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1,
2
,
3,
4,
5,
6
are geometric correction factors as stated by S. Hashemi
C is the compliance and can be defined as C =/P, where is the displacement and P is the
load.
F is the correction factor for effective shortening of the beams due to the large displacements
and the tilting of end blocks.
N is the correction factor for the increased stiffness obtained by using the end blocks.
is for rotation occurring at crack tip. This was found from the plot of (C/N)^(1/3) vs a as
shown in results section
G
I
is the fracture energy for mode I .
G
II
is the fracture energy for mode II.
Equation (1) to (9) was used for calculations of the results and is presented in the next
section.
(10)
(11)
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Group2 Fracture Mechanics Short Report 9
4. Result
Figure 6 Load displacement graph for DCB testing Mode I
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Group2 Fracture Mechanics Short Report 10
Figure 7 (C/N)^(1/3) vs crack length graph which is used to deduce
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Group2 Fracture Mechanics Short Report 11
Figure 8 R curved behaviour of DCB sample from mode I testing (fracture Energy vs crack length )
Mode II results
Figure 9 Load displacement graph for ELS testing Mode II
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Group2 Fracture Mechanics Short Report 12
Figure 10 R curved behaviour of ELS sample from mode II testing (fracture Energy vs crack length )
Summary table
G
IC
sample one intiation value Mode I DCB 300Jm
-2
G
IC
sample Two intiation value Mode I DCB 315Jm
-2
G
IIC
sample one intiation value Mode II ELS 815J m
-2
G
IIC
sample one intiation value Mode II ELS 435J m
-2
G
IIC
Propogation value
E11 for mode I Average value 117GPa
G
IC
sample one intiation value Mode I DCB 5%
offset value
305J m
-2
G
IC
sample two intiation value Mode I DCB 5%
offset value
375Jm
-2
Table 3 Summary table showing the different values deduced from the experiment conducted
The two failure mechanism observed during the mode I and II interlaminar facture test were :
(a) Interlaminar crack growth involving fibre bridging and pullout at crack tip.
(b) Interlaminar crack growth involving crack tip splitting.
All the specimens tested exhibited this mechanism , the degree of fibre bridging and
splitting was not the same for all material.
Sample calculation
(a) For mode I calculation the
3 / 1
|
.
|
\
|
N
C
vs a was plotted to find the value of the
correction factor .Load and displacement was measured in the machine and markers
were manually made using the CCTV for every cracklength this displacement was
matched and data processed. The mode I DCB test
1
=3/10
2
=3/2
(b) The mode 1 DCB test
3
=1,
4
=9/8[1-(l
2
/a)
2
],
3
=9/35
4
=9/8[1-(l
2
/a)
2
] ,
4
=9/8[1-(9.6/63)
2
]=
4
= 1.09
5
=9/35
Other correction factors are
F= 1-
1
(/L)
2
-
2
(l
1
/L
2
) = (1-((3/10)*(7.77/139.8)
2
)((3/2)*(7.77*8.04/(139.8
2
)) = 0.99
N= 1-
3
(l
2
/L)
3
-
4
(l
1
/L
2
)-
5
(/L)
Jithin Gopal
Group2 Fracture Mechanics Short Report 13
N=1-(1*(9.6/139.8)
3
-(1.098*((7.77*8.04)/139.8
2
)-(9/35*(7.7/139.8
2
) = 0.995
E
11
= =(37.2/7.77)*(8)*(1)*(633)/(19.28)*(1.693) = 90.46GPa
C= displacement /load = 7.77/37.2= 0.24
was deduced from the
3 / 1
|
.
|
\
|
N
C
vs a graph and for sample one was deduced as 5.5
G
IC
= (0.99/0.995)*(3*32.7*7.77)/(2*19.28)*(63+(6)) = 275 Jm
-2
Calculation similar were performed to obtain the results presented in this section and this was
to demonstrate a sample calculation.
5. Discussion
The interlaminar crack energy of ACG MTM 44-1 were measured using DCB and ELS
method. For mode I fracture testing. The facture mechanism observed for both testing was
involved fibre bridging, pull-out and crack tip splitting which lead to more fibre bridging.
The evidence of the above mentioned mechanism can been seen in load vs displacement
graph in figure 6 and figure 9.The interlaminar crack grew in stable ,continuous manner
thought he DCB specimen and the load displacement curves shown in figure 6 and 9.Load
displacement curves indicated linear elastic, nonlinear elastic and nonlinear inelastic
behaviour. Linear response was observed in the beginning of the test at lower load (~35N).
The second response was non-linear elastic response, which occurred in the middle of the
trace as the nearby material gets stiffer as the load increases. The third type was the nonlinear
inelastic response, which occurred at high loads and can be associated with onset of crack
growth and the decrease in slope of the load- displacement trace. The nonlinear inelastic
response in these materials can be associate with large displacement being present in the test
specimen this has been taken into account by using an correction factor, but other mechanism
which has affected the experiment are fibre birding and crack tip splitting. Fibres resist crack
opening by stretching and absorb energy and hence increasing the toughness. Toughness
increase with crack length for mode one sample this is evident with the resistance curve
behaviour as shown in figure 8.The value obtained for fracture energy for Initial crack was
found to be around 300Jm
-2
, the quality of this has been compared with other published
literature and for an epoxy system like MTM 44-1this is an comparable value .The effect of
crack length on G
IC
( fracture Energy ) is clear from figure 8, G
IC
value associated with the
onset of the crack is different to the values obtained for crack propagation and this is reflected
on the R curve as shown in Figure 8. Beam theory correction required to analyse the data and
the correction factors were applied a shown in the procedure section.
For mode II testing there is no recognised standard for testing of material in mode II. There
are four methods currently used but no agreement on which method to standardise. The
method used for this experiment was End Load Splitting (ELS) some of the problem
associate with ELS testing are role of friction during the test, how much energy is absorbed
by friction can this be calculated and accounted for in the analysis and is it possible to reduce
friction experimentally. Micro cracking has also been reported by several researchers and to
Jithin Gopal
Group2 Fracture Mechanics Short Report 14
model this and calculate this will be very complex. The fracture energy against crack length
is plotted as seen in Figure 10 and unlike mode I there is a difference in the nature , the
fracture energy is going up with crack length and this is due to the friction, fibre bridging,
crack tip splitting and this is reflected in the figure . There is a very big difference in the
crack Initiation values and propagation value and they can be quoted as450 and 950 Jm
-2
.
Mode II values obtained are comparable with the literature but has to be treated with caution
as there are no standard methods available and hence the details of the experimentation needs
to be checked before comparing like to like data. The load- displacement graph has a linear
and non-linear area similar to the mode I. The Fracture energy values obtained from Mode I
and Mode II cannot be compared ad they are very different and involved different
mechanism.
The quality of the fracture energy values have been compared with the published data and
they are comparable and as the test was carried out according to standard test methods the
results obtained are good quality . There were a few problems during the experiment like the
white ink used to mark the specimen was applied thick and during testing some of the cracks
were propagation under the crack and were difficult to detect. Despite the difficulties the data
analysed produced meaningful results and was comparable with published data.
6. Conclusion
Inter-laminar fracture behaviour of ACG MTM 44-1 was studied using Mode I DCB and
Mode II ELS.
- The load- displacement graph shows non-linear behaviour, mainly due to the large
displacements in the specimen and the fracture mechanism like fibre-bridging, crack
splitting and friction.
- Modified beam theory with correction factors were used to deduce the fracture energy
following S Hashemi et al (Hashemi, 1990b)
- The Fracture energy values obtained from Mode I and Mode II cannot be compared
and they are very different and involved different mechanism. Correction factors were
used to ensure the value obtained is more in sync with the actual testing.
- Mode I testing was done according to ISO 15024 but mode II testing has no agreed
international standard.
- The fracture energy obtained for two DCB sample tested are G
IC
initiation energy was
~300Jm
-2
and this was comparable with the literature for epoxy matrix and there was
an increase in the fracture energy with crack length which is associated with fibre
bridging, crack end splitting and friction.
- For mode II ELS testing the G
IIC
initiation energy was found to be ~450Jm
-2
and
there was an increase in the fracture energy with crack length which is associated with
fibre bridging, crack end splitting and friction.
Jithin Gopal
Group2 Fracture Mechanics Short Report 15
- Mode II fracture energy VS crack length graph was a bigger scatter and the R
curved behaviour was not very obvious. Initiation and propagation values were
compared with previous work done by S Hameshi and the values obtained are
comparable taking into the experimental error.
There were few problem associated with the testing in terms of data collection, the
marking fluid being thick and crack propagation not visible due to this. Overall the
experiment was success in measuring the fracture energy for this ACG MTM 44-1
material and obtained comparable data with published results.
7. References
Advanced Composite Group. (04/11/2011) ACG MTM 44-1 product information. [Online]
Available from: http://www.advanced-
composites.co.uk/data_catalogue/catalogue%20files/pds/PDS1189_MTM44-1_Issue7b.pdf .
Department of Aeronautics, Laboratories booklet 2011/2012 . (2011/2012) MSc in
composites Laboratory Handout. Tensile Testing. In: Anonymous pp. 32-46.
Hashemi, S. (1990a) The Analysis of Interlaminar Fracture in Uniaxial Fibre-Polymer
Composites. Proceedings of the Royal Society of London.Series A, Mathematical and
Physical Sciences. 427 (1872), 173-199.
Hodgkinson J M. (2000) Mechanical Testing of Advanced Fibre Composites. , Woodhead
Publishing Limited.
Naghipour, P. B. (2010) Effect of fiber angle orientation and stacking sequence on mixed
mode fracture toughness of carbon fiber reinforced plastics: Numerical and experimental
investigations. Materials Science Engineering.A, Structural Materials: Properties,
Microstructure and Processing. 527 (3), 509-517.
Taylor Ambrose Dr. (2011) Fracture. Lecture Notes Imperial College Course. 2, .
Williams, J. (1988) On the calculation of energy release rates for cracked laminates.
International Journal of Fracture. 36 (2), 101-119.