Version 5.

RH-402 Hydrogen Analyzer

RH-402 Instruction Manual

Patents are pending in U.S.A. and other countries. Minor revisions may not be reflected in this manual. 2004 LECO Corporation

Part Number 200-653 July 2004

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1
1

Introduction

Introduction Illustrations .......................................................................... 17 Warranty.............................................................................. 19 Warning and Caution Symbols................................................ 111 Interference to Other Devices ................................................ 112 Declaration of Conformity...................................................... 113 Major Equipment and Accessories List ..................................... 115 Components and Accessories List ........................................... 116 Options .............................................................................. 119 Specifications...................................................................... 120 Program Modification Levels................................................... 123

Installation Illustrations .......................................................................... 22 Installation ........................................................................... 23 Induction Furnace.................................................................. 25 Gas Connections.................................................................. 213 Furnace Cable ..................................................................... 215 Electrical Connections........................................................... 217 Incoming Reagent Tube ........................................................ 219 Measure Reagent Tube ......................................................... 220 Combustion Tube and Pedestal............................................... 224 Coil Spacing Check............................................................... 228 Internal Balance.................................................................. 229 Printer ............................................................................... 230

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13

Option Installation Illustrations .......................................................................... 32 External Balance.................................................................... 33 Data Transmit ....................................................................... 37 External Keyboard ............................................................... 320

System Setup Illustrations .......................................................................... 42 Controls and Indicators........................................................... 43 System Overview................................................................... 46 Menu Organization Chart......................................................... 48 Initial Power Up ................................................................... 411 System Check..................................................................... 414 System Controls .................................................................. 422

Operation Illustrations .......................................................................... 54 Sample Log-In ...................................................................... 55 Crucibles ............................................................................ 514 Sample Preparation.............................................................. 516 Constants Procedure ............................................................ 518 Analysis Procedure ............................................................... 525 Calibration Procedures .......................................................... 533 Blank Procedures ................................................................. 543 Data Buffers Procedures........................................................ 549 Counters Procedure .............................................................. 552 Stack Procedures ................................................................. 554 Alarms Procedure................................................................. 570 Alarm Table ........................................................................ 571 Analysis Programs................................................................ 575 Analysis Constants............................................................... 579 Analysis Parameters ............................................................. 584 Furnace Power Graphs .......................................................... 585

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Maintenance Illustrations .......................................................................... 62 Periodic Maintenance Schedule ................................................. 63 Catalyst Heater Tube.............................................................. 64 Coolant Level........................................................................ 66 Disposable Particle Filters ........................................................ 68 Loader Cover ........................................................................ 69 Incoming Reagent Tube ........................................................ 610 Measure Flow Reagent Tube .................................................. 611 Screen Filters ...................................................................... 615 O-rings .............................................................................. 616

Theory of Operation General Information............................................................... 73 Furnace Power Oscillator Circuit ............................................... 74 Thermal Conductivity Cell (TC Cell) ........................................... 75 Comparator Level .................................................................. 77 Barometric Pressure ............................................................. 710

Diagnostics Diagnostics Menu................................................................... 83 Leak Test ............................................................................. 84 Manual I/O Test .................................................................... 86 Service I/O Table ................................................................. 810 Sequence Test .................................................................... 812 Auto I/O Test...................................................................... 813 Ambient Monitor.................................................................. 816 Printer Diagnostics............................................................... 818

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Electronic Adjustments Illustrations .......................................................................... 92 A/D Converter Card Adjustment ............................................... 93 Balance Preamp Card Adjustment ............................................. 95 Furnace Power Control Card Adjustment .................................... 97 Heater Control Z.C. Card Adjustment ........................................ 99 Oven Heater Control Card Adjustment ..................................... 911 5 Volt Supply Adjustment ...................................................... 913 Other Volt Supplies .............................................................. 916 Power Supply Unit ............................................................... 917 TC Cell Adjustment .............................................................. 919 TC Cell Power Supply Card Adjustment .................................... 920

10

Service Illustrations ........................................................................ 102 Mechanical Adjustments........................................................ 103 Sample Loading Assembly Alignment ...................................... 106 Electronic Circuit Card Replacement ........................................ 108 Gas Flows..........................................................................1010 Valve States ......................................................................1012 Linearization ......................................................................1020 Break Points ......................................................................1022 Initializing the CPU for 80486 Systems ...................................1023

11 12

Illustrations Index

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Illustrations
Figure 11......... RH-402 System.........................................114 Figure 21......... Jumper Selections......................................24 Figure 22......... Oscillator Chassis .......................................28 Figure 23......... Furnace Transformer Primary Wiring .............211 Figure 24......... Facility Requirements .................................216 Figure 25......... Wiring Diagrams ........................................218 Figure 26......... Reagent Tube Removal ...............................221 Figure 27......... Incoming Reagent Tube Packing ...................221 Figure 28......... Measure Reagent Tube Packing ....................222 Figure 29......... Reagent Tube Assemblies............................223 Figure 210 ....... Combustion Tube and Pedestal Installation.....227 Figure 211 ....... Balance and Dust Cover Installation..............229 Figure 212 ....... Ribbon Cartridge Installation........................232 Figure 213 ....... Paper Installation.......................................232 Figure 31......... Balance Control Panel.................................36 Figure 32......... Balance Assembly ......................................36 Figure 41......... Controls and Indicators...............................45 Figure 42......... Keyboard .................................................47 Figure 43......... Oven Compartment ....................................417 Figure 51......... Crucible Position........................................515 Figure 52......... Typical Aluminum Sample ...........................516 Figure 53......... Plate DCmA vs. Temperature .......................585 Figure 54......... % Power vs. Temperature ...........................586 Figure 61......... Reagent Tube Removal ...............................612 Figure 62......... Incoming Reagent Tube Packing ...................612 Figure 63......... Measure Reagent Tube Packing ....................613 Figure 64......... Reagent Tube Assemblies............................614 Figure 91......... A/D Converter Card....................................94 Figure 92......... Balance Preamp Card .................................95 Figure 93......... Internal BalanceExploded View ..................96 Figure 94......... Furnace Power Control Card.........................98 Figure 95......... Heater Control Z.C. Card.............................910

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17

Figure 96......... Oven Heater Control Card ...........................912 Figure 97......... CPU Card..................................................915 Figure 98......... Power Supply Unit .....................................918 Figure 99......... Oven Compartment ....................................919 Figure 910 ....... TC Cell Power Supply Card ..........................921 Figure 101 ....... Sample Loading Assembly ...........................107 Figure 102 ....... Gas Flow Diagram......................................1013 Figure 103 ....... Leak Check Flow Diagram............................1014 Figure 104 ....... Gas Dose Sequence Diagram.......................1015 Figure 105 ....... Leak Check Sequence Diagram.....................1016 Figure 106 ....... Hot Extraction Analysis Procedure H Sequence Diagram....................1017 Figure 107 ....... Fusion Analysis Procedure F Sequence Diagram....................1018 Figure 108 ....... Combined Analysis Procedure C Sequence Diagram....................1019 Figure 111 ....... AnalyzeLeft Side View ..............................113 Figure 112 ....... AnalyzerRight Side View ...........................114 Figure 113 ....... FurnaceLeft Side View..............................115 Figure 114 ....... FurnaceRight Side View............................116 Figure 115 ....... Furnace TransformerPrimary Wiring............117 Figure 116 ....... Lower Sample Loading Assembly ..................118 Figure 117 ....... Upper Sample Loading Assembly ..................119 Figure 118 ....... 614-493 Display Assembly ..........................1110 Figure 119 ....... 603-732 Doser Valve..................................1111 Figure 1110 ..... 603-790 Pump Assembly.............................1112 Figure 1111 ..... 606-649 Solenoid Valve ..............................1113 Figure 1112 ..... 606-650 Solenoid Valve ..............................1113 Figure 1113 ..... 606-652 Solenoid Valve ..............................1113 Figure 1114 ..... 775-330 Solenoid Valve ..............................1114 Figure 1115 ..... 778-522 Solenoid Valve ..............................1114 Figure 1116 ..... TC Cell Assembly .......................................1115 Figure 1117 ..... 780-509 Vacuum Pump...............................1116

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Warranty
Equipment manufactured by LECO Corporation, St. Joseph, Michigan is warranted free from defect in material and workmanship for a period of six months from the date of installation. Equipment not manufactured by LECO is covered to the extent of warranty provided by the original manufacturer and this warranty does not cover any equipment, new or used, purchased from anyone other than LECO Corporation. All replacement parts shall be covered under warranty for a period of thirty days from date of purchase. LECO makes no other representation or warranty of any other kind, expressed or implied, with respect to the goods sold hereunder, whether as to merchantability, fitness for purpose, or otherwise. Expendable items such as crucibles, combustion tubes, chemicals, and items of like nature are not covered by this warranty. LECO's sole obligation under this warranty shall be to repair or replace any part or parts which, to our satisfaction, prove to be defective upon return prepaid to LECO Corporation, St. Joseph, Michigan. This obligation does not include labor to install replacement parts, nor does it cover any failure due to accident, abuse, neglect, or use in disregard of instructions furnished by LECO. In no event shall damages for defective goods exceed the purchase price of the goods, and LECO shall not be liable for incidental or consequential damages whatsoever. All claims in regard to the parts or equipment must be made within ten (10) days after Purchaser learns of the facts upon which the claim is based. Authorization must be obtained from LECO prior to returning any other parts. This warranty is voided by failure to comply with these notice requirements.

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Notice
The warranty on LECO equipment remains valid only when genuine LECO replacement parts are employed. Since LECO has no control over the quality or purity of consumable products not manufactured by LECO, the specifications for accuracy of results using LECO instruments are not guaranteed unless genuine LECO consumables are employed in conjunction with LECO instruments. If purchaser defaults in making payment for any parts or equipment, this warranty shall be void and shall not apply to such parts and equipment. No late payment or cure of default in payment shall extend the warranty period provided herein. LECO Corporation is not responsible for damage to any associated instruments, equipment, or apparatus nor will LECO be held liable for loss of profit or other special damages resulting from abuse, neglect, or use in disregard of instructions. The Buyer, their employees, agents, and successors in interest assume all risks and liabilities for the operation, use, and/or misuse of the product(s) described herein and agree to indemnify, hold harmless, and defend the seller from any and all claims and actions arising from any cause whatsoever, including seller's negligence for personal injury incurred in connection with the use of said product(s) and any and all damages proximately resulting therefrom.

Caution
The instrument should be operated only by technically qualified individuals who have fully read and understand these instructions. The instrument should be operated only in accordance with these instructions. The operator should follow all of the warnings and cautions set forth in the manual and the operator should follow and employ all applicable standard laboratory safety procedures.
LECO is a registered trademark of the LECO Corporation. Windows is a registered trademark of the Microsoft Corporation. Excel is a registered trademark of the Microsoft Corporation. Windows 95 is a trademark of the Microsoft Corporation. Windows 3.1 is a trademark of the Microsoft Corporation.

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Warning and Caution Symbols

The following symbols may be found on LECO equipment or their components. These symbols indicate the use of specific safety guidelines. Important safety information is highlighted in this manual by one of the following symbols as well as WARNING and CAUTION statements. Operator and service personnel must follow these instructions for personal safety and to prevent damage to the equipment.

WARNING

This symbol indicates a risk of electrical shock. Refer to the manual for specific instructions.

WARNING

This symbol indicates a high temperature surface. Refer to the manual for specific instructions.

!
CAUTION
This symbol indicates a caution. Refer to the manual for specific instructions.

LECO equipment should be operated only by technically qualified individuals who have fully read and understand the instructions detailed in this manual. The equipment should be operated only in accordance with these instructions. The operator should follow all of the warnings and cautions set forth in this manual and the operator should follow and employ all applicable standard laboratory safety procedures.

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Interference to Other Devices

This equipment has been tested and found to comply with the limits for a Class B digital device, pursuant to Part 15 of the FCC Rules and Regulations. These limits are designed to provide reasonable protection against harmful interference in a residential installation. This equipment generates, uses and can radiate radio frequency energy and, if not installed and used in accordance with the instructions, may cause interference to radio communications. However, there is no guarantee that interference will not occur in a particular installation. If this equipment does cause harmful interference to radio or television reception, which can be determined by turning the equipment off and on, the user is encouraged to try to correct the interference by one or more of the following methods:

Reorient or relocate the radio or television receiving antenna. Increase the separation between the equipment and the radio or television receiver. Connect the equipment to an outlet on a circuit different from that which the radio or television receiver is currently connected. Consult the radio or television dealer or an experienced radio/TV technician for help.

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Declaration of Conformity

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Figure 11 RH-402 System

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Major Equipment and Accessories List

Notes

Items listed below and repeated throughout this manual are subject to revision. Please consult the packing slip received with the instrument. For complete listing of packages, refer to the Components and Accessories List, on page 116.

RH402P RH-402 Hydrogen Analyzer Package 1 605-000-200 1 1 1 1 1 1 1 1 200-653 159-076-XXX 603-702 603-703 RH-402 Analyzer includes: Instruction Manual Software Package Component Package HF-402 Furnace includes: Component Package Printer Package (115V) Hazardous Material Package Accessory Package

605-100-100 601-480-110 607-762* 783-928

RH402PI RH-402 Hydrogen Analyzer Package 1 605-000-200 1 1 1 1 1 1 1 200-653 159-076-XXX 603-702 RH-402 Analyzer includes: Instruction Manual Software Package Component Package HF-402 Furnace includes: Component Package Printer Package (230V) Hazardous Material Package Accessory Package

605-100-100 1 603-703 611-298-110 607-762* 783-928

-XXX indicates software version. * Packed and shipped separately in the U.S.A. Not included with international shipments due to shipping restrictions. These items are essential for operation. Contact your local LECO distributor for quotation and delivery.

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Components and Accessories List

601-480-110 1 1 1 1 1 601-480 601-481 601-483 601-484 603-595 Printer Kit (115V) Dot Matrix Printer Paper Tray Paper 91 /2 X 11 (500 Sheets) Ribbon Cartridge Parallel Cable Assembly

603-702 Component Package 1 1 1 4 4 4 1 1 501-081 603-676 611-118 769-477 769-478 775-381 780-067 780-460 Glass Wool (1 LB) N2 Connector Software Fitting Fitting Fitting Nut Connector Assembly Balance Dust Cover

603-703 Component Package 1 1 1 2 1 1 2 2 2 2 2 190-745 537-103-040 537-152 603-463 603-704 603-9024 608-898 765-978 769-477 769-478 775-381 Screw Tube Coil Spacer Tube Furnace Cable Loader Insert Receptacle Cover Receptacle Fitting Fitting Fitting Nut

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603-705 Accessory Package 1 1 1 6 6 1 3 1 6 6 6 2 1 1 1 6 1 1 1 1 1 6 1 1 501-241 501-529 501-621 602-802 602-803 603-706 603-710 603-778 603-910 603-970 603-971 604-241 760-138 760-139 761-929 762-357 762-747 764-079 767-473 768-980 769-520 772-269 775-307 782-080 Vacuum Grease (5.3 Oz) 6.0 ppm H Pin Sample Degassed Copper Turning O-ring (Top/Bottom Seal) O-ring (Top/Bottom Seal) Pedestal Sample Quartz Crucible Alignment Tool O-ring (Top/Bottom Seal) Seal Seal Combustion Tube Tweezer Tweezer Crucible Tongs O-ring (Lower Sample Loader) 1.5 ppm H Pin Sample 5 Gram Weight Utility Funnel Tube Filter Carbon Crucible O-ring (Upper Sample Loader) Thumb Screw Combustion Tube Puller Assembly

607-762* Hazardous Material Package 1 1 1 501-171 502-174 761-747 Anhydrone (1 LB) Lecosorb (500 gr.) Schutze Reagent

* Packed and shipped separately in the U.S.A. Not included with international shipments due to shipping restrictions. These items are essential for operation. Contact your local LECO distributor for quotation and delivery.

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611-298-110 1 1 1 1 1 601-481 601-483 601-484 603-595 611-298

International Printer Kit (230V) Paper Tray Paper 91 /2 X 11 (500 Sheets) Printer Ribbon Cartridge Parallel Cable Assembly Dot Matrix Printer

783-928 Accessory Package 1 6 6 1 3 1 6 6 6 2 1 1 6 1 1 1 6 1 1 1 501-241 602-802 602-803 603-706 603-710 603-778 603-910 603-970 603-971 604-241 760-138 760-139 762-357 764-079 767-473 768-980 772-269 775-307 782-080 783-928-010 1 1 1 1 1 501-529 502-295 762-747 769-520-500 769-761-110 Vacuum Grease (5.3 Oz) O-ring (Top/Bottom Seal) O-ring (Top/Bottom Seal) Pedestal Sample Quartz Crucible Alignment Tool O-ring (Top/Bottom Seal) Seal Seal Combustion Tube Tweezer Tweezer O-ring (Lower Sample Loader) 5 Gram Weight Utility Funnel Tube Filter O-ring (Upper Sample Loader) Thumb Screw Combustion Tube Assembly Consumable Pack 6.0 ppm H Pin Sample Degassed Copper Turnings 1.5 ppm H Pin Sample Carbon Crucible (500/Pk) Carbon Crucible (10/Pk)

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Options
601-990 603-705 603-709 603-733 603-778-110 603-790-110 603-868-020 603-873-110 603-976 603-990 604-241 604-264 604-265 604-298 604-490 605-980 608-169 608-592 751-030-110 751-300-160 761-742 764-216 771-468-110 780-256-110 782-382 783-545 805-703 Bar Code Reader Kit Accessory Pack (for a complete listing, see Components and Accessories List, page 116) Upper Seal Tool Cable Assembly Crucible Alignment Tool Kit Replacement Pump Kit Actuator Replacement Kit Tank Kit Filter Kit Data Transmit Kit Reaction Tube Top and Bottom Seal Replacement Kit Slide Loading Head Kit Internal Keyboard Kit Balance Kit Keyboard Data Transmit Kit Keyboard Bracket Assembly Balance Interface Serial Kit 4 Place Balance Kit (L-250) Hydrogen Regulator Assembly Helium Regulator Capacitor Replacement Kit Observation Window Kit Keyboard Dust Cover Gas Dose Kit Receptacle Cover (30A)

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Specifications
Dynamic Range (at 5 Grams)* Low Range ......................................0.01 to 20 ppm High Range .....................................0.04 to 400 ppm Precision** Low ....................................................0.005 ppm or 2% RSD, whichever is greater High ...................................................0.02 ppm or 2% RSD, whichever is greater Readability ........................................0.001 ppm Analysis Time Hot Extraction .................................250 seconds nominal, 1200 seconds maximum. Fusion and Combined Extraction .........250 seconds nominal, 600 seconds maximum Calibration.........................................Gas dose or standards up to 200 analysis basis. Gas Dose (Allowable Analysis Time) ........20 seconds (Min) Comparator Level...............................0.01 to 100% Sample Size .......................................5 gram nominal, 0.375 inch diameter x 2.1 inches (max) Balance Sensitivity.............................0.001 to 20 grams (0.001 gr) Detection Method ...............................Thermal Conductivity Chemical Reagents.............................Anhydrous Magnesium Perchlorate, Sodium Hydroxide on Inert base, Reagent, Copper Turnings Gases Required Carrier and Pneumatic Gas.................Nitrogen, 99.99% pure, 40 psi (2.76 bars) 10% Doser Gas.......................................Hydrogen, 99.99% pure, 40 psi (2.76 bars) 10%

* Reducing or increasing sample mass may extend Range. ** Calibrated and conformance tested by gas analysis.

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Gas Flow............................................325 cc/min Regulators Nitrogen .........................................764-216, 0-125 psi, CGA580, 15 /16-14 Female RH Hydrogen........................................761-743, 0-125 psi, CGA350, 13 /16-14 Male LH Furnace Type .....................................High Frequency Induction, 4MHz/4.5 kW Sensitivity..........................................0.001 ppm Leak Check Limits ..............................900 to 1400 mm Hg TC Cell Low Range ......................................100 to 2000 mV High Range .....................................5 to 2000 mV Warning Indicator..............................Audible Alarm Data Storage......................................500 analysis results, 100 sample weight, 65,000 database results Memory .............................................20 MB Hard Disk (minimum) Keyboard ...........................................51 key alphanumeric , with 4 cursor keys and 8 function keys Display Type ..............................................Electroluminescent Size ...............................................7.70" x 4.80" (195 mm x 122 mm) Resolution.......................................640 x 200 Pixels Viewing Angle ..................................>120o Printer/Plotter...................................Dot Matrix, 300 cps Electrical Power Requirements Analyzer.........................................115/230 V~ (10%), 50/60 Hz, 6A at 115 V~, 3A at 230 V~ Furnace..........................................230 V~ (10%), 50/60 Hz, 4.5 kW under load, 30A at 230 V~ Printer............................................115 V~ (10%), 50/60 Hz

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Dimensions Analyzer Height ............................................30 inches (76 cm) Width.............................................24 inches (61 cm) Depth ............................................27 inches (69 cm) Weight ...........................................220 lb. (99 kg) Furnace Height ............................................30 inches (76 cm) Width.............................................16 inches (41 cm) Depth ............................................27 inches (69 cm) Weight ...........................................310 lb. (140 kg) Printer Height ............................................11 inches (28 cm) Width.............................................16.5 inches (42 cm) Depth ............................................16 inches (41 cm) Weight ...........................................20 lb. (9 kg) Shipping Weight.................................635 lb. (287 kg)

Note

Allow a 6 inch minimum access area around all units.

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Program Modification Levels

A major portion of this instruments functions are defined and controlled by software that may be updated. Most updates do not affect physical design of the instrument, but can improve performance and make operation easier. A 2-digit version number identifies software changes in all LECO microprocessor-based instruments. The first release of a program is always 1.0. Each minor change adds an increment of 1 to the right digit, i.e. 1.0, 1.1, 1.2, etc. Each major change adds an increment of 1 to the left digit and changes the right digit to 0, i.e. 2.0, 3.0, 4.0, etc. Software updates are accomplished using a new programming disk and performing the Software Program Update procedure, page 124.

Notes

Some software will have a 3-digit version number (i.e. 1.01, 2.23). The right hand digit is for internal use only. Before performing the software program update procedure, be sure to print all constants screens. Occasionally, new updates have system files that are incompatible with the current version and all the defaults will be restored with the update.

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Software Update Procedure

1. 2. Turn the system on. Observe the display. The instrument runs through a base and extended memory check twice. Immediately following the second check, press CTRL and C simultaneously (or press the F8 key) until the instrument displays: Terminate Batch Job (Y/N)? and then press the Y key. The following screen will appear.

3. 4.

Place the update disk into the disk drive and type: A:INSTALL. Press enter to begin installation. Carefully follow all instructions and prompts given during the program update. To reset the system after programming is completed, remove and store the disk, and: A. B. On the external keyboard, press CTRL, ALT and delete keys. On the built-in keyboard, press Shift, CTRL and 5 keys.

5.

6.

The system is now updated and ready for use.

Note

When the instrument name, version number, serial number, and copyright display, check that the version number reflects the updated version.

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Illustrations .......................................................................... 22 Installation ........................................................................... 23 Induction Furnace.................................................................. 25 Oscillator Tube Installation............................................. 26 AC Voltage Tap Selection............................................... 29 Coolant Installation .................................................... 212 Gas Connections.................................................................. 213 Furnace Cable ..................................................................... 215 Electrical Connections........................................................... 217 Incoming Reagent Tube ........................................................ 219 Measure Reagent Tube ......................................................... 220 Combustion Tube and Pedestal............................................... 224 Preliminary Installation................................................ 225 Installation................................................................ 226 Coil Spacing Check............................................................... 228 Internal Balance.................................................................. 229 Printer ............................................................................... 230 Printer Settings.......................................................... 233

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Illustrations
Figure 21......... Jumper Selections......................................24 Figure 22......... Oscillator Chassis .......................................28 Figure 23......... Furnace Transformer Primary Wiring .............211 Figure 24......... Facility Requirements .................................216 Figure 25......... Wiring Diagrams ........................................218 Figure 26......... Reagent Tube Removal ...............................221 Figure 27......... Incoming Reagent Tube Packing ...................221 Figure 28......... Measure Reagent Tube Packing ....................222 Figure 29......... Reagent Tube Assemblies............................223 Figure 210 ....... Combustion Tube and Pedestal Installation.....227 Figure 211 ....... Balance and Dust Cover Installation..............229 Figure 212 ....... Ribbon Cartridge Installation........................232 Figure 213 ....... Paper Installation.......................................232

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Installation

WARNING

ELECTRICAL SHOCK HAZARD This equipment operates from 230 V~. Contact with this voltage can be lethal. During installation do not apply power until instructed to do so. Before servicing this equipment, disconnect the power source.

1. 2.

Select a level work surface with convenient facility power, nitrogen, and hydrogen supply. Provide at least a 6 inch clearance all around the system for proper ventilation.

Note

Cooling fans and heat exchangers located at the top of the cabinets must not be blocked. Keep cabinet tops free of all articles. Remove the right and left side panels from the analyzer. Inspect the circuit cards for damage and make sure they are properly seated in their connectors. Carefully remove any tape or other packaging materials and remove the shipping card from the disk drive. Locate the vacuum pump on the right side of the RH-402 analyzer chassis bottom (figure 11-2, page 11-4). Place the 50/60 Hz switch to the proper power line frequency. During the manufacturing process, the RH-402 analyzer is set for operation at 230 V~. For operation from 115 V~, locate the voltage selector switch on the right side of the analyzer (figure 11-2, page 11-4) and switch it to the left, (115 V~) position. Swing out the electronics chassis, located on the left side of the RH-402 analyzer (figure 11-1, page 11-3), and locate the voltage select wire on the power supply unit (figure 2-1, page 24). Install the voltage select wire for 115 V~ operation.

3. 4. 5. 6.

7.

8.

9.

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23

TERMINAL #5 = RETURN = TERMINAL #6 TERMINAL #4 = +24V = TERMINAL #5

NOTE: CONNECTIONS REVERSED

+5V +5V RETURN RETURN RETURN +24V +12V -12V POWER FAIL +5V +5V +5V RETURN +5V RETURN +24V AUX RETURN +12V - 12V POWER FAIL 1 2 3 4 5 6 7 8 9

9 8 7 6 5 4 3 2 1

R50

CAPACITORS R39

CAPACITORS

OR
CP BOSCHERT
POWER SUPPLY

TRANSFORMER

DANGER HIGH VOLTAGE

CAPACITORS TRANSFORMER CAPACITORS 115V~ 230V~ VOLTAGE SELECT WIRE FUSE

1 2 3 AC HOT AC GROUND AC NEUTRAL/HOT

115V~ VOLTAGE SELECT WIRE

3 2 AC HOT AC NEUTRAL/HOT

FUSE

230V~

1 AC GROUND

TERMINAL #2 = AC GROUND = TERMINAL #1 TERMINAL #3 = AC NEUTRAL/HOT = TERMINAL #2 NOTE: CONNECTIONS REVERSED

BOSCHERT TM POWER SUPPLY

POWER-ONETM POWER SUPPLY

Figure 21 Jumper Selections

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Induction Furnace

WARNING

HIGH VOLTAGE HAZARD After the power has been turned on; both the oscillator and the furnace power supply produce lethal voltages. Contact the LECO service department for more information before servicing.

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Oscillator Tube Installation

WARNING

HIGH VOLTAGE HAZARD After the power has been turned on, both the oscillator and the furnace power supply produce lethal voltages. Contact the LECO service department for additional information before servicing.

WARNING

ELECTRICAL SHOCK HAZARD The capacitors on the oscillator chassis store a lethal amount of energy and must be discharged to avoid electric shock . Contact the LECO service department for more information before servicing the oscillator chassis.

1. 2. 3.

Remove the right and left side panels from the furnace. Remove the oscillator side panel from the right side of the furnace (figure 11-4, page 11-6). From the harness: A. B. C. Disconnect the bias voltage connector J101. Disconnect the high voltage connector J151. Disconnect the high voltage connector J152.

4. 5.

Disconnect the two coolant line connectors attached to the capacitor stack assembly (figure 2-2, page 28). Remove the two bolts and washers securing the oscillator assembly to the furnace.

!
CAUTION
POSSIBLE OPERATOR INJURY Use care when removing the oscillator chassis. The oscillator chassis is heavy.

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6.

Remove the oscillator assembly from the furnace. The oscillator assembly is heavy and should be handled carefully. Install the vacuum capacitor into the two fuse clips at the front-left corner of the oscillator chassis (figure 2-2, page 28). Locate and remove the four screws on the oscillator tube holding ring. Carefully unpack the oscillator tube and set the packing material aside. Carefully position the filament leads through the holding ring and seat the tube base on the ring. Locate the strap attached to the grid coil and attach it to the metal ring tube base using one of the screws. Secure the tube using the 3 remaining screws. Position the filament leads and attach the lugs to the filament transformer connections using the hardware provided. Connect the fuse clip (from the capacitor stack) to the plate connection on the top of the oscillator tube. Install the tube chimney over the oscillator tube (figure 2-2, page 28). Reinstall the oscillator assembly into the furnace by reversing steps 3 through 8.

7.

8. 9. 10. 11.

12.

13. 14. 15.

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27

550-047 PLATE CHOKE 608-537 250 Pf VACUUM CAPACITOR (3 REQD) 550-187 500 Pf - 15 kV CAPACITOR (6 REQ'D) 608-537 200 Pf - 20 kV CAPACITOR (3 REQUIRED)
500 500 500

521-042 FUSE CLIP (3 REQ'D)

771-425 OSCILLATOR TUBE

537-277 GRID COIL AND 550-048 GRID CHOKE TUBE FILAMENT LEADS

500 C1 100 100

550-187 500 Pf - 15 kV CAPACITOR (2 REQ'D)

550-187 500 Pf - 15 kV CAPACITOR 764-640 100 Pf - 15 kV CAPACITOR (6 REQ'D)

TB-105 COOLANT LINE CONNECTORS 614-592 COOLING FAN

Figure 22 Oscillator Chassis

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AC Voltage Tap Selection

WARNING

HIGH VOLTAGE HAZARD After the power has been turned on, both the oscillator and the furnace power supply produce lethal voltages. Contact the LECO service department for additional information before servicing.

WARNING

ELECTRICAL SHOCK HAZARD The capacitors on the oscillator chassis store a lethal amount of energy and must be discharged to avoid electric shock . Contact the LECO service department for more information before servicing the oscillator chassis.

Notes

The HF-402 furnace is set during the manufacturing process for operation at 230 V~, 60 Hz operation. Although the furnace will only operate from 210 to 240 V~, the power line frequency can be set for 50 Hz or 60 Hz. For additional information, refer to the Furnace Power Control Card Adjustment, page 9-7. For 50 Hz operation: A. Remove the front panel of the HF-402 furnace and locate the furnace power control card (figure 11-4, page 11-6). Set the line frequency switch, SW2, to 50 Hz (figure 9-4, page 98).

1.

B. 2.

Measure the facility line voltage with an accurate voltmeter and determine the facility line voltage.

Installation

RH-402

29

3.

Determine the correct taps settings for the measured line voltage using the following TB-105 filament transformer tap setting table.
180 to 240 V~ Operation Input Voltage 180 200 220 240 Use Tap Number 1 Black Wire 2 Red Wire 1 Black Wire 3 1 4 1 5 Red Wire Black Wire Red Wire Black Wire Red Wire

!
CAUTION
POSSIBLE INSTRUMENT DAMAGE The black tap wire must be connected to tap 1 only. The red tap wire must be connected to taps 2, 3, 4, or 5 only.

4. 5.

Install the taps on terminal strip TB-105 as shown in the table above (figure 2-3, page 211). Determine the correct tap settings for the measured line voltage using the following TB-104 plat tap settings table.
180 to 240 V~ Operation Input Voltage 180 V~ 200 V~ 220 V~ 240 V~ Use Tap Number 1 Black Wire 2 Red Wire 1 Black Wire 3 1 4 1 5 Red Wire Black Wire Red Wire Black Wire Red Wire

!
CAUTION
POSSIBLE INSTRUMENT DAMAGE The black tap wire must be connected to tap 1 only. The red tap wire must be connected to taps 2, 3, 4, or 5 only.

6. 7.

Install the taps on terminal strip TB-104 as shown in the table above (figure 2-3, page 211). Reinstall the oscillator compartment side panel.

210

RH-402

Installation

WARNING
THE OSCILLATOR AND FURNACE POWER SUPPLY CARRY LETHAL VOLTAGES WHEN THE HIGH VOLTAGE IS TURNED ON.

RF CHASSIS 772-984 10 AMP RFI FILTER

1 2 3 4 5

TB-105

HIGH VOLTAGE FEED-THROUGHS RED

1 2 3 4 5

BLACK 771-488 30 AMP RFI FILTER 771-487 HIGH VOLTAGE STANDOFFS

TB-104

789-379 TRANSFORMER AND PLATE ASSEMBLY

NOTE: THE POSITION OF THE RED WIRE TERMINATIONS ARE SHOWN FOR EXAMPLE ONLY. REFER TO THE TEXT FOR DETERMINING THE CORRECT CONNECTIONS.

Figure 23 Furnace Transformer Primary Wiring

Installation

RH-402

211

Coolant Installation

!
CAUTION
POSSIBLE MACHINE ERROR Only use distilled water when filling the coolant tank.

1.

Locate the coolant tank on the left side of the HF-402 furnace. Position the coolant tank valve handle forward towards the front of the furnace to turn off the flow of water (figure 11-3, page 11-5). Remove both hoses from the coolant tank and remove the tank. Fill the coolant tank with 2 gallons (7.5 liters) of distilled water. Reinstall the coolant tank into the furnace and reconnect the hoses. Turn the coolant tank valve 1 /4 turn clockwise to turn on the flow of water. Check for any water leaks from the hoses or coolant tank. Replace the right and left furnace side panels.

2. 3. 4. 5. 6. 7.

212

RH-402

Installation

Gas Connections

Notes

1. 2.

Fittings are provided in the component packs for gas connections. For a complete listing, refer to the Components and Accessories List, page 116. Refer to figure 2-4, page 216, for locations when making gas connections. Make sure the RH-402 analyzer and HF-402 furnace are turn off and disconnected from the facility power supply. Install a nitrogen regulator on the nitrogen gas tank and a hydrogen regulator on the hydrogen gas tank.

Note

3. 4. 5.

The pressure regulators and flows will be adjusted later.

Remove the shipping plugs from all ports on the rear panel of the RH-402 analyzer and HF-402 furnace. Verify that the gas sources are turned off. Connect the nitrogen supply to the N2 In port on the rear of the RH-402 analyzer using a connector.

Note

6. 7. 8.

Nitrogen serves as both the carrier and pneumatic gas.

Connect the hydrogen supply to the H2 Gas Dose In on the rear of the RH-402 analyzer using a connector. Space the RH-402 and HF-402 units 6 to 12 inches apart. Connect the pneumatic connector between the pneumatic ports on each unit.

Installation

RH-402

213

9. 10.

Connect one connector between the carrier flow ports on each unit. Connect the other connector between the analyze flow ports on each unit.

!
CAUTION
POSSIBLE OPERATOR INJURY The two remaining ports on the RH-402 are for exhaust gases. These ports must be exhausted away from the work area. Connect the exhaust ports to the lab exhaust system or a fume hood.

214

RH-402

Installation

Furnace Cable
1. Connect the proper end of the furnace interconnect cable to the back panel of the HF-402 furnace (figure 2-4, page 216). Connect the other end of the furnace cable to the back panel of the RH-402 analyzer.

2.

Installation

RH-402

215

764-216 REGULATOR 761-743 REGULATOR

HF-402 INDUCTION FURNACE

ID TAG 603-704 CABLE ANALYZE FLOW CARRIER FLOW ID TAG

RH-402 ANALYZER
J203 H2 40 PSI N2 40 PSI

780-067 CONNECTOR TO DATA TRANSMIT

PNEUMATIC

603-463 TUBING H2 GAS DOSE IN ANALYZE FLOW CARRIER FLOW

TO BALANCE 603-676 N2CONNECTOR

537-103-040 TUBING PNEUMATIC N2 I N (40 PSI) 10 GA WIRE GROUNDING STRAP

TC CELL EXHAUST H2GAS DOSE EXHAUST

TO 230V POWER SUPPLY

TO 115V POWER SUPPLY

!
CAUTION
POSSIBLE OPERATOR INJURY The two remaining ports on the RH-402 are for exhaust gases. These ports must be exhausted away from the work area. Connect the exhaust ports to the lab exhaust system or a fume hood.

Note

For the electrical requirements, gas flows, and gases required, refer to the Specifications section, page 120, for more information.

Figure 24 Facility Requirements

216

RH-402

Installation

Electrical Connections

Notes

1.

For the RH-402 Analyzer only, be sure the actual line voltage matches the correct position of the voltage selector switch. Refer to RH-402 Analyzer Installation, page 23. Refer to figure 2-5, page 218, for typical facility power wiring. The HF-402 Induction Furnace operates on 230 V~ only.

Be sure the facility power is connected as shown in one of the diagrams. A mating receptacle for the HF-402 furnace is supplied if necessary. Before applying power, verify that the facility wiring and connectors are operational and properly installed. The RH-402 analyzer will operate from either 115 V~ or 230 V~. The AC connector supplied on the RH-402 cable is intended for 230 V~ operation only. If 115 V~ operation is intended, a suitable connector (not supplied) must be substituted (figure 2-5, page 218).

2. 3.

Installation

RH-402

217

POWER CORD GREEN BLACK GREEN WHITE

POWER NEUTRAL GROUND 115 V~ 0 V~

BLACK WHITE

CHASSIS (CABINET) GROUND

115 V~ WIRING DIAGRAM (U.S.A.)

POWER CORD

POWER 220 V~ NEUTRAL 0 V~ GROUND

BROWN LIGHT BLUE GREEN/YELLOW

CHASSIS (CABINET) GROUND

220 V~ 3 WIRE WIRING DIAGRAM INTERNATIONAL

PLUG BLACK GREEN/YELLOW GREEN/ YELLOW G BLACK LIGHT BLUE CHASSIS (CABINET) GROUND X T B

BLACK

POWER 115 V~ GROUND POWER 230 V~ 115 V~

Y G X B

Y G X B

LIGHT BLUE

BLACK RECEPTACLE

* BLUE WIRE IS CUT OFF INSIDE THE UNIT AND IS NON-FUNCTIONAL

230 V~ 3 WIRE WIRING DIAGRAM U.S.A.

PLUG BLACK GREEN/YELLOW GREEN/ YELLOW G BLACK LIGHT BLUE CHASSIS (CABINET) GROUND X BLACK RECEPTACLE T B
LIGHT BLUE

BLACK

POWER 115 V~ GROUND POWER NEUTRAL 115 V~ 0 V~ 230 V~

Y G X B

Y G X B

* BLUE WIRE IS CUT OFF INSIDE THE UNIT AND IS NON-FUNCTIONAL

230 V~ 4 WIRE CENTER TAPPED WIRING DIAGRAM U.S.A.

Figure 25 Wiring Diagrams

218

RH-402

Installation

Incoming Reagent Tube

1. Remove the incoming reagent tube (figure 2-9, page 223): A. B. C. 2. Sliding the incoming reagent tube upward until the bottom end can swing free (figure 2-6, page 221). Tilt out the free incoming reagent tube end. Pull the incoming reagent tube downward off the top port.

Insert a screen filter into the bottom of each incoming reagent tube. Position the o-ring towards the bottom and push the screen filter up into the incoming reagent tube 1 /4 inch (figure 2-7, page 221). Pack the incoming reagent tube (figure 2-7, page 221) A. Loosely pack 3 /4 inch of glass wool into the bottom of each incoming reagent tube leaving the narrow section of the incoming reagent tube open. Fill the remaining bottom half of each incoming reagent tube with anhydrone by pouring it on top of the glass wool. Fill the top half of each incoming reagent tube with Lecosorb, leaving 3 /4 inch at the top. Loosely pack 3 /4 inch of glass wool into the top of each incoming reagent tube leaving the narrow section of the incoming reagent tube open.

3.

B.

C. D.

4.

Reinstall the incoming reagent tube: A. B. Push the top end of the incoming reagent tube over the top port. Tilt it inward and pull it down, pushing it over the bottom port.

5. 6.

Reset the incoming reagent tube counter. Refer to System Controls, page 422, for more information. The catalyst heater tube is packed during the manufacturing process. To repack the catalyst heater tube, refer to the Catalyst Heater Tube, page 64, for more information.

Installation

RH-402

219

Measure Reagent Tube

1. Remove the measure reagent tube (figure 2-9, page 223): A. B. C. 2. Slide each measure reagent tube upward until the bottom end can swing free (figure 2-6, page 221). Tilt out the free measure reagent tube end. Pull the measure reagent tube downward off the top port.

Insert a screen filter into the bottom of the measure reagent tube. Position the o-ring towards the bottom and push the screen filter up into the measure reagent tube 1 /4 inch (figure 2-8, page 2-22). Pack the measure reagent tube (figure 2-8, page 222): A. Loosely pack inch of glass wool into the bottom of each measure reagent tube leaving the narrow section of the measure reagent tube open. Fill the bottom anhydrone.
1

3.

B. C. D. E. F. 4.

/3 of the measure reagent tube with

Fill the middle 1 /3 of the measure reagent tube with Lecosorb. Pack 1 /8 inch of glass wool on top of the Lecosorb. Fill the top 1 /3 of the measure reagent tube with Schutze reagent. Pack 3 /4 inch of glass wool into the top of the measure reagent tube. Push the top end of the measure reagent tube over the top port. Tilt it inward and pull it down, pushing it over the bottom port.

Reinstall the measure reagent tube: A. B.

5.

Reset the measure reagent tube counter. Refer to System Controls, page 422, for more information.

220

RH-402

Installation

REAGENT TUBE

Figure 26 Reagent Tube Removal

775-601 REAGENT TUBE

501-081 GLASS WOOL

502-174 LECOSORB

501-171 ANHYDRONE

501-081 GLASS WOOL 775-306 SCREEN FILTER

Figure 27 Incoming Reagent Tube Packing

Installation

RH-402

221

775-601 REAGENT TUBE 501-081 3/4" GLASS WOOL 761-747 SCHUTZE REAGENT 501-081 1/8" GLASS WOOL 502-174 LECOSORB 501-171 ANHYDRONE

501-081 3/4" GLASS WOOL

775-306 SCREEN FILTER

Figure 28 Measure Reagent Tube Packing

222

RH-402

Installation

614-354 MOVABLE BLOCK

772-694 KNOB

778-114 O-RING

772-738 O-RING

782-041 COVER TUBE

502-295 COPPER TURNINGS

614-317 UPPER BLOCK (2 REQ'D)

776-729 CATALYST HEATER TUBE 603-956 CATALYST HEATER ASSEMBLY 772-520 O-RING (5 REQ'D) 614-318 LOWER BLOCK (3 REQ'D)

MEASURE REAGENT TUBE

INCOMING REAGENT TUBE

Figure 29 Reagent Tube Assemblies

Installation

RH-402

223

Combustion Tube and Pedestal

Notes

The HF-402 furnace side panels must be removed. The combustion tube and pedestal installation may be accomplished with either the gas on or the gas off. If gas is not used, the top seal and sample block must be moved by hand. The pneumatic connector on the HF-402 must be disconnected to release any pressure on the cylinders (figure 2-4, page 216). The furnace bypass solenoid, SV7, and the gas must be on when the installation is completed to prevent moisture and atmosphere contaminants from reaching the TC cell. To verify solenoid valve 7 is on, observe the solenoid interface card (figure 11-3, page 11-5). The light for SV7, labeled CR7, should be on.

224

RH-402

Installation

Preliminary Installation
1. 2. Turn the RH-402 analyzer power to the on position. Verify that the HF-402 furnace power switch is in the off position and the power cord is disconnected from facility power.

WARNING

ELECTRICAL SHOCK HAZARD Disconnect HF-402 furnace power cord from facility power.

3.

Remove the HF-402 furnace front panel section by sliding it to the right and removing the remaining the perforated panel (4 screws) over the furnace cavity using a 5 /32 inch hex wrench. Press the F8 key twice to display the diagnostic menu. Press the F1 (System Check) key. Press the F4 (Sequence Test) key. The monitor will display the following screen:

4. 5. 6.

Note

The furnace bypass solenoid, SV7, is turned on automatically when the sequence test program is accessed.

Installation

RH-402

225

Installation
1. 2. 3. 4. 5. 6. 7. 8. From the sequence test screen, press key #7 to open the top seal. Press the #8 key to open the block. Disconnect the locking mechanism and swing the optical sensor out of the way (figure 2-10, page 227). Turn the screw into the threaded hole of the top seal. Pull the seal up and out of the cavity top surface. Move the pedestal shaft to the fully raised position (key #4). Screw the pedestal onto the threaded pedestal rod until the pedestal is fully seated. Move the pedestal to the home position (key #0). With the front cover still removed, check the coil turn spacing using the coil spacer tool. Verify that the turns are spaced evenly and that the coil is 21 /2 inches high. Position the coil so that the bottom of the coil is 4.85 inches from the top of the furnace cavity. Position the pedestal 4.38 inches from the top of the furnace cavity. The pedestal can be adjusted with the screw located below the furnace cavity at the base of the pedestal shaft. Apply a small amount of vacuum grease to the outside bottom edge of the combustion tube. Lower the combustion tube (greased end down) over the pedestal and seat the combustion tube into the lower seal. Place a small amount of vacuum grease on the inner oring of the top seal and insert this seal back into place over the combustion tube.

9.

10. 11. 12.

Note

13. 14. 15.

Wipe off any fingerprints that may be left on the bubble portion of the combustion tube Remove the screw. Close the block and then the top seal. Do not reinstall the front panel or perforated panel. Continue with the Coil Spacing Check procedure on page 228.

226

RH-402

Installation

783-593 ROTARY ACTUATOR 603-711 PLATE CURRENT METER DC mA

603-860 SEAL CYLINDER

603-974 LOCKING MECHANISM

603-888 LOADER ASSEMBLY COVER

190-279 ADJUSTMENT SCREW (4 REQ'D) 603-870 SLIDE CYLINDER 603-871 MAGNETIC REED SWITCH (2 REQ'D)

603-862 SAMPLE LOADING BLOCK 603-955 OPTICAL SENSOR 777-605 MELT DETECTOR CARD

604-266 TOP SEAL

782-080 COMBUSTION TUBE PULLER 604-241 COMBUSTION TUBE

Figure 210 Combustion Tube and Pedestal Installation

Installation

RH-402

227

Coil Spacing Check

ELECTRICAL SHOCK HAZARD The oscillator and induction coil may contain lethal voltages. Use extreme caution when performing this procedure.

1. 2.

With the perforated front panel still removed, check the coil turn spacing using the coil spacer tool. Check to be sure the turns are spaced evenly and that the coil is positioned an equal distance around the combustion tube. Reform the coil carefully as required. Reinstall the perforated panel and the front panel that were removed earlier. Reinstalled the cabinet side panels and reconnected the furnace power cord.

3. 4.

228

RH-402

Installation

Internal Balance
1. Locate the J160 balance connector inside the round hole on the analyzer, connect it to the J160 receptacle located on the balance assembly. Insert the balance into the holder on the analyzer shelf (figure 2-11, below). Install the dust shield onto the balance pedestal then place the pan on the shield as shown. Install the dust cover over the balance by slipping the front tab under the balance plate than lowering the cover onto the balance.

2. 3.

780-460 BALANCE DUST COVER

772-608 PAN 772-602 SHIELD

614-326 BALANCE

J160 CONNECTOR

Figure 211 Balance and Dust Cover Installation

Installation

RH-402

229

Printer

Note

1.

Refer to figure 2-12 and figure 2-13 on page 232 when following these procedures. Unpack the printer. Locate the separate printer manual in the printer box and check the contents of the box against the manual list. Remove any tape, bags, or styrofoam from the printer. Remove the platen knob from the styrofoam before discarding. Remove the shipping retainer located inside the printer (save it in case the printer needs to be shipped). Install the platen knob by inserting the shaft into the hole in the right side of the printer. Match the flat side of the knob to the flat side of the platen shaft.

2.

3. 4.

Notes

5.

After extended periods of printing, allow time for the printhead to cool before touching it. Turn off the power before moving the printhead.

Install the ribbon cartridge. A. B. C. Open the access cover. Position the printhead between bail rollers and push the bail lever back. Place the flat end of the ribbon cartridge, knob facing up, into the ribbon plate, then lower the other end over the printhead and snap it into place. Turn the knob clockwise to take up ribbon slack. The headgap lever can be adjusted for one or two part forms (position 1), three or four part forms (position 2), or envelopes, and extra-thick paper (position 3).

D. E.

6.

Install the paper separator. A. B. Lift the rear cover. Hold the legs against the separator and place the separator tabs over the studs on the sides of the rear cover. Close the rear cover. RH-402 Installation

C. 230

7. 8. 9. 10. 11.

Set the printer next to the analyzer and the paper tray behind the printer. Attach the printer power cord to the printer. Connect the other end to the facility power source. The printer should be off. Connect the printer interface cable to the printer and the back of the analyzer. Install the paper. A. B. C. D. Move the paper lever and bail lever forward. Open the access and rear covers and feed the paper under the rear cover. Open the tractor covers and align the track feed holes on the paper with the tractor pins. Close the tractors. Turn the platen knob to feed the paper around the platen. Be sure the paper feeds underneath the black tabs in front of the tractors. To adjust the tractors: 1) 2) Lift the lock levers on both sides. Slide the tractors into position. Reference marks on the printer show the recommended left edge position for the two most common paper sizes.

E.

Note

Do not place the left edge of the paper more than 1/2 inch from the end of the platen or the printer will signal a paper out alarm.

12. 13. 14. 15. 16.

Close the rear cover and lay the paper separator flat. Open the guide wire to stop paper from curling back into the printer. Close the access cover. Paper can be fed from the bottom if the printer is placed on a stand. Refer to the printer manual for details. The control panel of the printer is used to configure the printer and its corresponding features. Refer to the operation section of the printer manual. The printer settings can be found on page 233.

Installation

RH-402

231

RIBBON CARTRIDGE

TAKE-UP KNOB

RIBBON PLATE

RIBBON SHIELD DO NOT REMOVE

Figure 212 Ribbon Cartridge Installation

ACCESS COVER

BAIL LEVER

TRACTOR COVER

LOCK LEVER

GUIDE WIRE

PAPER SEPARATOR

PAPER LEVER TRACK FEED HOLES PAPER PLATEN KNOB

PINS STUD ON/OFF SWITCH SEPARATOR TAB REAR COVER

Figure 213 Paper Installation

232

RH-402

Installation

Printer Settings
Group Font Item Print Mode Pitch Style Size Emulation Mode Graphics Paper Out Override Print Registration Operator Panel Functions Reset Inhibit Print Suppress Effective CPU Compensation Line Spacing Form Tear-Off Skip-Over Perforation Auto LF Auto CR Auto Feed XT Page Length Character Set Language Set Zero Character Parity Serial Data 7 or 8 Bits Protocol Diagnostic Test Busy Line Baud Rate DSR Signal DTR Signal Busy Time Settings Utility 10 CPI Normal Single Epson FXe Bi-directional No O Full Operation No Yes Standard 6 LPI Off No No No Invalid 11 inches Set I American Slashed None 8 Ready/Busy No SSD9600 BPS Valid Ready on Power Up 200 Milliseconds

General Control

Vertical Control

Symbol Sets

Serial I/F Option

Note

To restore the menu to its original factory settings, turn the printer off, hold down the Sel and Mode buttons, then turn the printer on again.

Installation

RH-402

233

Option Installation

Illustrations .......................................................................... 32 External Balance.................................................................... 33 Balance Interfacing....................................................... 34 Resetting the Balance ................................................... 35 Setting the Data Output Parameter ................................. 35 Data Transmit ....................................................................... 37 Installation.................................................................. 37 Data Transmit Cable Pin Assignments ......................... 38 Format Key ............................................................... 310 Data Transmit Format ................................................. 311 Gas Dose Answer Format ........................................ 311 Fusion Analysis Answer Format ................................ 312 Hot Extraction Analysis Answer Format ..................... 314 Combined Analysis Answer Format ........................... 316 Record Format ...................................................... 319 External Keyboard ............................................................... 320

Option Installation

RH-402

31

Illustrations
Figure 31......... Balance Control Panel .................................36 Figure 32......... Balance Assembly ......................................36

32

RH-402

Option Installation

External Balance

Notes

Refer to Balance Mode, page 424, to set the balance parameters and configure the analyzer to recognize the balance. If the balance and analyzer are not programmed with the same configuration parameter values, no weights may be transferred. To insure proper balance operation, balance interfacing, resetting the balance and setting the data output parameter procedures, beginning on the next page, must be performed. The following information is for the LECO four-place balance. If another balance is used, follow the instructions provided with the balance.

Option Installation

RH-402

33

Balance Interfacing
1. 2. Unpack the balance and assemble it as shown in the balance operation manual. Plug the AC adapter, supplied with the balance, into facility power. Connect the AC adapter cable to the power input jack on the rear of the balance. Adjust the balance feet to level the balance. The level bubble should be inside the circle when the balance is level. The level bubble is located on the rear of the balance. Locate the balance connector on the rear panel of the analyzer and connect one end of the balance interface cable to the balance connector. Connect the other end of the cable to the rear of the balance. To properly interface the balance with the analyzer, perform the Resetting The Balance procedure on the next page to reset the balance to the factory defaults. After the balance is reset, do not change any of the configuration codes except the one shown in this manual. The balance codes can be changed to custom configure the balance, if desired, after this procedure is completed.

3.

4.

5.

6.

34

RH-402

Option Installation

Resetting the Balance

1. Remove the hole plug on the lower front right corner of the balance and move the menu access switch to the right (figure 3-2, page 36). Turn the AC power on to the balance by pushing the power on button (figure 3-1, page 36). As soon as all the segments on the display light up, push the Tare button. The display will be blank for a few seconds and then display the menu code settings. Press F1 to display 9 in the left digit. Press Print to skip the center digit. Press F1 to display 1 as the right digit. Press Tare. Press CF. Turn the AC power off to the balance.

2.

3. 4. 5. 6. 7. 8.

Setting the Data Output Parameter

1. 2. Set the data output parameter to "Auto print regardless of stability" code 614 using this procedure. Turn the AC power on to the balance by pushing the power on button. As soon as all segments on the display light up, push the Tare button. The display will be blank for a few seconds and then display the menu code settings. Press F1 to display 6 in the left digit. Press Print to display the center digit. Press F1 to display 1 as the center digit. Press Print to display the right digit. Press F1 to display 4 as the right digit. Press Tare. Press CF. Reposition the menu access switch to the left and reinstall the hole plug.

3. 4. 5. 6. 7. 8. 9. 10.

Option Installation

RH-402

35

POWER ON CLEAR FUNCTION

TOGGLE

I/O CF

F1
i

INFORMATION TARE

TARE

TARE
PRINT

F2

Figure 31 Balance Control Panel

MENU ACCESS SWITCH

Figure 32 Balance Assembly

36

RH-402

Option Installation

Data Transmit

Installation

Note

1. 2. 3. 4. 5. 6. 7.

All character generation is coded in ASCII format.

Turn the power off to the analyzer. Locate the data transmit connector on the rear panel of the analyzer. Connect one end of the data transmit interface cable to the data transmit connector (figure 2-4, page 2-16). Connect the other end of the data transmit interface cable to the data receiving device. Configure the analyzer's output to match the peripheral device. (Refer to the Serial Ports on page 4-25.) Turn the power on to the analyzer. Use the Shift and F8 key to activate/deactivate the data transmit mode. The upper left corner of the screen displays XMIT when the data transmit mode is selected. To set the correct serial port parameters, refer to the Serial Ports on page 4-25. Select the desired format type, refer to System Configuration on page 4-22.

8. 9.

Note

For an example of the Data Transmit Format , refer to page 3-11.

Option Installation

RH-402

37

Data Transmit Cable Pin Assignments

9 Pin Connector Pin # 1 2 3 4 5 6 7 8 9 Signal Name CDCarrier Detect RDReceive Data TDTransmit Data DTRData Terminal Ready Ground DSRData Set Ready RTSRequest to Send CTSClear to Send RIRing Indicator Input Output Input Input Direction Input Input Output Output

25 Pin Adapter Pin # 1 2 3 4 5 6 7 8 20 22 Signal Name Chassis Ground TDTransmit Data RDReceive Data RTSRequest to Send CTSClear to Send DSRData Set Ready SGSignal Ground DCDCarrier Detect DTRData Terminal Ready RIRing Indicator Direction Output Input Output Input Input Input Output Input

38

RH-402

Option Installation

ASCII Character Definition Table

ACK BEL BS CAN CR DC1 DC2 DC3 DC4 DEL DLE

Acknowledge Bell, or alarm Backspace Cancel Carriage return Device control 1 Device control 2 Device control 3 Device control 4 Delete Data link escape

EM ENQ EOT ESC ETB ETX FF FS GS HT LF

End of Medium Enquiry End of transmission Escape End of transmission block End of text Form feed File separator Group separator Horizontal tab Line feed

NAK NUL RS SI SO SOH SP STX SUB SYN US VT

Negative acknowledge Null, or all zeros Record separator Shift in Shift Out Start of heading Space Start of text Substitute Synchronous idle Unit separator Vertical Tab

*American Standard Code for Information Interchange (ASCII) X3.4 - 1967 for use on tape 1967 USA Standards Institute. Reprinted by permission.

Option Installation

RH-402

39

Format Key
Commas (,) are used for character separation and are not parts of the transmission unless the comma appears in double quotes: ,. Exception: In the Record Format, fields are separated by commas as noted by ,,,. The second comma is transmitted as the field delimiter. Fields that contain a decimal point are always the same lengths although the decimal point position varies. Upper and lower case letters (excluding code symbols) and special symbols (=. +, etc.) represent actual characters transmitted.

Note

If more than one answer is transmitted at one time, the SOH transmits only at the beginning of the first answer transmitted and the EOT transmits only after the last answer is transmitted.
number of analysis (3 digit field) hours (00 to 23) minutes (00 to 60) day of month (01 to 31) year month, 3 letter representation (i.e. JAN) sample weight space start of heading carriage return line feed end of transmission start of header (HEX = 0X01) end of header (HEX = 0X04) carriage return (HEX = 0X0D) end of header (HEX = 0X0A) system channel number analysis type gas dose analysis fusion analysis hot extraction analysis combined analysis cell range low cell high cell

N h m d y A w SP SOH CR LF EOT 1- 2 - 3 - << 4- 5-# 6-# 6-0 6-1 6-2 6-3 7-# 7-0 7-1

310

RH-402

Option Installation

Data Transmit Format

Gas Dose Answer Format Line 1:
SOH 0 0 0 SOH 0 0 1 [ 0 0 2 4 Analysis Number 0 0 3 0 0 0 4 8 0 0 5 ] 0 0 6 0 0 7 0 0 8 A 0 0 9 0 0 1 0 0 0 1 1 0 0 1 2 3 Sample ID 0 1 3 1 0 1 4 0 0 1 5 0 0 1 6 0 0 1 7 9 0 1 8 0 1 9

Sample Classification 2 0 J 2 1 N 2 2 E 2 3 2 4 S 2 5 7 2 6 2 2 7 4 2 8 0 2 9 3 0 0 3 1 1 3 2 3 3 3 4 3 5 3 6 3 7 3 8 3 9 4 0

4 1 W

4 2 T

4 3

4 4 =

Sample Weight 4 4 4 4 5 6 2 7 . 8 2

4 9 3

5 0 6

5 1 4

5 2 g

5 3 C

5 4 h

5 5 :

5 6 C

Channel Name 5 5 5 6 7 h 8 a 9 n 0

6 1 #

6 2 0 CR 8 0

6 3 1 EOH 8 1

6 4

6 5 1

6 6 9

6 7 :

6 8 3

6 9 2

7 0

Time and Date 7 7 7 1 2 3 2 9 -

7 4 J

7 5 a

7 6 n

7 7 -

7 8 9

7 9 9

Line 2:
Hydrogen 0 2 0 3 H 0 4 2 0 5 0 6 = 0 7 0 8 2 0 9 . 1 0 8 1 1 0 1 2 5 1 3 p 1 4 p 1 5 m Blank 3 3 4 5 = 0 1 6 1 7 1 8 1 9

2 0 C

2 1 a

2 2 l

Calibration Factor 2 2 2 2 3 4 5 6 = 0 . 9

2 7 9

2 8 5

3 9 5

3 0

3 1 B

3 2 l

3 3 k

3 6 .

3 7 0

3 8 0

3 9 0

4 0

4 1 T

4 2 =

4 3 9

4 4 0

4 5

Time and Peak 4 4 4 6 7 8 P

4 9 =

5 0 1

5 1 6 CR 6 5

5 2 7

5 3 4 EOH 6 6

5 4

5 5 L

5 6 o

5 7 w

5 8

Cell Range 5 6 9 0 R

6 1 a

6 2 n

6 3 g

6 4 e

6 7

Option Installation

RH-402

311

Fusion Analysis Answer Format Line 1:

SOH 0 SOH 0 1 [ Analysis Number 0 0 0 0 2 4 3 0 4 8 5 ] 0 6 0 7 0 8 A 0 9 0 1 0 0 1 1 0 1 2 3 Sample ID 1 1 1 3 1 4 0 5 0 1 6 0 1 7 9 1 8 1 9

2 0 J

2 1 M

2 2 E

2 3

2 4 5

2 5 7

2 6 2

2 7 4

Sample Classification 2 2 3 3 3 8 9 0 1 2 0 0 1

3 3

3 4

3 5

3 6

3 7

3 8

3 9

4 0

4 1 W

4 2 T

4 3

4 4 =

Sample Weight 4 4 4 4 5 6 2 7 . 8 2

4 9 3

5 0 6

5 1 4

5 2 g

5 3 C

5 4 h

5 5 :

5 6 C

Channel Name 5 5 5 6 7 h 8 a 9 n 0

6 1 # CR

6 2 0

6 3 1 EOH 8 1

Time and Date 6 4 6 5 1 6 6 9 6 7 : 6 8 3 6 9 2 7 0 7 1 2 7 2 9 7 3 7 4 J 7 5 a 7 6 n 7 7 7 8 9 7 9 9

8 0

Line 2:
0 1 0 2 H 0 3 2 0 4 0 5 = 0 6 0 7 2 0 8 . 0 9 8 Hydrogen 1 1 0 0 1 5 1 2 1 3 p 1 4 p 1 5 m Blank 3 3 4 5 0 . 1 6 1 7 1 8 1 9

2 0 C

2 1 a

2 2 l

Calibration Factor 2 2 2 2 3 4 5 6 = 0 . 9

2 7 9

2 8 5

2 9 5

3 0

3 1 B

3 2 l

3 3 k

3 6 0

3 7 0

3 8 0

3 9

4 0

4 1 T

4 2 =

4 3 9

4 4 0

4 5

Time and Peak 4 4 4 6 7 8 P

4 9 =

5 0 1

5 1 6

5 2 7 CR 6 5

5 3 4

5 4

5 5 L

5 6 o

5 7 w

5 8

Cell Range 5 6 9 0 R

6 1 a

6 2 n

6 3 g

6 4 e

EOH 6 6

312

RH-402

Option Installation

Line 3:
0 1 O 0 2 u 0 3 t 0 4 g 0 5 a 0 6 s 0 7 0 8 H Outgas High and Low 0 1 1 1 1 9 0 1 2 3 I g h = 1 4 1 5 9 1 6 9 1 7 . 1 8 0 1 9 0 2 0 %

Outgas High and Low (Continued) 2 1 2 2 L 2 3 o 2 4 w 2 5 = 2 6 2 7 2 8 9 2 9 9 3 0 . 3 1 0 3 2 0 3 3 % 3 4

3 5 A

3 6 n

3 7 a

3 8 l

3 9 y

4 0 s

4 1 I

4 2 s

4 3

Analysis Low 4 4 4 4 5 6 l o w

4 7 =

4 8

4 9 9

5 0 9

5 1 .

5 2 0

5 3 0

5 4 %

Analysis High 5 6 5 7 H 5 8 i 5 9 g 6 0 h 6 1 = 6 2 6 3 9 6 4 9 6 5 . 6 6 0 6 7 0 6 8 % 6 9

Ramp 7 0 R 7 1 a 7 2 m 7 3 p 7 4 = 7 5 7 6 7 7 7 8 0

CR 7 9 7 0

EOH 8 1

Option Installation

RH-402

313

Hot Extraction Analysis Answer Format Line 1:

SOH 0 SOH 0 1 [ Analysis Number 0 0 0 0 2 4 3 0 4 8 5 ] 0 6 0 7 0 8 A 0 9 0 1 0 0 1 1 0 1 2 3 Sample ID 1 1 1 3 1 4 0 5 0 1 6 0 1 7 9 1 8 1 9

2 0 J

2 1 M

2 2 E

2 3

2 4 5

2 5 7

2 6 2

2 7 4

Sample Classification 2 2 3 3 3 8 9 0 1 2 0 0 1

3 3

3 4

3 5

3 6

3 7

3 8

3 9

4 0

4 1 W

4 2 T

4 3

4 4 =

Sample Weight 4 4 4 4 5 6 2 7 . 8 2

4 9 3

5 0 6

5 1 4

5 2 g

5 3 C

5 4 h

5 5 :

5 6 C

Channel Name 5 5 5 6 7 h 8 a 9 n 0

6 1 #

6 2 0

6 3 1

Time and Date 6 4 6 5 1 6 6 9 6 7 : 6 8 3 6 9 2 7 0 7 1 2 7 2 9 7 3 7 4 J 7 5 a 7 6 n 7 7 7 8 9 7 9 9 8 0

CR EOH 8 1 2

Line 2:
0 1 0 2 H 0 3 2 0 4 0 5 = 0 6 0 7 2 0 8 . 0 9 8 Hydrogen 1 1 0 0 1 5 1 2 1 3 p 1 4 p 1 5 m 1 6 1 7 1 8 1 9

2 0 C

2 1 a

2 2 l

2 3 =

Calibration Factor 2 2 2 2 4 5 6 7 0 . 9 9

2 8 5

2 9 5

3 0

3 1 B

3 2 l

3 3 k

3 4 =

Blank 3 3 5 6 0 .

3 7 0

3 8 0

3 9 0

4 0

4 1 T

4 2 =

4 3 9

4 4 0

4 5

Time and Peak 4 4 4 6 7 8 P

4 9 =

5 0 1

5 1 6

5 2 7 CR 6 5

5 3 4

5 4

5 5 L

5 6 o

5 7 w

5 8

Cell Range 5 6 9 0 R

6 1 a

6 2 n

6 3 g

6 4 e

EOH 6 6

314

RH-402

Option Installation

Line 3:
0 1 0 2 0 3 0 4 0 5 0 6 0 7 Space 0 0 8 9 1 0 1 1 1 2 1 3 1 4 1 5 1 6

Purge Time 1 7 P 1 8 u 1 9 r 2 0 g 2 1 e 2 2 2 3 T 2 4 i 2 5 m 2 6 e 2 7 = 2 8 2 9 9 3 0 0 3 1 3 2

3 3

3 4

3 5 A

3 6 n

3 7 a

3 8 l

3 9 y

4 0 s

4 1 i

Analysis Low and High 4 4 4 4 4 2 3 4 5 6 s l o w

4 7 =

4 8

4 9

5 0 9

5 1 9

5 2 .

5 3 0

5 4 0

5 5 %

Analysis Low and High (Continued) 5 6 5 7 H 5 8 I 5 9 g 6 0 h 6 1 = 6 2 6 3 6 4 9 6 5 9 6 6 . 6 7 0 6 8 0 6 9 % CR 8 0 EOH 8 1 8 2

Ramp 7 0 7 1 R 7 2 a 7 3 m 7 4 p 7 5 = 7 6 7 7 7 8 7 9 0

Option Installation

RH-402

315

Combined Analysis Answer Format Line 1:

SOH 0 SOH 0 1 [ Analysis Number 0 0 0 0 2 4 3 0 4 8 5 ] 0 6 0 7 0 8 A 0 9 0 1 0 0 1 1 0 1 2 3 Sample ID 1 1 1 3 1 4 0 5 0 1 6 0 1 7 9 1 8 1 9

2 0 J

2 1 M

2 2 E

2 3

2 4 5

2 5 7

2 6 2

2 7 4

Sample Classification 2 2 3 3 3 8 9 0 1 2 0 0 1

3 3

3 4

3 5

3 6

3 7

3 8

3 9

4 0

4 1 W

4 2 T

4 3

4 4 =

Sample Weight 4 4 4 4 5 6 2 7 . 8 2

4 9 3

5 0 6

5 1 4

5 2 g

5 3 C

5 4 H

5 5 :

5 6 C

Channel Name 5 5 5 6 7 h 8 a 9 n 0

6 1 # CR

6 2 0

6 3 1 EOH 8 1

Time and Date 6 4 6 5 1 6 6 9 6 7 : 6 8 3 6 9 2 7 0 7 1 2 7 2 9 7 3 7 4 J 7 5 a 7 6 n 7 7 7 8 9 7 9 9

8 0

Line 2:
0 1 S 0 2 U 0 3 R 0 4 F 0 5 = 0 6 0 7 0 Surf Result 0 0 1 8 . 9 0 0 4 1 1 2 1 2 1 3 P 1 4 P 1 5 M 1 6 1 7 1 8 p 1 9 = Surf Peak 2 2 2 0 7 1 2 2 3

2 4

2 5 B

2 6 U

2 7 L

2 8 K

2 9 =

3 0

3 1 0 CR 4 8

Bulk Result 3 3 2 3 . EOH 4 9 0

3 4 8

3 5 7

3 6

3 7 P

3 8 P

3 9 M

4 0

4 1

4 2 p

4 3 =

Bulk Peak 4 4 4 1 5 6

4 6

4 7

316

RH-402

Option Installation

Line 3:
0 1 T 0 2 O 0 3 T 0 4 A 0 5 L 0 6 = 0 7 0 8 2 Hydrogen 0 1 9 0 . 8 1 1 0 1 2 5 1 3 1 4 P Blank 2 8 9 2 9 5 3 0 5 3 1 3 2 B 3 3 l 3 4 k 3 5 = 3 6 0 3 7 . 3 8 0 3 9 0 4 0 0 1 5 P 1 6 M 1 7 1 8

Calibration Factor 2 1 C 2 2 a 2 3 l 2 4 = Time 4 4 9 2 5 0 2 6 . 2 7 9

4 1

4 2 T

4 3 =

4 5 0

4 6

4 7

4 8

4 9 L

5 0 o

5 1 w

Cell Range 5 5 5 2 3 4 R

5 5 a

5 6 n

5 7 g

5 8 e

CR EOH 5 6 9 0

Line 4:
Outgas High 0 1 O 0 2 u 0 3 t 0 4 g 0 5 a 0 6 s 0 7 0 8 H 0 9 i 1 0 g 1 1 h 1 2 = 1 3 1 4 1 1 5 0 1 6 0 1 7 . 1 8 0 1 9 0 2 0 % 2 1 2 2

2 3 S

2 4 u

2 5 r

2 6 f

2 7 a

2 8 c

2 9 e

3 0

Surface Analysis Low 3 3 3 3 3 1 A 2 n 3 a 4 l 5 y

3 6 s

3 7 i

3 8 s

3 9

4 0 l

4 1 o

4 2 w

Surface Analysis Low (Continued) 4 3 = 4 4 4 5 4 6 6 4 7 1 4 8 . 4 9 0 5 0 0 5 1 % 5 2 5 3

5 4 F

5 5 u

5 6 r

5 7 n

5 8 a

5 9 c

6 0 e

6 1

6 2 o

Furnace on Time 6 6 6 6 3 n 4 5 T 6 i

6 7 m

6 8 e

6 9 =

7 0

7 1

7 2

7 3 1

7 4 5

CR EOH 7 7 5 6

Option Installation

RH-402

317

Line 5:
0 1 B 0 2 u 0 3 l 0 4 k 0 5 0 6 A 0 7 n Bulk Analysis Low 0 0 1 1 8 9 0 1 a l y s 1 2 i 1 3 s Bulk High 2 7 2 8 H 2 9 I 3 0 g 3 1 h 3 2 = 3 3 3 4 3 5 9 3 6 9 3 7 . 3 8 0 3 9 0 4 0 % 1 4 1 5 l 1 6 o 1 7 w 1 8 =

Bulk Analysis Low (Continued) 1 9 2 0 2 1 9 2 2 9 2 3 . 2 4 0 2 5 0 2 6 %

4 1

4 2 R

4 3 a

4 4 m

Ramp 4 4 5 6 p =

4 7

4 8

4 9

5 0 0

5 1

5 2 M

Maximum Furnace on Time 5 5 5 5 5 3 4 5 6 7 a x i m u CR 7 4 7 5 7 6 1 7 7 0 7 8 0 7 9

5 8 m

5 9

Maximum Furnace on Time (Continued) 6 0 F 6 1 u 6 2 r 6 3 n 6 4 . 6 5 6 6 o 6 7 n 6 8 6 9 T 7 0 i 7 1 m 7 2 e 7 3 =

EOH 8 0 8 1

318

RH-402

Option Installation

Record Format Line 1:

SOH 0 SOH 0 1 4 Analysis 0 0 2 0 3 8 0 4 , 0 5 A 0 6 0 0 7 0 0 8 0 0 9 3 Sample ID 1 1 0 1 1 0 1 2 0 1 3 0 1 4 9 1 5 ,

1 6 J

1 7 M

1 8 E

1 9

2 0 5

2 1 7

2 2 2

2 3 4

Sample Classification 2 2 2 2 2 4 5 6 7 8 0 0 1 Operator 4 4 4 6 7 8

2 9

3 0

3 1

3 2

3 3

3 4

3 5

3 6 ,

3 7 O

3 8 P

3 9 E

4 0 R

4 1 A

4 2 T

4 3 O

4 4 R

4 5

4 9

5 0

5 1

5 2

5 3

5 4

5 5

5 6

5 7 ,

Weight 5 8 5 9 2 6 0 . 6 1 2 6 2 3 6 3 6 6 4 4 6 5 ,

System Channel Number 6 6 1 6 7 , 6 8 C 6 9 h

Channel Name 7 0 a 7 1 n 7 2 7 3 # 7 4 0 7 5 1 7 6 ,

Combined Analysis 7 7 3

Time and Date 7 8 , 7 9 1 8 0 9 8 1 : 8 2 3 8 3 2 8 4 8 5 2 8 6 9 8 7 8 8 J 8 9 a 9 0 n 9 1 9 2 9 9 3 9 9 4 ,

9 5

9 6 0

9 7 .

Answer 9 9 8 1 9 2

0 0 9

0 1 ,

0 2

0 3 0

Surf Answer 0 0 0 4 3 5 0 6 4

0 7 2

0 8 ,

0 9

1 0 0

Bulk Answer 1 1 1 1 . 2 0 3 8

1 4 7

1 5 ,

1 7 1

1 8 .

Calibration 1 2 2 9 0 1 0 0 1

2 2 9

2 3 ,

2 4 0

2 5 .

Blank 2 2 6 7 0 0

2 8 0

2 9 ,

3 0

3 1

Absolute Peak 3 3 3 2 3 4 1 6

3 5 ,

3 6

3 7

Bulk Peak 3 3 8 9 1 Bulk Time

4 0 6

4 1 ,

4 2

4 3

Surf Peak 4 4 4 5

4 6 7

4 7 ,

4 8

4 9

Analysis Time 5 5 5 0 2 H2 Range 6 6 1 1 7 2 0 Low Cell 6 6

5 3 , EOH 6 7

Surf Time 5 8 0 5 9 , 6 0 6 1 6 2 6 3 7 6 4 0 6 5 ,

5 4

5 5

5 6 2

5 7 0

Option Installation

RH-402

319

External Keyboard
1. 2. Connect the keyboard cable to the connector on the back panel of the analyzer. If the optional keyboard bracket is being used: A. B. Slide the keyboard into the bracket from the rear (open) edge. Hook the keyboard bracket under the front edge of the cabinet frame.

320

RH-402

Option Installation

System Setup

Illustrations .......................................................................... 42 Controls and Indicators........................................................... 43 Analyzer..................................................................... 43 Furnace...................................................................... 44 Printer........................................................................ 44 System Overview................................................................... 46 Menus ........................................................................ 46 Menu Organization Chart......................................................... 48 Initial Power Up ................................................................... 411 User/Superuser Log-In Option...................................... 413 System Check..................................................................... 414 Ambient Monitor ........................................................ 415 Normal Variations.................................................. 416 Gas Flow Adjustments................................................. 417 System Leak Check.................................................... 418 Barometric Pressure ................................................... 420 Security Code............................................................ 421 System Controls .................................................................. 422 System Configuration.................................................. 422 Definitions............................................................ 423 Balance Mode ............................................................ 424 Serial Ports............................................................... 425 Definitions............................................................ 426 Set Clock.................................................................. 427

System Setup

RH-402

41

Illustrations
Figure 41......... Controls and Indicators...............................45 Figure 42......... Keyboard .................................................47 Figure 43......... Oven Compartment ....................................417

42

RH-402

System Setup

Controls and Indicators

Analyzer

Note

Refer to figure 4-1, page 45, for control and indicator locations.

Power On/Off SwitchSwitches power on and off to the analyzer. Also acts as a 5 amp circuit breaker. Gas On/Off SwitchSwitches on the incoming carrier gas flow and the pump. Incoming N2 Pressure GaugeIndicates the pressure of the incoming carrier gas (40 psi/2.76 bars). Pump Pressure GaugeIndicates the pressure at the outlet of the pump (15 to 45 psi/1.04 to 3.12 bars). Flow From Furnace RotameterUsed to measure the flow rate of the gases leaving the combustion tube going to the detector (260 to 300 ml/min.) Flow To Furnace Rotameter And Adjustment KnobUsed to measure and adjust the flow rate of the carrier gas entering the combustion tube (950 ml/min.). Oven Heater On LEDThe TC cell is located in an oven that must be held at a constant temperature. This LED glows whenever the heating element inside the oven is on. Gas On LEDThis LED glows when the gas is on and the pump is operating. Keyboard Select SwitchThis switch enables the operator to choose either the built-in keyboard or the optional external keyboard. Internal BalanceThe balance is used to provide sample weight inputs to the analyzer. These weights are presented on the monitor display. Flat Panel DisplayThe monitor display is used as a visual communications link between the operator and the instrument. AlarmThe will make an audible beep when the alarm is triggered. KeyboardsEither the built-in keyboard or the optional external keyboard is used to enter data or to respond to prompts shown on the monitor display. Only one keyboard may be used at a time by selection with the keyboard switch.

System Setup

RH-402

43

Furnace

Note

Refer to figure 4-1, page 45, for control and indicator locations.

Power On/Off SwitchSwitches power on and off to the induction furnace. Also acts as a 30-amp circuit breaker. Loader Control SwitchControls the sample loading block assembly and the furnace pedestal. Plate Current MeterIndicates oscillator tube plate current in DCmA.

Printer
Printer (not shown)The printer is programmed to print out analysis data information presented on the display, and buffer or data plots.

44

RH-402

System Setup

769-398 INCOMING N2 PRESSURE GAUGE 0-60 PSI 781-786 FLOW TO FURNACE ROTAMETER 775-601 REAGENT TUBES 603-956 CATALYST HEATER ASSEMBLY 614-463 FLAT PANEL DISPLAY ASSEMBLY 608-586 SPEAKER ASSEMBLY

769-398 PUMP PRESSURE GAUGE 0-60 PSI 780-587 FLOW FROM FURNACE ROTAMETER 603-711 PLATE CURRENT METER

783-592 SAMPLE LOADING ASSEMBLY

608-590 KEYBOARD ASSEMBLY

700-692-010 DISK DRIVE 775-625 LOADER CONTROL SWITCH

614-570 POWER SWITCH 608-592 OPTIONAL KEYBOARD BRACKET 605-980 OPTIONAL EXTERNAL KEYBOARD 602-374 KEYBOARD SELECT SWITCH 775-625 GAS ON/OFF SWITCH 774-086 OVEN HEATER LED 614-326 INTERNAL BALANCE AND 780-460 COVER 774-086 GAS ON LED 614-314 ON/OFF POWER SWITCH CIRCUIT BREAKER

Figure 41 Controls and Indicators

System Setup

RH-402

45

System Overview

Menus
Function KeysThe function keys are shown as F keys and are along the top of the menu bar. Menu LineThe menu line is the area immediately below the Fkeys and explains what the corresponding F-key function is. These menu item change depending upon the operators previous and current selections.
F1 F2 F3 F4 F5 F6 F7 F8 -EXIT-

Analyze MenuThe analyze menu is the first to appear after accessing the system and contains all of the steps necessary for weighing the sample, logging in the sample, entering the weight, selecting the analysis channel, and beginning an analysis.
F1 Sample Log-in F2 Balance Tare F3 Manual Weight F4 Remove Weight F5 Analyze F6 Channel Select F7 F8 More

Diagnostic MenuThe diagnostics menu contains procedures for testing the system, observing the various operating parameters, printing and plotting data buffers, defining system securities, and logging-off.
F1 System Check F2 Ambient Monitor F3 Data Buffers F4 F5 Security Area F6 F7 F8 Return

System Update MenuThe system update menu contains all the functions for calibrating the instrument, determining blanks, entering system constants, configuring the system, making data observations and calculations, and examining system alarms.
F1 Calibration F2 Blanks F3 Constants F4 System Controls F5 Counters F6 Stack Routines F7 Alarms F8 More

46

RH-402

System Setup

*
0

Function [F] Keys..................................Used to select functions displayed in corresponding on-screen function boxes. Cursor - Control Keys ............................Used to move the cursor in the direction indicated by the arrow on each key. Number Keys .......................................Used to enter numbers. Return/Enter Key ..................................Used to enter keyed-in values. Escape [ESC] Key .................................Acts as an exit key from subroutines. Print Screen Key ...................................Used to print menus displayed on screen. Graphics characters do not print. Shift/F6...............................................Prints out the last analysis result. Shift/F7...............................................Turns the printer on/off. Shift/F8...............................................Turns data transmit on/off. Fn. .....................................................Used to select secondary characters.

Figure 42 Keyboard

System Setup

RH-402

47

Menu Organization Chart

Analyze [F1] Sample Log-In [F1] Select ID Code [F2] Previous Line [F3] Next Line [F4] Clear [F5] Out Of Sequence [F6] Standard Check [F7] Gas Dose [F8] Exit [F2] Balance Tare [F3] Manual Weights [F4] Remove Weights [F5] Analyze [F6] Channel Select [F7] Transmit Results (Pop-Up) [F8] More System Update [F1] Calibration [F1] Standard Calibration [F2] Gas Dose Calibration [F3] Manual Calibration [F5] Balance Calibration [F6] Set Barometric Pressure [F8] Exit [F2] Blanks [F1] Standard Blank [F2] Manual Blank [F8] Exit [F3] Constants [F1] Standard Constants [F2] Gas Dose Constants [F3] SPC Constants [F5] Break Points [F8] Exit

48

RH-402

System Setup

[F4] System Controls

[F1] System Configuration [F2] Balance Mode [F3] Serial Ports [F4] Set Clock [F8] Exit

[F5] Counters

[F1] Print [F2] Previous [F3] Next [F4] Restore Values [F5] Edit Limits [F6] Edit Elapsed [F8] Exit

[F6] Stack Routines

[F1] Weight Stack [F2] Answer Stack [F3] Transfer and Delete [F4] Restore Deletion [F5] Statistics [F7] Transmit Stack (Optional) [F8] Exit

[F7] Alarms

[F1] Print [F2] Reset/Clear [F6] Next Page [F8] Exit

[F8] More Diagnostics [F1] System Check [F1] Leak Test [F2] Manual I/O Test [F4] Sequence Test [F5] Auto I/O Test [F8] Print [F2] Ambient Monitor

System Setup

RH-402

49

[F3] Data Buffer

[F1] Screen Plot [F2] Buffer Print [F8] Exit

[F5] Security Area

[F1] Linearize [F4] Exit to DOS [F6] Security Code [F7] System Files [F8] Exit

[F8] Return

410

RH-402

System Setup

Initial Power Up

WARNING

ELECTRICAL SHOCK HAZARD This equipment uses 230 V~. Contact with this voltage can be lethal. Before servicing the equipment, disconnect it from the power source.

1. 2. 3. 4.

The analyzer and furnace power switch should be in the off position. Connect the analyzer to facility power. Lift the lever on the disk drive and remove any shipping or packing protection from the disk drive. Turn on the gas supplies and set the delivery nitrogen to 40 psi (2.76 bars) and the hydrogen pressure to 40 psi (2.76 bars). Set the analyzer power switch to the on position. Press the gas key to switch the carrier gas (nitrogen) flow on. Confirm that the incoming pressure (N2 ) gauge on the analyzer front panel indicates 40 psi (2.76 bars).

5. 6. 7.

Note

From this point on, if the system needs to be reset, simultaneously press the CTRL, ALT, and DEL keys on the external keyboard or simultaneously press the CTRL, Shift, and 5 keys on the built-in keyboard.

System Setup

RH-402

411

8.

Once the instrument is turned on, it loads the program, runs through a self-test, and displays the video select menu. When the video select menu appears, select F1 for black and white video, F4 for color video or F8 to exit.

Note

If any keys are hit during boot-up, a prompt displays to allow the operator to choose flat screen or color monitor. After one of these keys is pressed, the analyze menu is displayed. Set the furnace power switch to the on position. The instrument needs a 30 minute warm-up before the system check can be completed. After the video selection is made the analyze screen will appear.

9. 10. 11.

412

RH-402

System Setup

User/Superuser Log-In Option

Notes

Initially the instrument is not configured for superuser login; access to all areas is permitted for all users. Refer to the Security Code procedure, page 421, to set up the instrument for user/superuser access.

If the instrument is configured for superuser access, the instrument prompts the operator to choose user or superuser. If the F1 (User) key is pressed, the analyze menu is displayed. If the F4 (Superuser) key is pressed, the instrument prompts for entry of the password. This password was initially entered in the system security procedure. For more information, see Security Code, page 421.

System Setup

RH-402

413

System Check

Notes

All steps in the installation and initial power-up sections must be completed before performing these procedures. Gas supplies must be onthe nitrogen and hydrogen supplies should be set to 40 psi (2.76 bars). The analyzer and furnace power switches must be in the on position.

414

RH-402

System Setup

Ambient Monitor
1. 2. 3. Set the gas switch to the on position. With the analyze menu displayed, press the F8 (More) key twice to display the diagnostics menu Press the F2 (Ambient Monitor) key to display the temperature, voltages, and pressure used in the system.

Note

Before performing any system check procedures, be sure that these ambient monitor values fall within the range limits given here.
Ambient Monitor Parameter Ground Reference 5 Volt Reference +15 Volt Supply -15 Volt Supply 24 Volt Supply TC Supply Current TC Low Range TC High Range Oven Heater Catalyst Heater Doser Temperature System Pressure Nominal Value 0.00 Counts 5.0 Volts 15.00 Volts -15.00 Volts 24 Volts 0.060 Amps 1.0 Volt 0.05 Volt 45oC 600oC 25oC 747 mm Range 0.00 4.5 to 5.5 13.5 to 16.5 -13.5 to -16.5 21.6 to 26.4 0.055 to 0.065 0.1 to 2.0 0.01 to 2.0 40 to 50 575 to 625 Variable Variable

4.

Press the F1 (Print) key to receive a printed copy of the ambient monitor display. If any values are out of range, refer to the Electronics Adjustments section, beginning on page 9-1, the Alarm Table, page 571, or the System Update Menu, page 46. To better observe a monitor point that appears to be changing values, press the F4 (Monitor Channel) key. The lowest and highest levels monitored appear to the right of the point being monitored. Press the F2 (Previous Channel) or F3 (Next Channel) key to move the cursor up or down the list to observe the high and low values for each parameter. Press the F4 (Monitor All) key to display the high and low values for all the parameters. Press the F5 (Reset Counters) key to update the high and low parameters for the value(s) being observed. Press the F8 (Exit) key to return to the analyze menu.

5.

6.

7. 8. 9.

System Setup

RH-402

415

Normal Variations Parameter TC Cell Output Oven Temperature Catalyst Heater Temperature Gas Purifier Temperature System Pressure Variation <0 .010 volts 1o C 1o C 1o C 1 mm Time 60 seconds 60 seconds 60 seconds 60 seconds 60 seconds

Note

These variations are for the ambient monitor nominal value range limits shown in the table on the previous page.

416

RH-402

System Setup

Gas Flow Adjustments

1. 2. Turn on the front panel gas switch. Confirm that the incoming pressure (left) gauge reads 40 psi (2.76 bars) and the pump pressure gauge reads approximately 40 psi (2.76 bars). Use the rotameter adjustment knob, figure 4-1, page 4-5, to set the nitrogen flow to the furnace (left rotameter) at the line on the rotameter (1 l/min). Set the right rotameter (measure flow), figure 4-1, page 4-5, to the line indicated on the rotameter (300 ml/min). This flow is adjusted with the flow controller in the oven compartment (figure 4-3, page 417) that is accessed through the plugged hole in the oven compartment side panel.

3.

4.

FLOW CONTROLLER

ADJUSTMENT SCREW

Figure 43 Oven Compartment

System Setup

RH-402

417

System Leak Check

Notes

This test must be performed at the time of initial installation and prior to analyzing samples. It is recommended that the system leak check be accomplished at the start of each workday. The criterion for system leak check pass/fail is a 5 mmHg per minute loss. If a leak is present, Gas Leak In System will appear on the display. If a pass condition exists, System Leak Check OK will appear on the display. With the analyze menu displayed, press the F8 (More) key to display the system update menu. With the system update menu displayed, press the F8 (More) key to display the diagnostic menu. With the diagnostic menu displayed, press the F1 (System Check) key and then F1 (Leak Check) again. The monitor will display the following screen.
Printer: NR Gas -OFFChan #01 15:22:40 19 Dec 99

1. 2. 3.

Leak Check 45 Second System Delay Current Pressure (mm Hg) System Timeout (seconds) 1150.0 30

F1 Restart

F2

F3

F4

F5

F6

F7

F8 -Exit-

418

RH-402

System Setup

4.

The display will be live, that is, the timer will be counting down from 45 seconds and the current pressure will display the current system pressure. This portion of the test is to establish an equilibrium starting point. After the 45 second system time-out, the monitor will display the following screen.

5.

The arrow on the right of the display will indicate the system status. The elapsed time shown in the example will continue. If the leak check fails, press the F1 (Restart) key to test the system again. If it continues to fail, look for leaks in the system. If the leak check is satisfactory, press the F8 (Exit) key to terminate the test. Press the gas key to turn the gas back on.

6.

7. 8.

System Setup

RH-402

419

Barometric Pressure

Notes

Since barometric pressure affects gas dosing, the correct barometric pressure must be entered. If it is necessary to adjust the pressure reading for altitude, refer to the Barometric Pressure procedure, page 710, for more information.

1. 2. 3.

With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F1 (Calibration) key. Press the F6 (Barometric Pressure) key. The following screen will appear.

4.

Enter the current barometric pressure in mm hg, then press the Enter key. The analyze screen will appear.

420

RH-402

System Setup

Security Code

Note

Entry of a security password using this procedure will require the security password to be entered before access as a superuser is permitted. With the analyze menu displayed, press the F8 (More) key to display the system update menu. With the system update menu displayed, press the F8 (More) key to display the diagnostic menu. With the diagnostic menu displayed, press the F6 (Security Code) key. The monitor will display:

1. 2. 3.

4.

Enter any alphanumeric security code that fits between the brackets on the display.

Note

The security code should be written down by the supervisor as it will allow/forbid future entry of the superuser procedure. After the new security password is recorded by the supervisor, press the Enter key. Press the F8 (Exit) key anytime before the enter key to exit this procedure and return to the analyze menu.

5. 6.

System Setup

RH-402

421

System Controls

System Configuration

Notes

1. 2. 3.

This procedure permits the operator to select values for system parameters. Before editing, refer to the System Configuration Definitions, page 423. With the analyze menu displayed, press the F8 (More) key once to display the system update menu. Press the F4 (System Controls) key. Press the F1 (System Configuration) key. The following screen will be displayed.

4.

Use the F2 (Previous Value) and F3 (Next Value) keys to move the highlighted cursor line. The parameter that is highlighted can be edited. To edit, enter the value on the keyboard (for Yes or No configurations, press 1 for Yes and 0 for No) and press Enter. Press the F5 (Reset Values) key to restore the last saved values, or press the F1 (Print) key to receive a printed record of the new configuration. Press the F8 (Exit) key to return to the analyze menu. Exiting saves all changes.

5.

6.

422

RH-402

System Setup

Definitions Database Record LimitWhen the maximum number is reached the database must be transferred to disk. Range: 500 to 65,000. Print SpacingPermits the operator to select the number of blank lines between printed analysis results. Selections: 0, 1, 2, or 3. Automatic PlottingPermits the operator to print a plot of the element concentration level after analysis. Selections: On or Off. Enable Keyboard BeepPermits the operator to turn the keyboard beeper on or off. Selections: On or Off.

Note

Disabling the keyboard beep does not disable the alarm beep.

Data Transmit Format Permits the operator to select the transmitted data format. Selections: Record or Answer.

Note

Refer to Data Transmit Format , page 311, for more information.

System Setup

RH-402

423

Balance Mode

Notes

This procedure permits the operator to select the balance type used with the instrument. * LECO Built-In Balance (3 place) * LECO LB-80 Balance (4 place) * LECO 150/250/350/ Balance, Internal Weight Entry * LECO 150/250/350/ Balance, External Weight Entry Before editing, determine which balance type is interfaced with the instrument. With the analyze menu displayed, press the F8 (More) key once to display the system update menu. Press the F4 (System Controls) key. Press the F2 (Balance Mode) key. The following screen will be displayed.

1. 2. 3.

4.

Press F2 (Previous Line) key or F3 (Next Line) key to select the desired balance type. Press Enter to save the change. Press F8 (Exit) key to return to the analyze menu. Exiting saves all changes.

5.

424

RH-402

System Setup

Serial Ports
Notes

1. 2. 3.

This procedure configures the serial ports for use with an external peripheral device. Two serial ports are available, Comm Port 1 and Comm Port 2. With the analyze menu displayed, press the F8 (More) key once to display the system update menu. Press the F4 (System Controls) key. Press the F3 (Serial Ports) key. The following screen will be displayed.

4. 5. 6.

Press F1 (Print) key to receive a printout of the serial port configurations on the system printer. Press F2 (Previous Line) key or F3 (Next Line) key to select the desired parameter to change. Press F4 (Select) key to select the parameter value. A. B. Press F6 (Comm Port 1) to change the parameter values of serial port 1. Press F7 (Comm Port 2) to change the parameter values of serial port 2.

7.

Press F8 (Exit) key to return to the analyze menu. Exiting saves all changes.

System Setup

RH-402

425

Definitions Baud RatePermits the operator to select the data transmission speed in bits per second. Selections: 110, 150, 300, 600, 1200, 2400, 4800, and 9600 bps. ParityPermits the operator to select the method of error checking used. Selections: None, Odd, Even, Marking, or Spacing. Stop BitsPermits the operator to select the number of bits that are used to signal the end of a transmitted data byte. Selections: 1 or 2. Data BitsPermits the operator to select the number of bits per byte for data that will be transmitted. Selections: 7 or 8. HandshakePermits the operator to select the type of handshaking used between the instrument and the peripheral device. Selections: None or XON/XOFF.

426

RH-402

System Setup

Set Clock

Notes

1. 2. 3.

The clock operates in the twenty-four format. Hours must be entered from one to twenty-four. Both the time and date will be displayed on the upper line of the analyze screen.

With the analyze menu displayed, press the F8 (More) key once to display the system update menu. Press the F4 (System Controls) key. Press the F4 (Set Clock) key. The following screen will be displayed.

4. 5.

At the prompt, enter the time as HH:MM:SS then press enter. At the prompt, enter the date as MM-DD-YY. Then press enter, the analyze screen will appear and changes will be saved. Press F8 (Exit) to return to the analyze screen without changing the time or date.

6.

System Setup

RH-402

427

Operation

Illustrations .......................................................................... 54 Sample Log-In ...................................................................... 55 Standard Check Sample Log-In....................................... 57 Out Of Sequence Log-In ................................................ 58 Weight Entry ............................................................... 59 Internal Balance (AWT)Automatic Procedure .............. 59 External Balance (MWT)Manual Weight Procedure..... 510 Interfaced BalanceAutomatic Procedure .................. 510 Remove Weight Procedure ........................................... 511 Channel Select Procedure ............................................ 512 Transmit Results........................................................ 513 Crucibles ............................................................................ 514 Sample Preparation.............................................................. 516 Sample Type ............................................................. 516 Sample Size .............................................................. 517 Constants Procedure ............................................................ 518 Standard Constants.................................................... 519 Definitions............................................................ 520 Gas Dose Constants ................................................... 521 Definitions............................................................ 522 S.P.C. Constants........................................................ 523 Definitions............................................................ 524 Analysis Procedure ............................................................... 525 Before Analysis .......................................................... 525 Small Samples ...................................................... 526 Blank Determination .............................................. 527 Gas Dosing........................................................... 528 Analysis.................................................................... 529 After Daily Analysis ................................................ 532

Operation

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51

Calibration Procedures .......................................................... 533 Standard Calibration ................................................... 534 Gas Dose Calibration................................................... 537 Manual Calibration...................................................... 540 Database Calibration................................................... 541 Blank Procedures ................................................................. 543 Hydrogen Blank ......................................................... 543 Manual Blank............................................................. 546 Database Blank.......................................................... 547 Data Buffers Procedures........................................................ 549 Screen Plot ............................................................... 549 Print Buffer ............................................................... 551 Counters Procedure .............................................................. 552 Stack Procedures ................................................................. 554 Weight Stack............................................................. 554 Answer Stack ............................................................ 555 Database Option ................................................... 558 Transfer and Delete.................................................... 559 Database Option ................................................... 561 Restore Deletion ........................................................ 562 Statistics .................................................................. 563 Database Option ................................................... 566 Transmit Stack .......................................................... 567 Database Option ................................................... 569 Alarms Procedure................................................................. 570 Alarm Table ........................................................................ 571 Analysis Programs................................................................ 575 Hot Extraction AnalysisProcedure H............................. 576 Fusion AnalysisProcedure F ....................................... 577 Combined AnalysisProcedure C .................................. 578

52

RH-402

Operation

Analysis Constants............................................................... 579 Hot Extraction AnalysisProcedure H............................. 579 Fusion AnalysisProcedure F ....................................... 580 Combined AnalysisProcedure C .................................. 581 Surface Analysis .................................................... 581 Bulk Analysis ........................................................ 581 Gas Dose .................................................................. 583 Analysis Parameters ............................................................. 584 Furnace Power Graphs .......................................................... 585

Operation

RH-402

53

Illustrations
Figure 51......... Crucible Position........................................515 Figure 52......... Typic al Aluminum Sample ...........................516 Figure 53......... Plate DCmA vs. Temperature .......................585 Figure 54......... % Power vs. Temperature ...........................586

54

RH-402

Operation

Sample Log-In

Notes

The sample log-in procedure allows the operator to enter the ID code, classification, and operator name. The select ID code function provides for storage and retrieval of eight predetermined ID codes. * The ID code allows the operator to enter a name for each sample, such as a heat number, department name, etc. The classification feature is used to categorize samples by grade, etc. Operator log-in allows the operator name to be entered for each sample.

* *

The element windows and display area appear on the right on most screens. The element windows display the answer of the last/current analysis, the display area shows data related to the last /current analysis. Press Clear to erase the values being entered (ID Code, Classification, etc.). The (Shift/4) and (Shift/6) keys move the cursor left and right, the (Shift/8) and (Shift/2) keys move the cursor up and down. With the analyze menu displayed, press the F1 (Sample Log-In) key. The display will be similar to the following example.

1.

Operation

RH-402

55

2.

To edit or choose an ID code, press the F1 (Select ID Code) key. Each time this key is pressed, the highlighted cursor line moves down one row.

Note

At any point during the selection/editing process, pressing the F8 (Exit) key will take the highlighted/edited information and display it on the edit line of the analyze menu. A classification, on the same line as the highlighted ID code, can be edited by pressing the F2 (Previous) key. This moves the cursor line to classification in the right column. To edit the operator name, press the F2 (Previous) key again. The entire right column toggles from classification to operator. The F3 (Next) key has the same function as the F2 (Previous) key, except it moves the edit block from ID code to operator to classification. Press the Enter key to store the sample weight and ID information in the weight stack. (The area in memory that stores ID codes and sample weights until they are analyzed). If more than one sample with the same ID code, classification, and operator name will be analyzed, the sample log-in information only needs to be entered once and the samples can be placed in the stack through one of the weight procedures. Press the F8 (Exit) key to return to the analyze menu.

3.

4.

5.

6.

7.

8.

56

RH-402

Operation

Standard Check Sample Log-In

Note

Standard check operates in conjunction with SPC constants that define an acceptable range for a specific standard. When an answer is out-of-range a message prints with the answer. With the analyze menu displayed, press the F1 (Sample Log-In) key. Press the F6 (Standard Check) key to highlight the standard check ID code. Enter any edits, then press the F8 (Exit) key to return to the analyze menu. Press either the F2 (Balance Tare) or F3 (Manual Weight) key to enter the standard sample weight. Refer to Weight Entry, page 59, for more information. Press the enter key to place the standard check in the weight stack.

1. 2. 3. 4.

5.

Operation

RH-402

57

Out Of Sequence Log-In

Note

1. 2. 3. 4.

A sample entered out of sequence, can be a standard check.

With the analyze menu displayed, press the F1 (Sample Log-In) key. Press the F5 (Out Of Sequence) key to highlight the out of sequence ID code. Enter any edits, then press the F8 (Exit) to return to the analyze menu. Press either the F2 (Balance Tare) or F3 (Manual Weight) key to enter the weight. Refer to Weight Entry, page 59, for more information. Press the Enter key to place the sample at the top of the weight stack. Only one out of sequence sample can be in the weight stack at any time.

5.

58

RH-402

Operation

Weight Entry
Balance selections are chosen in the system configuration procedure. Up to 100 samples can be stored in the weight stack. The next five samples and the last sample in the weight stack are displayed on the left side of the analyze menu screen. With the exception of out of sequence, samples are stored and processed on a first in/first out basis. The automatic and manual weight procedures can also be used with a separate external balance or an interfaced external balance. Refer to the System Configuration procedure, page 422, to set the balance option. It is the operators responsibility to arrange the samples to match the order of the weight stack and organize them so that they can be identified.

Internal Balance (AWT)Automatic Procedure 1. Place an empty pan on the balance and then press the F2 (Balance Tare) key. The monitor displays -Tare- and the weight should be 0.000 g when the display stabilizes. Place sample on balance pan. When the weight stabilizes, press the Enter key. The ID code and its corresponding weight are now stored in the stack. Remove the sample from the balance. If the same ID code is used for additional samples, they can be added to the weight stack without returning to the sample log-in screen by following steps 1 through 4. If additional samples with a different ID code will be added to the stack it is necessary to return to the sample log-in screen.

2. 3.

4. 5.

6.

Operation

RH-402

59

External Balance (MWT)Manual Weight Procedure 1. Press the F3 (Manual Weight) key. The display defaults to a weight of 5.0000 grams and can be entered in this form for standard blanks. Or enter the desired weight using the keyboard (the internal balance is not monitored) and then press the Enter key. If the same ID code is used for additional samples, they can be added to the weight stack without returning to the sample log-in screen by following step 1. If additional samples with a different ID code will be added to the stack it is necessary to return to the sample log-in screen.

2.

3.

Interfaced BalanceAutomatic Procedure 1. Press the F2 (Balance Tare) key. A weight entry occurs two ways: A. When external weight entry is chosen in system configuration, remote displays in the weight entry display and the operator must press the print key on the LECO balance to send a sample weight to the analyzer, then press the enter key to add a weight to the stack. When internal weight entry is chosen in system configuration, the external balance continuously sends weight readings to the instrument and the operator must press the enter key to add a weight to the stack.

B.

2.

If the same ID code is used for additional samples, they can be added to the weight stack without returning to the sample log-in screen by repeating step 1. If additional samples with a different ID code will be added to the stack it is necessary to return to the sample log-in screen.

3.

510

RH-402

Operation

Remove Weight Procedure

1. Press the F4 (Remove Weight) key to remove the last weight entered into the weight stack (this includes an out of sequence entry). Each time the F4 (Remove Weight) key is pressed, another weight is removed. If a weight needs to be deleted and it is not the last weight entered: A. B. C. D. E. F. G. With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F6 (Stack Routines) key. Press the F1 (Weight Stack) key. Press the F7 (Print) key to print the weight stack. Press the F8 (Exit) key to return to the analyze menu. Press the F4 (Remove Weight) key repeatedly until the weight to be removed is deleted. Use the manual weight function to reenter the desired weights that were removed.

2.

Operation

RH-402

511

Channel Select Procedure

Notes

1. 2. 3. 4.

There are four analysis channels. Each channel contains variable parameters required for analysis of different materials. For additional information, refer to Analysis Constants, page 579.

Press the F6 (Channel Select) key. The monitor displays the analysis constants for all four channels. Press the corresponding function key to select the desired analysis channel. If a printout of the channel selections is required, press the F5 (Print) key. Press the F8 (Exit) key to return to the analyze menu.

512

RH-402

Operation

Transmit Results

Notes

This function only displays if the data transmit kit is installed and then only after an analysis is complete and the automatic data transmit has been disabled. Transmission is possible until the next analysis begins. For additional information, refer to Data Transmit, page 37, and System Configuration, page 422.

After an analysis, press the F7 (Transmit Results) key to transmit the last result to a host computer.

Notes

If an analysis is aborted, the result can still be transmitted. If an analysis is reset, no answer is calculated and therefore cannot be transmitted.

Operation

RH-402

513

Crucibles

Note

There are 3 types of crucibles to be used with the RH-402 system: * 603-710 Short Quartz * 769-520 Short Graphite * 769-761 Tall Graphite

The quartz crucibles can be used with any procedure and are used to fuse titanium. If quartz crucibles are used, the sample material must be such that it will couple with the RF field for the heating effect as the quartz will not couple. If a bath is used, this will generally provide the coupling necessary for heating, but will also require outgassing as with the fusion method. Graphite crucibles provide in themselves the necessary coupling for outgassing. Outgassing must be accomplished as graphite tends to absorb moisture and atmosphere that must be removed prior to analysis. It is not recommended that graphite crucibles be used with the hot extraction method as this method does not provide for outgassing, only purging. Tall graphite crucibles are recommended for aluminum samples.

Note

The quartz crucibles are used in the same manner as the graphite crucibles. The quartz crucibles will be tilted slightly while in position. This is normal. Figure 5-1, page 515, represents the typical quartz crucible position.

514

RH-402

Operation

REACTION /

Figure 51 Crucible Position

Operation

RH-402

515

Sample Preparation

Sample Type

Notes

This is intended as general information. For special applications, consult the Applications section of this manual or contact LECO Corporation. It is recommended that samples be handled with tweezers or scoops and not touched.

Aluminum SamplesAluminum samples must be chamfered on one end to ensure the sample drops into the crucible. Prepare aluminum samples (or any large sample) with a 45o leading edge. A typical aluminum sample should have a 0.34 inch diameter and measure 2.0 inches in length (figure 5-2, below). Pin SamplesPin samples can be dropped directly into the loading port of the HF-402 Chip SamplesChip samples can be analyzed only if directly loaded into the crucible and analyzed in the manual mode. Chips can also be analyzed by weighing them into tin capsules. Powder SamplesPowder samples can be analyzed only if directly loaded into the crucible and analyzed in the manual mode. Powders can also be analyzed by weighing them into tin capsules.

Note

When using tin capsules, only fill the capsule have full. Do not crimp tin capsule.

2.00"

0.34"

Figure 52 Typical Aluminum Sample

516

RH-402

Operation

Sample Size

Note

Weight and physical dimensions limit size of the sample that cab be dropped into the loading head.

DiameterThe maximum diameter of a sample that can be dropped through the loading head of the HF-402 induction furnace is 0.375 inches (9.5 mm). LengthThe maximum length of a sample that can be dropped through the loading head of the HF-402 induction furnace is 2.1 inches (53.3 mm).

Operation

RH-402

517

Constants Procedure
Before analyzing a sample, the system constants must be entered. The ranges for each constant are listed next to the constant. Values set lower than the allowable range limit default to the lowest range limit, values set higher than the allowable range limit default to the highest range limit.

Notes

For initial analyses, enter the suggested nominal value for a given constant. Print each constants screen before editing to allow reentry of original constants in case of incorrect editing.

518

RH-402

Operation

Standard Constants
1. 2. 3. With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F3 (Constants) key. Press the F1 (Standard Constants) key. The standard constants screen will appear.

4. 5.

Press the F1 (Print) key to receive a printed copy of this screen. Press the F3 (Next Value) or F2 (Previous Value) key to move the highlighted cursor line to the constant to be edited. Press the F5 (Change Channel) key to edit a different channel. Press the F7 (Change Name) key to edit the name of the current channel. Press the F8 (Exit) key to return to the analyze screen.

6. 7. 8.

Operation

RH-402

519

Definitions Purge TimeThe amount of time (in seconds) that the system is purged of impurities prior to the sample dropping into the crucible. Range: 0 to 1200 seconds. Default Value: 20 seconds. Analysis Power LowPercent of furnace power to be reached before sample will drop to begin analysis. Range: 0 to 100%. Default: 75%. Analysis Power HighPercent of furnace power to be reached during analysis. Range: 0 to 100%. Default Value: 75%. Ramp TimeThe amount of time (in seconds) it will take the furnace to go from the lower power to high power. Range: 0 to 600 seconds. Default Value: 0 seconds. Minimum Analysis TimeThe shortest amount of time (in seconds) the analysis is performed. Range: 5 to 1200 seconds. Default Value: 250 seconds. Comparator LevelThe comparator level is determined by the peak output of the detector. Refer to the Comparator Level procedure, page 77, for more detailed information. Range: 0.01 to 100%. Default Value: 0.25. Crucible AdjustThe adjustment (in millimeters) made to the crucible pedestal to compensate for the different crucible sizes. Range: 0 to 16 mm. Default Value: 0.

520

RH-402

Operation

Gas Dose Constants

Notes

1. 2. 3.

The gas dose constants are used to control dose analysis and calibration. When replacing the gas dose loop, enter the new value found on the loop tag.

With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F3 (Constants) key. Press the F3 (Gas Dose Constants) key. The display will be similar to the following example.

4. 5.

Press the F1 (Print) key to receive a printed copy of this screen. Press the F3 (Next Value) or F2 (Previous Value) key to move the highlighted cursor line to the constant to be edited. Press the F8 (Exit) key to return to the analyze menu.

6.

Operation

RH-402

521

Definitions Gas Dose PowerThe percentage of furnace power used during gas dose calibration. Range 0 to 100%. Default Value: 0.00%. Minimum Gas Dose TimeThe shortest amount of time (in seconds) the gas dose analysis is performed. Range: 20 to 1200 seconds. Default Value: 80 seconds. Comparator LevelThe comparator level is determined by the peak output of the detector. Refer to the Comparator Level procedure, page 77, for more detailed information. Range: 0.01 to 100%. Default Value: 0.25. Known H2 Gas Dose ValueThe known value (in ppm) of the gas dose loop. This value is printed on the tag attached to the dosing valve located on the right-rear floor of the RH-402.

522

RH-402

Operation

S.P.C. Constants

Notes

The statistical process control limits can be used to monitor statistical stability. The control limits are used when performing the Standard Check procedure, page 57. A control standard can be designated for each analysis channel but each standard must be the same as the standard used to perform a standard check.

1. 2. 3.

With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F3 (Constants) key. Press the F3 (S.P.C. Constants) key. The display will be similar to the following example.

4. 5.

Press the F1 (Print) key to receive a printed copy of this screen. Press the F3 (Next Value) or F2 (Previous Value) key to move the highlighted cursor line to the constant to be edited. Enter the value of the standard listed on the bottle or certificate. Enter the upper and lower allowable control limits. Press the F6 (Change Channel) key to change the S.P.C. constants channel. Press the F8 (Exit) key to return to the analyze screen.

6. 7. 8. 9.

Operation

RH-402

523

Definitions Example: Standard = 0.913% Standard Deviation = 0.007% Hydrogen Control StandardThe expected value of the standard check analysis. Example: 0.913% Upper Control LimitThe highest acceptable value expected from a standard check analysis. Example: 0.913% + 0.007% = 0.920% Lower Control LimitThe lowest acceptable value expected from a standard check analysis. Example: 0.913% - 0.007% = 0.906%

524

RH-402

Operation

Analysis Procedure

Before Analysis

Note

The following information outlines the general operation procedure. Detailed procedures are outlined in the System Overview section, beginning on page 46.

1.

Be sure all steps described in the Installation section, beginning on page 2-1, have been completed before operating the analyzer. Only the analyze menu is used to carry out an actual analysis. The system update menu and diagnostic menu are used for updating constants and parameters, calibration routines, and diagnostic routines. System constants must be entered prior to any analyses. Perform the System Overview procedure, including the system leak check, at the beginning of each day. Refer to Diagnostic Menu, page 83, for additional information. Refer to Analysis Programs , page 575, to determine which analysis program, procedure, and channel to use.

2.

3. 4.

5.

Operation

RH-402

525

Small Samples Small samples can become trapped in the loading head or miss the crucible when dropped using conventional loading methods. The small sample loader insert ensures that small samples can be directly loaded into the crucible each time. The insert is used as follows: 1. 2. 3. 4. 5. Place a new crucible on the furnace pedestal. Place the loader insert into the sample port of the sample loading block. Using tweezers, place the sample (e.g. pin sample) into the loader insert. The loader insert may remain in place until larger samples are run. Continue with the analysis procedure as outlined in the instruction manual.

526

RH-402

Operation

Blank Determination 1. 2. 3. 4. Enter a 5-gram weight into the stack by pressing the F3 (Manual Weight) key and then press the enter key. Press the loader control key and place a crucible on the pedestal. Press the loader control key again, analysis will start. Repeat steps 1 through 3 five times and enter the average blank value in the manual blank program by performing the blank procedure on page 5-43.

Operation

RH-402

527

Gas Dosing

Notes

1. 2.

The dosing calibration value is printed on a tag attached to the dosing valve assembly located on the right-rear floor of the RH- 402 analyzer cabinet (figure 11-2, page 11-4). Hydrogen or helium can be used for gas dosing. If helium is used, divide the gas dose factor by 1.642 and enter the result as a new known gas dose. Three gas dose analyses are recommended for calibration.

With the analyze menu displayed, press the F1 (Sample Log-In) key. Press the F7 (Gas Dose) key. After entering the desired number of doses, press the Enter key and the gas dose analysis will begin.

Note

Gas dosing can be performed over a hot or cold crucible. When gas dosing over a hot crucible, some losses will occur.

528

RH-402

Operation

Analysis

Note

1. 2. 3. 4. 5.

Refer to Analysis Programs, page 5-75, for information concerning the different types of analysis.

Select channel number and name by pressing the F6 (Channel Select) key on the analyze menu. On the analyze menu, press the F1 (Sample Log-In) key. Respond to the prompts for ID code, type, and operator. With the analyze menu displayed, press the F5 (Analyze) key, then the F2 (Tare) key. This will tare the balance. Place sample in the balance pan and close the cover on the balance. Press the Enter key. The weight will be displayed at the lower right side of the display monitor as next sample. Press the loader control key on the front of the HF-402 furnace. The sample loading head will open. The following screen will appear.

6.

Note

The display line assumes the same classification and ID code, but the ID code is automatically incremented by 1. The AWT (auto-weight) still is 00.000 as the next sample has not yet been weighed. If the samples remain the same in name, it is not necessary to reenter new classifications and ID codes. After the balance has been tared and the next sample weighed, pressing the Enter key will enter the entire line of information as it is shown on the display.

Operation

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529

7.

Load the furnace as follows: A. B. C. D. Using the crucible tweezers, place a new crucible on the pedestal. Using tweezers, place the sample (just weighed) into the sample port at the top of the sample load block. Press the Loader Control key on the front of the furnace. The sample load block will slide to the right and the upper sample block will slide down to seal the blocks.

Notes

During the outgassing of the empty crucibles, the monitor will display: Outgas Time : 6 <low power outgas> (Example only) The outgas time is a live display and will be counting down. This may change to high power outgas depending on the constants selected.

8.

At this time a new sample can be prepared. The classification and ID codes may be entered and the balance tared; as well as the sample being weighed and entered. After the outgassing is completed, the furnace will cool down for the period of time as set in the system constants. The display will appear as follows: Outgas time: 20 <outgas cool down> (Example only) When the cool down period is completed, the sample will drop (auto mode only) and the furnace will again begin to heat. The display will again be live and will appear as follows: Hydrogen - ppm 0.217 (Example only)

9.

10.

Note

There is a three-second delay prior to integration after the sample drop. This partially corrects for the changes in cell reading due to the movement of the crucible.

11.

When the analysis time is complete, the furnace will begin a 30 second cool down period. This time is not settable in system constants.

530

RH-402

Operation

12.

After printing the analysis result, the cool down phase will begin. The information will be automatically placed in the answer stack. Press the loader control key. The piston will drop and the used crucible will be exposed for removal. Be sure to use the crucible tongs, the crucible will be very hot.

13.

WARNING

HIGH TEMPERATURE HAZARD After the analysis, the crucible will be extremely hot. Use the crucible tongs to remove the crucible.

Operation

RH-402

531

After Daily Analysis 1. The power for the RH-402 analyzer should remain on at all times. The HF-402 furnace power may be shut off overnight if desired. The flow controls should remain in the on position. The gas should be switched off overnight. Press the gas key to switch the gas on again at the start of the next shift; allow 30 minutes for the TC cell to warm up and stabilize.

2. 3.

532

RH-402

Operation

Calibration Procedures
1. 2. Check the system calibration daily to ensure accuracy. Recalibrating can be performed through standard calibration, gas dose calibration, manual calibration, or database calibration. Each channel needs to be calibrated separately. For most accurate analysis results: A. B. C. Use a standard with a percentage slightly higher than that of the samples to be tested. When both blank and calibration procedures are performed, set the blank first. Analyze a minimum of three standard samples to be used for calibration.

3. 4.

Operation

RH-402

533

Standard Calibration
1. 2. 3. 4. With the analyze menu displayed, press the F1 (Sample Log-In) key and log-in a standard sample. Press the F8 (Exit) key to return to the analyze menu. Weigh the standard samples, enter the weights, and then press the F5 (Analyze) key. After the three standard samples have been analyzed, press the F8 (More) key to display the system update menu. Press the F1 (Calibration) key. Press the F1 (Standard Calibration) key. Enter the value, including the decimal point, of the calibration standard used for the calibration analysis. Press the F1 (Enter) key to display the answer select screen.

5. 6. 7. 8.

534

RH-402

Operation

9.

The last eleven analyses are displayed. Choose a minimum of three standard analyses to be used to calculate a new calibration. A. Press the F3 (Yes) key to include a sample. Each time F3 is pressed, the sample is highlighted and the cursor moves up one line. Press the F5 (Up/Down Arrow) key to toggle the vertical cursor direction. Press the F1 (Next Page) key to display the next eleven analyses. Press the F2 (Next Line) key to move the cursor to the next answer. Press the F4 (No) key to omit a highlighted sample on the cursor line that has been selected for calibration. There are six display screens that can be viewed by pressing (Shift/4) and (Shift/6). 1) 2) 3) 4) 5) 6) G. #, ID code, hydrogen, weight, channel, and time & date. #, ID code, hydrogen, weight, calibration, blank, time, and peak. #, ID code, bulk, weight, calibration, blank, time, and peak. #, ID code, surface, weight, calibration, blank, time, and peak. #, ID code, hydrogen, surface, bulk, weight, time & date. #, ID code, weight, classification, & operator.

B. C. D. E. F.

To choose standard samples analyzed by intervals, press the F6 (Database) key. Refer to Database Calibration, page 541, for detailed instruction. Press the F7 (Process Results) key and the instrument takes the chosen answers and performs the requested calculations.

H.

Operation

RH-402

535

10.

The display should be similar to the following example.

A. B. C. D.

Press the F5 (Todays Results) key to recalculate todays answers. Press the F6 (Stack Select) key to display the answer select screen and choose answers for recalculation. Press the F4 (Used for Calib.) key to recalculate the answers used to calculate the new calibration factor. Press the F1 (Print) key to receive a printout of the samples used to calculate the new calibration, the calibration channel and the old and new calibrations. Press the F8 (Exit) key to return to the analyze menu.

E.

536

RH-402

Operation

Gas Dose Calibration

Notes

1. 2. 3.

Before performing this procedure, enter the gas dose constants, found on the tag attached to the doser valve, in the Gas Dose Constants procedure, page 521. Select the power level desired to gas dose over a hot crucible.

With the analyze menu displayed, press the F1 (Sample Log-In) key. Press the F7 (Gas Dose) key. The display prompts for entry of the number of analyses. Enter a minimum of three. Press the F3 (Yes) key to insert a new crucible for gas dosing over a hot crucible. Press the loader control button, the instrument automatically performs the gas dose analyses. After the analyses, press the F8 (More) key to display the system update menu. Press the F1 (Calibration) key. Press the F2 (Gas Dose Calibration) key. The display will be similar to the following example.

4. 5. 6.

Operation

RH-402

537

7.

The last eleven analyses are shown. Choose a minimum of three gas dose analyses to be used to calculate a new calibration. A. Press the F3 (Yes) key to include a sample. Each time F3 is pressed, the next sample is highlighted and the cursor moves up one line. Press the F5 (Up/Down Arrow) key to toggle the vertical cursor direction. Press the F1 (Next Page) key to display the next eleven analyses. Press the F2 (Next Line) key to move the cursor to the next answer. Press the F4 (No) key to omit a highlighted sample on the cursor line that has been selected for calibration. There are six display screens that can be viewed by pressing (Shift/4) and (Shift/6). 1) 2) 3) 4) 5) 6) G. #, ID Code, Hydrogen, Weight, Channel, and Time & Date. #, ID Code, Hydrogen, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Bulk, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Surface, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Hydrogen, Surface, Bulk, Weight, Time & Date. #, ID Code, Weight, Classification, and Operator.

B. C. D. E. F.

To choose gas dose samples analyzed by intervals, press the F6 (Database) key. Refer to the Database Calibration procedure, page 541, for detailed instruction. Press the F7 (Process Results) key and the instrument takes the chosen answers and performs the requested calculations.

H.

538

RH-402

Operation

8.

The following display screen will appear.

9. 10. 11. 12.

Press the F5 (Todays Results) key to recalculate todays answers. Press the F6 (Stack Select) key to display the answer select screen and choose answers for recalculation. Press the F4 (Used for Calib.) key to recalculate the answers used to calculate the calibration factor. Press the F1 (Print) key to receive a printout of the samples used to calculate the new calibration, the calibration channel and the old and new calibrations. Press the F8 (Exit) key to return to the analyze menu.

13.

Operation

RH-402

539

Manual Calibration

Notes

This procedure permits the operator to manually change the calibration factor. This procedure should be used to enter a calibration factor that has been lost. Normal calibration should be performed using the standard calibration procedure.

1. 2. 3. 4. 5.

With the analyze menu displayed, run a minimum of three analyses using the selected standard. With the system update menu displayed, press the F1 (Calibration) key. Press the F3 (Manual Calibration) key. Enter the new calibration and then press the F1 (Enter) key. The display will be similar to the following example.

A. B. C. D.

Press the F5 (Todays Results) key to recalculate todays answers. Press the F6 (Stack Select) key to display the answer select screen and choose answers for recalculation. Press the F1 (Print) key to receive a printout of the old and new calibrations and the calibration channel. Press the F8 (Exit) key to return to the analyze menu.

540

RH-402

Operation

Database Calibration

Note

Database calibration allows standard samples to be calibrated by intervals. This procedure is accessed through the answer select screen in the standard calibration or gas dose calibration procedure. Press the F6 (Database) key to display this screen:

1.

2. 3.

Press the F3 (Next Line) or F2 (Previous Line) key to move the cursor one line up or down. Results by date are handled as follows: A. B. C. Results From and Results Since include the dates entered. Results Before excludes the date entered. Results Between includes the first date and excludes the last date.

4.

Press the F6 (Long Search) key to have the instrument search the entire database in internal memory (up to 32,000 records). Press the F7 (Short Search) key to have the instrument search the answer stack only (up to 500 records).

5.

Operation

RH-402

541

6.

After the instrument performs the search, the monitor displays the number of samples found. Press any key to continue. The instrument recalibrates the answers chosen and the display will be similar to the following example.

A. B. C. D.

Press the F5 (Todays Results) key to recalculate todays answers. Press the F6 (Stack Select) key to display the answer select screen and choose answers for recalculation. Press the F4 (Used for Calib.) Key to recalculate the answers used to calculate the new calibration factor. Press the F1 (Print) key to receive a printout of the samples used to calculate the new calibration, the calibration channel and the old and new calibrations. Press the F8 (Exit) key to return to the analyze menu.

E. 7.

Press the F8 (Exit) key to return to the answer select screen without choosing any samples.

542

RH-402

Operation

Blank Procedures
Blank analysis is performed to determine and account for background hydrogen within the system (e.g. in the crucibles). The system blanks should be determined and compensated for when the gas supply or crucible lot has been changed.

Notes

Blank compensation should be based on a minimum of three blank analyses. Blank analysis should be performed on the channel to be compensated.

Hydrogen Blank
1. 2. 3. 4. Enter a 5 gram weight into the stack by pressing the F3 (Manual Weight) key and then entering the weight. Press the loader control key and place a crucible on the pedestal. Press the loader control key again. An analysis will begin. Repeat steps 1 through 3, five times. The results will be stored in the answer stack and used in the steps below to determine the standard blank. Press the F8 (More) key to display the system update menu. Press the F2 (Blanks) key. Press the F1 (Standard Blank) key.

5. 6. 7.

Operation

RH-402

543

8.

The display prompts for the entry of the blank value. Enter the value of the hydrogen blank standard. The display will then be similar to the following example.

Note

A blank value of 0.000 should be entered unless a hydrogen standard blank was analyzed to determined then blank value. In this case, the value of the hydrogen blank standard should be entered.

9.

The last eleven analyses are listed. Choose a minimum of three blank analyses for blank compensation. A. Press the F3 (Yes) key to include a sample. Each time F3 is pressed, the next sample is highlighted and the cursor moves up one line. Press the F5 (Up/Down Arrow) key to toggle the vertical cursor direction. Press the F1 (Next Page) key to display the next eleven analyses. Press the F2 (Next Line) key to move the cursor to the next answer. Press the F4 (No) key to omit a highlighted sample on the cursor line that has been selected for blank computation.

B. C. D. E.

544

RH-402

Operation

F.

There are six display screens that can be viewed by pressing (Shift/4) and (Shift/6). 1) 2) 3) 4) 5) 6) #, ID Code, Hydrogen, Weight, Channel, and Time & Date. #, ID Code, Hydrogen, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Bulk, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Surface, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Hydrogen, Surface, Bulk, Weight, and Time & Date. #, ID Code, Weight, Classification, and Operator.

G.

To choose samples analyzed by intervals, press the F6 (Database) key. Refer to the Database Blank procedure, page 547, for detailed instruction. Press the F7 (Process Results) key and the instrument takes the chosen answers and performs the requested calculations.

H.

10.

The display will be similar to the following example.

11. 12.

Press the F1 (Print) key to print the old and new blank values. Press the F8 (Exit) key to return to the analyze menu.

Operation

RH-402

545

Manual Blank

Notes

This procedure permits the operator to manually change or enter a new blank value. This procedure should be used to enter a blank value that has been lost. Blank value calculation should be performed using the Standard Blank procedure, page 543.

1. 2. 3. 4. 5. 6. 7.

With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F2 (Blanks) key. Press the F2 (Manual Blank) key. At the prompt, enter the new blank value. Press the F1 (Enter) key to display the old and new hydrogen blank. Press F1 (Print) to print the old and new hydrogen blank values. Press F8 (Exit) to return to the analyze menu.

546

RH-402

Operation

Database Blank

Note

Database blank allows blanks to be calculated from samples chosen by intervals. This procedure is accessed through the answer select screen in the standard blank procedure. Press the F6 (Database) key. The display will be similar to the following example.

1.

2. 3.

Press the F3 (Next Line) or F2 (Previous Line) key to move the cursor one line up or down. Results by date are handled as follows: A. B. C. Results From and Results Since include the dates entered. Results Before excludes the date entered. Results Between includes the first date and excludes the last date.

4.

Press the F6 (Long Search) key to have the instrument search the entire database in internal memory (up to 32,000 records). Press the F7 (Short Search) key to have the instrument search the answer stack only (up to 500 records). Press the F8 (Stats) key to calculate a new hydrogen blank value.

5. 6.

Operation

RH-402

547

Note

After the instrument performs the search, the monitor displays the number of samples found, recalibrates the answers chosen, and displays the old and new blanks. The display will be similar to the following example.

A.

Press the F1 (Print) key to receive a printout of the samples used to calculate the new blank, the blank channel and the old and new blanks. Press the F8 (Exit) key to return to the analyze menu.

B. 7.

Press the F8 (Exit) key to return to the answer select screen without choosing any samples.

548

RH-402

Operation

Data Buffers Procedures

Screen Plot

Notes

1. 2. 3. 4.

The data buffers store the data from the last analysis performed. The data can be printed in a digital number format or plotted on screen. Observing the data buffers can be used to evaluate a sample burn and flow characteristics of an analysis. With the analyze menu displayed, press the F8 (More) key twice to display the diagnostics menu. Press the F3 (Data Buffers) key. Press the F1 (Screen Plot) key to display a plot of the last analysis. Press F4 (Change Limits) to examine different portions of the curve by changing the limits of the axes. The monitor will prompt for new starting and ending times and then the starting and ending signals. The Enter key must be pressed after each entry. Press the F5 key to Edit Null Points as follows: A. B. Move the cursor to the desired location using the F1 through F4 keys. Press the F5 (Set/Unset) key to set or unset the null point. 1) 2) C. If a white dot or hash mark is already in that position, it will be removed (unset). If a white dot or hash mark is not already in that position, one will be displayed (set).

5.

The number of areas to be computed will be displayed at the top of the screen (Null PTS =). To compute areas with the new null points, press the F6 (Compute Area) key. The individual area calculations are printed, along with the total.

Operation

RH-402

549

Notes

Initially null points are selected according to where the slope of the curve changes. This allows the area between each null point to be computed separately. A maximum of nine null points may be entered.

D. 6.

Press F7 (Print Plot) to obtain a printout of the plot with the null points.

Press the F8 (Exit) key to return to the analyze screen.

550

RH-402

Operation

Print Buffer

Notes

1. 2. 3. 4.

This procedure provides a numerical printout of the cell data collected for the last analysis. To stop printing, press the F8 (Exit) key.

With the analyze menu displayed, press the F8 (More) key twice to display the diagnostics menu. Press the F3 (Data Buffers) key. Press the F2 (Buffer Print) key. Press F1 (Hydrogen Buffer) to print the contents of the buffer. The buffer printout contains data collected from the IR cell during the analysis. Information that can be obtained from the buffer printout includes: A. The first line of information contains the (peak) value or point of highest offset, the time period from when data accumulation first began (start) and the number of data points accumulated over the entire analysis (end). There are 11 columns of numbers. The first column increments by 10 with each line. This designates the number of data points accumulated at the start of each line. The numbers in each of the 10 remaining columns in each line represent the digital offset for each data point period; 18 data point periods are equivalent to 1 second of real time.

5.

B.

C.

6.

Press F2 (Derivative Buffer) to print the contents of the derivative buffer. This buffer is a derivative of the temperature buffer. Press F3 (Temperature Buffer) to print the contents of the temperature buffer. Press the F8 (Exit) key to return to the analyze screen.

7. 8.

Operation

RH-402

551

Counters Procedure

Notes

This procedure allows the operator to set and edit the system counters. After a system counter value has been reached, refer to the Periodic Maintenance Schedule, page 63, for additional information before continuing with analysis. With the analyze menu displayed, press the F8 (More) key to display the system update menu. From the system update menu, press the F5 (Counters) key. The counters screen will appear.
Printer: NR Gas -OFFChan #01 11:28:42 11 Dec 99

1. 2.

System Counters Copper Catalyst Carrier Gas LCB/ANH Analysis Gas Schutze/LCB/ANH Furnace Coolant Furnace Tube Number or Analyses

Limit 20000 2000 300 5000 300 7604

Elapsed 7604 1602 124 3122 124

F1 Print

F2 Previous

F3 Next

F4

F5

F6 Change Channel

F7

F8 -Exit-

3. 4. 5. 6.

Press the F1 (Print) key to receive a printout of the system counters. Press the F3 (Next) key to advance the highlighted area to the next counter line. Press the F2 (Previous) key to return the highlight to the previous counter line. Press the F4 (Restore Values) key to restore the counters to their default values.
Default Values Copper Catalyst Carrier Gas LCB/ANH Analysis Gas Schutze/LCB/ANH Furnace Coolant Furnace Tube 20,000 2,000 300 5,000 75

552

RH-402

Operation

7.

Press the F5 (Edit Limits) key change the counter limits. Press the appropriate number keys to change a value and use the enter key to advance to the next line. Press any of the function keys to enter the new values.

Note

When the limit values are exceeded, a message will be printed with the answer instructing the user to change the reagents. The message will continue to be printed until the counters are reset. Refer to the Periodic Maintenance Schedule, page 63, for additional information.

8.

Press the F6 (Edit Elapsed) key to change the elapsed values. Press the appropriate number keys to change an elapsed value and use the enter key to advance to the next line. The values that are displayed on screen will be saved when the F8 (Exit) key is pressed. Press the F8 (Exit) key to return to the analyze screen.

9.

Operation

RH-402

553

Stack Procedures

Weight Stack

Notes

1. 2. 3.

Stack routines allow data to be observed or calculated. The answer stack contains the analytical results from the last 500 analyses. The weight stack contains the weights of up to 100 samples that have not been analyzed.

With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F6 (Stack Routines) key. Press the F1 (Weight Stack) key. The display will be similar to the following example.

4. 5. 6. 7. 8.

Press the F3 (Next Line) or F2 (Previous Line) key to move through the stack. Press the F5 (Next Page) key to display another page of weights. Press the F4 (Previous Page) key to display the previous page. Press the F1 (Print) key to print the weight stack. Press the F8 (Exit) key to return to the analyze menu.

554

RH-402

Operation

Answer Stack

Notes

When accessed directly from the stack routine procedures, the answer stack is for viewing and printing only. An editable version of the answer stack, referred to as the answer select screen, is used in the following procedures: Standard Calibration, Gas Dose Calibration, Standard Blank, Transfer And Delete, Statistics, and Transmit Stack. The answer stack consists of up to five hundred of the most recent analyses performed. The last thirteen analyses appear on screen with the cursor on the last sample in the list. The system hard disk stores up to 32,000 analysis results, including the answers listed in the answer stack. The answers on the hard disk can be accessed through the Database Options procedure, page 558. With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F6 (Stack Routines) key. Press the F2 (Answer Stack) key. The display will be similar to the following example.

1. 2. 3.

4. 5.

Press the F3 (Next Line) or F2 (Previous Line) key to move the cursor one line up or down. Press the F5 (Next Page) key to display the next thirteen analyses.

Operation

RH-402

555

6. 7. 8.

Press the F4 (Previous Page) key to display the previous thirteen analyses. Press the F8 (Exit) key to return to the analyze menu. Press the F1 (Print) key. The display will be similar to the following example.

9.

The last eleven analyses are displayed. Choose the samples to be printed. A. Press the F3 (Yes) key to include a sample. Each time F3 is pressed, the sample is highlighted and the cursor moves up one line. Press the F5 (Up/Down Arrow) key to toggle the vertical cursor direction. Press the F1 (Next Page) key to display the next eleven analyses. Press the F2 (Next Line) key to move the cursor to the next answer. Press the F4 (No) key to omit a highlighted sample on the cursor line that has been selected for printing. There are six display screens that can be viewed by pressing (Shift/4) and (Shift/6). 1) 2) 3) #, ID Code, Hydrogen, Weight, Channel, and Time & Date. #, ID Code, Hydrogen, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Bulk, Weight, Calibration, Blank, Time, and Peak.

B. C. D. E. F.

556

RH-402

Operation

4) 5) 6) G.

#, ID Code, Surface, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Hydrogen, Surface, Bulk, Weight, and Time & Date. #, ID Code, Weight, Classification, and Operator.

To choose samples analyzed by date, log-in, or analysis values, press the F6 (Database) key. See the Database Option, page 558, for detailed instruction. Press the F7 (Process Results) key. The instrument prints the selected answers and then returns to the analyze menu.

H.

Operation

RH-402

557

Database Option 1. Press the F6 (Database) key. The display will be similar to the following example.

2. 3.

Press the F3 (Next Line) or F2 (Previous Line) key to move the cursor one line up or down. Results by date are handled as follows: A. B. C. Results From and Results Since include the dates entered. Results Before excludes the date entered. Results Between includes the first date and excludes the last date.

4.

Press the F6 (Long Search) key to have the instrument search the entire database internal memory (up to 32,000 records). Press the F7 (Short Search) key to have the instrument search the answer stack only (up to 500 records). After the instrument performs the search, the display indicates the number of samples found and prints them. Press any key to continue. Press the F8 (Exit) key to return to the answer select screen without choosing any samples.

5. 6.

7.

558

RH-402

Operation

Transfer and Delete

Notes

This procedure provides a means of deleting answers from the hard disk, transferring answers to floppy disk, or both. A message prints when the number of records in the database reaches the maximum value set in the system configuration procedure. Use a formatted IBM DOS disk for the transfer. Approximately 1800 records can be outputted to a single disk. Data is copied to drive A: as a file in ASCII comma separated format. See the Data Transmit section, page 311, for more information. It is not possible to reload results from floppy disk back into the database. With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F6 (Stack Routines) key. Press the F3 (Transfer and Delete) key. The display will be similar to the following example.

1. 2. 3.

4.

The last 500 analyses are available for transfer through this screen. To choose answers: A. Press the F3 (Yes) key to include a sample. Each time F3 is pressed, the next sample is highlighted and the cursor moves up one line. Press the F5 (Up/Down Arrow) key to toggle the vertical cursor direction.

B.

Operation

RH-402

559

C. D. E. F.

Press the F1 (Next Page) key to display the next eleven analyses. Press the F2 (Next Line) key to move the cursor to the next answer. Press the F4 (No) key to omit a highlighted sample on the cursor line that has been selected for transferring. There are six display screens that can be viewed by pressing (Shift/4) and (Shift/6). 1) 2) 3) 4) 5) 6) #, ID Code, Hydrogen, Weight, Channel, and Time & Date. #, ID Code, Hydrogen, Weight, Calibration, Blank, Time and Peak. #, ID Code, Bulk, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Surface, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Hydrogen, Surface, Bulk, Weight, and Time & Date. #, ID Code, Weight, Classification, and Operator.

G.

To choose samples analyzed by date, log-in, or analysis values, press the F6 (Database) key. See the Database Option, page 561, for detailed instruction. Press the F7 (Process Results) key to begin the transfer and/or delete process. Follow instructions displayed on the monitor to transfer answers to floppy disk.

H.

5.

The display prompts: Transfer Results to Floppy? A. B. C. D. Press the Y key to transfer results. The default file name displays. Press the Enter key, or edit the default file name and then press the Enter key. Follow the on-screen instructions. Press the N key to move on to the delete part of the procedure.

6. 7.

The screen then prompts: Delete Selected Results? Enter either Yes or No and then press the Enter key. The instrument displays the number of records in the old database, the number of records in the new database, and the number of records deleted. Press any key to continue and the instrument automatically exits to the analyze menu.

560

RH-402

Operation

Database Option 1. Press the F6 (Database) key. The display will be similar to the following example.

2. 3.

Press the F3 (Next Line) or F2 (Previous Line) key to move the cursor one line up or down. Results by date are handled as follows: A. B. C. Results From and Results Since include the dates entered. Results Before excludes the date entered. Results Between includes the first date and excludes the last date.

4.

Press the F6 (Long Search) key to have the instrument search the entire database internal memory (up to 32,000 records). Press the F7 (Short Search) key to have the instrument search the answer stack only (up to 500 records). After the instrument performs the search, the display indicates the number of samples found and prints them. Press any key to continue. Press the F8 (Exit) key to return to the analyze menu.

5. 6.

7.

Operation

RH-402

561

Restore Deletion

Notes

1. 2. 3. 4.

This procedure can be used to restore a database deleted in error. A previously deleted database cannot be restored if another database selection has since been transferred and/or deleted. Answers stored since the last deletion are not included in the restored stack.

With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F6 (Stack Routines) key. Press the F4 (Restore Deletion) key. A question is displayed on the monitor asking if the data deleted in the transfer and delete should be undeleted. Type in YES, then press the Enter key. The instrument confirms that the database has been restored. Press any key to return to the analyze menu.

5.

562

RH-402

Operation

Statistics
1. 2. 3. With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F6 (Stack Routines) key. Press the F5 (Statistics) key. The display will be similar to the following example.

4.

The last 500 analyses are available for statistical calculation through this screen. To choose answers: A. Press the F3 (Yes) key to include a sample. Each time F3 is pressed, the next sample is highlighted and the cursor moves up one line. Press the F5 (Up/Down Arrow) key to toggle the vertical cursor direction. Press the F1 (Next Page) key to display the next eleven analyses. Press the F2 (Next Line) key to move the cursor to the next answer. Press the F4 (No) key to omit a highlighted sample on the cursor line that has been selected for statistics.

B. C. D. E.

Operation

RH-402

563

F.

There are six display screens that can be viewed by pressing (Shift/4) and (Shift/6). 1) 2) 3) 4) 5) 6) #, ID Code, Hydrogen, Weight, Channel, and Time & Date. #, ID Code, Hydrogen, Weight, Calibration, Blank, Time and Peak. #, ID Code, Bulk, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Surface, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Hydrogen, Surface, Bulk, Weight, and Time & Date. #, ID Code, Weight, Classification, and Operator.

G.

To choose samples analyzed by date, log-in, or analysis values, press the F6 (Database) key. Refer to the Database Option, page 566, for detailed instruction. Press the F7 (Process Results) key and the instrument calculates an average based on the selected values and displays it with the standard deviation, coefficient of variation, and number of points selected, similar to the following example.

H.

Note

Pressing the F5 key toggles the screen between average, bulk, surface, total, and weight statistics. Press the F8 key to exit.

564

RH-402

Operation

I.

Press F4 (Process Chart) key to receive a graphic chart printout of the analyses used for the average value. Percent hydrogen and the control limits are given on the vertical axis while the sample number is listed on the horizontal axis. Press F5 (Continue Stats) to continue with the statistics procedure. Press the F8 (Exit) key to return to the analyze menu.

J. K.

Operation

RH-402

565

Database Option 1. Press the F6 (Database) key. The display will be similar to the following example.

2. 3.

Press the F3 (Next Line) or F2 (Previous Line) key to move the cursor one line up or down. Results by date are handled as follows: A. B. C. Results From and Results Since include the dates entered. Results Before excludes the date entered. Results Between includes the first date and excludes the last date.

4.

Press the F6 (Long Search) key to have the instrument search the entire database internal memory (up to 32,000 records). Press the F7 (Short Search) key to have the instrument search the answer stack only (up to 500 records). After the instrument performs the search, the display indicates the number of samples found and prints them. Press any key to continue. Press the F8 (Exit) key to exit this procedure.

5. 6.

7.

566

RH-402

Operation

Transmit Stack

Notes

1. 2. 3. 4.

This procedure, which allows selected data to be transmitted, displays only if the optional data transmit kit is installed. See Data Transmit, page 311, and Serial Ports, page 425, for additional information.

With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F6 (Stack Routines) key. Press the F6 (Transmit Stack) key. Press the F1 (Xmit) key. The display will be similar to the following example.

5.

The last 500 analyses are available for transmission through this screen. To choose answers: A. Press the F3 (Yes) key to include a sample. Each time F3 is pressed, the sample is highlighted and the cursor moves up one line. Press the F5 (Up/Down Arrow) key to toggle the vertical cursor direction. Press the F1 (Next Page) key to display the next eleven analyses. Press F2 (Next Line) key to move the cursor to the next answer.

B. C. D.

Operation

RH-402

567

E.

Press the F4 (No) key to omit a highlighted sample on the cursor line that has been selected for transmission. There are six display screens that can be viewed by pressing (Shift/4) and (Shift/6). 1) 2) 3) 4) 5) 6) #, ID Code, Hydrogen, Weight, Channel, and Time & Date. #, ID Code, Hydrogen, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Bulk, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Surface, Weight, Calibration, Blank, Time, and Peak. #, ID Code, Hydrogen, Surface, Bulk, Weight, and Time & Date. #, ID Code, Weight, Classification, and Operator.

F.

G.

To choose samples analyzed by date, log-in, or analysis values, press the F6 (Database) key. Refer to the Database Option, page 569, for detailed instruction. Press the F7 (Process Results) key and the selected answers are automatically sent to the receiver in the format chosen in step 5. When transmission is finished, the display indicates the number of records sent.

H.

6.

Press the F8 (Exit) key to return to the analyze menu.

568

RH-402

Operation

Database Option 1. Press the F6 (Database) key. The display will be similar to the following example.

2. 3.

Press the F3 (Next Line) or F2 (Previous Line) key to move the cursor one line up or down. Results by date are handled as follows: A. B. C. Results From and Results Since include the dates entered. Results Before excludes the date entered. Results Between includes the first date and excludes the last date.

4.

Press the F6 (Long Search) key to have the instrument search the entire database internal memory (up to 32,000 records). Press the F7 (Short Search) key to have the instrument search the answer stack only (up to 500 records). After the instrument performs the search, the display indicates the number of samples found and prints them. Press any key to continue. Press the F8 (Exit) key to return to the answer select screen without choosing any samples.

5. 6.

7.

Operation

RH-402

569

Alarms Procedure

Note

In the event of a condition which might harm the unit or lead to incorrect results, an alarm occurs and the word Alarm appears on the top center of the monitor display. From the analyze menu, press the F8 (More) key to display the system update menu. Press the F7 (Alarms) key. The monitor will display a list of alarms that occurred since the system was last reset. If no alarms have occurred, the monitor will display No Alarms Listed in the Alarm Stack. Press the F1 (Print) key to print the alarm list.

1. 2.

3.

Note

4. 5.

Refer to the Alarm Table, page 571, for probable causes and possible solutions.

Press the F2 (Reset/Clear) key to reset/clear the alarm before proceeding. Press the F8 (Exit) key to exit the alarms procedure.

570

RH-402

Operation

Alarm Table
Alarm Definition and/or Probable Cause Hardware problem at COMM Port 1. Should not occur. System is trying to map to a third disk or to an invalid disk. Error is possible resulting from a damaged disk. Possible wrong or missing format. One or more linearization constants set to zero. Possible Solutions and Additional Information Check to see if auxiliary device is connected to COMM Port 1 and that device is functional. Reset the program. Refer to Initial Power-Up procedure, page 411.

AUX Device Error Critical!

Argument Error

Bad Address Mark

Verify and reinsert proper disk.

Break Point or Slope Set to Zero

Edit linearization constants or linearize instrument.

CON device Error Critical!

Hardware problem with the monitor console.

Call LECO Service Department. Select calibration standards that are close to expected results.

Calibration Out of Range

0.01 {/=} Calibration Factor {/=} 9.99 Cannot open or create file on hard disk or floppy disk.

Can't Open Data File

Information will not be saved. Determine that correct data transmit card has been installed. Reset counters via the System Update Menu Counter procedure, page 552. Check that disk is properly inserted. Try new disk.

COMM Port Initialization Error

Problem initializing serial port.

Counter Limit Exceeded

Counters not reset before reaching maximum limit.

DSK Device Error Critical!

Hardware problem with the disk drive device.

Operation

RH-402

571

Alarm

Definition and/or Probable Cause

Possible Solutions and Additional Information Check to see if data transmit card has been installed. Check to see if data transmit peripherals are connected.

Data Xmit Output Error

Problem transmitting data from instrument to peripheral device.

Disk Drive Door Open

Close locking lever on disk drive. Drive will not respond. Write protection tab is installed on disk. Disk is installed improperly.

Reissue command.

Disk Write Protected

Verify disk is properly inserted and that no write protect tab exist.

Divide by Zero Error

Software problem.

Call LECO Service Department.

Error Setting Stepper

Stepper motor driver card not receiving information.

Call LECO Service Department. Check out stepper motor functions through sequence test. May need to replace stepper motor card. Programs will not be saved. Check: balance connections; balance card installation; programming of balance. Search for another file. Look for file on another disk. Verify and reinstall proper disk.

Error Writing File

Not enough space on disk after the file has been created.

External Balance Print Error

Problem in communication with external balance.

FAT Table Error Critical!

Problem with hard disk.

File Not Found

File requested not found on disk.

Floppy Disk Error

Data or seek error. Disk is possibly damaged.

572

RH-402

Operation

Alarm

Definition and/or Probable Cause Should not occur unless the program is corrupted. Possible program error. Incorrect data entry.

Possible Solutions and Additional Information Analysis is aborted. Reinstall program onto hard disk. Follow display prompts and refer to Set Clock procedure, page 427. Verify proper disk. Follow display prompts and refer to Set Clock procedure, page 427. Reinstall program onto hard disk. Call LECO Service Department. Repeat procedure and select answers.

Illegal Case Tried to Run

Illegal Date Set

Illegal File Format

Disk not formatted for instrument.

Illegal Time Set

Incorrect data entry. Should never occur. This is caused by DOS environment problem. Problem with hardware. Results were not selected before a calculation was requested. Not enough memory to store screen beneath help notes.

Invalid Directory

NUL Device Error Critical!

No Answers Selected

Not Enough Memory

Notes will not appear. Check that printer is switched on. Press printer reset button. Determine that printer connections are correct. Check for proper paper load. Replace Printer.

PRN Device Error Critical!

Hardware problem with printer.

Printer Error

Loss of handshake with printer. Defective printer. Hardware problem with printer. Defective printer. Sample weight stack has reached its limit (100 weights).

Printer Time-Out

Replace Printer.

Sample Weight Stack Exceeded.

If less than 100 weights have been entered, display weight stack and clear erroneous weights.

Operation

RH-402

573

Alarm

Definition and/or Probable Cause

Possible Solutions and Additional Information Certain procedures within security area cannot be accessed. Refer to Security Code procedure, page 421.

Security Access Denied

Invalid password attempted.

Serial Numbers Do Not Match

Serial numbers on software do not match serial number on back of unit. Selection was made to use option that is not connected.

Use correct software.

Special Option Does Not Exist

Connect option and try again.

TC Cell Saturated

TC cell out of range.

Use high range or smaller sample size. Abort analysis. Adjust TC cell preamp card to 1000 mV.

TC Cell is out of Range

100 mV TC range 2000 mV. System will reset itself. As the block opens, the stepper should open downward. If it is not fully opened in 10 seconds, an alarm will occur. Software problem.

Time-Out Initializing Slide Block

System reverts to idle mode. Check stepper motor and stepper motor card.

Window Error

Call LECO Service Department.

574

RH-402

Operation

Analysis Programs

Notes

There are 3 separate and distinct analysis programs to select from: * * * Hot Extraction AnalysisProcedure H Fusion AnalysisProcedure F Combined AnalysisProcedure C

Any of the analysis programs may be used on any of the 4 channels; however, the RH-402 is factory-set as follows: * * * * Channel 1Hot Extraction Analysis Channel 2Fusion Analysis (Low Range) Channel 3Fusion Analysis (High Range) Channel 4Combined Analysis

Operation

RH-402

575

Hot Extraction AnalysisProcedure H

This type of analysis is used when the sample is to be heated and not fused. Only quartz crucibles should be used in this procedure (system purging is used and not outgassing). Graphite crucibles tend to absorb hydrogen and therefore require outgassing (preheating) prior to an analysis. Quartz crucibles do not require outgassing. Hydrogen determination in steel is an application for the hot extraction method. Typical program settings for analyzing steel using the hot extraction procedure are:
Constants Purge Time Analysis Power Low Analysis Power High Ramp Time Minimum Analysis Time 20 seconds 75% 75% 0 seconds 250 seconds

Comparator Level 0.25 Crucible Adjust 0 Parameters Procedure H Short Crucible Low Range 4 Significant Figures Sample Loading (Not Applicable)

The sample is loaded directly into the crucible prior to analysis; the instrument will not instruct the operator for auto or manual loading procedures. As the analysis starts, the system is purged (for the amount of time entered as a constant), the sample is heated, hydrogen gas is driven off, and the analysis will end automatically. The results appear on the display.

576

RH-402

Operation

Fusion AnalysisProcedure F
During fusion analysis, the sample actually fuses while the hydrogen being driven off is being measured. Graphite crucibles are recommended as outgassing is included in the procedure, but quartz crucibles may also be used.

Note

Quartz is not recommended with sample materials that fuse heavily with the quartz. A danger of splintering upon cooling exists.

If any bath material is to be used, it should be loaded directly into the crucible so that it may be heated during crucible outgassing. The sample itself should be placed into the loading head after weighing is complete. After the outgassing is complete, the crucible is raised to the loading head and the sample is dropped into it. The crucible is lowered and the analysis heating takes place. The analysis will end automatically. Applications of the fusion method include determination of hydrogen in copper. Typical procedure settings for determining hydrogen in copper are:
Constants High Power Outgas High Power Outgas Time Low Power Outgas Analysis Power Low Analysis Power High Ramp Time Low Power Outgas Time Outgas Cool Down Minimum Analysis Time 100% 60 seconds 80% 80% 0 seconds 100 seconds 2 seconds 150 seconds

Comparator Level 0.25 Crucible Adjust 0 Parameters Procedure F Short Crucible Low Range 3 Significant Figures Auto Sample Loading

Note

Refer to the Analysis Parameter section, page 584, for definitions and selection of low range or high range parameters.

Operation

RH-402

577

Combined AnalysisProcedure C
The combined analysis procedure provides a method by which two separate analyses can take place on the same sample. The crucible is outgassed first and then the sample is dropped into the crucible. The first sample heating takes place with the answer being calculated and displayed. The sample is heated again and a second answer is calculated and displayed. This procedure would be typically used for determination of hydrogen in aluminum. This procedure is representative of surface and bulk analyses. Either the first or second heating of the sample may be bypassed if desired, but outgassing of the graphite crucibles should be accomplished.

Note

Quartz crucibles are not recommended for use with aluminum as sample fusion with the quartz crucibles is possible causing crucible splintering upon cool down.

Typical program settings for analyzing aluminum are:

Constants High Power Outgas High Power Outgas Outgas Cool Down Surface Analysis Analysis Power Low Furnace On Time Analysis Time Bulk Analysis Analysis Power Low Analysis Power High Ramp Time Maximum Furnace On Time Minimum Analysis Time Comparator Level Crucible Adjust Parameters Procedure C Tall Crucible Low Range 3 Significant Figures Auto Sample Loading Melt Detect Enabled 100% 100 seconds 100 seconds 60.00% 15 seconds 100 seconds 53.00% 53.00% 0 seconds 50 seconds 200 seconds 0.10 0

Note

To bypass surface analysis, enter 0s for surface analysis contents. To bypass bulk analysis, enter 0s for parameters and 100 for comparator level.

578

RH-402

Operation

Analysis Constants

Notes

Listed below are the definitions, ranges, and default values of the analysis constants. Constants are grouped by analysis method. Refer to the Analysis Parameters section, page 584, for parameter definitions.

Hot Extraction AnalysisProcedure H

Purge TimeThe amount of time (in seconds) that the system is purged of impurities prior to sample loading. Range: 0 to 1200 seconds. Default Value: 20 seconds. Analysis Power LowPercent of furnace power to be reached before the sample will drop to begin analysis. Range: 0 to 100%. Default: 75%. Analysis Power HighPercent of furnace power to be reached during analysis. Range: 0 to 100%. Default Value: 75%. Ramp TimeThe amount of time (in seconds) it will take the furnace to go from the lower power to high power. Range: 0 to 1200 seconds. Default Value: 0 seconds. Minimum Analysis TimeThe shortest amount of time (in seconds) the analysis is performed. Range: 5 to 1200 seconds. Default Value: 250 seconds. Comparator LevelThe comparator level is determined by the peak output of the detector. Refer to the Comparator Level section, page 77, for more detailed information. Range: 0.01 to 100%. Default Value: 0.25. Crucible AdjustThe adjustment (in millimeters) made to the crucible pedestal to compensate for the different crucible sizes. Range: 0 to 16 mm. Default Value: 0.

Operation

RH-402

579

Fusion AnalysisProcedure F
High Power OutgasPercentage of furnace power used to outgas the empty crucible (to remove contaminants) before an analysis is started. Range: 0 to 100%. Default Value: 100%. High Power Outgas (Time)The amount of time (in seconds) which high power outgassing is performed. Range: 0 to 600 seconds. Default Value: 60 seconds. Low Power OutgasPercentage of furnace power used to outgas the empty crucible before analysis and establish a baseline. The low power outgas level will also be the furnace power level during analysis. Range: 0 to 100%. Default Value: 80% low range; 80% high range. Analysis Power LowPercent of furnace power to be reached before sample will drop to begin analysis. Range: 0 to 100%. Default: 80%. Analysis Power HighPercent of furnace power to be reached during analysis. Range: 0 to 100%. Default Value: 80%. Ramp TimeThe amount of time (in seconds) it will take the furnace to go from the low power to high power. Range 0 to 600 seconds. Default Value: 0 seconds. Low Power Outgas (Time)The amount of time (in seconds) in which low power outgassing is performed. Range: 5 to 600 seconds. Default Value: 100 second slow range; 100 seconds high range. Outgas Cool DownThe amount of time (in seconds) which the furnace cools before opening. Range: 0 to 1200 seconds. Default Value: 2 seconds. Minimum Analysis TimeThe shortest amount of time (in seconds) the analysis is performed. Range: 1 to 600 seconds. Default Value: 150 seconds low range; 200 seconds high range. Comparator LevelThe comparator level is determined by the peak output of the detector. Refer to the Comparator Level section, page 77, for more detailed information. Range: 0.001 to 100 %. Default Value: 0.25. Crucible AdjustThe adjustment (in millimeters) made to the crucible pedestal to compensate for the different crucible sizes. Range: 0 to 16 mm. Default Value: 0.

580

RH-402

Operation

Combined AnalysisProcedure C
High Power OutgasPercentage of furnace power used to outgas the empty crucible (to remove contaminants) before an analysis is started. Range: 0 to 100%. Default Value: 100%. High Power Outgas (Time)The amount of time (in seconds) which high power outgassing is performed. Range: 0 to 600 seconds. Default Value: 100 seconds. Outgas Cool DownThe amount of time (in seconds) that the furnace cools before opening. Range: 20 to 600 seconds. Default Value: 100 seconds. Surface Analysis Analysis Power LowThe percentage of furnace power to be reached during analysis. Range: 0 to 100%. Default Value: 60%. Furnace On TimeThe amount of time (in seconds) the furnace power is on during analysis. Range: 0 to 600 seconds. Default Value: 15 seconds. Analysis TimeThe amount of time (in seconds) the analysis is performed. Range: 5 to 600 seconds. Default Value: 100 seconds. Bulk Analysis Analysis Power LowPercent of furnace power to be reached before sample will drop to begin analysis. Range: 0 to 100%. Default: 53%. Analysis Power HighThe percentage of furnace power to be reached during analysis. Range: 0 to 100%. Default Value: 53%. Ramp TimeThe amount of time (in seconds) it will take the furnace to go from the low power to high power. Range: 0 to 600 seconds. Default Value: 0 seconds. Maximum Furnace on TimeThe longest amount of time (in seconds) the analysis is performed. Range: 0 to 600 seconds. Default Value: 50 seconds. Minimum Analysis TimeThe shortest amount of time (in seconds) the analysis is performed. Range: 5 to 600 seconds. Default Value: 200 seconds.

Operation

RH-402

581

Comparator LevelThe comparator level is determined by the peak output of the detector. Refer to the Comparator Level section, page 77, for more detailed information. Range: 0.01 to 100%. Default Value: 0.10. Crucible AdjustThe adjustment (in millimeters) made to the crucible pedestal to compensate for the different crucible sizes. Range: 0 to 16 mm. Default Value: 0.

582

RH-402

Operation

Gas Dose
Minimum Gas Dose TimeThe shortest amount of time (in seconds) the gas dose analysis is performed. Range: 0 to 600 seconds. Default Value: 80 seconds. Comparator LevelThe comparator level is determined by the peak output of the detector. Refer to the Comparator Level section, page 77, for more detailed information. Range: 0.01 to 100%. Default Value: 0.25. Known H2 Gas Dose ValueThe known value (in ppm) of the gas dose loop. This value is printed on the tag attached to the dosing valve located on the right-rear floor of the RH-402. Gas Dose PowerThe percentage of furnace power used during gas dose calibration. Range: 0 to 100%. Default Value: 0.00%.

Operation

RH-402

583

Analysis Parameters

Notes

Analysis parameters are user-selected as are the analysis constants for each program. This adds flexibility of operation. Analysis parameters appear in the lower right-hand corner of the display as follows: * * * * * Analysis Type Crucible Type Range Significant Figures Sample Loading

Parameters are selected in the Constants procedure, page 518.

Analysis TypeThe user selects from Hot Extraction, Fusion, or Combined Analysis. Refer to Analysis Programs, page 575. Crucible TypeThe user selects from short or tall crucibles. Certain analysis programs dictate the use of the type of crucible and are explained in the Crucibles section, page 514. RangeThe user selects either low range (0.001 to 20 ppm H2 ) or high range (0.01 to 400 ppm H2 ). Significant FiguresThis is the total number of digits for the answer readout. The decimal point will float to provide the designated significant digits. The user selects from a range of 1 to 4 digits. Sample LoadingThe user selects from manual or auto sample loading. Certain analysis programs dictate which of the loading modes must be used and will be explained later. Refer to Analysis Programs, page 575. Melt DetectThe melt detect function can be enabled or disabled in the combined analysis. As an aluminum sample begins to melt, a temperature change is detected and the furnace shuts off; the sample slowly melts thereby preventing fusion with the crucible.

584

RH-402

Operation

Furnace Power Graphs

The following graphs will serve as an aid for determining crucible temperatures in relation to % power and current (Plate) DCmA. It must be further noted that crucible temperature may differ from actual sample temperature. Initially the crucible temperature will be higher with the end result of the crucible and sample being almost the same. The analysis power level (% power) is a system constant and is settable. The current (mA) is observable on the front panel meter.

Figure 53 Plate DCmA vs. Temperature

Operation

RH-402

585

Figure 54 % Power vs. Temperature

586

RH-402

Operation

Maintenance

Illustrations .......................................................................... 62 Periodic Maintenance Schedule ................................................. 63 Catalyst Heater Tube.............................................................. 64 Coolant Level........................................................................ 66 Filling The Coolant Tank ................................................ 66 Draining The Coolant Tank............................................. 67 Disposable Particle Filters ........................................................ 68 Loader Cover ........................................................................ 69 Incoming Reagent Tube ........................................................ 610 Measure Flow Reagent Tube .................................................. 611 Screen Filters ...................................................................... 615 O-rings .............................................................................. 616

Maintenance

RH-402

61

Illustrations
Figure 61......... Reagent Tube Removal ...............................612 Figure 62......... Incoming Reagent Tube Packing ...................612 Figure 63......... Measure Reagent Tube Packing ....................613 Figure 64......... Reagent Tube Assemblies............................614

62

RH-402

Maintenance

Periodic Maintenance Schedule

Equipment/Materials Replacement/Cleaning Schedule Repack the catalyst heater tube when the copper turnings are depleted or every six months. Refer to page 64. Add distilled water when water level is low. Refer to page 66. Replace the disposable particle filters every 6 to 12 months. Refer to page 68. Replace if leakage is determined during a leak check. Refer to page 69. Replace the anhydrone and Lecosorb every ninety days or if the anhydrone becomes wet. Refer to page 610. Replace when Schutze reagent is 2 /3 black. Refer to page 611. Clean when the reagents are replaced. Refer to page 615. Replace when worn and cracked. Refer to page 616. Inspection Schedule If the carrier gas supply is less then 99.99% pure, inspect the copper turnings every month.

Catalyst Heater Tube

Coolant Level

Check coolant level monthly.

Disposable Particle Filters

Loader Cover

Check for scratches and leakage monthly.

Incoming Reagent Tube

Inspect the reagents weekly.

Measure Reagent Tube

Inspect the reagent daily.

Screen Filters

Inspect when the reagents are replaced.

O-rings

Inspect for wear every month.

Maintenance

RH-402

63

Catalyst Heater Tube

Note

The catalyst reagent materials should be replaced every six months if pure nitrogen (99.99% or better) is used. If the nitrogen carrier is contaminated with oxygen, the copper turnings will deplete in a shorter period of time. Turn the carrier gas supply off. Remove the knob and remove the movable block from the top of the catalyst heater assembly (figure 6-4, page 614).

1. 2.

WARNING

HIGH TEMPERATURE HAZARD The catalyst heater tube is extremely hot. Wear heat-resistant gloves when removing the tube.

3.

Using heat-resistant gloves, lift the catalyst heater tube and remove it from the catalyst heater assembly. HIGH TEMPERATURE HAZARD Set the tube aside on a cooling tray and permit the catalyst tube to cool to room temperature before proceeding.

WARNING

4.

Obtain a shallow, acid-resistant pan that will hold one or more catalyst heater tubes.

!
CAUTION
POSSIBLE OPERATOR INJURY This procedure must be performed under a fume hood. Wear safety glasses and acid-resistance gloves.

64

RH-402

Maintenance

5.

Very slowly and carefully, add 70% concentrated nitric acid (HNO3 ) to the pan. Add only enough acid to cover half of the catalyst heater tube. The copper will begin to react with the nitric acid to produce a reddish-brown poisonous gas (NO2 ). When the copper is dissolved, rinse with water and remove the remainder of the copper and/or cupric oxide with a rod. If the catalyst heater tube is still not clean, return it to a fresh acid bath. When the catalyst heater tube is clean, rinse it thoroughly with distilled water and allow to dry. Pack the catalyst heater tube with 22 grams of copper turnings.

6. 7.

8. 9.

Note

When replacing the catalyst reagent materials, pack the copper firmly with a metal rod. If it is packed too loosely, it will deplete prematurely. If it is packed too tightly, the copper will form clumps in the catalyst heater tube, which are difficult to remove.

10.

Reinstall the repacked catalyst heater tube into the catalyst heater assembly. Make sure the bottom end of the tube is positioned and sealed over the o-ring. Reinstall the movable block and screw to secure and seal the catalyst heater tube.

11.

Maintenance

RH-402

65

Coolant Level
Check the water level in the coolant tank and add distilled water when necessary. Check coolant level monthly.

Notes

Filling The Coolant Tank

WARNING

ELECTRICAL SHOCK HAZARD This equipment operates from 230 V~. Contact with this voltage can be lethal. Disconnect the power source.

1. 2. 3. 4.

Turn the furnace off and disconnect from the facility power source. Remove the left side panel of the HF-402 furnace and locate the coolant tank (figure 11-3, page 115). Position the coolant tank valve handle forward towards the front of the furnace to turn off the flow of water. Remove both hoses from the coolant tank and remove the tank.

!
CAUTION
POSSIBLE MACHINE DAMAGE Only use distilled water in the cooling system of the HF-402 induction furnace.

5. 6.

Fill the coolant tank with distilled water to a level of one inch below the inlet hole. Reinstall the coolant tank into the furnace and reinstall the hoses.

66

RH-402

Maintenance

7. 8. 9. 10.

Turn the coolant tank valve 1 /4 turn clockwise to turn on the flow of distilled water. Reinstall the left side panel of the furnace. Reconnect the facility power. Turn Furnace power on.

Draining The Coolant Tank

WARNING

ELECTRICAL SHOCK HAZARD This equipment operates from 230 V~. Contact with this voltage can be lethal. Disconnect the power source.

1. 2.

Turn the furnace off and disconnect from the facility power source. Remove the left side panel of the HF-402 furnace and locate the coolant tank drain valve (figure 11-3, page 115). Attach a 3 /8 inch flexible hose to the coolant tank drain valve and route the hose to the lab water drain. Open the coolant tank drain valve and drain the water out of the coolant tank and cooling system. Close the coolant tank drain valve and remove the flexible hose. Reinstall the left side panel of the furnace. Reconnect the facility power. Turn Furnace power on.

3. 4. 5. 6. 7. 8.

Maintenance

RH-402

67

Disposable Particle Filters

The two disposable particle filters, located in the analyze flow line of the induction furnace, should be replaced every 6 to 12 months.

68

RH-402

Maintenance

Loader Cover

Note

Replace if leakage is determined during a leak check.

Check the loader cover for scratches periodically. A scratched loader cover may present problems with leak checks.

Maintenance

RH-402

69

Incoming Reagent Tube

Notes

1.

Replace the content every ninety days or if the anhydrone becomes wet. Refer to figure 6-2, page 6-12, for packing information.

Remove incoming reagent tube (figure 6-4, page 614): A. B. C. Slide the incoming reagent tube upward until the bottom end can swing free (figure 6-1, page 612). Tilt out the free incoming reagent tube end. Pull the incoming reagent tube downward off the top port.

2.

Insert a screen filter into the bottom of the incoming reagent tube. Position the o-ring towards the bottom and push the screen filter up into the incoming reagent tube 1 /4 inch. Pack the incoming reagent tube, as follows: A. Loosely pack 3 /4 inch of glass wool into the bottom of the incoming reagent tube leaving the narrow section of the incoming reagent tube open. Fill the remaining bottom half of each incoming reagent tube with anhydrone by pouring it on top of the glass wool. Fill the top half of the incoming reagent tube with Lecosorb, leaving 3 /4 inch at the top. Loosely pack 3 /4 inch of glass wool into the top of the incoming reagent tube leaving the narrow section of the incoming reagent tube open. Push the top end of the incoming reagent tube over the top port. Tilt it inward and pull it down, pushing it over the bottom port.

3.

B.

C. D.

4.

Reinstall the incoming reagent tube: A. B.

5.

Reset the incoming reagent tube counter. Refer to Counters, page 5-52.

610

RH-402

Maintenance

Measure Flow Reagent Tube

Notes

1.

Replace contents when 2/3 of the Schutze reagent has turned black. Refer to figure 6-3, page 6-13, for packing information.

Remove measure reagent tube (figure 6-4, page 614): A. B. C. Slide the measure reagent tube upward until the bottom end can swing free (figure 6-1, page 612). Tilt out the free measure reagent tube end. Pull the measure reagent tube downward off the top port.

2.

Insert a screen filter into the bottom of the measure reagent tube. Position the o-ring towards the bottom and push the screen filter up into the measure reagent tube 1 /4 inch (figure 6-3, page 612). Pack the measure reagent tube, (figure 6-3, page 6-13), as follows: A. Loosely pack inch of glass wool into the bottom of the measure reagent tube leaving the narrow section of the measure reagent tube open (figure 6-2, page 612). Fill the bottom anhydrone.
1

3.

B. C. D. E. F. 4.

/3 of the measure reagent tube with

Fill the middle 1 /3 of the measure reagent tube with Lecosorb. Pack 1 /8 inch of glass wool on top of the Lecosorb. Fill the top 1 /3 of the measure reagent tube with schutze reagent. Pack 3 /4 inch (19 mm) of glass wool into the top of the measure reagent tube. Push the top end of the measure reagent tube over the top port. Tilt it inward and pull it down, pushing it over the bottom port.

Reinstall the measure reagent tube: A. B.

5.

Reset the measure reagent tube counter. Refer to Counters, page 5-52.

Maintenance

RH-402

611

REAGENT TUBE

Figure 61 Reagent Tube Removal

775-601 REAGENT TUBE

501-081 GLASS WOOL

502-174 LECOSORB

501-171 ANHYDRONE

501-081 GLASS WOOL 775-306 SCREEN FILTER

Figure 62 Incoming Reagent Tube Packing

612

RH-402

Maintenance

775-601 REAGENT TUBE 501-081 3/4" GLASS WOOL 761-747 SCHUTZE REAGENT 501-081 1/8" GLASS WOOL 502-174 LECOSORB 501-171 ANHYDRONE

501-081 3/4" GLASS WOOL

775-306 SCREEN FILTER

Figure 63 Measure Reagent Tube Packing

Maintenance

RH-402

613

614-354 MOVABLE BLOCK

772-694 KNOB 772-738 O-RING

778-114 O-RING

782-041 COVER TUBE

502-295 COPPER TURNINGS

614-317 UPPER BLOCK (2 REQ'D)

776-279 CATALYST HEATER TUBE 603-956 CATALYST HEATER ASSEMBLY 772-520 O-RING (5 REQ'D) 614-318 LOWER BLOCK (3 REQ'D)

MEASURE REAGENT TUBE

INCOMING REAGENT TUBE

Figure 64 Reagent Tube Assemblies

614

RH-402

Maintenance

Screen Filters

Note

1. 2.

Clean when the reagents are replaced.

Clean the screen filters in the reagent tubes whenever the reagents are replaced. Tap the screen filters lightly to remove any dust. If necessary, clean the screen filters in an ultrasonic cleaner.

Maintenance

RH-402

615

O-rings

Notes

1.

The o-rings listed below should be checked for wear and cracking. Replace when worn and cracked.

The quad ring located in the top seal block, (figure 11-7, page 11-9), should be checked periodically for wear. A. B. C. Remove and wipe off any dirt. Apply a small amount of vacuum grease Replace the o-ring.

2.

The o-ring located in the upper sample loading assembly on the shutter assembly, (figure 11-7, page 11-9), should be cleaned and checked periodically for wear. A. B. C. Remove and wipe off any dirt. Apply a small amount of vacuum grease. Replace the o-ring.

3.

The o-ring located in the bottom seal block, (figure 11-6, page 11-8), should be cleaned and checked periodically for wear. A. B. C. Remove and wipe off any dirt. Apply a small amount of vacuum grease. Replace the o-ring.

616

RH-402

Maintenance

Theory of Operation

General Information............................................................... 73 Furnace Power Oscillator Circuit ............................................... 74 Thermal Conductivity Cell (TC Cell) ........................................... 75 Comparator Level .................................................................. 77 Barometric Pressure ............................................................. 710

Theory of Operation

RH-402

71

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72

RH-402

Theory of Operation

General Information
The RH-402 analyzer and HF-402 induction furnace system is a microprocessor-controlled instrument that measures the hydrogen content of ferrous and nonferrous metals. With the aid of the built-in display and keyboard, the operator may program the unit. The unit features diagnostic programs for troubleshooting a variety of system components. The operator enters gas dosing calibration parameters. Prior to an analysis, the sample is weighed on the built-in balance and automatically entered. At this time the ID information can also be entered. Outgassing, analysis temperature and times as well as many other parameters can be programmed by the operator. During an analysis, graphite crucibles are outgassed to drive off any trapped hydrogen that may be present. At a programmed interval, the sample is automatically added to the crucible and another heating cycle begins. As the sample is heated, the hydrogen (as H2 ) is released into the nitrogen carrier gas stream and carried through the measure flow portion of the system. The measure flow passes through the Schutze reagent, which converts carbon monoxide (CO) to CO2 . The Lecosorb then removes the CO2 and moisture is removed by the anhydrone. The sample gas will then flow to the thermal conductivity cell (TC cell), page 75, where the hydrogen content is measured. The results are printed automatically as well as displayed on the monitor. Past results may be recalculated based on new factors of calibration.

Theory of Operation

RH-402

73

Furnace Power Oscillator Circuit

The oscillator used in the induction furnace is a Colpitts oscillator. This power oscillator is basically a class C tuned amplifier with a portion of the output voltage returned to the input as regenerative feedback. The oscillator starts immediately upon application of the DC plate voltage (filaments are already on). Initially the bias is zero on the control grid because grid current must flow to produce a voltage drop across the grid choke and grid resistor. With zero bias, a larger plate current flows and any noise on the grid is amplified which excites the resonant tank circuit into oscillations. The alternating voltage on the tank capacitors produce an alternating component of plate current that maintains the oscillations. Also, because of the capacitive voltage divider a signal from the tank circuit is 180o out of phase with the plate. This signal is fed to the grid for regenerative feedback. Initially oscillations are small (low grid current) and the tube is working as a class A amplifier. The oscillation quickly increases in magnitude and is only limited by the grid bias. This quick increase causes the tube to saturate and permits the oscillator to work in class C operation. The output has then stabilized at the resonant frequency of the tank and at a power output sufficient to maintain oscillations. The oscillator tube is a power triode 3CX2500H3.

74

RH-402

Theory of Operation

Thermal Conductivity Cell (TC Cell)

The thermal conductivity cell has the ability to detect the difference in the thermal conductivity of gases (see table below). The cell consists of two pair of matched filaments used in four legs of a wheatstone bridge. The reference filaments are maintained in a constant gas, flow and temperature environment while the measure filament is maintained in a constant flow and temperature environment, but the gas composition is allowed to vary. All filaments are mounted in a metal block located in a temperature-controlled oven.
Gas Hydrogen Helium Neon Oxygen Nitrogen Air (Dry) Carbon Monoxide Water Vapor Argon Carbon Dioxide Sulfur Dioxide Thermal Conductivity of Gases Thermal Conductivity Symbol Mol. Wt. (calories/cm secoC x 105) H2 He Ne O2 N2 Air CO H2O Ar CO 2 SO 2 2 4 20 32 28 29 28 18 40 44 64 39 33 10.4 5.7 5.6 5.4 5.4 4.0 3.8 3.3 4.6

The wheatstone bridge is balanced with a specified bridge current while both filaments are essentially in identical environments. The bridge current is based on the thermoelectrical characteristics of the filaments and must be maintained within the limits specified. The bridge current causes self-heating of the filaments. The temperature of the filaments is always much higher than the ambient oven temperature in which the cell is located. The oven temperature is maintained at 45o C 0.2o C, which virtually eliminates any effects of normal room temperature variations. As long as both filaments remain in the same environment under which the bridge was balanced, the bridge output will remain at its minimum reading. Any disturbance of this environment will result in a change in bridge output.

Theory of Operation

RH-402

75

Once the bridge is balanced and stabilized under proper conditions, the only variations in bridge output will be due to variations in the type and quantity of gas present at the measure filaments. The bridge is balanced with nitrogen flowing in the measure chamber and reference chamber. The introduction of hydrogen will cause the temperature of the measure filament to increase since hydrogen has a higher thermal conductivity than nitrogen. In this instance the bridge will become unbalanced and an output will be available to the preamp which will result in a positive reading. The amount of hydrogen will determine the magnitude of the readings. The sensitivity of the system is governed by bridge current and the difference in thermal conductivity between the analyze gas, hydrogen, and the carrier gas, nitrogen. The computer reads the cell output 18 times/second. The A/D converter changes the output into a binary number that is stored in the RAM memory. Noise suppression is applied to the stored data and then integration is performed. Next, adjustments are made for calibration (slope), weight compensation, and blank, if a blank was used. When these calculations are complete the results are displayed as ppm hydrogen.

76

RH-402

Theory of Operation

Comparator Level

Note

One comparator level is associated with each analysis method. Selecting a different method also selects a new comparator level.

An analysis that lasts excessively long causes unnecessarily long delays, while an analysis that isnt long enough can cause loss of significant analyte data collection. Since not all samples combust in the same manner, analyses should not be performed based on time alone. The length of each analysis is determined on an individual basis by the minimum analysis time and the comparator level. Analysis ends when the minimum time limit is reached and the analyte rate drops below the comparator level after passing its peak. This comparator level is a preset constant (k) plus a percent of the peak:

COMPARATOR LEVEL = k + (X)(P)

P X Detector output peak Selected comparator level percentage

During an analysis, the output of the detector is collected in the form of digital data and summed to arrive at the analysis result. If this data were plotted, it would reflect the curve of the detector output.

Theory of Operation

RH-402

77

Shown below are two examples of the same detector output curve (buffer plot). The first example shows the amount of detector output collected during an analysis with a comparator level setting at 6% while the second example illustrates at 25%.

End of Analysis where "X" equals 6%

START OF ANALYSIS
P

DETECTOR OUTPUT

COMPARATOR LEVELEND OF ANALYSIS

DETECTOR OUTPUT COLLECTED

End of Analysis where "X" equals 25.0%

DETECTOR OUTPUT
P

START OF ANALYSIS

COMPARATOR LEVELEND OF ANALYSIS

DETECTOR OUTPUT COLLECTED

The following conclusions can be drawn from the examples: 1. 2. 3. A high comparator level shortens analysis time. A low comparator level includes more sample gas, and therefore more hydrogen, into result calculations. A comparator level that is too low, however, results in the inclusion of very low concentrations that dont significantly effect the result (noise), but lengthen the analysis.

A comparator level of 1.0% usually provides optimum performance by allowing the collection of all significant output within a reasonable time.

78

RH-402

Theory of Operation

Extremely low output peaks may need a larger comparator level to exclude insignificant output levels produced toward the end of analysis and cut down on drift. The minimum time should be extended to match what would be considered a reasonable time length for the analysis of such samples. The combination of a high comparator level and an extended minimum analysis time insures that all significant output is collected and analysis time lengths are consistent without being extensive. Whenever the comparator level changes, check the system calibration since interaction can occur.
COMPARATOR LEVEL (SET TOO HIGH)

DETECTOR OUTPUT COLLECTED

SIGNIFICANT DETECTOR OUTPUT EXCLUDED

COMPARATOR LEVEL (SET TOO LOW)

INSIGNIFICANT DETECTOR OUTPUT

DETECTOR OUTPUT COLLECTED

Theory of Operation

RH-402

79

Barometric Pressure
A pressure transducer that is attached to a flow control valve senses barometric pressure which directly affects gas volume. This pressure transducer operates the control valve to maintain a consistent flow through the detection systems. Therefore, it is important to input correct barometric pressure for proper regulation. Pressure is often reported in inches of mercury (Hg) which must be converted to millimeters (mm) of mercury. To convert from inches of Hg to mm of Hg, multiply the barometric pressure by 25.4. Pressure varies inversely with altitude and, if pressure readings are measured and reported from an altitude other than operation, adjustments should be made accordingly. The table illustrates that as altitude increases, pressure decreases.
Altitude (feet) 0 250 500 750 1,000 2,000 3,000 4,000 5,000 6,000 7,000 8,000 9,000 10,000 Pressure (mm Hg) 760 753 746 740 733 707 681 656 632 609 586 564 543 523

Adjust reported level to reflect the operation level with this formula:
Operation Pressure (from table) 760 Reported Barometric Pressure at 0 feet Adjusted Pressure at Operation

Enter the answer to this formula in the barometric pressure procedure.

710

RH-402

Theory of Operation

Example: Barometric pressure is reported at 750 mm Hg at sea level (0 feet) but operation altitude is 1000 feet. Adjust the reported sea level pressure to operation level pressure by using the formula:
733 mm Hg 760 mm Hg

750 mm Hg

723 mm Hg

In this example, the barometric pressure to be entered into the instrument is 723 mm Hg.

Theory of Operation

RH-402

711

Diagnostics

Diagnostics Menu................................................................... 83 Leak Test ............................................................................. 84 Manual I/O Test .................................................................... 86 Service I/O Table ................................................................. 810 Sequence Test .................................................................... 812 Auto I/O Test...................................................................... 813 Ambient Monitor.................................................................. 816 Printer Diagnostics............................................................... 818 Printer Test #1 .......................................................... 818 Printer Test #2 .......................................................... 818

Diagnostics

RH-402

81

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82

RH-402

Diagnostics

Diagnostics Menu
1. 2. 3. With the analyze menu displayed, press the F8 (More) key to display the system update menu. With the system update menu displayed, press the F8 (More) key to display the diagnostic menu. With the diagnostic menu displayed, press the F1 (System Check) key. The following screen will appear:

Note

The unit must have a 30 minute minimum warm up before the system check can be completed.

Diagnostics

RH-402

83

Leak Test

Notes

1.

This test must be performed at the time of initial installation and prior to analyzing samples. It is recommended that the leak check be accomplished at the start of each workday. The criterion for system leak check pass/fail is a 5 mm Hg per minute loss. With the system check procedure menu displayed, press the F1 (Leak Test) key. The following screen will appear:
Printer: NR Gas -OFFLeak Check 45 Second System Delay. Current Pressure (mm Hg) System Timeout (seconds) 1150.0 30 Chan #01 15:22:40 19 Dec 99

F1 Restart

F2

F3

F4

F5

F6

F7

F8 -Exit-

84

RH-402

Diagnostics

2.

The display will be live, that is, the timer will be counting down from 45 seconds and the current pressure will be monitoring the system pressure. This portion of the test is to establish an equilibrium starting point. After the 45 second system time-out, the following screen will appear:

3. 4. 5.

The arrow on the right of the display will indicate the system status. The elapsed time will continue. If an additional leak check is desired, press the F1 (Restart) key. If the leak check is satisfactory, press the F8 (Exit) key to return to the analyze menu.

Diagnostics

RH-402

85

Manual I/O Test

Notes

This procedure permits the service technician or operator to observe, generate a waveform, or write a logic 1 or 0 at all address locations listed in the Service I/O Table. For example, all switches, solenoids, and the monitor display can be tested to verify proper operation. Refer to the Service I/O Table, page 810, for address information. This table lists the title, abbreviation, and hex address along with other important information. The menu line allows the operator to press the F1 key to observe, the F2 key to generate a waveform, or the F3 key to write a logic 1 or logic 0. With the system check procedure menu displayed, press the F2 (Manual I/O Test) key. The following screen will appear:

1.

86

RH-402

Diagnostics

2.

Press the F1 key to observe an address. The following screen will appear:

Note

Observe can be used to monitor the I/O lines. Address lines on the Service I/O Table, page 810, that have an X in the column under observe can be diagnosed using this procedure. Press the appropriate keys, then press the Enter key. The display following screen will appear:

3.

4.

Press the F1 key to observe the next address, the F2 key to observe the previous address, or the F8 key to exit this procedure and return to the analyze mode.

Diagnostics

RH-402

87

5.

With the I/O test menu displayed, press the F2 (Waveform) key. The following screen will appear:

Note

Waveform can be used to test strobe lines. A separate oscilloscope is required for this procedure. The waveform occurs every 180 microseconds and is approximately 750 microseconds wide. Address lines on the Service I/O Table, page 810, that have an X in the column under waveform can be diagnosed using this procedure.

6.

Press the appropriate keys for the desired address, and then press the Enter key. The following screen will appear:

7.

Press the F1 key to generate a waveform for the next address, the F2 key for the previous address, or the F8 key to exit the procedure and return to the analyze menu.

88

RH-402

Diagnostics

8.

With the I/O test menu displayed, press the F3 (Write) key. The following screen will appear:

Note

Write is used to control individual solenoids, relays, or LED's. This is a functional test. The address line being written to carries an on status when it is set to a logic 1 or an off status when it is set to a logic 0. Address lines on the Service I/O Table, page 810, that have an X in the column under write can be diagnosed using this procedure.

9.

Press the appropriate keys for the desired address, then press the enter key. The following screen will appear:

10.

Press the F1 key to access the next address, the F2 key to access the previous address, the F3 key to write a logic 1, the F4 key to write a logic 0, or the F8 key to exit this procedure and return to the analyze menu.

Diagnostics

RH-402

89

Service I/O Table

Name Gas Switch N Pressure Switch Spare Data Input Block Closed Switch Furnace Load Switch Spare Data Input Spare Data Input Spare Data Input Ground Reference 5 Volt Reference TC High Range Optical Sensor TC Supply Current TC Low Range Oven Temperature Catalyst Heater Doser Temperature 24 Volt Supply Address 0130 0131 0132 0133 0134 0135 0136 0137 0200 0210 0220 0230 0250 0260 0270 02C0 02E4 02D4 Location Data Select Input 1 Data Select Input 2 Data Select Input 3 Data Select Input 4 Data Select Input 5 Data Select Input 6 Data Select Input 7 Data Select Input 8 A/D Channel 0 A/D Channel 1 A/D Channel 2 A/D Channel 3 A/D Channel 5 A/D Channel 6 A/D Channel 7 A/D Channel 12 A/D Channel 14 Mux 2 A/D Channel 13 Mux 1 Observe X X X X X X X X X X X X X X X X X X Wave form X X X X X X X X Write

810

RH-402

Diagnostics

Name 15 Volt Supply -15 Volt Supply Gas On Solenoid N Solenoid

Address 02D8

Location AX/D Channel 13 Mux 2 A/D Channel 13 Mux 1 Solenoid Drive Output 1 Solenoid Drive Output 2 Solenoid Drive Output 3 Solenoid Drive Output 4 Solenoid Drive Output 5 Solenoid Drive Output 6 Solenoid Drive Output 7 Solenoid Drive Output 8 Solenoid Drive Output 9 Solenoid Drive Output 10 Solenoid Drive Output 11

Observe X

Wave form

Write

02DA

01A8

01A9

H Solenoid Pressure Transducer Solenoid Doser Solenoid TC Cell Exhaust Solenoid Furnace Bypass Solenoid Furnace Exhaust Solenoid Block Seal Solenoid Block Slide Solenoid Sample Drop Solenoid

01AA

01AB

01AC

01AD

01AE

01AF

01B0

01B1

01B2

Diagnostics

RH-402

811

Sequence Test

Note

1.

This procedure is used to test certain furnace functions.

With the system check procedure menu displayed, press the F4 (Sequence Test) key. The following screen will appear:

2.

Use the number keys (not function keys) to access the various steps of the sequence test. The monitor display will indicate changes in status as keys are pressed. Press the F1 (Furnace Temp) key to allow entry of a different furnace power level (0 to 100 percent) via the number keys. The speed of the CPU card has been preset to the fastest speed (3). If it is necessary to slow this speed, pressing the S key will toggle between the available speeds (1, 2, or 3). Press the F8 key to exit this procedure and return to the analyze menu.

3.

4.

5.

812

RH-402

Diagnostics

Auto I/O Test

Note

This procedure performs the same functions as the manual I/O test, but enables the technician to directly access address information on screen. With the system check procedure menu displayed, press the F5 (Auto I/O Test) key. The following screen will appear:

1.

2.

Press the F1 key to observe the data select inputs. The following screen will appear:

3.

Press the F8 key to exit the data select input display and return to the display in step 1.

Diagnostics

RH-402

813

4.

Press the F2 key to observe the A/D channel inputs. The following screen will appear:

5. 6.

Press the F8 key to exit the A/D channel input display and return to the display in step 1. Press the F3 key to observe the solenoid drive outputs. The following screen will appear:

814

RH-402

Diagnostics

7.

Press the F1 key to display the next page of outputs. The following screen will appear:

8. 9. 10. 11. 12.

Press the F2 key to advance the cursor highlight to the next line. Press the F3 key to return the cursor highlight to the previous line. Press the F4 key to toggle output state between 0 and 1. Press the F8 key to exit the solenoid drive output display and return to the display in step 1. With the display in step 1 on the monitor, press the F8 key to exit this procedure and return to the analyze menu.

Diagnostics

RH-402

815

Ambient Monitor
1. 2. 3. Set the gas switch to the on position. With the analyze menu displayed, press the F8 (More) key twice to display the diagnostics menu Press the F2 (Ambient Monitor) key to display the temperature, voltages, and pressure used in the system.

Note

Before performing any system check procedures, be sure that these ambient monitor values fall within the range limits given here.
Parameter Ground Reference 5 Volt Reference +15 Volt Supply -15 Volt Supply 24 Volt Supply TC Supply Current TC Low Range TC High Range Oven Heater Catalyst Heater Doser Temperature System Pressure Ambient Monitor Nominal Value 0.00 Counts 5.0 Volts 15.00 Volts -15.00 Volts 24 Volts 0.060 Amps 1.0 Volt 0.05 Volt 45oC 600oC 25oC 747 mm Range 0.00 4.5 to 5.5 13.5 to 16.5 -13.5 to -16.5 21.6 to 26.4 0.055 to 0.065 0.1 to 2.0 0.01 to 2.0 40 to 50 575 to 625 Variable Variable

TC Cell Oven Temperature Catalyst Heater Temperature Gas Purifier Temperatures System Pressure

Normal Variations <0.010 volts 1oC 1oC 1oC 1 mm

60 seconds 60 seconds 60 seconds 60 seconds 60 seconds

4.

Press the F1 (Print) key to receive a printed copy of the ambient monitor display. If any values are out of range, refer to the Electronics Adjustments section, beginning on page 9-1, the Alarm Table, page 571, or the System Update Menu, page 46. To better observe a monitor point that appears to be changing values, press the F4 (Monitor Channel) key. The lowest and highest levels monitored appear to the right of the point being monitored.

5.

816

RH-402

Diagnostics

A.

Press the F2 (Previous Channel) or F3 (Next Channel) key to move the cursor up or down the list to observe the high and low values for each parameter. Press the F4 (Monitor All) key to display the high and low values for all the parameters. Press the F5 (Reset Counters) key to update the high and low parameters for the value(s) being observed.

B. C. 6.

Press the F8 (Exit) key to return to the analyze menu.

Diagnostics

RH-402

817

Printer Diagnostics

Printer Test #1
1. 2. Turn off the printer. Hold down the LF button while turning the printer on. Then printer prints one page of available print styles. When the print is complete, the Sel light glows. To stop this test, press the Mode button.

3.

Printer Test #2
1. 2. Turn off the printer. Hold down the TOF/Quiet button while turning the printer on. The printer prints a continuous sample of the default print style. To stop this test, press the Mode button.

3.

818

RH-402

Diagnostics

Electronic Adjustments

Illustrations .......................................................................... 92 A/D Converter Card Adjustment ............................................... 93 Balance Preamp Card Adjustment ............................................. 95 Furnace Power Control Card Adjustment .................................... 97 Heater Control Z.C. Card Adjustment ........................................ 99 Oven Heater Control Card Adjustment ..................................... 911 5 Volt Supply Adjustment ...................................................... 913 Other Volt Supplies .............................................................. 916 Power Supply Unit ............................................................... 917 TC Cell Adjustment .............................................................. 919 TC Cell Power Supply Card Adjustment .................................... 920

Electronic Adjustments

RH-402

91

Illustrations
Figure 91......... A/D Converter Card....................................94 Figure 92......... Balance Preamp Card .................................95 Figure 93......... Internal BalanceExploded View ..................96 Figure 94......... Furnace Power Control Card.........................98 Figure 95......... Heater Control Z.C. Card.............................910 Figure 96......... Oven Heater Control Card ...........................912 Figure 97......... CPU Card..................................................915 Figure 98......... Power Supply Unit .....................................918 Figure 99......... Oven Compartment ....................................919 Figure 910 ....... TC Cell Power Supply Card ..........................921

92

RH-402

Electronic Adjustments

A/D Converter Card Adjustment

Note

1. 2. 3.

This card should be adjusted if the ground reference, displayed on the ambient monitor, exceeds 4 counts. Enter the Ambient Monitor procedure, page 415, on the diagnostic menu. Observe the ground reference entry on the monitor. It should read 0.00 counts. If the display exceeds 4.0 counts, adjust R1 on the A/D card for a 0.00 count display (figure 9-1, page 94).

Electronic Adjustments

RH-402

93

777-377-110 A / D CONVERTER CARD

ELECTRONICS CHASSIS

TP4 TP5 TP6 TP7 TP3 TP2 TP1 TP0 TP15 TP14 TP13 TP12 TP11 TP10 TP9 TP8 C5 R2 C4

R3 C3 + C2 +

IC1 C1 R1

CONTROL R1

R1 ADJUSTMENT

Figure 91 A/D Converter Card

94

RH-402

Electronic Adjustments

Balance Preamp Card Adjustment

Note

1. 2. 3. 4.

For adjustment locations, refer to figure 9-2 below, and figure 9-3, page 96. Remove the balance module from the analyzer. Remove the balance mechanism from the metal housing cover. Locate R3 gain adjust on the balance preamp card. Place a finger lightly on the balance mechanism pedestal and adjust R3 until the pedestal vibrates. Then adjust R3 until the vibration just stops.

R3 J160

H G R3 C2 C1

+
D

Figure 92 Balance Preamp Card

Electronic Adjustments

RH-402

95

190-228 SCREW (3 REQ'D)

772-595 HOUSING COVER

772-580 BALANCE MECHANISM ASSEMBLY 770-673 BALANCE PREAMP CARD 193-004 WASHER 750-245 2N4922 TRANSISTOR WITH 775-979 SIL-PAD 772-582 MAGNET& HOUSING
COIL WIRES

772-594 RESISTOR R5

FROM R5 RESISTOR

R3 TRANSISTOR SOCKET

190-624 SCREW (3 REQ'D)

193-088 WASHER (2 REQ'D)

772-579 BALANCE BASE 771-722 RECEPTACLE

Figure 93 Internal BalanceExploded View

96

RH-402

Electronic Adjustments

Furnace Power Control Card Adjustment

Notes

Adjust this card when switching line frequencies. This adjustment affects the operating power level of the HF-402 furnace when the system is in the manual mode or whenever furnace power must be controlled without the programmed software.

WARNING

ELECTRICAL SHOCK HAZARD This equipment operates from 230 V~. Contact with this voltage can be lethal. During installation do not apply power until instructed to do so. Before servicing this equipment, disconnect the power source.

1. 2. 3.

Turn off the HF-402 furnace power off and disconnect from facility power source. Remove the front panel of the HF-402 Furnace and locate the furnace power control card. Locate switch 2 (SW2) (figure 9-4, page 98) and set to the desired line frequency. Set this switch to the left for 60 Hz operation or to the right for 50 Hz operation (as viewed in figure 9-4, page 98). Locate switch 1 (SW1) (figure 9-4, page 9-8) and set to either auto or manual furnace power mode. Set the switch to the left for manual mode or to the right for automatic mode. Auto mode is the typical operating mode while the manual setting is for service or diagnostics. The furnace enable switch is used in conjunction with the furnace power control card and is located on the base of the furnace cabinet next to the card. The switch should be set to the auto position (left) for operation. The manual position (right) is for service or diagnostic purposes. When the furnace enable switch is in the manual position, the furnace can be operated two ways:

4.

5.

Electronic Adjustments

RH-402

97

A.

Set SW1 on the furnace power control card to manual; R13 can be used to adjust the furnace. Relative furnace power can be read on the plate current meter on the front of the furnace. Set SW1 on the furnace power control card to auto; furnace power can be set through the Sequence Test procedure, page 8-12.

B.

C2 C1 + R1 R3 U1 R5 R7 U2 CR1 R4 R6 R8 BR2 C4 CR2 C7 R10 R11 C8 C9 C11 U8 Q2 U6 R14 R15 R16 R17 R18 U7 R19 U9 R20 R2 C5 C3

J556

BR1

+
U3

R9

U4

U5

C6

+ +
C12 C13

Q1 C10

R12

SW2

R13

SW1

C14 SW2 U10

Y1

MANUAL

AUTO

60Hz

50Hz

Figure 94 Furnace Power Control Card

98

RH-402

Electronic Adjustments

C16

C15

Heater Control Z.C. Card Adjustment

Notes

The purpose of this adjustment is to adjust the temperature set point of the heater control card. This is to ensure proper temperature tracking of the furnace and to provide for accurate temperature readouts. The adjustment is necessary only when the card is replaced or the temperature falls out of range (45oC 2 oC). Initial adjustment is made at the factory.

WARNING

HIGH VOLTAGE HAZARD The following steps require the unit's high voltage source be on. This will permit hazardous voltages to be present within the cabinet area.

WARNING

ELECTRICAL SHOCK HAZARD Care and extreme caution must be exercised when working in proximity of the electrical circuits of the instrument.

1.

Press the F8 (More) key twice and then press the F2 (Ambient Monitor) key to observe the catalyst heater temperature. Remove the left side panel of the analyzer Swing open the electronics chassis and locate the heater control Z.C. card (figure 11-1, page 11-3). Adjust R24 on the Heater Control Z.C. card (figure 9-5, page 9-10), so that the gas purifier temperature display on the ambient monitor screen reads 600o C. Allow the temperature to stabilize between adjustments. Close the electronics chassis and replace the left side panel.

2. 3. 4.

5.

Electronic Adjustments

RH-402

99

R1 R2 R5 R3 R4 C1 C2 C6

+
C3

+
C5 R6 R7 U2 R8 C4 A J449

U1 R9

C7 R10 R20 R24 CR3 Q4 R25 C8 R12 R13 C9 R14 R15 R18 C10 Q1 Q2 CR1 R11 L

Q3

R19 R16 R17 C11 C12 C13 CR2

R27

R23

CR4 LED1

TB1 C14

R21 R22 R28 TP1 TP2

TP3

TP1

TP2

R24

Figure 95 Heater Control Z.C. Card

910

RH-402

Electronic Adjustments

R26

U3

Oven Heater Control Card Adjustment

Note

This procedure should be completed if the oven temperature falls out of range (45oC 2 oC) as displayed on the message center. This adjustment requires a digital voltmeter.

WARNING

HIGH VOLTAGE HAZARD The following steps require the unit's high voltage source be on. This will permit hazardous voltages to be present within the cabinet area.

WARNING

ELECTRICAL SHOCK HAZARD Care and extreme caution must be exercised when working in proximity of the electrical circuits of the instrument.

1. 2. 3. 4.

Remove the analyzers left side panel and oven compartment side panel (figure 11-1, page 113). Locate the oven heater control card. Locate R1, TP1, and TP2 (figure 9-6, page 912). Connect the digital voltmeter leads (+ to TP1 and - to TP2). When readings have stabilized, adjust R1 to the oven temperature desired. A voltmeter reading of 100 mV is equivalent to 1o C; thus, for an oven temperature of 45o C, R1 should be adjusted so that the voltmeter reads 4.5 volts. Disconnect the digital voltmeter. Reinstall the oven compartment side panel and allow the temperature to stabilize. Recheck the temperature reading displayed on the message center. It should be 45o C 2o C.

5. 6.

Electronic Adjustments

RH-402

911

R1

TP2

TP1

TP2

TP1 TP3 C2

U1
C3 C4

C1
R1 R3

R4 R5 R6
R7 R8 C6 R13 R14 R15 R9 C7 C8

U2

K1

R2

C5

R16

U3

R12

R10 R11

C9

Q1 U4 R17
C12 C13

+
C14

CR1

U5

C10

C11

J539

Figure 96 Oven Heater Control Card

912

RH-402

Electronic Adjustments

5 Volt Supply Adjustment

Note

If the power supply unit is replaced, the +5 V adjustment should be checked to determine if it is in range. System lockups or erratic results may occur if the +5 V adjustment is out of range.

WARNING

HIGH VOLTAGE HAZARD The following steps require the unit's high voltage source be on. This will permit hazardous voltages to be present within the cabinet area.

WARNING

ELECTRICAL SHOCK HAZARD Care and extreme caution must be exercised when working in proximity of the electrical circuits of the instrument.

1. 2.

Remove the left side panel of the analyzer and locate the CPU card (figure 11-1, page 113). Using a digital voltmeter, measure the voltage across pins 3 and 4 on connector J057F (figure 9-7, page 915). The voltage should measure between 4.85 - 4.90 volts. If the voltage is out of range, continue this adjustment. Switch the power to the analyzer off and unplug from facility power.

3.

WARNING

ELECTRICAL SHOCK HAZARD Disconnect power cord from the facility power.

Electronic Adjustments

RH-402

913

4. 5.

Locate the power supply unit and remove the power supply cover. Determine if the power supply unit is a Boschert or Power-One brand (figure 9-8, page 918). A. B. For a Boschert Power Supply, locate potentiometer R39. For a Power-One Power Supply, locate potentiometer R50.

6.

Reconnect the analyzer to facility power and switch the power on. While measuring the voltage across pins 3 and 4 on J057F of the CPU card, adjust the potentiometer on the power supply unit until the measured voltage is within range (4.85 - 4.90 V). Again switch the power off and disconnect the analyzer from facility power. Replace the shield that covers the power supply unit, then power up the analyzer.

7.

914

RH-402

Electronic Adjustments

J057F

U1

R3

666-057-010-X

ISA BUS 486SX BOARD U2

R4 R6

R5

C1 R7 CR1

C2

TP1 L1 RN1 RN2 RN3 C3 U3 U5 TP2 RN4 U7 R9 C4 U4 R8 R10 R11

B1

C5

J057I J057J U8 F1 R12 R13 C7 C8 F2 J057K C13

R1

R2

J057H J057G

J057E

J057F

TP3

C6

U6 U10 R15 U12 C11 C12 U13 RN6 RN7 RN8 RN9 Y1 U14 RN5 C10

C14

Figure 97 CPU Card

Electronic Adjustments

RH-402

915

Other Volt Supplies

The 5 volt reference and all other volt supplies are not adjustable. If they are out of range, change the power supply: * * * The 5 volt reference is located on the A/D card. The 12, +24 and +5 Volt are located on the power supply unit. The 15 Volt supply is on its own card.

916

RH-402

Electronic Adjustments

Power Supply Unit

Notes

1.

Field service should not be performed on the power supply unit. Remove and replace as necessary. The power supply unit is located on the right side of the analyzer.

The instrument may contain either a Boschert brand or Power-One brand power supply unit. Both units serve the same purpose and are interchangeable in all instruments, however, the units are wired differently.

Note

Figure 9-8, page 9-18, illustrates the pin outs for each chassis. Notice that the numbering of the terminal configuration in the Boschert power supply is reversed in the Power-One unit. When installing either unit, be sure to connect wires accordingly. When replacing the power supply unit, the voltage select wire should be set for 230 V~.

2.

Electronic Adjustments

RH-402

917

TERMINAL #5 = RETURN = TERMINAL #6 TERMINAL #4 = +24V = TERMINAL #5

NOTE: CONNECTIONS REVERSED

+5V +5V RETURN RETURN RETURN +24V +12V -12V POWER FAIL + 5V + 5V + 5V RETURN + 5V RETURN + 24 V AUX RETURN +12V -12V POWER FAIL 1 2 3 4 5 6 7 8 9

9 8 7 6 5 4 3 2 1

R50

CAPACITORS R39

CAPACITORS

OR
CP BOSCHERT
POWER SUPPLY

TRANSFORMER

DANGER HIGH VOLTAGE

CAPACITORS TRANSFORMER CAPACITORS 115V~ 230V~ VOLTAGE SELECT WIRE FUSE

1 2 3 AC NEUTRAL/HOT

115V~ VOLTAGE SELECT WIRE

FUSE

230V~

3 2 1 AC HOT AC NEUTRAL/HOT AC GROUND

AC HOT AC GROUND

TERMINAL #2 = AC GROUND = TERMINAL #1 TERMINAL #3 = AC NEUTRAL/HOT = TERMINAL #2 NOTE: CONNECTIONS REVERSED

BOSCHERT

TM

POWER SUPPLY

POWER-ONE TM POWER SUPPLY

Figure 98 Power Supply Unit

918

RH-402

Electronic Adjustments

TC Cell Adjustment

Notes

1. 2. 3.

The TC cell offset adjustment hole will be plugged. This adjustment was made at the factory. Readjust if the TC cell is out of range. Refer to Ambient Monitor, page 8-16, for nominal value and range. The analyzer should have completed a 2 to 3 hour warm-up.

Access the ambient monitor procedure from the diagnostic menu. Observe the TC cell low and high readings. Remove the analyzer's left side panel (figure 11-1, page 11-3) and open the oven compartment and locate the bridge balance and cell offset adjustments on the TC cell (figure 9-9, below). Adjust the bridge balance adjustment until approximately 1.00 is displayed on the ambient monitor for the hydrogen TC cell low reading. Remove the plug from the cell offset adjustment hole. The hydrogen TC cell high reading should be 0.050 5% (the gain of the high range is 1 /20 of the low range). If it is not, adjust the cell offset adjustment until the correct reading is displayed on the ambient monitor. Press the F8 (Exit) key to return to the diagnostic menu.
775-376 TC CELL

4.

5. 6.

7.

OFFSET ADJUST

BRIDGE BALANCE ADJUST

Figure 99 Oven Compartment

Electronic Adjustments

RH-402

919

TC Cell Power Supply Card Adjustment

1. 2. 3. In the ambient monitor procedure of the diagnostic menu, observe the TC supply current on the display. Adjust control R1 for a TC supply current of approximately 60 MA (0.060A) (figure 9-10, page 921). This setting will affect calibration, a test sample should be run after each adjustment to ensure a system calibration factor of approximately 1.00. Repeat adjustments and sample analysis as necessary.

4.

920

RH-402

Electronic Adjustments

R1

TP1

TP2

TP3

TP4

R1

U1

R3 R4 R5 R6 Q1 Q2 HS2

R2 C4 U2

C1 C3 R7 R8 CR1 L1 C4

HS3 U3 R14 Q4 R15 R12 Q5 R13 CR2 R16 C5

R9

Q3 BR1

Q6

R11 C5

RT1

J548

Figure 910 TC Cell Power Supply Card

Electronic Adjustments

RH-402

921

10

Service

Illustrations ........................................................................ 102 Mechanical Adjustments........................................................ 103 Magnetic Reed Switches .............................................. 103 Block Closed Switch............................................... 104 Block Open Switch................................................. 105 Sample Loading Assembly Alignment ...................................... 106 Electronic Circuit Card Replacement ........................................ 108 Gas Flows..........................................................................1010 Analysis Valve State..................................................1010 Purification..........................................................1010 Measure Flow.......................................................1010 Outgas Valve State ...................................................1011 Gas Dose Valve State ................................................1011 Valve States ......................................................................1012 Linearization ......................................................................1020 Linearize..................................................................1021 Break Points ......................................................................1022 Initializing the CPU for 80486 Systems ...................................1023 486 CPU Setup Procedure ...........................................1023

Service

RH-402

101

Illustrations
Figure 101 ....... Sample Loading Assembly ...........................107 Figure 102 ....... Gas Flow Diagram......................................1013 Figure 103 ....... Leak Check Flow Diagram............................1014 Figure 104 ....... Gas Dose Sequence Diagram.......................1015 Figure 105 ....... Leak Check Sequence Diagram.....................1016 Figure 106 ....... Hot Extraction Analysis Procedure H Sequence Diagram....................1017 Figure 107 ....... Fusion Analysis Procedure F Sequence Diagram....................1018 Figure 108 ....... Combined Analysis Procedure C Sequence Diagram....................1019

102

RH-402

Service

Mechanical Adjustments

Magnetic Reed Switches

Notes

Because the switches are magnetically operated and the magnets are located inside the pneumatic cylinder, it is important to keep the switches firmly pressed against the cylinder at all times. These adjustments may be necessary if the loading head will not open or close even though the gas is on.

Service

RH-402

103

Block Closed Switch

1. 2.

From the diagnostic menu, press F1 for system check. Press F2 for manual I/O test and then F1 for observe. Observe the address 133. Look at the far right digit in the line Value = XXXXXXXXXXXXXXXX Binary (X's representing logic 1 or 0). Lift up the loader assembly cover, (figure 10-1, page 10-7) and determine which switch is the block closed switch by tracing the wiring from the cylinder to connector J154. Loosen the clamping screw on the block closed switch. While holding the switch firmly against the cylinder, slide the switch as far as possible to the left and then slowly to the right until the right-most digit on the screen changes from a 0 to a 1. Note this position. Continue sliding the switch to the right until the digit changes back to a 0. Mark this position. If the digit does not change to a 0, use the right-most position of the switch for marking purposes. Measure the distance between the point where the digit changed from 0 to 1 and the point where the digit changed back to 0 (or the physical end of movement) and divide by three. Move the switch this distance to the right of the point where the digit changed from 0 to 1 (the left position). Tighten the clamping screw on the switch. Check for proper operation of the switch by opening and closing the block using the sequence test procedure (from the diagnostic menu, press F1 for system check and then F4 for sequence test). Return to the manual I/O test procedure and observe address 133 again. The rightmost digit should be a 1. If it is not, readjustment is necessary.

3.

4.

5.

6.

7.

8.

104

RH-402

Service

Block Open Switch 1. From the diagnostic menu, press F1 for system check. Press F1 again for furnace power. Set the furnace power for 10% (10.000) and then press the Enter key. Lift up the loader assembly cover, (figure 10-1, page 10-7) and determine which switch is the block open switch by tracing the wiring from the cylinder to connector J155. Loosen the clamping screw on the block open switch. While holding the switch firmly against the cylinder, slide it as far as possible to the left and then slowly to the right until the furnace turns on. Note this position. Continue sliding the switch to the right until the furnace turns off. Mark this position. If the furnace does not shut off, use the right-most position of the switch as the furnace off position. Measure the distance between the point where the furnace turned on and where it turned off (or the physical end of movement) and divide by three. Move the switch this distance to the right of the point where the furnace turned on (the left position). Tighten the clamping screw on the switch. Check for proper operation of the switch by opening and closing the block using the sequence test procedure (from the diagnostic menu, press F1 for system check and then F4 for sequence test). From the sequence test procedure select a power level for the furnace. If the furnace does not switch on, readjustment is necessary.

2.

3.

4.

5.

6.

7.

Service

RH-402

105

Sample Loading Assembly Alignment

Notes

1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11.

The sample loading assembly may require periodic alignment adjustments. The instructions below outline an alignment procedure using the alignment tool.

With the analyze menu displayed, press the F8 key twice to display the diagnostic menu. With the diagnostic menu displayed, press the F1 key for the system check procedure. With the system check menu displayed, press the F4 key for the sequence test procedure. From the sequence test screen, press 7 to open the seal. Now press 8 from the sequence test screen to open the block. Unlock the locking mechanism on the optical sensor and swing it out of the way (figure 10-1, page 107). Remove the front panel of the furnace. With a graphite crucible in place, adjust the motor pulley until the crucible is 1 /4 inch from the top of the top seal. Drop the alignment tool into the port of the sample loading block. From the sequence test screen, press 8 to close the block. Now press 9 to open the sample drop.

Note

If the sample loading assembly is properly aligned, the tool will drop into position. If it does not, continue with this adjustment procedure.

12. 13.

Lift the loader assembly cover to expose the slide cylinder (figure 10-1, page 10-7). Loosen the adjustment screws on the slide cylinder (figure 10-1, page 10-7) and adjust the cylinder until the alignment tool drops into position. Tighten the adjustment screws and remove the alignment tool. From the sequence test screen, press 8 to open the block.

14. 15.

106

RH-402

Service

16. 17. 18. 19.

Swing the locking mechanism back into place and lock it. From the sequence test screen, press 8 to close the block. Press 7 to close the seal. Press F8 to exit sequence test. Replace the front panel of the furnace.

783-593 ROTARY ACTUATOR 603-711 PLATE CURRENT METER DC mA

603-860 SEAL CYLINDER

603-974 LOCKING MECHANISM

603-888 LOADER ASSEMBLY COVER

190-279 ADJUSTMENT SCREW (4 REQ'D) 603-870 SLIDE CYLINDER 603-871 MAGNETIC REED SWITCH (2 REQ'D) 603-862 SAMPLE LOADING BLOCK 777-605 MELT DETECTOR CARD

603-955 OPTICAL SENSOR

604-266 TOP SEAL

Figure 101 Sample Loading Assembly

Service

RH-402

107

Electronic Circuit Card Replacement

1. Set the power switch to the off position and unplug the instrument from facility power.

WARNING

ELECTRICAL SHOCK HAZARD Disconnect power cord from facility power.

2. 3. 4. 5. 6. 7. 8.

Remove the left side panel and swing out the electronics chassis (figure 11-1, page 11-3). Remove the two screws and washer and remove the power supply cover. Disconnect the harness assembly from the power supply card. Disconnect the video input cable from the flat panel interface card. Remove the six nuts and washers that secure the flat panel assembly to the instrument. Lay the assembly on a work surface, card side up. To replace the power supply card: A. B. C. D. E. Release the power supply ribbon cable from the clamp and disconnect it from the card. Remove the four screws and remove the card. Install the new card using the four screws. Reattach the cable to the card and secure with the clamp. If no other replacements are necessary, go to step 10.

9.

To replace the flat panel interface card: A. B. C. Release the flat panel interface cable from the clamp and disconnect it from the card. Remove the four screws and remove the card. Install the new card using the four screws.

10.

Reattach the cable to the card and secure with the clamp.

108

RH-402

Service

11. 12.

Reattach the flat panel assembly to the instrument using the six washers and nuts removed in step 6. Reconnect the harness assembly detached in step 4. The harness assembly must be reattached with the black wire on top. Reconnect the video input cable detached in step 5. Plug the instrument into facility power and set the power switch to the on position.

13. 14.

Service

RH-402

109

Gas Flows

Note

Use the Gas Flow Diagrams, Sequence Diagrams, (figures 10-2 through 10-8 on pages 10-12 through 10-18) and Valve States, page 10-12, in conjunction with the following descriptions.

Analysis Valve State

Purification When the gas switch on the front panel is turned on, nitrogen at 40 psi (2.76 bars) enters the analyzer through the inlet port on the cabinet back panel. Particulates are removed from the incoming carrier/pneumatic gas in a 0.6-micron filter, while trace oxygen is removed in the catalyst heater, containing copper turnings heated to 600o C. A second micron filter removes any remaining particulates from the gas.

Measure Flow During an analysis, purified gas is split into two paths. One path flows through the reference side of the thermal conductivity cell and is exhausted out the back of the unit. This flow is factory set at 50 ml/min but may be adjusted. The second path serves as the measure flow and is set for 900 to 950 ml/min as read on the furnace rotameter. Measure flow is filtered through a 6 inch reagent tube containing lecosorb and anhydrone reagents to remove carbon dioxide and water impurities. Excess flow entering the furnace is automatically exhausted through a particle filter and exits through SV8 (furnace exhaust solenoid). Flow is drawn through the furnace; picking up hydrogen gas as it is given off by the heated sample. Particulate matter is again filtered from the flow which now measures 260 to 300 ml/min as read from the furnace rotameter. A second 6 inch reagent tube containing Schutze reagent, lecosorb, and anhydrone removes additional impurities that form during the heating of the sample. (Schutze reagent converts carbon monoxide to carbon dioxide, which in turn, is removed with lecosorb). Gases are pumped through a 15micron filter and the adjustable flow controller on the measure side of the TC cell. After the thermal conductivity of the gases are measured, flow is exhausted on the back of the unit.

1010

RH-402

Service

Outgas Valve State

In this valve state, flow is identical to the analyze valve state except that the furnace bypass solenoid (SV7) is on. Flow is split into two paths before entering the reaction chamber; one path is routed through the bottom of the furnace, up through the reaction tube and is exhausted through SV8. The second path is routed through the TC cell as described in the analyze valve state.

Gas Dose Valve State

In the gas dose valve state, measure flow is identical to that in the analyze valve state. A third pathway splits off after gas exits the catalyst heater and second particle filter. During a gas fill, nitrogen passes through SV2 (gas dose carrier solenoid) and R1 (flow restrictor) and enters the 6 port gas doser. Carrier gas flows from port D to port E while hydrogen dosing gas fills the 100 l loop (inlet port through SV3, port B to C, and out from port F to G). After the fill period, the linear slide valve switches to allow the nitrogen carrier gas to sweep the dose gas from the loop (port D to C and out from port F to E). Gases are mixed in a 15 ml chamber and then dumped into the measure flow. The linear slide valve is controlled by SV5 (doser solenoid).

Service

RH-402

1011

Valve States

Notes

The following chart shows the system valve states and the relationship to the operating solenoid valves. 1" represents the on state while 0" represents the off state.

Gas Dose Carrier Solenoid

Furnace Exhaust Solenoid

Gas On Solenoid

Furnace Bypass Solenoid

TC Cell Exhaust Solenoid

Pump Solenoid

Doser Solenoid

Hydrogen Gas Dose Solenoid

Sample Drop Solenoid SV11 0 0 0 0 0 0 0 0 1 0 0 0 0

Pressure Transducer Solenoid

Slide Block Solenoid

Top Seal Solenoid

Solenoids

Valve State Gas Off Analyze Gas Dose Fill Gas Dose Equilibrate Gas Dose Dump Gas Dose Post Out Gas Sample Load 1 Sample Load 2 Sample Drop Leak Check 1 Leak Check 2 Leak Check 3

SV0 0 1 1 1 1 1 1 1 1 1 0 0 0

SV1 0 1 1 1 1 1 1 1 1 1 1 0 0

SV2 0 0 1 1 1 1 0 0 0 0 0 0 0

SV3 0 0 1 0 0 0 0 0 0 0 0 0 0

SV4 0 0 0 0 0 0 0 0 0 0 1 1 1

SV5 0 0 0 0 1 0 0 0 0 0 0 0 0

SV6 0 1 1 1 1 1 1 1 1 1 0 0 1

SV7 0 0 0 0 0 0 1 1 1 0 0 0 0

SV8 0 1 0 0 0 0 1 1 1 1 0 0 0

SV9 0 0 0 0 0 0 0 1 1 0 0 0 0

SV10 0 0 0 0 0 0 0 0 1 0 0 0 0

SV12 0 0 1 1 1 1 0 0 0 0 0 0 0

1012

RH-402

Service

Solenoid

PRESSURE SWITCH 25 PSI FILTER SV1 N2IN 40 PSI

PRESSURE GAUGE 0 - 60 CATALYST HEATER Cu 6000 GAS ON SOLENOID FLOW CONTROLLER FLOW METER W/ADJUST FLOW CONTROLLER FILTER

TC REFERENCE TC EXHAUST

SV6

TC MEASURE

FILTER SV2 D R 50cc SV3 H2 I N 40 PSI B R2 100cc G E SCHUTZE REAGENT DOSER EXHAUST SV5 DOSER SOLENOID 6 TUBE LECOSORB ANHYDRONE N.O. EXHAUST GAS DOSER F C 100 ul PUMP R3 250cc PRESSURE GAUGE 0 - 60

LECOSORB ANHYDRONE 6 TUBE

COM

S12

SV4 N.C. (IN)

FILL DUMP

15ml CHAMBER FLOWMETER

RH-402 ANALYZER

HF-402 FURNACE
SV9 TOP SEAL SV10

EXHAUST SV8

SAMPLE LOADING ASSEMBLY SAMPLE

SLIDE BLOCK

FILTER SV7 FILTER N. 0. (EXH.) R. F. COIL

SV11

SAMPLE DROP

FURNACE BYPASS SOLENOID N. C. (IN)

REACTION TUBE

Figure 102 Gas Flow Diagram Service RH-402 1013

PRESSURE SWITCH 25 PSI FILTER SV1 N2IN 40 PSI

PRESSURE GAUGE 0 - 60 CATALYST HEATER Cu 600

0

FILTER

GAS ON SOLENOID FLOW CONTROLLER FLOW METER W/ADJUST FLOW CONTROLLER

TC REFERENCE TC EXHAUST

SV6

TC MEASURE

FILTER SV2 R 50cc SV3 H2 I N 40 PSI B R2 100cc G E ANHYDRONE 6 TUBE LECOSORB N.O. EXHAUST SCHUTZE REAGENT SV4 N.C. (IN) D GAS DOSER C 100 ul F PUMP R3 250cc PRESSURE GAUGE 0 - 60 COM

LECOSORB ANHYDRONE 6 TUBE

S12

DOSER EXHAUST SV5 DOSER SOLENOID 15ml FILL DUMP

CHAMBER FLOWMETER

RH-402 ANALYZER

HF-402 FURNACE
SV9 TOP SEAL SV10

EXHAUST SV8

SAMPLE LOADING ASSEMBLY SAMPLE

SLIDE BLOCK

FILTER SV7 FILTER N. 0. (EXH.) R. F. COIL

SV11

SAMPLE DROP

FURNACE BYPASS SOLENOID N. C. (IN)

REACTION TUBE

Figure 103 Leak Check Flow Diagram

1014

RH-402

Service

Figure 104 Gas Dose Sequence Diagram

Service

RH-402

1015

Figure 105 Leak Check Sequence Diagram

1016

RH-402

Service

Figure 106 Hot Extraction AnalysisProcedure H Sequence Diagram

Service

RH-402

1017

Figure 107 Fusion AnalysisProcedure F Sequence Diagram

1018

RH-402

Service

Figure 108 Combined AnalysisProcedure C Sequence Diagram

Service

RH-402

1019

Linearization

Notes

Only one break point can be linearized at a time. Compare the peak values received from the standard to the break values listed in the table. The standard that is used should exhibit a similar peak offset. Sample weights can be adjusted to bring the peak offset closer. The auto linearization is based on the last three analyses of one selected standard. They must be the last three analyses performed and must have the proper concentration for the point being linearized.

1020

RH-402

Service

Linearize
1. 2. 3. From the analyze screen, press F8 (More) key twice to display the diagnostic menu. From the diagnostic menu press F5 (Security Area) key to display the security menu. From the security menu press F1 (Linearize) key. The following screen will appear.

4.

Press the F5 key to edit breaks of the selected cell. Type over the current values using the number keys. Press the Enter key to accept the value on the current line. Press the F6 key to edit slopes of the selected cell. Type over the current values using the number keys. Press the Enter key to accept the value on the current line. Press the F4 (Iterate Slope) key to manually linearize the TC cell one breakpoint at a time. At the appropriate prompts, enter the breakpoint number to linearize and the standard value to use. The breakpoint and slope will then be recalculated for that point using the last three analysis results. Pressing F7 will reset linearization values to their default values. Slopes will revert to 1.0000 while breaks and adjustments will revert to 56000. Press the F8 key to exit the linearization procedure.

5.

6.

7.

8.

Service

RH-402

1021

Break Points

Notes

1. 2. 3.

Break points are listed on the tag attached to the TC cell. When a new TC cell is installed, break points on the cell linearization tag should be entered here.

With the analyze menu displayed, press the F8 (More) key to display the system update menu. Press the F3 (Constants) key. Press the F5 (Break Points) key. The display will be similar to the following example.

4. 5.

Press the F1 (Print) key to receive a printed copy of this screen. Press the F3 (Next Value) or F2 (Previous Value) key to move the highlighted cursor line to the constant to be edited. Press the F5 (Hydrogen Slopes) key to change the slope values. Press the F6 (Hydrogen Breaks) key to change the break values. Press the F8 (Exit) key to return to the analyze screen.

6. 7. 8.

1022

RH-402

Service

Initializing the CPU for 80486 Systems

486 CPU Setup Procedure

Note

The CMOS configuration may have to be set for an 80486 CPU card.

During the new CPUs boot process when the message WAIT . . . . is displayed, press the delete key. The display will be similar to the following example.
AMBIOS SETUP PROGRAM - BIOS SETUP UTILITIES 1992 American Megatrends Inc., All Rights Reserved STANDARD CMOS SETUP ADVANCED CMOS SETUP ADVANCED CHIPSET SETUP PERIPHERAL MANAGEMENT SETUP AUTO DETECT HARD DISK HARD DISK UTILITY WRITE TO CMOS AND EXIT DO NOT WRITE TO CMOS AND EXIT

Use the arrow keys to move the highlight cursor to Standard CMOS Setup and press the enter key to access this procedure. The display will be similar to the following example.
AMBIOS SETUP PROGRAM - STANDARD CMOS SETUP 1992 American Megatrends Inc., All Rights Reserved Date (mn/date/year):Tue, May 16 1995 Time (hour/min/sec):14 : 52 : 09 Cyln Hard Disk C: Type : 2 Hard Disk D: Type : Not Installed Floppy Drive A: 1.44 MB, 31/2 Floppy Drive B: Not Installed Primary Display: Color 80 x 25 Keyboard: Not Installed Month : Jan, Feb, Dec Date : 01, 02, 03,...31 Year : 1901, 1902,.2099 Base Memory :640 KB Ext. Memory :1024KB Head Wpcom Lzone Sect Size 615
Sun 30 7 14 21 28 Mon 1 8 15 22 29 5

4
Tue 2 9 16 23 30 6

300
Wed 3 10 17 24 31 7

615
Thu 4 11 18 25 1 8 Fri 5 12 19 26 2 9

17

20 MB
Sat 6 13 20 27 3 10

Service

RH-402

1023

Use the page up and page down keys to set the date and time. Hard disk types may be manually entered using this procedure, or they can be automatically entered using the Auto Detect Hard Disk procedure. Floppy drive A is installed at the factory and should be set for a 1.44 MB, 31 /2 inch drive. If floppy drive B is installed, select the proper drive type. The primary display should be set for color 80 x 25. If an external keyboard is connected, set the keyboard setting to Installed. After all Standard CMOS Setup settings are correct, press the Esc key to return to the main setup menu.

Note

Pressing the Enter key within a setup screen will move the highlight cursor to the next editable field.

Use the arrow keys to move the highlight cursor to advanced CMOS setup and press the Enter key to access this procedure. The display will be similar to the following example.
AMBIOS SETUP PROGRAM - ADVANCED CMOS SETUP 1992 American Megatrends Inc., All Rights Reserved Typematic Rate Programming Typematic Rate Delay (msec) Typematic Rate (Chars/Sec) Above 1 MB Memory Test Memory Test Tick Sound Memory Parity Error Check I/O Channel Check Error Hit <DEL> Message Display Hard Disk Type 47 RAM Area Wait For <F1> If Any Error System Boot Up Num Lock Floppy Drive Seek At Boot System Boot Up Sequence System Boot Up CPU Speed Internal Cache Memory Turbo Switch Function Password Checking Option Video ROM Shadow C000, 16K : : : : : : : : : : : : : : : : : : Enabled 500 30 Disabled Enabled Enabled Disabled Enabled 0:300 Disabled On Disabled C:, A: High Enabled Disabled Setup Enabled

Video ROM Shadow C400, 16K : Adaptor ROM Shadow C800, 16K : Adaptor ROM Shadow CC00, 16K : Adaptor ROM Shadow D000, 16K : Adaptor ROM Shadow D400, 16K : Adaptor ROM Shadow D800, 16K : Adaptor ROM Shadow DC00, 16K : Adaptor ROM Shadow E000, 16K : Adaptor ROM Shadow E400, 16K : Adaptor ROM Shadow E800, 16K: Adaptor ROM Shadow EC00, 16K : Adaptor ROM Shadow F000, 64K : BootSector Virus Protection :

Enabled Disabled Disabled Disabled Disabled Disabled Disabled Disabled Disabled Disabled Disabled Enabled Disabled

1024

RH-402

Service

Use the arrow keys to move the highlight cursor to advanced chipset setup and press the Enter key to access this procedure. This procedure consists of three screen displays. None of these settings should be changed. The parameters are shown here only for the purpose of listing proper settings. The first display will be as follows.
AMBIOS SETUP PROGRAM - ADVANCED CMOS SETUP 1992 American Megatrends Inc., All Rights Reserved Read Cycle Start Point RAS Precharge Time RAS To CAS Delay CAS Width For Read/Write RAS Timeout MA [10:0] & RAMW# Drive (mA) Refresh Mode Refresh Type Refresh Period Page Mode Ext. Parity Error Input Parity generation Middle BIOS Flash Memory Support ROM Wait States Slow CPU Speed Emulation Slow CPU Clock Divider Fast BUS CLK Freq. Change : : : : : : : : : : : : : : : : : : Begin T2 3 CLK2s 3 CLK2s 2/2 Enabled 24-24-24 Sync RAS ONLY 15.625 Enabled Disabled Disabled Disabled Disabled 3 W/S /2 /4 Disabled Fast BUS CLOCK Region Addr Fast BUS CLK Divider Slow BUS CLK Divider Extended DMA Mode Extended DMA Page 8-Bit DMA Wait States 16-Bit DMA Wait States DMA Clock DMA MEMR# Signal Delay I/O Address Decode Slot Drive Current Disk I/O Timing Command Delay - I/O Cycle Command Delay - Mem Cycle 16-Bit Wait States 8-Bit Wait States CWE Turn-off Time Fast Internal RC# : : : : : : : : : : : : : : : : : : 0 KB /8 /8 Disabled Lower 3 W/S 3 W/S SCLK/2 Normal 16 bit 24 mA Slow 1 1 1 W/S 5 W/S Late Enabled

Use the arrow keys to scroll through the parameters. The second display in the advance chipset setup procedure is as follows.
AMBIOS SETUP PROGRAM - ADVANCED CMOS SETUP 1992 American Megatrends Inc., All Rights Reserved Conditional Wait States Secondary Cacheability Cache Cntrlr Clock Adjust Cache Write Wait States Cache Valid Bit Cache Dirty Bit C000, 16KB, Cacheability C400, 16KB, Cacheability C800, 16KB, Cacheability CC00, 16KB, Cacheability D000, 16KB, Cacheability D400, 16KB, Cacheability D800, 16KB, Cacheability DC00, 16KB, Cacheability E000, 16KB, Cacheability E400, 16KB, Cacheability E800, 16KB, Cacheability EC00, 16KB, Cacheability : Enabled : Disabled : Enabled : 1 W/S : Enabled : Enabled : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache F000, 64KB, Cacheability Prog. Region 1 BUS Type Prog. Region 1 Cacheable Prog. Region 1 Size Prog. Region 1 Address (KB) Mem. Region 1, Sub-Region 1 Mem. Region 1, Sub-Region 2 Mem. Region 1, Sub-Region 3 Mem. Region 1, Sub-Region 4 Mem. Region 1, Sub-Region 5 Mem. Region 1, Sub-Region 6 Mem. Region 1, Sub-Region 7 Mem. Region 1, Sub-Region 8 Prog. Region 2 BUS Type Prog. Region 2 Cacheable Prog. Region 2 Size Prog. Region 2 Address (KB) Mem. Region 2, Sub-Region 1 : : : : : : : : : : : : : : : : : : NonCache ISA BUS Yes 512 KB 0 Disabled Disabled Disabled Disabled Disabled Disabled Disabled Disabled ISA BUS Yes 512 KB 0 Disabled

Service

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1025

The third display in the advanced chipset setup procedure is as follows. Please note that most of the third display is a repeat of the second display. Only the last seven items in the right hand column are displayed for the first time.
AMBIOS SETUP PROGRAM - ADVANCED CMOS SETUP 1992 American Megatrends Inc., All Rights Reserved C400, 16KB, Cacheability C800, 16KB, Cacheability CC00, 16KB, Cacheability D000, 16KB, Cacheability D400, 16KB, Cacheability D800, 16KB, Cacheability DC00, 16KB, Cacheability E000, 16KB, Cacheability E400, 16KB, Cacheability E800, 16KB, Cacheability EC00, 16KB, Cacheability F000, 64KB, Cacheability Prog. Region 1 BUS Type Prog. Region 1 Cacheable Prog. Region 1 Size Prog. Region 1 Address (KB) Mem. Region 1, Sub-Region 1 Mem. Region 1, Sub-Region 2 : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : NonCache : ISA BUS : Yes : 512 KB : 0 : Disabled : Disabled Mem. Region 1, Sub-Region 3 Mem. Region 1, Sub-Region 4 Mem. Region 1, Sub-Region 5 Mem. Region 1, Sub-Region 6 Mem. Region 1, Sub-Region 7 Mem. Region 1, Sub-Region 8 Prog. Region 2 BUS Type Prog. Region 2 Cacheable Prog. Region 2 Size Prog. Region 2 Address (KB) Mem. Region 2, Sub-Region 1 Mem. Region 2, Sub-Region 2 Mem. Region 2, Sub-Region 3 Mem. Region 2, Sub-Region 4 Mem. Region 2, Sub-Region 5 Mem. Region 2, Sub-Region 6 Mem. Region 2, Sub-Region 7 Mem. Region 2, Sub-Region 8 : : : : : : : : : : : : : : : : : : Disabled Disabled Disabled Disabled Disabled Disabled SA BUS Yes 512 KB 0 Disabled Disabled Disabled Disabled Disabled Disabled Disabled Disabled

If settings are all properly set, press the Esc key to return to the main setup menu. Use the arrow keys to move the highlight cursor to Peripheral Management Setup and press the Enter key to access this procedure. The display will be similar to the following example.
AMBIOS SETUP PROGRAM - ADVANCED CMOS SETUP 1992 American Megatrends Inc., All Rights Reserved Programming Option On-Board Floppy Drive On-Board IDE Drive First Serial Port Address Second Serial Port Address IRQ Active State Parallel Port Mode : : : : : : : Auto Disabled Disabled Disabled Disabled High Normal

Unless user supplied peripherals have been added, factory settings (shown above) should be used. Press the Esc key to return to the main setup menu.

1026

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Service

Use the arrow keys to move the highlight cursor to auto detect hard disk and press the Enter key to access this procedure. The system will automatically check hard disk C: and display the pertinent information in a display similar to the following example.
AMBIOS SETUP PROGRAM - ADVANCED CMOS SETUP 1992 American Megatrends Inc., All Rights Reserved Cyln Type : 47 = USER TYPE 968 Head 5 Wpcom 65535 LZone 968 Sect 17 Size 40

(MB) Hard Disk C:

Accept Parameters for C:

(Y/N) ?

If the parameters displayed are correct, press the Y key and then the Enter key. The display will prompt for auto detection of hard disk D:. If hard disk D: is installed, press the Y key and then the Enter key. When finished, press the Esc key to return to the main setup menu. If the parameters displayed are correct, press the Y key and then the enter key. The display will prompt for auto detection of hard disk D:. If hard disk D: is installed, press the Y key and then the enter key. When finished, press the Esc key to return to the main setup menu. Use the arrow keys to move the highlight cursor to hard disk utility and press the Enter key to access this procedure. The display will be similar to the following example.
AMBIOS SETUP PROGRAM - ADVANCED CMOS SETUP 1992 American Megatrends Inc., All Rights Reserved Cyln Type : 2 915 Head 4 Wpcom 300 LZone 615 Sect 17 Size 20

(MB) Hard Disk C :

Hard Disk Type can be changed from the Standard CMOS SETUP option in the Main Menu Hard Disk Format Auto Interleave Media Analysis

From this display, the hard disk can be formatted, causing all data on the hard disk to be erased. This is not recommended. Also from this display, selecting Media Analysis will analyze the hard disk media for defects.

Service

RH-402

1027

To save changes made during setup, use the arrow keys to move the highlight cursor to Write To CMOS And Exit and press the Enter key. The display will prompt for a Yes or No response for saving and exiting. If changes are not to be saved, use the arrow keys to move the highlight cursor to Do Not Write To CMOS And Exit and press the Enter key. The system will revert to the previously saved settings.

1028

RH-402

Service

11

Illustrations

Figure 111 ....... AnalyzeLeft Side View ..............................113 Figure 112 ....... AnalyzerRight Side View ...........................114 Figure 113 ....... FurnaceLeft Side View..............................115 Figure 114 ....... FurnaceRight Side View............................116 Figure 115 ....... Furnace TransformerPrimary Wiring............117 Figure 116 ....... Lower Sample Loading Assembly ..................118 Figure 117 ....... Upper Sample Loading Assembly ..................119 Figure 118 ....... 614-493 Display Assembly ..........................1110 Figure 119 ....... 603-732 Doser Valve..................................1111 Figure 1110 ..... 603-790 Pump Assembly.............................1112 Figure 1111 ..... 606-649 Solenoid Valve ..............................1113 Figure 1112 ..... 606-650 Solenoid Valve ..............................1113 Figure 1113 ..... 606-652 Solenoid Valve ..............................1113 Figure 1114 ..... 775-330 Solenoid Valve ..............................1114 Figure 1115 ..... 778-522 Solenoid Valve ..............................1114 Figure 1116 ..... TC Cell Assembly .......................................1115 Figure 1117 ..... 780-509 Vacuum Pump...............................1116

Illustrations

RH-402

111

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112

RH-402

Illustrations

777-425 DIGITAL SETPOINT CARD 777-013 DATA SELECT CARD 770-610 SOLENOID DRIVE CARD 777-573 BALANCE CONTROL CARD 666-213 DUAL FILTERED D-SHELL CARD 666-074-104 PC CONTROLLER CARD 666-057-110 CPU CARD 666-016-120 GRAPHIC PROM CARD 777-508-140 I / O CARD

777-377-110 A/D CONVERTER CARD 777-396 + 15V POWER SUPPLY CARD 777-572 MULTIPLEX CARD

777-449-110 HEATER CONTROL Z.C. CARD BEHIND ELECTRONICS CHASSIS 603-503 POWER SUPPLY CARD
777-638 INTERCONNECT CARD

777-876 DISPLAY INTERFACE CARD

614-493 DISPLAY ASSEMBLY

608-590 KEYBOARD ASSEMBLY

608-586 SPEAKER ASSEMBLY

777-529 STEPPER MOTOR CONTROL CARD 777-706 INTELLIGENT DUAL SERIAL CARD 700-692-010 DISK DRIVE

608-850-107 HARD DISK

775-722 FLOW CONTROLLER

777-594 OVEN HEATER CONTROL CARD

781-920 PRESSURE TRANSDUCER ASSEMBLY

603-818 FAN ASSEMBLY 783-799 TC CELL AND 775-377 CELL COVER

Figure 111 AnalyzeLeft Side View

Illustrations

RH-402

113

614-591 FAN 603-740 SV1 SOLENOID VALVE ASSEMBLY 603-741 SV2 SOLENOID VALVE ASSEMBLY 775-722 FLOW CONTROLLER

603-744 SV5 SOLENOID VALVE ASSEMBLY 783-542 SV12 SOLENOID VALVE ASSEMBLY 666-147 TC CELL POWER SUPPLY CARD 777-340 SOLENOID INTERFACE CARD 603-745 SV6 SOLENOID VALVE ASSEMBLY 603-743 SV4 SOLENOID VALVE ASSEMBLY 603-742 SV3 SOLENOID VALVE ASSEMBLY 773-585 PRESSURE SWITCH (25 PSI)

768-980 PARTICLE FILTER

780-460 BALANCE COVER ASSEMBLY 614-326 BALANCE ASSEMBLY

775-625 GAS ON/OFF SWITCH

774-086 GAS ON LED 781-833 INLINE VOLUME

768-980 PARTICLE FILTER 780-537 RFI FILTER 603-935 DOSER LOOP ASSEMBLY 603-732 DOSER VALVE ASSEMBLY 777-547 AMBIENT TEMP SET CARD

614-314 ON/OFF SWITCH CIRCUIT BREAKER 771-317 RELAY K1 K2

TB-101 50/60 Hz SWITCH 780-509 VACUUM PUMP ASSEMBLY 603-731 TRANSFORMER ASSEMBLY

778-951 POWER TRANSFORMER CIRCUIT BREAKER (5 AMP) VOLTAGE SELECTION 115/230 V ~ SWITCH

Figure 112 AnalyzerRight Side View

114

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Illustrations

777-562 PLATE CURRENT DETECTOR CARD

HEAT EXCHANGER CONNECTIONS 603-711 PLATE CURRENT METER (DCmA)

COOLANT TANK VALVE (SHOWN IN OFF POSITION) 606-724 COOLANT TANK 603-888 LOADER ASSEMBLY COVER

SV8 SV9 SV10 SV11 615-721 DIVIDER PANEL SV7 777-340 SOLENOID INTERFACE CARD

768-980 PARTICLE FILTER

603-787 RFI FILTER

775-625 LOADER CONTROL SWITCH

787-797 PRESSURE SWITCH

603-790 COOLANT PUMP ASSEMBLY

775-604 COOLANT VALVE

614-463 TRANSFORMER 603-880 RELAY

614-570 ON/OFF SWITCH CIRCUIT BREAKER 781-165 RELAY

Figure 113 FurnaceLeft Side View

Illustrations

RH-402

115

603-357 HEAT EXCHANGER

781-371 COOLING FAN

771-582 INDUCTION COIL ASSEMBLY 777-533 STEPPER MOTOR DRIVE CARD

500 500 500

603-931 TUBE CHIMNEY

FEED THROUGHS

TUBE FILAMENT LEADS

603-809 CRUCIBLE LIFT MOTOR

500 C1 100 100

TB-105
779-271 CABINET SAFETY INTERLOCK SWITCH

TB-104

614-463 TRANSFORMER

771-488 RFI FILTER 771-487 HIGH VOLTAGE STANDOFFS (2 REQ'D)

789-379 TRANSFORMER AND PLATE ASSEMBLY

777-601 FURNACE POWER CONTROL CARD 763-950 FURNACE ENABLE SWITCH

WARNING
THE OSCILLATOR AND FURNACE POWER SUPPLY CARRY LETHAL VOLTAGES WHEN THE HIGH VOLTAGE IS TURNED ON.

Figure 114 FurnaceRight Side View

116

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Illustrations

WARNING
THE OSCILLATOR AND FURNACE POWER SUPPLY CARRY LETHAL VOLTAGES WHEN THE HIGH VOLTAGE IS TURNED ON.

RF CHASSIS 772-984 10 AMP RFI FILTER

1 2 3 4 5

TB-105

HIGH VOLTAGE FEED-THROUGHS RED

1 2 3 4 5

BLACK 771-488 30 AMP RFI FILTER 771-487 HIGH VOLTAGE STANDOFFS

TB-104

789-379 TRANSFORMER AND PLATE ASSEMBLY

NOTE: THE POSITION OF THE RED WIRE TERMINATIONS ARE SHOWN FOR EXAMPLE ONLY. REFER TO THE TEXT FOR DETERMINING THE CORRECT CONNECTIONS.

Figure 115 Furnace TransformerPrimary Wiring

Illustrations

RH-402

117

603-809 MOTOR 194-056 NUT (4 REQ'D) 190-004 SCREW (2 REQ'D)

771-582 COIL ASSEMBLY 604-241 REACTION TUBE

774-658 SWITCH 190-034 SCREW (2 REQ'D) 805-814 ACTUATOR

615-712 HEAT SHIELD 603-706 PEDESTAL 762-357 0-RING 603-910 0-RING 775-333 FITTING 190-742 SCREW (4 REQ'D) 769-899 ROD

603-807 STEPPER MOUNT PLATE 603-775 STANDOFF (3 REQ'D) 190-483 SCREW (4 REQ'D) 604-238 BOTTOM SEAL BLOCK 190-706 THUMBSCREW (3 REQ'D)

190-945 SCREW (2 REQ'D) 193-147 WASHER (2 REQ'D) 604-244 BRACKET

603-806 BASE PLATE

605-819 SPLIT CLAMP (3 REQ'D) 604-240 SLIDE ROD (3 REQ'D) 603-795 LIFT ROD ASSEMBLY 190-701 SCREW 190-151 THUMBSCREW (3 REQ'D) 603-804 SHAFT GUIDE 603-798 FLANGE 603-803 BEARING MOUNT 190-742 SCREW

775-666 MICROSWITCH 194-030 NUT (2 REQ'D) 190-314 SCREW

194-059 NUT 604-243 ACTUATOR

190-235 SCREW (2 REQ'D)

193-054 WASHER (2 REQ'D) 603-808 SWITCH

780-836 WASHER 780-837 PULLEY SET SCREW (2 REQ'D)

603-810 PULLEY SET SCREW (2 REQ'D) 603-932 PULLEY BELT

Figure 116 Lower Sample Loading Assembly

118

RH-402

Illustrations

* PART OF 603-139 PIVOT BRACKET

Figure 117 Upper Sample Loading Assembly

Illustrations

RH-402

119

POWER SUPPLY CARD ASSEMBLY (SUPPLIED WITH 782-590 DISPLAY)

190-229 SCREW (8 REQ'D) 550-174 WASHER (4 REQ'D) 777-876 CGA INTERFACE CARD ASSEMBLY

190-235 SCREW (6 REQ'D) 193-054 WASHER (6 REQ'D)

782-594 PANEL

770-744 SPACER (8 REQ'D)

778-949 SPACER (6 REQ'D) 782-590 DISPLAY 782-586 CABLE 12 COND 782-587 CABLE 14 COND

614-494 FRAME (2 REQ'D)

Figure 118 614-493 Display Assembly

1110

RH-402

Illustrations

603-813 VALVE STEM

190-294 SCREW (2 REQ'D) 772-269 O-RING (8 REQ'D)

193-127 WASHER (2 REQ'D)

603-812 6 PORT BLOCK

601-939 O-RING (6 REQ'D) 601-941 FITTING (6 REQ'D)

169-711 LABEL 601-935 MOUNT 601-938 VALVE STEM CLAMP 601-934 COUPLING

602-672 SPRING

601-933 CYLINDER 778-523 FITTING (2 REQ'D)

601-932 BRACKET

193-127 WASHER (2 REQ'D) 190-036 SCREW (2 REQ'D)

Figure 119 603-732 Doser Valve

Illustrations

RH-402

1111

CLAMP SCREW

SET SCREW IMPELLER HOUSING

WASHER (4 REQ'D)

TOP CLAMP

PUMP HOUSING

SPACER

IMPELLER SHAFT

CAP

O-RING

WASHER (4 REQ'D) SCREW (4 REQ'D)

MAGNETIC IMPELLER

BOTTOM CLAMP

Figure 1110 603-790 Pump Assembly

1112

RH-402

Illustrations

SPRING VALVE BODY O-RING ARMATURE

SPACER ARMATURE HOUSING HOUSING & COIL NUT

Figure 1111 606-649 Solenoid Valve

VALVE BODY

SPACER

HOUSING & COIL

NUT

Figure 1112 606-650 Solenoid Valve

STEM NUT HOUSING AND COIL SPACER O-RING O-RING

Figure 1113 606-652 Solenoid Valve

Illustrations

RH-402

1113

ADJUSTMENT SCREW (2 REQ'D) SCREW (2 REQ'D)

VALVE BODY BRACKET

SCREW (2 REQ'D)

COIL & HOUSING

FITTING (3 REQ'D) 773-661 FITTING (3 REQ'D)

SPACER

Figure 1114 775-330 Solenoid Valve

SCREW (2 REQ'D)

COIL AND HOUSING SPACER

VALVE BODY

RUBBER WASHER (3 REQ'D)

SCREW (2 REQ'D)

Figure 1115 778-522 Solenoid Valve

1114

RH-402

Illustrations

OVEN

TC CELL FITTING (4 INCLUDED)

775-376 TC CELL

190-666 SCREW (2 REQ'D)

193-053 WASHER (8 REQ'D) 190-231 SCREW (8 REQ'D) 767-629 EXTENSIONS (8 REQ'D) BRIDGE ZERO ADJUSTMENT HOLE

777-563 TC CELL PREAMP CARD 614-339 STANDOFF (2 REQ'D)

775-377 COVER

193-008 WASHER (2 REQ'D) 190-279 SCREW (2 REQ'D) 773-162 PLUG

Figure 1116 TC Cell Assembly

Illustrations

RH-402

1115

589-186 FITTING ADAPTER

775-338 TEE FITTING

SCREW (4 REQ'D) HEAD PLATE

O-RING VALVE PLATE

INTERMEDIATE PLATE

DIAPHRAGM

SCREW

CONNECTING ROD SET SCREW

ECCENTRIC 194-056 NUT (4 REQ'D) 781-677 RUBBER MOUNT (4 REQ'D) 190-227 SCREW (2 REQ'D) 773-583 SLIDE SWITCH 780-512 BRACKET 194-055 NUT (2 REQ'D) SCREW

781-675 BRACKET

SCREW (2 REQ'D)

194-056 NUT (4 REQ'D)

Figure 1117 780-509 Vacuum Pump

1116

RH-402

Illustrations

12

Index

% Power vs. Temperature................................................... 586 486 CPU Setup Procedure ................................................... 1023 486 Systems .................................................................... 1023 5 Volt Supply Adjustment ................................................... 913 50 Hz Operation................................................................ 29 A A/D Converter Card ........................................................... 94 A/D Converter Card Adjustment........................................... 93 AC Voltage Tap Selection.................................................... 29 Accessories List ................................................................ 115, 116 Accessory Package ............................................................ 117, 118 After Daily Analysis............................................................ 532 Alarm.............................................................................. 43 Alarm Table...................................................................... 571 Alarms Procedure .............................................................. 570 Aluminum Sample ............................................................. 516 Aluminum Samples, Sample Type ........................................ 516 Ambient Monitor, Diagnostics.............................................. 816 Ambient Monitor, System Check .......................................... 415 Analysis........................................................................... 529 Analysis Constants ............................................................ 579 Analysis Parameters .......................................................... 584 Analysis Power High, Bulk Analysis, Procedure C..................... 581 Analysis Power High, Procedure F......................................... 580 Analysis Power High, Procedure H........................................ 579 Analysis Power High, Standard Constants.............................. 520 Analysis Power Low, Bulk Analysis, Procedure C...................... 581 Analysis Power Low, Procedure F ......................................... 580 Analysis Power Low, Procedure H......................................... 579

Index

RH-402

121

Analysis Power Low, Standard Constants............................... 520 Analysis Power Low, Surface Analysis, Procedure C ................. 581 Analysis Procedure ............................................................ 525 Analysis Programs ............................................................. 575 Analysis Time, Specifications............................................... 120 Analysis Time, Surface Analysis, Procedure C ......................... 581 Analysis Type, Analysis Parameters ...................................... 584 Analysis Valve State.......................................................... 1010 Analyze Menu, System Overview.......................................... 46 AnalyzeLeft Side View ..................................................... 113 Analyzer, Controls and Indicators......................................... 43 AnalyzerRight Side View .................................................. 114 Answer Stack ................................................................... 555 ASCII Character Definition Table .......................................... 39 Auto I/O Test, Diagnostics.................................................. 813 Automatic Plotting, System Configurations............................. 423 B Balance and Dust Cover Installation ..................................... 229 Balance Assembly, Illustration ............................................. 36 Balance Control Panel, Illustration ........................................ 36 Balance Interfacing............................................................ 34 Balance Mode ................................................................... 424 Balance Preamp Card......................................................... 95 Balance Preamp Card Adjustment ........................................ 95 Balance, External.............................................................. 33 Balance, Internal............................................................... 229 Balance, Resetting the ....................................................... 35 Balance, Setting the Data Output Parameter.......................... 35 Barometric Pressure .......................................................... 420, 710 Baud Rate, Serial Ports ...................................................... 426 Before Analysis ................................................................. 525 Blank Determination.......................................................... 527 Blank Procedures .............................................................. 543 Block Closed Switch, Magnet Reed Switches .......................... 104 Block Open Switch, Magnetic Reed Switches .......................... 105 Break Points..................................................................... 1022 122 RH-402 Index

Built-In Printer/Plotter, Specifications ................................... 121 Bulk Analysis, Procedure C.................................................. 581 C Calibration Procedures ....................................................... 533 Calibration, Specifications................................................... 120 Catalyst Heater Tube ......................................................... 64 Caution Symbols ............................................................... 111 Caution,Operator .............................................................. 110 Channel Select Procedure ................................................... 512 Chip Samples, Sample Type................................................ 516 Coil Spacing Check............................................................ 228 Combined Analysis Answer Format ....................................... 316 Combustion Tube and Pedestal............................................ 224 Combustion Tube and Pedestal Installation ............................ 226, 227 Combustion Tube and Pedestal Installation, Preliminary Steps ........................................................... 225 Comparator Level.............................................................. 77 Comparator Level, Bulk Analysis, Procedure C ........................ 582 Comparator Level, Gas Dose ............................................... 583 Comparator Level, Gas Dose Constants................................. 522 Comparator Level, Procedure F............................................ 580 Comparator Level, Procedure H............................................ 579 Comparator Level, Specifications ......................................... 120 Comparator Level, Standard Constants ................................. 520 Component Package .......................................................... 116 Components and Accessories List ......................................... 116 Constants Procedure .......................................................... 518 Controls and Indicators ...................................................... 43 Controls and Indicators, Illustrations .................................... 45 Coolant Installation ........................................................... 212 Coolant Level ................................................................... 66 Coolant Tank, Draining The................................................. 67 Coolant Tank, Filling The .................................................... 66 Counters Procedure ........................................................... 552 CPU Card ......................................................................... 915

Index

RH-402

123

Crucible Adjust, Bulk Analysis, Procedure C............................ 582 Crucible Adjust, Procedure F ............................................... 580 Crucible Adjust, Procedure H............................................... 579 Crucible Adjust, Standard Constants..................................... 520 Crucible Position ............................................................... 515 Crucible Type, Analysis Parameters ...................................... 584 Crucibles ......................................................................... 514 D Data Bits, Serial Ports........................................................ 426 Data Buffers Procedures ..................................................... 549 Data Storage.................................................................... 121 Data Transmit .................................................................. 37 Data Transmit Cable Pin Assignments................................... 38 Data Transmit Format ........................................................ 311 Data Transmit Format, System Configurations........................ 423 Database Blank................................................................. 547 Database Calibration.......................................................... 541 Database Option, Answer Stack........................................... 558 Database Option, Statistics................................................. 566 Database Option, Transfer and Delete................................... 561 Database Option, Transmit Stack......................................... 569 Database Record Limit, System Configuration ........................ 423 Declaration of Conformity................................................... 113 Definitions, Gas Dose Constants .......................................... 522 Definitions, S.P.C. Constants............................................... 524 Definitions, Serial Ports...................................................... 426 Definitions, Standard Constants........................................... 520 Definitions, System Configurations ....................................... 423 Detection Method, Detection Method .................................... 120 Diagnostic Menu, System Overview ...................................... 46 Diagnostics Menu .............................................................. 83 Diameter, Sample Size....................................................... 517 Dimensions ...................................................................... 122 Display, Specifications ....................................................... 121 Disposable Particle Filters ................................................... 68

124

RH-402

Index

Doser Valve...................................................................... 1111 Draining The Coolant Tank.................................................. 67 Dynamic Range, Specifications ............................................ 120 E Electrical Connections ........................................................ 217 Electrical Power Requirements............................................. 121 Electronic Circuit Card Replacement ..................................... 108 Enable Keyboard Beep, System Configurations ....................... 423 External Balance............................................................... 33 External Balance (MWT)Manual Weight Procedure ................ 510 External Keyboard............................................................. 320 F Facility Requirements......................................................... 216 Filling The Coolant Tank ..................................................... 66 Flat Panel Display.............................................................. 43 Flow From Furnace Rotameter, Analyzer................................ 43 Flow To Furnace Rotameter And Adjustment Knob, Analyzer ....................................................................... 43 Format Key, Data Transmit ................................................. 310 Function Keys, Menus ........................................................ 46 Furnace Cable................................................................... 215 Furnace On Time, Surface Analysis, Procedure C..................... 581 Furnace Power Control Card................................................ 98 Furnace Power Control Card Adjustment ............................... 97 Furnace Power Graphs ....................................................... 585 Furnace Power Oscillator Circuit ........................................... 74 Furnace Transformer Primary Wiring..................................... 211 Furnace TransformerPrimary Wiring ................................... 117 Furnace Type, Specifications ............................................... 121 Furnace, Controls and Indicators.......................................... 44 Furnace, Induction ............................................................ 25 FurnaceLeft Side View ..................................................... 115 FurnaceRight Side View ................................................... 116 Fusion Analysis Answer Format............................................ 312

Index

RH-402

125

G Gas Connections ............................................................... 213 Gas Dose ......................................................................... 583 Gas Dose Answer Format.................................................... 311 Gas Dose Calibration.......................................................... 537 Gas Dose Constants .......................................................... 521 Gas Dose Power, Gas Dose ................................................. 583 Gas Dose Power, Gas Dose Constants................................... 522 Gas Dose Sequence Diagram............................................... 1016 Gas Dose Valve State ........................................................ 1011 Gas Dose, Specifications..................................................... 120 Gas Dosing ...................................................................... 528 Gas Flow.......................................................................... 121 Gas Flow Adjustments, System Check................................... 417 Gas Flow Diagram............................................................. 1014 Gas Flows ........................................................................ 1010 Gas On LED, Analyzer Indicators.......................................... 43 Gas On/Off Switch, Analyzer Controls ................................... 43 Gases Required................................................................. 120 General Information, Theory of Operation.............................. 73 H Handshake, Serial Ports ..................................................... 426 Hazardous Material Package................................................ 117 Heater Control Z.C. Card .................................................... 910 Heater Control Z.C. Card Adjustment.................................... 99 High Power Outgas (Time), Procedure C ................................ 581 High Power Outgas (Time), Procedure F ................................ 580 High Power Outgas, Procedure C.......................................... 581 High Power Outgas, Procedure F .......................................... 580 Hot Extraction Analysis Answer Format ................................. 314 Hydrogen Blank ................................................................ 543 Hydrogen Control Standard, S.P.C. Constants ........................ 524

126

RH-402

Index

I Illustrations List ................................................................ 17 Incoming N2 Pressure Gauge, Analyzer Controls...................... 43 Incoming Reagent Tube ..................................................... 219, 610 Incoming Reagent Tube Packing .......................................... 221 Induction Furnace ............................................................. 25 Initial Power Up ................................................................ 411 Initializing the CPU for 80486 Systems .................................. 1023 Installation....................................................................... 23 Installation, Data Transmit ................................................. 37 Interfaced BalanceAutomatic Procedure .............................. 510 Interference to Other Devices ............................................. 112 Internal Balance ............................................................... 229, 43 Internal Balance (AWT)Automatic Procedure........................ 59 Internal BalanceExploded View ......................................... 96 International Printer Kit...................................................... 118 J Jumper Selections ............................................................. 24 K Keyboard......................................................................... 47 Keyboard Select Switch, Analyzer Controls ............................ 43 Keyboard, External............................................................ 320 Keyboard, Specifications .................................................... 121 Keyboards ....................................................................... 43 Known H2 Gas Dose Value, Gas Dose .................................... 583 Known H2 Gas Dose Value, Gas Dose Constants ..................... 522 L Leak Check Flow Diagram................................................... 1015 Leak Check Limits ............................................................. 121 Leak Check Sequence Diagram............................................ 1017 Leak Test, Diagnostics ....................................................... 84 Length, Sample Size .......................................................... 517 Linearization..................................................................... 1020 Linearize.......................................................................... 1021 Loader Control Switch, Furnace Controls ............................... 44

Index

RH-402

127

Loader Cover.................................................................... 69 Low Power Outgas (Time), Procedure F ................................. 580 Low Power Outgas, Procedure F........................................... 580 Lower Control Limit, S.P.C. Constants................................... 524 Lower Sample Loading Assembly.......................................... 118 M Magnetic Reed Switches ..................................................... 103 Major Equipment............................................................... 115 Manual Blank.................................................................... 546 Manual Calibration............................................................. 540 Manual I/O Test, Diagnostics............................................... 86 Maximum Furnace On Time, Bulk Analysis, Procedure C ........... 581 Measure Flow Reagent Tube................................................ 611 Measure Flow, Analysis Valve State...................................... 1010 Measure Reagent Tube....................................................... 220 Measure Reagent Tube Packing............................................ 222 Mechanical Adjustments..................................................... 103 Melt Detect, Analysis Parameters ......................................... 584 Memory ........................................................................... 121 Menu Line ........................................................................ 46 Menu Organization Chart .................................................... 48 Menus, System Overview.................................................... 46 Minimum Analysis Time, Bulk Analysis, Procedure C ................ 581 Minimum Analysis Time, Procedure F .................................... 580 Minimum Analysis Time, Procedure H.................................... 579 Minimum Analysis Time, Standard Constants ......................... 520 Minimum Gas Dose Time, Gas Dose...................................... 583 Minimum Gas Dose Time, Gas Dose Constants ....................... 522 N Normal Variation, Ambient Monitoc ...................................... 816 Normal Variations, Ambient Monitor...................................... 416 Notice, Operator ............................................................... 110 O Options ........................................................................... 119 O-rings............................................................................ 616 Oscillator Chassis, Illustration.............................................. 28 128 RH-402 Index

Oscillator Tube Installation.................................................. 26 Other Volt Supplies............................................................ 916 Out Of Sequence Log-In ..................................................... 58 Outgas Cool Down, Procedure C........................................... 581 Outgas Cool Down, Procedure F ........................................... 580 Outgas Valve State ........................................................... 1011 Oven Compartment ........................................................... 417 Oven Compartment, Illustration........................................... 919 Oven Heater Control Card................................................... 912 Oven Heater Control Card Adjustment .................................. 911 Oven Heater On LED, Analyzer Indicators .............................. 43 P Paper, Installation............................................................. 232 Parity, Serial Ports ............................................................ 426 Periodic Maintenance Schedule ............................................ 63 Pin Samples, Sample Type.................................................. 516 Plate Current Meter, Furnace Indicators ................................ 44 Plate DCmA vs. Temperature............................................... 585 Powder Samples, Sample Type ............................................ 516 Power On/Off Switch, Analyzer Controls ................................ 43 Power On/Off Switch, Furnace Controls ................................. 44 Power Supply Unit ............................................................. 917, 918 Power Up ......................................................................... 411 Precision, Specifications ..................................................... 120 Preliminary Steps, Combustion Tube and Pedestal Installation.......................... 225 Print Buffer ...................................................................... 551 Print Spacing, System Configurations.................................... 423 Printer............................................................................. 230, 44 Printer Diagnostics ............................................................ 818 Printer Kit ........................................................................ 116 Printer Test #1 ................................................................. 818 Printer Test #2 ................................................................. 818 Printer, Settings................................................................ 233 Procedure CCombined Analysis Sequence Diagram............... 1019

Index

RH-402

129

Procedure CCombined Analysis, Analysis Program............................................................ 578, 581 Procedure FFusion Analysis Sequence Diagram.................... 1018 Procedure FFusion Analysis, Analysis Program ...................... 577, 580 Procedure HHot Extraction Analysis Sequence Diagram.............................................. 1017 Procedure HHot Extraction Analysis, Analysis Constants............................................. 579 Procedure HHot Extraction Analysis, Analysis Program............................................... 576 Program Modification Levels ................................................ 123 Pump Assembly ................................................................ 1112 Pump Pressure Gauge, Analyzer Controls............................... 43 Purge Time, Procedure H .................................................... 579 Purge Time, Standard Constants.......................................... 520 Purification, Analysis Valve State ......................................... 1010 R Ramp Time, Bulk Analysis, Procedure C................................. 581 Ramp Time, Procedure F .................................................... 580 Ramp Time, Procedure H .................................................... 579 Ramp Time, Standard Constants.......................................... 520 Range, Analysis Parameters ................................................ 584 Readability, Specifications .................................................. 120 Reagent Tube Assemblies, Illustration................................... 614 Reagent Tube Assemblies, Illustrations ................................. 223 Reagent Tube Packing........................................................ 612 Reagent Tube Removal....................................................... 221, 612 Reagents Required ............................................................ 120 Record Format .................................................................. 319 Regulators ....................................................................... 121 Remove Weight Procedure .................................................. 511 Resetting the Balance ........................................................ 35 Restore Deletion ............................................................... 562 RH402P Package ............................................................... 115 RH402PI Package .............................................................. 115 Ribbon Cartridge, Installation.............................................. 232

1210

RH-402

Index

S S.P.C. Constants............................................................... 523 Sample Loading Assembly .................................................. 107 Sample Loading Assembly Alignment .................................... 106 Sample Loading, Analysis Parameters ................................... 584 Sample Log-In.................................................................. 55 Sample Preparation ........................................................... 516 Sample Size ..................................................................... 517 Sample Size, Specifications................................................. 120 Sample Type .................................................................... 516 Sample Weight Range ........................................................ 120 Screen Filters ................................................................... 615 Screen Plot ...................................................................... 549 Security Code................................................................... 421 Sensitivity, Specifications ................................................... 121 Sequence Test, Diagnostics ................................................ 812 Service I/O Table .............................................................. 810 Set Clock......................................................................... 427 Setting the Data Output Parameter, Balance.......................... 35 Setup Procedure, 486 System............................................. 1023 Shipping Weight................................................................ 122 Significant Figures, Analysis Parameters ................................ 584 Small Samples.................................................................. 526 Software Update Procedure ................................................. 124 Solenoid Valve.................................................................. 1113, 1114 Specifications ................................................................... 120 Stack Procedures .............................................................. 554 Standard Calibration .......................................................... 534 Standard Check Sample Log-In............................................ 57 Standard Constants........................................................... 519 Statistics ......................................................................... 563 Stop Bits, Serial Ports........................................................ 426 Superuser Log-In Option .................................................... 413 Surface Analysis, Procedure C ............................................. 581 System Check .................................................................. 414 System Configuration......................................................... 422 Index RH-402 1211

System Controls................................................................ 422 System Leak Check........................................................... 418 System Overview .............................................................. 46 System Update Menu, System Overview................................ 46 T TC Cell Adjustment............................................................ 919 TC Cell Assembly............................................................... 1115 TC Cell Power Supply Card.................................................. 921 TC Cell Power Supply Card Adjustment ................................. 920 TC Cell, Specifications........................................................ 121 Thermal Conductivity Cell (TC Cell) ...................................... 75 Transfer and Delete........................................................... 559 Transformer, Furnace, Primary Wiring................................... 211 Transmit Results............................................................... 513 Transmit Stack ................................................................. 567 Tube packing, Incoming Reagent ......................................... 221 Tube Packing, Measure Reagent........................................... 222 U Upper Control Limit, S.P.C. Constants................................... 524 Upper Sample Loading Assembly.......................................... 119 User/Superuser Log-In Option............................................. 413 V Vacuum Pump .................................................................. 1116 Valve States .................................................................... 1012 W Warning Indicator, Specifications ......................................... 121 Warning Symbols .............................................................. 111 Warranty......................................................................... 19 Weight Entry .................................................................... 59 Weight Stack.................................................................... 554 Wiring Diagrams ............................................................... 218 Wiring, Furnace Transformer............................................... 211

1212

RH-402

Index