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  • Preparation of Soluble Salts

    Загружено:

    Fidree Aziz
    207 просмотров23 страницы
    This document describes the process of preparing soluble salts. Soluble salts are formed through neutralization reactions between acids and bases or acids and metallic oxides/carbonates. The general process involves adding the reactants, heating the solution, cooling and crystallizing the salt, filtering out the salt crystals, and drying the crystals. Key steps include neutralization, evaporation/heating, cooling/crystallization, filtration, and drying. The document provides detailed diagrams and explanations of each step in preparing common soluble salts like NaCl, KBr, and ZnCl2.

    Исходное описание:

    soluble salts

    Оригинальное название

    8.1 (b) Soluble salts

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    This document describes the process of preparing soluble salts. Soluble salts are formed through neutralization reactions between acids and bases or acids and metallic oxides/carbonates. The general process involves adding the reactants, heating the solution, cooling and crystallizing the salt, filtering out the salt crystals, and drying the crystals. Key steps include neutralization, evaporation/heating, cooling/crystallization, filtration, and drying. The document provides detailed diagrams and explanations of each step in preparing common soluble salts like NaCl, KBr, and ZnCl2.

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    © All Rights Reserved
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    Отметить как неприемлемый контент
    207 просмотров23 страницы

    Preparation of Soluble Salts

    Загружено:

    Fidree Aziz
    This document describes the process of preparing soluble salts. Soluble salts are formed through neutralization reactions between acids and bases or acids and metallic oxides/carbonates. The general process involves adding the reactants, heating the solution, cooling and crystallizing the salt, filtering out the salt crystals, and drying the crystals. Key steps include neutralization, evaporation/heating, cooling/crystallization, filtration, and drying. The document provides detailed diagrams and explanations of each step in preparing common soluble salts like NaCl, KBr, and ZnCl2.

    Авторское право:

    © All Rights Reserved
    Скачайте в формате PPT, PDF, TXT или читайте онлайн в Scribd
    Отметить как неприемлемый контент
    из 23

    PREPARATION

    OF SOLUBLE SALT

    KPT 3013 1
    Salt Preparation

    Soluble salts Insoluble salts

    Salt type Non-salt type Except


    (Na+, K+, NH4) (Na+, K+, NH4)

    Acid +Alkaline Acid + Metallic oxide

    Acid + Metal

    KPT 3013 Acid + metallic carbonate 2


    Acid + Alkali Salt

    HCl + NaOH NaCl + H2O


    KOH + HBr KBr + H2O
    Neutralization reaction
    acid + alkali react with each other
    form salt & water
    H+(acid) + OH-(alkali) H2O(water
    Cl-(-ve of acid) + Na (+ve from alkali)
    salt(NaCl)
    KPT 3013 3
    (HCl + NaOH) NaCl

    Titration method

    Evaporation/Heating

    Cooling/crystallization

    Filtration

    Dry
    KPT 3013 4
    Zn + 2HCl ZnCl2 + H2
    Add metallic
    oxide/metal/carbonate oxide

    Heating

    Filtration

    Recrystallisation

    KPT 3013 5
    Heating Filtration Evaporation

    KPT 3013 Dry Filtration 6


    Titration

    Burette

    Retort stand
    HCl

    Erlenmeyer
    25 ml NaOH + Flask
    phenolphthalein
    (2 drops)

    KPT 3013 7
    Evaporation/Heating

    Heat the salt


    solution until
    saturated~1/3
    from initial volume

    Triport
    Stand

    Heat
    KPT 3013 8
    Cooling/crystallization

    Crystallization
    Salt
    Crystal

    KPT 3013 9
    Filtration

    Salt crystal

    Filter paper

    Filter funnel

    Filtered
    KPT 3013 solution 10
    Dry

    Filter paper
    Soluble salt
    crystal

    Dried by
    filter paper

    KPT 3013 11
    Metallic metal
    CuO/MgO/ZnO
    Add metallic metal/metal/metallic
    Metal carbonate powder until saturated
    Zn/Mg

    Metallic carbonate
    ZnCO3/ MgCO3/CuCO3 Rode glass

    30ml acid

    KPT 3013 12
    Heating

    salt solution Rode glass

    Heat

    KPT 3013 13
    Evaporation

    Salt solution Rode glass

    Heat

    KPT 3013 14
    Filtration

    Saturated salt
    crystal
    Rode glass

    Filter paper
    Remainder: metallic
    oxide/excess metal

    Salt solution

    KPT 3013 15
    Filtration

    Rode glass

    Pure salt
    crystal

    salt solution

    KPT 3013 16
    Salt crystal characteristic

    Flatted surface
    Straight side
    Shape edge
    Uniform
    geometry
    Degree between
    neighboring
    surface is
    constant
    KPT 3013 17
    KPT 3013 18
    Heating

    Impurities
    salt solution

    Heat

    KPT 3013 19
    Filtration

    Impurities
    salt solution
    Rode glass

    Remainder

    Salt solution

    KPT 3013 20
    Evaporation

    Salt
    Rode glass
    solution

    Heat

    KPT 3013 21
    Filtration

    Impurities
    salt solution
    Rode glass

    Remainder

    Salt solution

    KPT 3013 22
    Filtration

    Rode glass

    Pure salt
    crystal

    salt solution

    KPT 3013 23

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