

2446

2725

11.41

89

2433

2655

9.12

59

2437

2715

11.41

94

2476

2711

9.49

81

2442

2673

9.46

72

2458

2713

10.37

2450

2709

10.57

57

2457

2731

11.15

19

2358

2560

8.57

52

2440

2704

10.82

44

2374

2697

13.61

51

2457

2754

12.09

30

2236

2496

11.63

56

2480

2712

9.35

41

2371

2665

12.40

77

2494

2740

9.86

36

2400

2665

11.04

54

2443

2690

10.11

2363

2634

11.47

64

2442

2692

10.24

38

2338

2536

8.47

90

2441

2696

10.45

2396

2675

11.64

82

2432

2728

12.17

25

2307

2537

9.97

50

2445

2724

11.41

2344

2618

11.69
10.32

Saturated A (Water
mass
absorption)%
W2 (gm) A= 100( W2W1)/W1

Sample 19

Sample 21

53
Sample 20

29
Sample 22

Saturated
mass

2380

2680

12.61

69

2365

2609

18

2374

2579

8.64

66

2387

2617

9.64

13

2355

2641

12.14

58

2377

2649

11.44

31

2351

2627

11.74

63

2301

2556

11.08

22

2358

2586

9.67

79

2363

2614

10.62

11

2341

2624

12.09

61

2373

2705

13.99

26

2377

2663

12.03

70

2356

2670

13.33

32

2345

2547

8.61

71

2351

2612

11.10

39

2326

2600

11.78

65

2312

2540

9.86

17

2328

2520

8.25

2393

2633

10.03

55

2298

2512

9.31

57

2393

2687

12.29

78

2313

2617

13.14

56

2357

2615

10.95

73

2338

2618

11.98

93

2318

2620

13.03

79

2384

2631

10.36

85

2332

2626

12.61

86

2308

2602

12.74

84

2299

2609

13.48

76

2310

2609

12.94

94

2316

2604

12.44

53

2363

2583

9.31

82

2353

2653

12.75

81

2323

2619

12.74

67

2351

2689

14.38

62

2308

2620

13.52

54

2346

2630

12.11

68

2399

2671

11.34

74

2377

2660

11.91

Sample 23

96
Sample 24

187
Sample 25
Brick

Sample 26
Brick
identification

W1(gm)
W2 (gm)

A (Water
absorption)%
A= 100( W2W1)/W1

12.71

20

2334

2607

11.70

2572

8.94

35

2383

2572

7.93

2342

2566

9.56

15

2482

2566

9.34

59

2302

2571

11.69

45

2336

2571

10.06

80

2379

2673

12.36

37

2300

2673

11.65

89

2330

2642

13.39

2357

2642

12.09

52

2321

2569

10.69

14

2366

2569

8.58

77

2288

2557

11.76

27

2341

2557

9.23

91

2329

2624

12.67

47

2363

2624

11.05

64

2398

2665

11.13

2358

2665

13.02

2352

2647

12.54

Dry mass

Saturated A (Water
mass
absorption)%
W2 (gm) A= 100( W2W1)/W1

identification

W1(gm)

88

2313

2607

90

2361

50

Sample 27
9

2325

2608

12.17

24

2334

2614

12.00

16

2361

2548

7.92

2328

2623

12.67

2354

2646

12.40

40

2400

2672

11.33

46

2344

2551

8.83

28

2304

2568

11.46

41

2347

2623

11.76

Dry mass

Saturated
mass

A5

RESULTS OF TESTS SPECIMENS FOR


COMPRESSIVE STRENGTH OF BRICKS

189

Brick
Identific
ation

FACING BRICK BED FACE


Dimension 1 (mm)
Area 1
Dimension 2 (mm)
mm2
Length
Width
Length
Width

Area 2
mm2

Sample 1
Smaller Max load Compressive
area
Kn
strength
mm2
N/mm2

18

216.10

98.50

21285.85

216.20

98.50

21295.70 21285.85

894.10

42.00

12

212.85

100.00

21285.00

217.85

99.90

21763.22 21285.00

988.80

46.46

14

217.75

99.35

21633.46

217.90

99.65

21713.74 21633.46

944.90

43.68

10

218.95

99.95

21884.05

218.75

99.65

21798.44 21798.44

1036.90

47.57

17

219.50

100.55

22070.73

219.40

100.75

22104.55 22070.73

840.90

38.10

11

217.25

99.40

21594.65

217.10

99.85

21677.44 21594.65

820.90

38.01

16

219.50

100.25

22004.88

220.10

100.20

22054.02 22004.88

776.90

35.31

217.20

99.80

21676.56

217.45

99.65

21668.89 21668.89

913.90

42.18

215.20

97.60

21003.52

215.55

98.20

21167.01 21003.52

694.90

33.08

216.60

98.70

21378.42

216.30

98.65

21338.00 21338.00

844.90

39.60

71

217.05

100.50

21813.53

218.15

100.75

21978.61 21813.53

1064.30

48.79

63

219.25

101.00

22144.25

219.50

101.10

22191.45 22144.25

957.30

43.23

39

217.30

99.50

21621.35

217.35

99.45

21615.46 21615.46

964.30

44.61

68

219.90

101.45

22308.86

220.50

101.35

22347.68 22308.86

977.00

43.79

69

217.50

99.85

21717.38

217.05

100.05

21715.85 21715.85

1091.90

50.28

35

217.55

99.10

21559.21

217.70

99.00

21552.30 21552.30

1106.00

51.32

40

216.95

99.25

21532.29

217.00

99.15

21515.55 21515.55

1113.00

51.73

41

217.50

99.55

21652.13

217.10

99.50

21601.45 21601.45

1187.00

54.95

29

217.00

100.00

21700.00

217.20

99.85

21687.42 21687.42

965.00

44.50

37

217.00

99.40

21569.80

216.45

99.25

21482.66 21482.66

1159.90

53.99

Sample 2

Sample 3
96

220.85

102.25

22581.91

221.25

102.25

22622.81 22581.91

803.40

35.58

91

214.00

97.95

20961.30

214.00

97.65

20897.10 20897.10

874.10

41.83

90

214.25

98.35

21071.49

214.20

98.40

21077.28 21071.49

942.30

44.72

43

219.20

101.95

22347.44

219.20

101.80

22314.56 22314.56

797.90

35.76

41

218.20

101.30

22103.66

218.00

101.30

22083.40 22083.40

684.80

31.01

88

214.35

97.95

20995.58

214.40

97.15

20828.96 20828.96

947.80

45.50

87

217.20

100.45

21817.74

217.75

100.25

21829.44 21817.74

885.90

40.60

82

219.90

101.70

22363.83

220.20

101.50

22350.30 22350.30

793.90

35.52

42

217.45

100.15

21777.62

217.00

100.10

21721.70 21721.70

930.90

42.86

89

215.95

99.75

21541.01

215.50

99.65

21474.58 21474.58

776.90

36.18

Sample 4
51

216.00

98.60

21297.60

216.10

98.80

21350.68 21297.60

777.90

36.53

80

219.50

101.10

22191.45

219.55

101.45

22273.35 22191.45

912.90

41.14

15

215.25

98.75

21255.94

214.30

98.50

21108.55 21108.55

1020.90

48.36

62

218.60

101.75

22242.55

219.40

101.88

22352.47 22242.55

855.80

38.48

78

218.20

101.70

22190.94

218.65

101.20

22127.38 22127.38

676.70

30.58

11

215.35

97.66

21031.08

214.50

97.59

20933.06 20933.06

614.70

29.37

73

217.80

101.35

22074.03

217.35

100.15

21767.60 21767.60

589.60

27.09

20

219.00

101.85

22305.15

220.01

101.45

22320.01 22305.15

853.70

38.27

75

217.95

100.65

21936.67

217.14

100.55

21833.43 21833.43

777.60

35.62

72

215.55

99.95

21544.22

215.75

99.95

21564.21 21544.22

639.60

29.69

190

Brick
Identific
ation

Dimension 1 (mm)

Area 1
mm2

Sample 5
Dimension 2 (mm)

Length

Width

Length

Width

216.85

98.95

21457.31

216.10

98.80

Area 2
mm2

Smaller Max load Compressive


area
Kn
strength
mm2
N/mm2

21350.68 21350.68

1203.00

56.34

221.30

102.65

22716.45

221.00

102.40

22630.40 22630.40

928.00

41.01

57

217.70

101.75

22150.98

217.80

101.65

22139.37 22139.37

1276.90

57.68

48

221.20

101.45

22440.74

221.30

101.50

22461.95 22440.74

938.00

41.80

12

220.55

101.35

22352.74

220.30

101.40

22338.42 22338.42

761.90

34.11

55

215.30

100.00

21530.00

215.25

99.98

21520.70 21520.70

1000.90

46.51

217.25

99.50

21616.38

217.35

99.54

21635.02 21616.38

1123.80

51.99

217.20

99.65

21643.98

217.30

99.55

21632.22 21632.22

1275.80

58.98

10

219.45

100.95

22153.48

219.40

100.55

22060.67 22060.67

882.70

40.01

219.50

101.35

22246.33

219.35

101.50

22264.03 22246.33

935.80

42.07

32

220.00

102.95

22649.00

221.00

103.75

22928.75 22649.00

903.90

39.91

31

220.65

102.25

22561.46

220.60

102.10

22523.26 22523.26

879.00

39.03

69

219.35

101.15

22187.25

219.10

101.30

22194.83 22187.25

1015.90

45.79

35

217.70

100.00

21770.00

217.70

99.90

21748.23 21748.23

1055.90

48.55

34

220.25

101.75

22410.44

219.85

101.75

22369.74 22369.74

904.00

40.41

33

219.25

100.95

22133.29

219.30

101.25

22204.13 22133.29

958.00

43.28

29

221.25

102.50

22678.13

221.00

102.75

22707.75 22678.13

877.90

38.71

21

220.00

99.25

21835.00

219.85

99.30

21831.11 21831.11

1066.00

48.83

94

210.00

98.35

20653.50

209.80

98.70

20707.26 20653.50

1126.90

54.56

68

218.65

98.70

21580.76

218.45

98.50

21517.33 21517.33

1238.90

57.58

Sample 6

Sample 7
21

215.50

99.35

21409.93

215.50

99.55

21453.03 21409.93

1322.10

61.75

18

215.60

100.45

21657.02

215.75

100.50

21682.88 21657.02

1280.10

59.11

13

215.75

100.75

21736.81

215.95

100.75

21756.96 21736.81

1190.10

54.75

214.00

98.75

21132.50

214.00

97.50

20865.00 20865.00

1512.10

72.47

15

215.75

100.00

21575.00

215.25

100.00

21525.00 21525.00

1292.10

60.03

23

215.75

100.50

21682.88

216.00

100.50

21708.00 21682.88

1291.10

59.54

22

213.65

99.25

21204.76

213.75

99.15

21193.31 21193.31

1348.10

63.61

17

215.00

99.00

21285.00

215.00

98.75

21231.25 21231.25

1404.10

66.13

10

215.25

100.00

21525.00

215.40

100.25

21593.85 21525.00

1007.10

46.79

216.50

100.70

21801.55

216.25

100.75

21787.19 21787.19

967.10

44.39

44

217.00

100.85

21884.45

216.95

100.75

21857.71 21857.71

993.70

45.46

47

215.95

100.75

21756.96

216.25

100.75

21787.19 21756.96

1112.70

51.14

28

215.85

100.25

21638.96

215.80

100.25

21633.95 21633.95

1087.70

50.28

29

215.50

100.25

21603.88

215.45

100.35

21620.41 21603.88

1077.80

49.89

26

215.25

99.75

21471.19

214.75

99.80

21432.05 21432.05

617.80

28.83

37

215.00

99.40

21371.00

215.10

99.50

21402.45 21371.00

1183.80

55.39

39

215.75

99.25

21413.19

214.95

99.45

21376.78 21376.78

1208.80

56.55

40

214.85

98.90

21248.67

215.00

98.80

21242.00 21242.00

1127.80

53.09

31

213.00

98.75

21033.75

213.00

98.55

20991.15 20991.15

1435.30

68.38

45

215.25

99.75

21471.19

215.25

99.90

21503.48 21471.19

1142.30

53.20

Sample 8

191
Sample 9
Brick
Identific
ation

Dimension 1 (mm)
Length

Area 1
mm2

Width

Dimension 2 (mm)
Length

Width

Area 2
mm2

Smaller Max load Compressive


area
Kn
strength
mm2
N/mm2

43

215.45

98.00

21114.10

215.50

97.90

21097.45 21097.45

1128.30

53.48

38

217.30

100.25

21784.33

216.75

100.35

21750.86 21750.86

916.20

42.12

25

216.25

101.00

21841.25

216.25

100.65

21765.56 21765.56

1169.80

53.75

48

217.35

101.30

22017.56

217.45

101.60

22092.92 22017.56

1066.80

48.45

42

214.30

99.75

21376.43

214.50

99.75

21396.38 21376.43

1020.30

47.73

32

216.75

100.50

21783.38

216.75

100.50

21783.38 21783.38

1098.30

50.42

36

216.70

99.85

21637.50

215.00

99.85

21467.75 21467.75

1089.30

50.74

27

214.90

99.40

21361.06

214.75

99.35

21335.41 21335.41

1161.90

54.46

41

214.95

99.55

21398.27

214.90

99.65

21414.79 21398.27

1299.80

60.74

34

217.30

101.50

22055.95

217.25

101.35

22018.29 22018.29

1049.80

47.68

50

215.25

99.80

21481.95

215.35

99.75

21481.16 21481.16

1035.60

48.21

54

214.00

99.00

21186.00

213.95

99.20

21223.84 21186.00

1105.60

52.19

77

215.95

99.60

21508.62

215.90

99.75

21536.03 21508.62

1126.60

52.38

82

216.50

100.40

21736.60

216.65

100.25

21719.16 21719.16

881.60

40.59

64

214.15

99.25

21254.39

214.25

99.10

21232.18 21232.18

1177.50

55.46

56

215.25

99.00

21309.75

215.00

99.15

21317.25 21309.75

1139.50

53.47

51

216.45

100.75

21807.34

215.25

101.00

21740.25 21740.25

1091.50

50.21

52

215.00

99.80

21457.00

214.75

99.85

21442.79 21442.79

1007.50

46.99

57

215.65

100.25

21618.91

215.45

100.15

21577.32 21577.32

1077.50

49.94

59

215.25

99.75

21471.19

215.15

99.70

21450.46 21450.46

1043.50

48.65

39

215.50

100.00

21550.00

215.45

100.00

21545.00 21545.00

977.00

45.35

13

216.15

99.80

21571.77

216.00

100.40

21686.40 21571.77

931.00

43.16

31

216.45

99.95

21634.18

216.25

100.00

21625.00 21625.00

922.00

42.64

Sample 10

Sample 11

18

215.00

98.85

21252.75

215.35

98.30

21168.91 21168.91

1132.00

53.47

217.90

100.25

21844.48

218.25

100.50

21934.13 21844.48

838.00

38.36

17

214.00

97.50

20865.00

214.25

97.50

20889.38 20865.00

842.00

40.35

29

215.75

99.75

21521.06

215.75

99.75

21521.06 21521.06

886.00

41.17

25

214.65

98.25

21089.36

214.00

98.25

21025.50 21025.50

1025.00

48.75

32

215.35

97.75

21050.46

214.40

97.70

20946.88 20946.88

928.00

44.30

26

216.90

100.00

21690.00

216.75

100.20

21718.35 21690.00

945.00

43.57

69

216.10

99.15

21426.32

216.25

99.15

21441.19 21426.32

1109.00

51.76

62

221.00

102.60

22674.60

220.75

102.75

22682.06 22674.60

797.00

35.15

65

214.25

98.00

20996.50

214.25

97.50

20889.38 20889.38

998.00

47.78

76

216.30

100.50

21738.15

216.25

100.50

21733.13 21733.13

869.00

39.99

86

217.55

99.30

21602.72

217.50

99.40

21619.50 21602.72

904.00

41.85

96

216.35

99.75

21580.91

216.00

99.25

21438.00 21438.00

971.00

45.29

81

216.35

99.75

21580.91

216.45

99.75

21590.89 21580.91

914.00

42.35

71

216.50

99.85

21617.53

216.45

99.40

21515.13 21515.13

1270.00

59.03

70

220.75

102.45

22615.84

220.75

102.50

22626.88 22615.84

769.00

34.00

61

220.50

102.45

22590.23

220.80

102.50

22632.00 22590.23

815.00

36.08

Sample 12

192

Brick
Identific
ation

Dimension 1 (mm)

Area 1
mm2

Sample 13
Dimension 2 (mm)

Area 2
mm2

Smaller Max load Compressive


area
Kn
strength
mm2
N/mm2

Length

Width

Length

Width

64

216.50

99.15

21465.98

216.25

99.10

21430.38 21430.38

1374.00

64.11

74

217.20

99.40

21589.68

217.00

99.50

21591.50 21589.68

1056.00

48.91

88

216.35

100.45

21732.36

216.35

100.55

21753.99 21732.36

889.00

40.91

90

215.25

97.80

21051.45

215.65

97.50

21025.88 21025.88

1216.00

57.83

54

216.75

100.00

21675.00

216.75

100.05

21685.84 21675.00

1109.00

51.16

84

217.70

100.25

21824.43

218.05

99.90

21783.20 21783.20

838.00

38.47

67

220.60

102.30

22567.38

220.55

102.00

22496.10 22496.10

881.00

39.16

85

217.35

99.50

21626.33

217.75

99.50

21666.13 21626.33

924.00

42.73

82

216.70

100.10

21691.67

216.95

100.00

21695.00 21691.67

856.00

39.46

77

215.25

99.75

21471.19

215.30

99.75

21476.18 21471.19

790.00

36.79

Sample 14
40

215.75

99.25

21413.19

216.10

99.30

21458.73 21413.19

844.00

39.41

46

214.35

97.75

20952.71

214.00

97.40

20843.60 20843.60

865.00

41.50

28

215.95

93.00

20083.35

216.00

98.00

21168.00 20083.35

1007.00

50.14

217.10

100.25

21764.28

217.00

100.45

21797.65 21764.28

905.00

41.58

216.30

100.70

21781.41

216.25

100.55

21743.94 21743.94

866.00

39.83

216.70

100.00

21670.00

216.50

100.00

21650.00 21650.00

891.00

41.15

16

215.00

97.00

20855.00

214.65

97.00

20821.05 20821.05

1179.00

56.63

47

214.25

97.45

20878.66

214.15

97.35

20847.50 20847.50

1013.00

48.59

27

215.90

99.70

21525.23

216.25

99.75

21570.94 21525.23

936.00

43.48

14

217.10

101.10

21948.81

217.00

101.30

21982.10 21948.81

892.00

40.64

FACING BRICK STRETCHER FACE

Sample 1

27

218.00

67.50

14715.00

214.90

67.45

14495.01 14495.01

570.00

39.32

38

217.00

67.30

14604.10

216.50

66.75

14451.38 14451.38

569.00

39.37

30

217.55

64.50

14031.98

217.30

64.50

14015.85 14015.85

488.00

34.82

217.25

67.75

14718.69

217.00

68.00

14756.00 14718.69

573.00

38.93

60

217.10

68.35

14838.79

217.15

68.00

14766.20 14766.20

581.00

39.35

43

217.95

66.90

14580.86

217.50

67.00

14572.50 14572.50

540.00

37.06

66

216.85

67.30

14594.01

216.85

68.00

14745.80 14594.01

538.00

36.86

25

218.00

67.10

14627.80

217.65

66.00

14364.90 14364.90

529.00

36.83

23

216.50

67.90

14700.35

216.50

68.00

14722.00 14700.35

544.00

37.01

44

217.70

67.75

14749.18

217.00

67.75

14701.75 14701.75

490.00

33.33

Sample 2
74

217.00

68.80

14929.60

217.55

70.00

15228.50 14929.60

504.90

33.82

76

217.25

68.75

14935.94

217.00

68.00

14756.00 14756.00

394.80

26.76

77

217.30

68.75

14939.38

217.25

68.70

14925.08 14925.08

499.80

33.49

61

217.80

69.25

15082.65

217.95

69.50

15147.53 15082.65

491.80

32.61

79

220.65

67.20

14827.68

220.75

67.50

14900.63 14827.68

427.90

28.86

97

218.30

68.80

15019.04

218.55

70.00

15298.50 15019.04

569.90

37.95

92

214.85

68.00

14609.80

214.25

67.75

14515.44 14515.44

455.90

31.41

100

217.10

67.85

14730.24

217.25

67.70

14707.83 14707.83

410.00

27.88

98

218.50

68.00

14858.00

218.95

67.50

14779.13 14779.13

456.00

30.85

95

219.75

68.60

15074.85

219.75

68.20

14986.95 14986.95

404.00

26.96

193

Brick
Identific
ation

FACING BRICK STRETCHER FACE


Dimension 1 (mm)
Area 1
Dimension 2 (mm) Area 2
mm2
mm2
Length
Width
Length
Width

Sample 3
Smaller Max load Compressive
area
Kn
strength
mm2
N/mm2

37

214.50

68.55

14703.98

214.25

68.00

14569.00 14569.00

513.90

35.27

66

214.30

66.20

14186.66

214.25

66.80

14311.90 14186.66

535.00

37.71

59

216.00

68.00

14688.00

216.00

67.55

14590.80 14590.80

634.00

43.45

30

218.25

69.50

15168.38

217.75

69.65

15166.29 15166.29

516.00

34.02

28

220.55

69.00

15217.95

220.75

68.25

15066.19 14482.86

497.80

34.37

52

217.00

66.85

14506.45

217.15

66.55

14451.33 14451.33

429.80

29.74

46

220.65

68.05

15015.23

220.45

68.00

14990.60 14990.60

336.60

22.45

219.25

69.25

15183.06

219.35

69.30

15200.96 15183.06

522.80

34.43

216.50

66.95

14494.68

216.55

66.88

14482.86 14482.86

506.80

34.99

214.25

66.35

14215.49

214.20

66.40

14222.88 14215.49

503.80

35.44

215.00

67.20

14448.00

215.00

67.00

14405.00 14405.00

495.10

34.37

16

215.10

67.20

14454.72

214.75

67.00

14388.25 14388.25

514.10

35.73

12

216.00

67.25

14526.00

215.70

66.95

14441.12 14441.12

479.10

33.18

14

215.00

67.25

14458.75

214.75

66.70

14323.83 14323.83

576.20

40.23

11

215.00

67.35

14480.25

214.40

67.00

14364.80 14364.80

496.20

34.54

37

214.50

68.55

14703.98

214.25

68.00

14569.00 14569.00

513.90

35.27

66

214.30

66.20

14186.66

214.25

66.80

14311.90 14186.66

535.00

37.71

59

216.00

68.00

14688.00

216.00

67.55

14590.80 14590.80

634.00

43.45

30

218.25

69.50

15168.38

217.75

69.65

15166.29 15166.29

516.00

34.02

28

220.55

69.00

15217.95

220.75

68.25

15066.19 14482.86

397.80

27.47

49

213.90

67.00

14331.30

214.00

62.75

13428.50 13428.50

549.60

40.93

60

215.25

67.00

14421.75

215.00

66.20

14233.00 14233.00

704.60

49.50

55

214.00

67.00

14338.00

213.80

67.00

14324.60 14324.60

639.50

44.64

76

215.25

66.75

14367.94

215.40

66.85

14399.49 14367.94

651.50

45.34

72

214.00

67.00

14338.00

214.15

67.00

14348.05 14338.00

557.50

38.88

95

214.75

67.00

14388.25

215.00

67.50

14512.50 14388.25

644.50

44.79

58

215.75

67.00

14455.25

215.90

67.25

14519.28 14455.25

635.50

43.96

94

215.25

67.00

14421.75

215.25

67.00

14421.75 14421.75

513.50

35.61

89

213.25

66.00

14074.50

213.25

66.25

14127.81 14074.50

774.50

55.03

61

215.25

67.00

14421.75

214.85

67.00

14394.95 14394.95

618.50

42.97

90

213.85

67.00

14327.95

214.00

66.75

14284.50 14284.50

541.50

37.91

68

216.00

67.45

14569.20

215.75

67.70

14606.28 14569.20

412.50

28.31

73

215.15

67.25

14468.84

215.35

67.45

14525.36 14468.84

487.50

33.69

92

214.55

67.75

14535.76

214.85

67.55

14513.12 14513.12

551.50

38.00

53

214.50

66.90

14350.05

214.25

66.85

14322.61 14322.61

487.50

34.04

81

213.95

66.50

14227.68

214.00

66.90

14316.60 14227.68

680.50

47.83

84

215.00

67.00

14405.00

215.30

67.30

14489.69 14405.00

539.50

37.45

93

215.25

66.75

14367.94

214.90

66.25

14237.13 14237.13

539.50

37.89

66

215.20

67.00

14418.40

215.25

67.45

14518.61 14418.40

506.50

35.13

88

215.40

66.90

14410.26

215.25

67.00

14421.75 14421.75

531.50

36.85

Sample 4

Sample 5

Sample 6

194

Brick
Identific
ation

FACING BRICK STRETCHER FACE


Dimension 1 (mm)
Area 1
Dimension 2 (mm) Area 2
mm2
mm2
Length
Width
Length
Width

Sample 7
Smaller Max load Compressive
area
Kn
strength
mm2
N/mm2

11

215.55

67.50

14549.63

215.50

67.65

14578.58 14549.63

323.00

22.20

217.00

67.75

14701.75

217.25

68.00

14773.00 14701.75

460.00

31.29

22

215.00

67.00

14405.00

214.85

66.75

14341.24 14341.24

653.00

45.53

19

214.70

67.20

14427.84

214.55

66.75

14321.21 14321.21

541.00

37.78

44

217.95

68.25

14875.09

217.55

68.25

14847.79 14847.79

285.00

19.19

30

214.85

63.10

13557.04

214.90

65.75

14129.68 13557.04

407.00

30.02

41

217.40

67.85

14750.59

217.45

67.75

14732.24 14732.24

481.00

32.65

38

214.00

66.35

14198.90

214.55

66.75

14321.21 14198.90

227.00

15.99

36

218.50

69.00

15076.50

217.80

68.00

14810.40 14810.40

411.00

27.75

216.00

67.80

14644.80

216.10

67.95

14684.00 14644.80

351.00

23.97

93

216.50

67.70

14657.05

216.50

67.45

14602.93 14602.93

422.00

28.90

89

217.30

67.80

14732.94

217.65

67.75

14745.79 14732.94

350.00

23.76

56

215.75

66.75

14401.31

215.45

66.75

14381.29 14381.29

381.00

26.49

57

217.20

68.90

14965.08

217.25

68.80

14946.80 14946.80

382.00

25.56

80

217.00

67.95

14745.15

217.35

68.55

14899.34 14745.15

373.00

25.30

94

216.25

67.45

14586.06

216.25

67.50

14596.88 14586.06

407.00

27.90

91

215.55

67.25

14495.74

215.95

68.00

14684.60 14495.74

430.00

29.66

52

214.95

67.00

14401.65

215.25

66.55

14324.89 14324.89

443.00

30.93

59

216.55

65.00

14075.75

216.65

66.25

14353.06 14075.75

435.00

30.90

50

214.35

66.00

14147.10

214.00

66.25

14177.50 14147.10

486.00

34.35

70

98.50

67.30

6629.05

62

100.35

67.75

45

67.25

100.10

Sample 8

FACING BRICK HEADER FACE

Sample 1

98.75

66.95

6611.31

6611.31

62.60

9.47

6798.71

99.50

67.00

6666.50

6666.50

62.20

9.33

6731.73

100.50

67.30

6763.65

6731.73

60.30

8.96

99.15

66.75

6618.26

100.25

67.25

6741.81

6618.26

60.80

9.19

16

99.55

66.85

6654.92

99.25

67.50

6699.38

6654.92

53.00

7.96

36

100.00

67.05

6705.00

100.95

67.00

6763.65

6705.00

56.30

8.40

64

100.65

67.30

6773.75

99.75

67.45

6728.14

6728.14

53.30

7.92

24

100.31

66.80

6700.71

100.20

66.50

6663.30

6679.68

61.20

9.16

99.80

66.65

6651.67

99.50

66.45

6611.78

6611.78

57.90

8.76

19

100.00

66.95

6695.00

99.95

67.10

6706.65

6695.00

61.00

9.11

17

101.10

68.95

6970.85

101.55

6948.05

6948.05

18.50

2.66

Sample 2
68.42

60

99.65

68.05

6781.18

99.91

68.00

6793.88

6781.18

27.00

3.98

16

100.85

67.25

6782.16

100.65

67.00

6743.55

6743.55

23.60

3.50

19

100.10

67.85

6791.79

100.15

67.77

6787.17

6787.17

26.70

3.93

71

100.00

68.75

6875.00

99.95

68.30

6826.59

6826.59

15.60

2.29

84

98.55

67.95

6696.47

97.25

67.55

6569.24

6569.24

29.70

4.52

81

100.15

67.30

6740.10

100.25

67.85

6801.96

6740.10

24.30

3.61

99

100.10

68.20

6826.82

99.85

68.25

6814.76

6814.76

20.80

3.05

85

96.45

67.70

6529.67

98.55

68.05

6706.33

6529.67

27.90

4.27

86

98.60

67.95

6699.87

99.00

68.30

6761.70

6699.87

28.40

4.24

195

Brick
Identific
ation

FACING BRICK HEADER FACE


Dimension 1 (mm)
Area 1
Dimension 2 (mm)
mm2

Area 2
mm2

Sample 3
Smaller Max load Compressive
area
Kn
strength
mm2
N/mm2

Length

Width

Length

Width

45

98.15

69.10

6782.17

98.20

69.10

6785.62

6782.17

34.10

5.03

67

97.50

67.75

6605.63

97.35

67.75

6595.46

6595.46

28.00

4.25

58

101.00

67.75

6842.75

101.35

67.75

6866.46

6842.75

31.70

4.63

22

100.75

68.75

6926.56

99.30

68.75

6826.88

6826.88

14.90

2.18

26

99.50

68.80

6845.60

99.90

68.80

6873.12

6845.60

31.60

4.62

14

100.80

68.10

6864.48

100.95

68.42

6907.00

6864.48

47.30

6.89

56

99.00

66.20

6553.80

99.15

66.15

6558.77

6553.80

30.60

4.67

49

100.50

67.75

6808.88

100.65

67.70

6814.01

6808.14

31.80

4.67

97.65

67.60

6601.14

97.80

67.68

6619.10

6601.14

35.90

5.44

50

98.80

71.00

7014.80

98.90

70.95

7016.96

7014.80

17.60

2.51

24

100.50

67.25

6758.63

100.25

67.30

6746.83

6746.83

36.50

5.41

19

100.35

67.10

6733.49

100.20

67.25

6738.45

6733.49

36.10

5.36

20

101.25

67.00

6783.75

100.25

66.85

6701.71

6701.71

34.40

5.13

99.50

66.70

6636.65

99.25

66.60

6610.05

6610.05

41.00

6.20

98.80

66.50

6570.20

99.30

66.75

6628.28

6570.20

26.70

4.06

45

98.15

69.10

6782.17

98.20

69.10

6785.62

6782.17

34.10

5.03

67

97.50

67.75

6605.63

97.35

67.75

6595.46

6595.46

28.00

4.25

58

101.00

67.75

6842.75

101.35

67.75

6866.46

6842.75

31.70

4.63

22

100.75

68.75

6926.56

99.30

68.75

6826.88

6826.88

34.90

5.11

26

99.50

68.80

6845.60

99.90

68.80

6873.12

6845.60

31.60

4.62

83

99.70

67.30

6709.81

99.75

6658.31

6658.31

70.80

10.63

Sample 4

Sample 5
66.75

96

99.50

67.25

6691.38

99.00

67.25

6657.75

6657.75

37.30

5.60

79

100.25

67.00

6716.75

100.00

67.00

6700.00

6700.00

28.70

4.28

65

99.25

66.25

6575.31

98.55

66.60

6563.43

6563.43

47.10

7.18

71

100.75

67.00

6750.25

100.25

67.00

6716.75

6716.75

37.00

5.51

86

99.50

67.25

6691.38

99.80

67.60

6746.48

6691.38

76.40

11.42

74

98.80

66.75

6594.90

99.10

66.50

6590.15

6590.15

50.30

7.63

80

100.00

67.25

6725.00

100.25

66.65

6681.66

6681.66

44.50

6.66

91

100.80

67.00

6753.60

100.25

67.30

6746.83

6746.83

40.80

6.05

75

98.30

66.10

6497.63

97.75

66.25

6475.94

6475.94

49.00

7.57

Sample 6
1

98.55

67.95

6696.47

97.25

67.55

6569.24

6569.24

29.60

4.51

100.15

67.30

6740.10

100.25

67.85

6801.96

6740.10

37.90

5.62

100.10

68.20

6826.82

99.85

68.25

6814.76

6814.76

26.80

3.93

96.45

67.70

6529.67

98.55

68.05

6706.33

6529.67

30.80

4.72

100.22

67.55

6769.86

100.34

67.95

6818.10

6769.86

28.60

4.22

98.73

68.10

6723.51

99.96

68.55

6852.26

6723.51

33.60

5.00

99.55

69.10

6878.91

98.99

68.56

6786.75

6786.75

31.70

4.67

100.33

68.44

6866.59

98.95

67.99

6727.61

6727.61

21.20

3.15

97.10

69.99

6796.03

100.22

67.89

6803.94

6796.03

20.20

2.97

10

98.60

67.95

6699.87

99.00

68.30

6761.70

6699.87

46.00

6.87

196

Brick
Identific
ation

FACING BRICK HEADER FACE


Dimension 1 (mm)
Area 1
Dimension 2 (mm)
mm2
Length
Width
Length
Width

Area 2
mm2

Sample 7
Smaller Max load Compressive
area
Kn
strength
mm2
N/mm2

79

99.45

66.25

6588.56

99.95

66.90

6686.66

6588.56

36.00

5.46

80

99.50

66.30

6596.85

99.80

66.70

6596.85

6596.85

15.80

2.40

58

99.75

67.50

6733.13

99.75

67.40

6723.15

6723.15

21.30

3.17

73

99.75

66.70

6653.33

99.65

66.55

6631.71

6631.71

24.80

3.74

78

100.05

67.00

6703.35

100.45

66.85

6715.08

6703.35

37.23

5.55

66

98.25

67.00

6582.75

99.10

67.00

6639.70

6582.75

20.80

3.16

63

99.70

66.30

6610.11

99.45

66.25

6588.56

6588.56

28.00

4.25

53

98.50

66.55

6555.18

98.80

66.75

6594.90

6555.18

37.00

5.64

55

97.25

64.75

6296.94

99.25

66.55

6605.09

6296.94

4.70

0.75

69

99.25

67.00

6649.75

99.50

67.50

6716.25

6649.75

19.60

2.95

40

100.60

67.75

6815.65

100.25

68.00

6817.00

6815.65

57.00

8.36

45

97.75

66.85

6534.59

97.50

66.75

6508.13

6508.13

58.00

8.91

15

98.25

66.20

6504.15

98.50

66.10

6510.85

6504.15

36.00

5.53

35

99.00

67.00

6633.00

99.35

67.25

6681.29

6633.00

40.00

6.03

Sample 8

37

98.50

67.00

6599.50

97.00

66.10

6411.70

6411.70

47.00

7.33

100.50

66.75

6708.38

100.35

66.85

6708.40

6708.38

43.00

6.41

20

100.00

66.85

6685.00

100.55

66.85

6721.77

6685.00

41.00

6.13

99.65

66.90

6666.59

99.95

67.00

6696.65

6666.59

46.00

6.90

99.90

66.45

6638.36

99.35

66.50

6606.78

6606.78

32.00

4.84

24

99.70

66.75

6654.98

99.45

66.50

6613.43

6613.43

38.00

5.75

197

Brick
Identific
ation
-

COMMON BRICKS BED FACE


Dimension 1 (mm)
Area 1
Dimension 2 (mm)
mm2
Length
Width
Length
Width

Area 2
mm2

Sample 1
Smaller
area
mm2

Max load Compressive


Kn
strength
N/mm2

216.10

99.25

21447.93

216.20

99.50

21511.90

21447.93

825.30

38.48

215.90

97.45

21039.46

215.50

97.45

21000.48

21000.48

829.30

39.49

217.50

100.05

21760.88

217.45

100.25

21799.36

21760.88

631.30

29.01

218.55

99.15

21669.23

219.05

99.95

21894.05

21669.23

866.30

39.98

217.85

98.95

21556.26

217.70

101.45

22085.67

21556.26

671.30

31.14

217.25

100.80

21898.80

217.25

101.20

21985.70

21898.80

791.30

36.13

217.95

99.65

21718.72

217.70

100.25

21824.43

21718.72

546.30

25.15

219.20

101.25

22194.00

219.25

100.40

22012.70

22012.70

866.30

39.35

218.80

100.85

22065.98

219.45

101.20

22208.34

22065.98

613.30

27.79

219.00

100.65

22042.35

219.50

101.50

22279.25

22042.35

750.30

34.04

214.75

100

21475

215.7

99.75

21516.075

21475

850

39.58

214.25

100.75

21585.688

213.85

100.00

21385

21385

813

38.02

215.50

100.8

21722.4

215.55

100.75 21716.663

21716.66

783

36.06

214.55

100.25

21508.638

215.5

99.45

21431.475

21431.48

582

27.16

214.90

100.75

21651.175

215.10

100.70

21660.57

21651.18

855

39.49

216.55

100.75

21817.413

216.25

100.95 21830.438

21817.41

730

33.46

216.00

100.25

21654.00

216.45

101.00

21654

543

25.08

216.25

100.5

21733.125

216.15

100.15 21647.423

21647.42

786

36.31

21861.45

216.20

100.75

21782.15

216.25

101.45 21938.563

21782.15

745

34.20

215.70

100.4

21656.28

215.5

99.90

21528.45

21528.45

695

32.28

216.20

99.05

21414.61

216.20

21479.47

21414.61

830.00

38.76

215.90

97.00

20942.30

215.50

97.45

21000.48

20942.30

790.00

37.72

216.50

100.25

21704.13

217.45

100.30

21810.24

21704.13

636.00

29.30

217.75

99.25

21611.69

219.05

99.95

21894.05

21611.69

840.00

38.87

217.85

98.35

21425.55

217.70

101.25

22042.13

21425.55

567.00

26.46

217.35

100.20

21778.47

217.25

101.20

21985.70

21778.47

794.00

36.46

218.20

99.15

21634.53

217.70

100.25

21824.43

21634.53

543.00

25.10

218.75

101.05

22104.69

219.25

100.40

22012.70

22012.70

833.00

37.84

218.80

100.85

22065.98

219.45

101.20

22208.34

22065.98

614.00

27.83

219.00

100.65

22042.35

219.50

101.50

22279.25

22042.35

749.00

33.98

216.00

98.60

21297.60

216.00

98.60

21297.60

21297.60

607.90

28.54

219.50

101.10

22191.45

219.50

101.35

22246.33

22191.45

573.90

25.86

214.25

98.35

21071.49

214.20

98.40

21077.28

21071.49

473.90

22.49

Sample 3
99.35

Sample 4

219.60

101.95

22388.22

219.20

101.80

22314.56

22314.56

562.90

25.23

218.20

101.30

22103.66

218.45

101.30

22128.99

22103.66

501.90

22.71

214.35

97.00

20791.95

214.40

97.55

20914.72

20791.95

512.90

24.67

217.20

101.45

22034.94

217.25

100.25

21779.31

21779.31

462.90

21.25

219.80

101.65

22342.67

220.15

101.55

22356.23

22342.67

544.90

24.39

217.45

100.45

21842.85

217.34

100.15

21766.60

21766.60

437.80

20.11

215.95

99.95

21584.20

215.35

99.75

21481.16

21481.16

475.90

22.15

198

Brick
Identific
ation

COMMON BRICKS BED FACE


Dimension 1 (mm)
Area 1
Dimension 2 (mm)
mm2
Length
Width
Length
Width

219.25

98.00

220.55

218.20

Area 2
mm2

Sample 5
Smaller
area
mm2

Max load Compressive


Kn
strength
N/mm2

21486.50

219.20

101.20

22183.04

21486.50

452.10

21.04

100.65

22198.36

220.85

100.95

22294.81

22198.36

604.10

27.21

99.65

21743.63

218.40

100.15

21872.76

21743.63

851.10

39.14

220.25

100.25

22080.06

220.75

101.00

22295.75

21798.44

849.20

38.96

221.25

102.95

22777.69

221.25

103.75

22954.69

22070.73

744.20

33.72

221.40

101.60

22479.00

221.60

101.95

22592.12

21594.65

711.20

32.93

218.95

100.75

22306.05

219.30

100.85

22116.41

22004.88

779.20

35.41

220.00

100.95

22103.00

219.80

100.95

22188.81

21668.89

687.20

31.71

218.20

100.70

22154.00

218.45

100.45

21943.30

21003.52

824.20

39.24

219.30

100.00

21820.00

219.25

100.25

21979.81

21338.00

857.20

40.17

216.35

97.60

21115.76

216.00

98.00

21168.00

21115.76

434.90

20.60

218.50

100.10

21871.85

218.75

101.25

22148.44

21871.85

573.90

26.24

214.20

98.25

21045.15

214.25

98.45

21092.91

21045.15

400.80

19.04

219.55

101.95

22383.12

219.25

100.80

22100.40

22100.40

560.00

25.34

217.20

100.30

21785.16

218.40

101.30

22123.92

21785.16

502.80

23.08

214.05

97.35

20837.77

214.25

97.75

20942.94

20837.77

512.90

24.61

216.20

101.25

21890.25

217.30

100.25

21784.33

21784.33

450.90

20.70

218.80

100.65

22022.22

219.50

101.45

22022.22

14999.66

542.90

36.19

218.45

101.45

22161.75

217.00

100.55

21819.35

21819.35

400.80

18.37

215.05

99.95

21494.25

215.35

99.65

21459.63

21459.63

465.90

21.71

216.35

97.60

21115.76

216.00

98.00

21168.00

21115.76

625.03

29.60

218.50

100.10

21871.85

218.75

101.25

22148.44

21871.85

828.94

37.90

214.20

98.25

21045.15

214.25

98.45

21092.91

21045.15

564.01

26.80

219.55

101.95

22383.12

219.25

100.80

22100.40

22100.40

680.69

30.80

217.20

100.30

21785.16

218.40

101.30

22123.92

21785.16

623.05

28.60

214.05

97.35

20837.77

214.25

97.75

20942.94

20837.77

700.15

33.60

216.20

101.25

21890.25

217.30

100.25

21784.33

21784.33

690.56

31.70

218.80

100.65

22022.22

219.50

101.45

22268.28

22022.22

466.87

21.20

218.45

101.45

22161.75

217.00

100.55

21819.35

21819.35

440.75

20.20

215.05

99.95

21494.25

215.35

99.65

21459.63

21459.63

987.14

46.00

Sample 6

Sample 7

Sample 8
-

214.55

97.75

20972.26

215.00

98.25

21123.75

20972.26

872.50

41.60

213.45

96.80

20661.96

213.30

96.80

20647.44

20647.44

883.60

42.79

213.45

96.80

20661.96

213.30

97.45

20786.09

20661.96

751.60

36.38

216.00

98.70

21319.20

215.50

98.60

21248.30

21248.30

815.50

38.38

214.85

98.50

21162.73

215.00

98.50

21177.50

21162.73

876.60

41.42

215.00

98.00

21070.00

214.95

97.50

20957.63

20957.63

1017.60

48.56

212.25

98.00

20800.50

212.25

97.75

20747.44

20747.44

1032.60

49.77

217.00

99.75

21645.75

217.00

99.00

21483.00

21483.00

849.60

39.55

214.00

98.00

20972.00

214.95

97.75

21011.36

20972.00

913.60

43.56

212.45

96.25

20448.31

212.25

96.00

20376.00

20376.00

832.60

40.86

199

Brick
Identific
ation

COMMON BRICKS BED FACE


Dimension 1 (mm)
Area 1
Dimension 2 (mm)
mm2
Length
Width
Length
Width

Area 2
mm2

Sample 9
Smaller
area
mm2

Max load Compressive


Kn
strength
N/mm2

216.36

96.75

20932.83

216.25

98.25

21246.56

20932.83

713.50

34.09

213.25

96.80

20642.60

213.30

96.80

20647.44

20642.60

793.60

38.44

210.30

97.80

20567.34

210.30

97.45

20493.74

20493.74

751.60

36.67

215.45

98.70

21264.92

215.50

98.60

21248.30

21248.30

758.50

35.70

214.85

98.50

21162.73

215.00

98.50

21177.50

21162.73

856.60

40.48

212.55

98.30

20893.67

214.95

97.50

20957.63

20893.67

988.60

47.32

212.25

98.00

20800.50

212.25

97.75

20747.44

20747.44

1015.60

48.95

217.00

99.75

21645.75

217.00

99.00

21483.00

21483.00

792.60

36.89

214.00

98.00

20972.00

214.95

97.75

21011.36

20972.00

953.60

45.47

212.45

96.25

20448.31

212.25

96.00

20376.00

20376.00

832.60

40.86

215.50

97.75

21065.13

215.75

97.55

21046.41

21046.41

1081.50

51.39

215.25

98.95

21298.99

214.90

98.00

21060.20

21060.20

1221.60

58.01

214.00

97.45

20854.30

214.10

97.50

20874.75

20854.30

1077.60

51.67

213.85

97.70

20893.15

214.15

97.95

20975.99

20893.15

1027.50

49.18

215.00

98.00

21070.00

215.00

98.00

21070.00

21070.00

1061.60

50.38

214.50

98.00

21021.00

214.35

98.25

21059.89

21021.00

1032.60

49.12

214.00

98.50

21079.00

214.65

97.25

20874.71

20874.71

980.60

46.98

214.70

97.75

20986.93

214.65

97.25

20874.71

20874.71

974.60

46.69

211.10

96.25

20318.38

211.25

96.35

20353.94

20318.38

958.60

47.18

215.40

98.35

21184.59

215.25

98.10

21116.03

21116.03

722.60

34.22

216.00

98.00

21168.00

216.25

98.25

21246.56

21168.00

813.80

38.44

215.90

97.35

21017.87

215.40

97.60

21023.04

21017.87

926.60

44.09

213.45

98.00

20918.10

213.75

99.15

21193.31

20918.10

928.00

44.36

214.95

97.60

20979.12

215.25

97.25

20933.06

20933.06

797.60

38.10

212.75

96.00

20424.00

213.00

96.00

20448.00

20424.00

1002.60

49.09

213.80

98.75

21112.75

214.25

98.00

20996.50

20996.50

948.60

45.18

212.00

96.65

20489.80

216.65

97.00

21015.05

20489.80

1001.60

48.88

214.45

98.35

21091.16

214.55

98.25

21079.54

21079.54

833.60

39.55

212.00

94.75

20087.00

212.20

95.75

20318.15

20087.00

967.60

48.17

216.00

97.25

21006.00

215.75

97.00

20927.75

20927.75

691.60

33.05

Sample 10

Sample 11

Sample 12
-

213.00

96.95

20650.35

213.50

97.75

20869.63

20650.35

1003.50

48.59

215.75

99.65

21499.49

215.45

99.30

21394.19

21394.19

740.60

34.62

212.25

96.95

20577.64

212.00

97.25

20617.00

20577.64

914.60

44.45

212.95

97.25

20709.39

213.00

97.25

20714.25

29709.39

765.50

25.77

217.40

98.75

21468.25

217.95

98.50

21468.08

21468.08

899.60

41.90

212.60

97.35

20696.61

212.55

96.90

20596.10

20596.10

1032.60

50.14

214.25

98.75

21157.19

214.20

98.75

21152.25

21152.25

952.60

45.04

215.10

99.00

21294.90

215.35

99.25

21373.49

21294.90

930.60

43.70

214.40

97.75

20957.60

214.90

97.30

20909.77

20909.77

870.60

41.64

215.40

98.35

21184.59

215.25

98.10

21116.03

21116.03

722.60

34.22

STATISTICAL TABLES

201
Table B1:

5 per cent points of the F-distribution (Adapted from Loveday, 1975)

2
3
4

1
161.4
18.5
10.13
7.71

2
199.5
19.0
9.55
6.94

3
215.7
19.2
9.28
6.59

4
224.6
19.2
9.12
6.39

5
230.2
19.3
9.01
6.26

6
234.0
19.3
8.94
6.16

7
236.8
19.4
8.89
6.09

8
238.9
19.4
8.85
6.04

10
241.9
19.4
8.79
5.96

12
243.9
19.4
8.74
5.91

24
249.0
19.5
8.64
5.77

254.3
19.5
8.53
5.63

5
6
7
8
9

6.61
5.99
5.59
5.32
5.12

5.79
5.14
4.74
4.46
4.26

5.41
4.76
4.35
4.07
3.86

5.19
4.53
4.12
3.84
3.63

5.05
4.39
3.97
3.69
3.48

4.95
4.28
3.87
3.58
3.37

4.88
4.21
3.79
3.50
3.29

4.82
4.15
3.73
3.44
3.23

4.74
4.06
3.64
3.35
3.14

4.68
4.00
3.57
3.28
3.07

4.53
3.84
3.41
3.12
2.90

4.36
3.67
3.23
2.93
2.71

10
11
12
13
14

4.96
4.84
4.75
4.67
4.60

4.10
3.98
3.89
3.81
3.74

3.71
3.59
3.49
3.41
3.34

3.48
3.36
3.26
3.18
3.11

3.33
3,20
3.11
3.03
2.96

3.22
3.09
3.00
2.92
2.85

3.14
3.01
2.91
2.83
2.76

3.07
2.95
2.85
2.77
2.70

2.98
2.85
2.75
2.67
2.60

2.p1
2.79
2.69
2.60
2.53

2.74
2.61
2.51
2.42
2.35

2.54
2.40
2.30
2.21
2.13

15
16
17
18
19

4.54
4.49
4.45
4.41
4.38

3.68
3.63
3.59
3.55
3.52

3.29
3,.24
3.20
3.16
3.13

3.06
3.01
2.96
2.93
2.90

2.90
2.85
2.81
2.77
2.74

2.79
2.74
2.70
2.66
2.63

2.71
2.66
2.61
2.58
2.54

2.64
2.59
2.55
2.51
2.48

2.54
2.49
2.45
2.41
2.38

2.48
2.42
2.38
2.34
2.31

2.29
2.24
2.19
2.15
2.11

2.07
2.01
1.96
1.92
1.88

20
21
22
23
24

4.35
4.32
4.30
4.28
4.26

3.49
3.47
3.44
3.42
3.40

3.10
3.07
3.05
3.03
3.01

2.87
2.84
2.82
2.80
2.78

2.71
2.68
2.66
2.64
2.62

2.60
2.57
2.55
2.53
2.51

2.51
2.49
2.46
2.44
2.42

2.45
2.42
2.40
2.37
2.36

2.35
2.32
2.30
2.27
2.25

2.28
2.25
2.23
2.20
2.18

2.08
2.05
2.03
2.00
1.98

1.84
1.81
1.78
1.76
1.73

25
26
27
28
29

4.24
4.23
4.21
4.20
4.18

3.39
3.37
3.35
3.34
3.33

2.99
2.98
2.96
2.95
2.93

2.76
2.74
2.73
2.71
2.70

2.60
2.59
2.57
2.56
2.55

2.49
2.47
2.46
2.45
2.43

2.40
2.39
2.37
2.36
2.35

2.34
2.32
2.31
2.29
2.28

2.24
2.22
2.20
2.19
2.18

2.16
2.15
2.13
2.12
2.10

1.96
1.95
1.93
1.91
1.90

1.71
1.69
1.67
1.65
1.64

30
32
34
36
38

4.17
4.15
4.13
4.11
4.10

3.32
3.29
3.28
3.26
3.24

2.92
2.90
2.88
2.87
2.85

2.69
2.67
2.65
2.63
2.62

2.53
2.51
2.49
2.48
2.46

2.42
2.40
2.38
2.36
2.35

2.33
2.31
2.29
2.28
2.26

2.27
2.24
2.23
2.21
2.19

2.16
2.14
2.12
2.11
2.09

2.09
2.07
2.05
2.03
2.02

1.89
1.86
1.84
1.82
1.81

1.62
1.59
1.57
1.55
1.53

40
60
120

4.08
4.00
3.92
3.84

3.23
3.15
3.07
3.00

2.84
2.76
2.68
2.60

2.61
2.53
2.45
2.37

2.45
2.37
2.29
2.21

2.34
2.25
2.18
2.10

2.25
2.17
2.09
2.01

2.18
2.10
2.02
1.94

2.08
1.99
1.91
1.83

2.00
1.92
1.83
1.75

1.79
1.70
1.61
1.52

1.51
1.39
1.25
1.00

1 =
2 = 1

202

Table B2:

Distribution of tc (Adapted from Kennedy and Neville, 1985)

Degrees of
freedom (df)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
40
60
120

0.10
6.314
2.920
2.353
2.12
2.015
1.943
1.895
1.860
1.833
1.812
1.796
1.782
1.771
1.761
1.753
1.746
1.740
1.734
1.729
1.725
1.721
1.717
1.714
1.711
1.708
1.706
1.703
1.701
1.699
1.697
1.684
1.671
1.658
1.645

Probability,
0.05
0.01
12.706
63.657
4.303
9.925
3.182
5.841
2.776
4.604
2.571
4.032
2.447
3.707
2.365
3.499
2.306
3.355
2.262
3.250
2.228
3.169
2.201
3.106
2.179
3.055
2.160
3.012
2.145
2.977
2.131
2.947
2.120
2.921
2.110
2.898
2.101
2.878
2.093
2.861
2.086
2.845
2.080
2.831
2.074
2.819
2.069
2.807
2.064
2.797
2.060
2.787
2.056
2.779
2.052
2.771
2.048
2.763
2.045
2.756
2.042
2.750
2.021
2.704
2.000
2.660
1.980
2.617
1.960
2.576

0.001
636.619
31.598
12.941
8.610
6.859
5.959
5.405
5.041
4.781
4.587
4.437
4.318
4.221
4.140
4.073
4.015
3.965
3.922
3.883
3.850
3.819
3.792
3.767
3.745
3.725
3.707
3.690
3.674
3.659
3.646
3.551
3.460
3.373
3.290

203

Table B3:

Range coefficient d (Adapted from Kennedy and Neville, 1985)

Number of
observations,
n
2
3
4
5
6
7
8
9
10
11
12
13

Table B.4:
Number in
subgroup

2
3
4
5
6
7
8
9
10
11

Coefficient,
d
0.8862
0.5908
0.4857
0.4299
0.3945
0.3698
0.3512
0.3367
0.3249
0.3152
0.3069
0.2998

Number of
observations,
n
14
15
16
17
18
19
20
24
50
100
1000

Coefficient,
d
0.2935
0.2880
0.2831
0.2787
0.2747
0.2711
0.2677
0.2567
0.2223
0.1994
0.1543

Factors for control lines for mean and range charts values (BS
2846:1991)
For mean
Warning Action
line
line

Lower
action
line

For range
Lower
Upper
warning warning
line
line

Upper
action
line

'
A0.025

'
A0.001

'
D0.999

'
D0.975

'
D0.025

'
D0.001

1.229
0.668
0.476
0.377
0.316
0.274
0.244
0.220
0.202
0.186

1.937
1.054
0.750
0.594
0.498
0.432
0.384
0.347
0.317
0.294

0.00
0.04
0.10
0.16
0.21
0.26
0.29
0.32
0.35
0.38

0.04
0.18
0.29
0.37
0.42
0.46
0.5
0.52
0.54
0.56

2.81
2.17
1.93
1.81
1.72
1.66
1.62
1.58
1.55
1.53

4.12
2.99
2.58
2.36
2.22
2.12
2.04
1.99
1.94
1.90

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