Академический Документы
Профессиональный Документы
Культура Документы
Rakibul Islam I Shafiul Alam I Shefaul Islam I Nadia Munsef I Masudul Huda Khan I Abdullah al Faruk
Liquid-liquid extraction is a reliable process of extracting a targeted compound from a solution, with the help of another solvent which is immiscible with the former, but has higher affinity to the targeted compound.
After extraction
After extraction
Extract
Kp = Co/Caq
Kp = Partition coefficient/distribution constant Co= Concentration of the analyte present in the organic phase Caq = Concentration of the analyte present in the aqueous phase
Effectiveness of an extraction:
The effectiveness of an extraction is solely depend upon the volume of the solvents. It can be calculated by appropriate partition coefficient.
Volumes are measured initially and it is used in calculation. The phase is separated and diluted to a known volume. Marker substances can be used
Solubility
Miscibility
Density
3. Ionic species may get absorbed and accumulate around the droplets.
Mechanical means, Centrifugation, Addition of monovalent and divalent ions, Ethanol or higher alcohol, Silicone-defoaming agent, Thermal shock, Altering the ratio of the solvents, Thin-bed of an adsorbent
Effect of temperature
Liquid-Liquid Extraction
Effect of PH