C. U. Shah College Of Pharmacy & Research, Wadhwan City.

List Of Experiments
Class : Second B. Pharm Subject: Nos. Of Pages: Nos. Of Practical: Prepared By/Teacher In charge: Name & Signature Mr N.Oza,Mr Satyajit Dated: Copies To: HD/STORE/PRINCIPAL Department Code : CCPR/Ceutics/PE/2012 Revision: I Last Revision: Lab. No. Approvals: HOD:

Principal/Director Instrument/ equipment with numbers

Sr. No 1

Experiment Title

Reference 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam

Materials per Student/Batch Name

Glass Wares Qty 2g 5g 2g 5g

To determine the true density of given powder by solvent displacement method

heavy magnesium carbonate light magnesium carbonate heavy magnesium oxide light magnesium oxide

specific gravity bottle, pipette, sieve no.20, weighing balance

To determine the bulk density of given powder samples manually and by bulk density apparatus

heavy magnesium carbonate lactose monohydrate light magnesium oxide

70 g 80 g 35 g

measuring cylinder, sieve no. 20

bulk density apparatus

To determine the tapped density of given powder samples manually and by bulk density apparatus

To determine the percentage porosity of given powder sample

To determine the angle of repose of given powder at different concentration of glidant

3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta

heavy magnesium carbonate lactose monohydrate light magnesium oxide

70 g 80 g 35 g

measuring cylinder, sieve no. 20

bulk density apparatus

Acetone distilled water light magnesium carbonate heavy magnesium carbonate lactose monohydrate talc.

30 ml 30 ml 40 g 70 g 80 g

specific gravity bottle, pipette, sieve no.20, weighing balance measuring cylinder

bulk density apparatus

lactose monohydrate talc magnesium stearate

50 g 2g 1g

funnel, burette, burette stand

To determine the angle of repose of given granules at different concentration of glidant

To determine the flow property of given sample having different particle of repose.

2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad

lactose monohydrate granules talc magnesium stearate

50 g 2g 1g

funnel, burette, burette stand

Heavy magnesium carbonate heavy magnesium oxide

50 g 50 g

funnel, burette, burette stand sieve no.100,60,44 ,18

To determine the Carrs Index of given powder sample and determine the flow property

To determine the Hausner ratio of given powder sample and determine the flow property.

10

To determine the Carrs Index of given granules sample and determine the flow property.

Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam

lactose heavy carbonate

monohydrate 60 g magnesium
70 g

measuring cylinder, weighing balance, white paper

bulk density apparatus

lactose heavy carbonate

monohydrate 60 g magnesium
70 g

measuring cylinder, weighing balance, white paper

bulk density apparatus

lactose heavy carbonate

monohydrate 60 g magnesium
70 g

measuring cylinder, weighing balance, white paper

bulk density apparatus

11

To determine the Hausner ratio of given granules sample and determine the flow property.

12

To determine the average particle size of the given powder and to study their size distribution by microscopy

13

To determine the average globule size of the given emulsion and distribution by microscopy

3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta

lactose heavy carbonate

monohydrate 60 g magnesium
70 g

measuring cylinder, weighing balance, white paper

bulk density apparatus

Calcium Carbonate

5g

eyepiece micrometer, glass slides

Microscope

emulsion

10 ml

14

To determine the viscosity of a given liquid by Ostwalds viscometer

15

To determine the CST (Critical solution temperature) of two component system containing phenol and water

2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad

Benzene Xylene Liquid Paraffin

Beaker Stopwatch

Ostwalds viscometer

Phenol Distilled water

30 ml 30 ml

Beaker, Test tubes, Test tubes holder ,Pipette, Rubber gloves, Thermometer , Water bath, Test tube stand.

16

To study the effect of temperature on the viscosity of given liquid sample

17

To determine the effect of concentration on viscosity by Oswalds viscometer

18

To determine the surface tension (Stalagnometer)

Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam

Glycerin Distilled water Acetone Tween 20 Tween 80

30 ml 30 ml 30 ml 3 ml 3 ml

specific gravity bottle, Clamp stand.

Viscometer,

Glycerin

30 ml

Viscometer, Stop watch,

Benzene Xylene Paraffin

30 ml 30 ml 30 ml

beaker, specific gravity bottle

Stalagnometer,

19

To demonstrate the sedimentation method using Andreasen pipette for measurement of particle size

20

To prepare 100 ml of a pharmaceutical buffer of pH 5.0 (acetate buffer) and verify the same by measuring pH using a pH meter

3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta 1.Practical Physical Pharmacy, Gaud and Gupta 2. A text book of Physical Pharmacy, C.V.Subra hmanyam 3Physical Pharmacy Practical Text, Guru Prasad Mohanta

suspension

10 ml

Standard buffer Acetic acid Sodium acetate

22 g 53 g

weighing balance

pH meter