Академический Документы
Профессиональный Документы
Культура Документы
FLUIDIZATION
Is the phenomena of fine solids being
transformed into a fluid like state by the
flow of an upflowing gas or liquid.
Liquid particulate fluidization
Gas aggregative fluidization
Fluidized Beds
Particulate
Aggregative
Just fluidized
Bubbles or slug
appear
Turbulent/fast
fluidization
U = Ut
homogeneous
Liquid
(mostly)
U
2
mf
gd p
Gas
(mostly
U
2
mf
gd p
Fluidized Beds
Hydrodynamics
Pressure drop
Minimum fluidization velocity
Particulate vs aggregative
Bed expansion
Applications
Combustion
Heat exchange
Drying
Granulation
Coating
Etc.
Fluid does not impart enough drag to overcome gravity and particles do
not move. Fixed Bed.
High Velocity
At high enough velocities fluid drag plus buoyancy overcomes the
gravity force and the bed expands. Fluidized Bed.
p for Increasing u0
Until onset of fluidization p increases, then becomes constant.
Response to Superficial
Velocities
Fluidization
Advantages
Solids can be removed from and added to the bed
continuously. This is an important advantage over the
fixed bed.
All the fine powders have a very large specific surface
area, which is good for high rates heat transfer.
The continuous stirring action of the gas bubbles in
fluidised beds generally provides good solid mixing, on
the other hand it can also provide segregation.
Combination of stirring action and high rate of heat
transfer provides isothermal conditions radially and
axially. This may be important in many chemical and
catalytic process.
10
Advantages
Fluidisation will eliminate catalyst pelleting, an
important cost item in many catalytic processes.
It is suitable for large-scale operations.
The smooth, liquid-like flow of particles allows
continuous automatically controlled operations
with easy handling.
Compared with a fixed bed of the same
powder operated at the same bed depth and gas
velocity, the pressure drop over a fluidised bed
is much smaller.
11
Disadvantages
For some applications the gas bubbles
make scale-up more difficult and provide
a means whereby the reacting gases can
avoid contact with solids.
Particle entrainment, which is the
carryover of particles from bed by the
gas, is almost inevitable, installation for
fines recovery may be required.
12
Disadvantages
Particle attrition, size reduction and metal
surface erosion occur in regions where gas
velocities are high. Thus the fluidisation
properties of the material may become
different and require adjustment of the gas
rate. Expensive designs may be required to
minimise wear in reactor and transfer line.
The quick equilibration of temperature means
it is unsuitable for a reaction which is best
carried out in a reactor giving a temperature
gradient along the reaction path.
13
Basic Setup
1. Shell
2. Powder
3. Blower
4. Gas distributor
5. Heat exchange
fluidizing gas
6. Internal heating or
cooling
7. External heating or
cooling
8. Cyclones
9. Solids feeder
10.Solids offtake
11.Spray feed
14
Pressure drop versus fluid velocity for packed and fluidized beds
15
Bed pressure
drop, p
C
B
Umf
Gas velocity, U
Pressure drop versus fluid velocity for packed and fluidized beds
16
17
p H(1 )(p f )g
18
p H(1 )(p f )g
For gases:
19
p H(1 )(p f )g
For gases:
p 20 kPa
20
Minimum Fluidization
Velocity
(UthemfErgun
) equation
Can
be predicted using
( p)
(1 ) 2 U
(1 ) f U 2
150
1.75
3
2
H
x sv
x sv
3
(1 )
2
Re
1.75
Re
mf
mf
3
3
where
Ar
3
f ( p f )gx sv
U mf x sv f
21
Umf x sv f
Remf
22
f ( p f ) gd
3
sv
Remf
Umf x sv f
Umf
23
24
Densities
Particle density
Absolute density
Bed density
Bulk density
25
solid material
pores
Particle density
26
solid material
pores
hydrodynamic volume
Particle density
mass of particle
solid material
pores
Absolute density
28
solid material
pores
material volume
Absolute density
mass of particle
volume of solids material making up the particle
29
Bed density =
Bulk density =
30
Bed height, H
Bed volume = HA
Bed density =
Bulk density =
31
Bed height, H
Bed volume = HA
Bed density =
Bulk density =
mass of particles
volume occupied by particles and voids between them
32
33
xp
1
mi
xi
34
xp
1
mi
xi
Harmonic mean
of the mass
distribution
35
xp
1
mi
xi
Harmonic mean
of the mass
distribution
Surface-volume
mean diameter
D(3, 2)
36
37
Beyond Umf
Fluidization may be bubbling or non-bubbling:
38
Beyond Umf
Fluidization may be bubbling or non-bubbling:
Some combinations of fluid and particle properties
Only bubbling
39
Beyond Umf
Fluidization may be bubbling or non-bubbling:
Some combinations of fluid and particle properties
Only bubbling
40