MINI PROJECT

All about Biodiesel

Mahathir Nur Muhammad

Yasinta Lola
Reno Susanto
Nadhella Fahira Faradisha
Nada Zulmy Mayora
DECOLORIZITION
BIODIESEL AND
PURIFICATION
GLYCEROL
 Biodiesel Process

1nd 2 nd 3nd 4nd

TRANSESTERIFICATIO
WCO N WATER WASHING DEHYDRATION
METODE
- Filtration KOH = 0.14 kg 5% (v/v) hot water 85 °C 100℃
- Reduction H2O MeOH = 2 L Heating to 90 °C 30 min
Temperature = 100 °C WCO = 10 L 30 min process
Time = 30 min Process time = 3 hours 30 min separating time
Cooldown into 60 °C Temperature = 60 °C 3 times repetition
Separating time = 60 min
 Biodiesel Process

51nd 64nd

CRUDE BIODIESEL DECOLORIZATION

BIODIESEL
 V = 150 rpm
Feed
Crude Biodiesel

Biocharcoal

Pure Biodiesel

Analysis
 Analysys

Sulfure
Water Content pH Density Viscosity
Content

Residual
Acid Value Flash Point Ash Content
Carbon
Expected Result
PURIFICATION
GLYSEROL
 STEPS TO PURIFICATION
GLYCEROL

SEPARATION ROTARY EVAPORATION

1 H3PO4
4 0.15 Bar

SETTLING ABSORB
2 1 hours
5 + biochar

FILTRATION ANALYSIS
3 Filter paper
6 Kadar glyseror
Kadar air
Viskositas
Nilai PH
Titik leleh, didih, nyala
 Flowchart

Settling
Filtrasi
1 hour

Fatty Acid Fatty acid Out

Crude Glyserol Glyserol Glyserol

85℃ Salt
Salt
H3PO4
5% (v/v)
300 rpm Settling
30 min ½ Day
 Flowchart

Analysis

Rotary °C
Glyserol Pure Glyserol
Evaporator

Biochar
Water 200 rpm in 30
min
 Analysys

Glycerol
Water Content pH Density viscosity
Content

Pour Point MONG Content Flash Point Ash Content

Boiling Point
TRALALA THIS IS IT

Concentration of gliserol
> 99%
Thank you