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- 098
SIMULATION STUDY FOR ENERGY OPTIMISATION IN SOLVENT
EXTRACTION UNIT
Ranvir Singh*, Manoj Srivastava, Manoj Kumar, U.C.Agrawal, M.O.Garg & S.M. Nanoti
Indian Institute of Petroleum, Dehradun (India)
D.S.Laud
HPCL, Mahul Refinery, Mumbai (India)
ABSTRACT
Solvent Extraction units for dearomatisation of lube distillates are large energy consuming units in lube refineries.
Solvent recovery is a very crucial step in these units which also involves input of large amount of energy. The present
paper discusses results of simulation studies carried out for the solvent extraction unit of an existing lube refinery by
simulation using available simulation tools (ASPEN PLUS & SPRINT heat exchanger network designs). Results of the
case study with two different alternatives have been presented in the paper. In the first of these alternatives addition of a
single flash drum has been proposed in extract circuit, which can lead to reduction in hot utility target by as much as
35.2%. In the other case, pseudo component approach has been used to predict the physical properties (specific
gravity, mean average boiling point, pseudo critical temperature & pressure, Watson characterization factor, heat
capacity etc.) of different hydrocarbon mixtures viz feed, raffinate and extract. The 500N distillate stock, which is
complex mixture of hydrocarbons coming from vacuum unit, has been considered as feedstock in the study. Physical
properties obtained through simulation have been compared with the actual property values obtained in test run under
controlled process conditions such as throughput, pressure drop, temperature and other parameters. Good agreement
has been found between the simulation results and the test run results. It has been established that the existing unit can
be operated with as much as 20% higher throughput without any hardware changes or provision of any new hot or cold
utilities.
Key words: solvent extraction, optimization, simulation, heat integration, flash drum.
RAF
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FIGURE 3 : COMPOSITE CURVES FOR EXTRACT CIRCUIT BASE FIGURE 4: GRAND COMPOSITE CURVE FOR EXTRACT CIRCUIT BASE
400
350
350
300
TEMPERATUTRE
300
TEMPERATU
250
250
200
200
150
150
100
HOT COMPOSITE 100
50 COLD COMPOSITE
50
0 0
0 5000 10000 15000 20000 25000 30000 2000 4000 6000 800 10000 12000
0
ENTHALPY kW ENTHALPY kW
187.79
297.44
22,23ext 1 E 4215
N:1 N:28
90.62
188.37
25,27ext 2 E4212
N:2 N:16
94.01
149.00
bfw E4214 7
N:21 N:7
N:0
186.10 A:107.5373 185.68
*Q:1046.0 185.60
rcw E4212 9
N:17 N:9
N:0
49.00
A:153.2925
35.00
*Q:910.0
saltwater E4202 10
N:23 N:10
N:0
380.00
A:66.27748
400.00 *Q:2137.0
103-104 I f 1 2 Rcw
N:1 N:26 N:24
128-108 II f 2 1 3 Rcw
N:2 N:18 N:10 N:22
230.54 188.10
297.00
99.84
188.00
N:7 N:14
N:0
75.00 A:59.24859 49.78 45.87 43.66
*Q:5330.0 40.00
steam 9 HP steam
N:9 N:28
N:0
A:62.49553
*Q:1690.0